CN104940058A - Essence composition and preparation method thereof - Google Patents
Essence composition and preparation method thereof Download PDFInfo
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- CN104940058A CN104940058A CN201510296193.4A CN201510296193A CN104940058A CN 104940058 A CN104940058 A CN 104940058A CN 201510296193 A CN201510296193 A CN 201510296193A CN 104940058 A CN104940058 A CN 104940058A
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Abstract
The invention relates to an essence composition and its preparation method and belongs to the technical field of cosmetics processing. The essence composition is prepared from the following substances: prinsepia utilis rogle oil, tea oil, small marigold flower oil, glycerin, linoleic acid, dimethyl silicone oil, coenzyme Q10, cetyl alcohol, lanolin, tocopheryl acetate, methyl p-hydroxybenzoate, ethyl p-hydroxybenzoate, carbomer, Tetrasodium ethylenediamine tetraacetate, Disodium ethylene diamine tetraacetate, ethylhexylglycerin, essence and deionized water. The invention has advantages as follows: the composition has remarkable moisture retention, crease-resistance, anti-aging, spot-removing and anti-inflammatory effects and is easily absorbed by human skin; and after the composition is smeared on skin, skin can become fine and smooth, wrinkles can be minimized, and spots can be removed.
Description
Technical field
The invention belongs to cosmetics processing technique field, be specifically related to a kind of essence composition and method of making the same.
Background technology
Princepia utilis (Prinsepia utilis Royle), Chinese formal name used at school always spends Folium Prinsepiae Utilis, belongs to Rosaceae Prinsepia Royle plant, another name Folium Prinsepiae Utilis, fruit of buying oil.Du Ping etc. produce the vitamin of Studies of Prinsepia Utilis Royle quintessence oil, aminoacid, fatty acid, the composition analysis of mineral element and content to Lijing and measure.Result shows, and Princepia utilis oil is rich in the multivitamins such as vitamin A. D. E, K and beta-carotene; Amino acid contained A wide selection of colours and designs, total content reaches 46.97%, and wherein 7 kinds of essential amino acid content account for 28.1% of total amino acid content; Institute's fatty acids has 13 kinds, and wherein unsaturated fatty acid content is high, and based on oleic acid and linoleic acid, satisfied fatty acid, monounsaturated fatty acid and polyunsaturated fatty acid proportion of composing are close to 0.7:1:1, and its nutrition of lipids structure comparison is applicable to human body needs.
Research finds, Princepia utilis oil remains the bioactive ingredients of pure natural, its main component is polyunsaturated fatty acid and monounsaturated fatty acid, with human body lipid closely, so skin permeation to ooze skin good especially, human body skin is also very easy to absorb, and can keep the moisture of skin, nutrition and elasticity, is the base starting material of the rare pure natural skin care item of current cosmetic industry.The fashion trend of world today's cosmetics is back to natures, environmental protection, and adopt pure natural raw material substitution chemosynthesis raw material, Princepia utilis oil is so a kind of pure natural skin protection oils and fats just, has broad application prospects.Therefore, further exploitation is that the cosmetics of primary raw material become the technical problem needing solution badly with Princepia utilis oil.
Summary of the invention
The object of this invention is to provide a kind of facial treatment essence fluid composition with moisturizing, crease-resistant, freckle effect.
Another object of the present invention is to provide the preparation method of this essence compositions.
The technical solution used in the present invention is a kind of essence compositions, is made up of the material of following parts by weight: Princepia utilis oil 5 ~ 8 parts; Tea oil 1 ~ 3 part; Little marigold caul-fat 1 ~ 3 part; Glycerol 1 ~ 6 part; Linoleic acid 1 ~ 3 part; Dimethicone 3 ~ 5 parts; Coenzyme Q10 1 ~ 3 part; Spermol 2 ~ 4 parts; Lanoline 1 ~ 4 part; Tocopherol acetas 0.1 ~ 0.5 part; Methyl parahydroxybenzoate 0.01 ~ 0.05 part; Ethylparaben 0.01 ~ 0.05 part; Carbomer 0.1 ~ 0.5 part; 0.01 ~ 0.1 part, EDTA tetra-sodium; EDETATE SODIUM 0.01 ~ 0.05 part; Sensiva SC50 0.1 ~ 1 part; 0.1 ~ 1 part, essence; Deionized water 80 ~ 100 parts.
Particularly preferred, described essence compositions is made up of the material of following parts by weight: Princepia utilis oil 6 parts; Tea oil 2 parts; Little marigold caul-fat 2 parts; Glycerol 2 parts; Linoleic acid 2 parts; Dimethicone 4 parts; Coenzyme Q10 2.5 parts; Spermol 3 parts; Lanoline 1.5 parts; Tocopherol acetas 0.25 part; Methyl parahydroxybenzoate 0.01 part; Ethylparaben 0.02 part; Carbomer 0.5 part; 0.05 part, EDTA tetra-sodium; EDETATE SODIUM 0.02 part; Sensiva SC50 0.5 part; 0.3 part, essence; Deionized water 85 parts.
The present invention also provides a kind of essence compositions, and the preparation method of described Princepia utilis oil comprises the following steps:
A, the thick oil of preparation: ground by Princepia utilis, add water furnishing pasty state, adds ethanol in proper amount and dilute hydrochloric acid, repeatedly to vibrate lixiviate through petroleum ether, leave standstill, take out petroleum ether layer, then the solvent in petroleum ether layer is evaporated, obtain slightly oil; Wherein, the addition of ethanol is 5% ~ 10% of pastel weight, and the addition of dilute hydrochloric acid is 0.01% ~ 0.05% of pastel weight.Add ethanol in proper amount and dilute hydrochloric acid, the active component in Princepia utilis can be extracted better, thus increase the activity of compositions, improve the effect of its moisturizing, crease-resistant, anti-aging, speckle dispelling, antiinflammatory.
The number of times of petroleum ether lixiviate is adopted to be preferably 2 times, 3 times, 4 times.The Princepia utilis adopted is fresh Princepia utilis, is specially the Princepia utilis after gathering then.
B, refining: by above-mentioned thick oil decolorization, deodorize, obtains Princepia utilis oil.
The present invention also provides a kind of preparation method of described essence compositions, comprises the following steps:
(1) A phase: take deionized water, glycerol, carbomer, EDTA tetra-sodium and EDETATE SODIUM, heating mixing, obtains aqueous phase;
(2) B phase: take Princepia utilis oil, tea oil, little marigold caul-fat, linoleic acid, dimethicone, coenzyme Q10, spermol, lanoline, tocopherol acetas and Sensiva SC50 again, heating mixing, obtains oil phase;
(3) C phase: essence;
(4) be added to described B in A phase, emulsifying, obtains emulsion;
(5) temperature of described emulsion is adjusted to 55 ~ 60 DEG C, adds methyl parahydroxybenzoate, ethylparaben; Mixing; Be cooled to 40 ~ 50 DEG C again, add C phase, mixing, is cooled to less than 35 DEG C, obtains final product.
Adopt above-mentioned preparation method, can allow composition mix homogeneously of different nature, be conducive to keeping constant product quality when carrying out cold cycling test, avoid occurring quality problems because climate difference is excessive, after tested, the stable phase of product can reach 3 years.The active substance in compositions also can be made not to be destroyed, effectively to ensure that the quality of product.
Beneficial effect of the present invention is: resulting composition has the effect of significant moisturizing, crease-resistant, anti-aging, speckle dispelling, antiinflammatory; Also easily be absorbed by the skin, skin after smearing skin, can be made moist.
Detailed description of the invention
For making those skilled in the art understand production technology of the present invention and technique effect in detail, introduce application of the present invention and technique effect further with concrete production instance below.
Embodiment 1
The preparation of Princepia utilis oil
A, the thick oil of preparation: ground by Princepia utilis, add water furnishing pasty state, adds ethanol in proper amount and dilute hydrochloric acid, repeatedly to vibrate lixiviate through petroleum ether, leave standstill, take out petroleum ether layer, then the solvent in petroleum ether layer is evaporated, obtain slightly oil; Wherein, the addition of ethanol is 8% of pastel weight, and the addition of dilute hydrochloric acid is 0.02% of pastel weight.
B, refining: by above-mentioned thick oil decolorization, deodorize, obtains Princepia utilis oil.
The preparation method of essence compositions
By weight
(1) A phase: take deionized water 90 parts, glycerol 4 parts, carbomer 0.3 part, 0.05 part, EDTA tetra-sodium and EDETATE SODIUM 0.03 part, heating mixing, obtains aqueous phase;
(2) B phase: take Princepia utilis oil 5 parts, tea oil 2 parts, little marigold caul-fat 2 parts, linoleic acid 2 parts, dimethicone 4 parts, ubiquinone again
102 parts, spermol 3 parts, lanoline 3 parts, tocopherol acetas 0.3 part and Sensiva SC50 0.5 part, heating mixing, obtains oil phase;
(3) C phase: 0.5 part, essence;
(4) be added to described B in A phase, emulsifying, obtains emulsion;
(5) temperature of described emulsion is adjusted to 58 DEG C, adds methyl parahydroxybenzoate 0.03 part, ethylparaben 0.03 part; Mixing; Be cooled to 45 DEG C again, add C phase, mixing, is cooled to less than 35 DEG C, obtains final product.
Embodiment 2
The preparation of Princepia utilis oil
A, the thick oil of preparation: ground by Princepia utilis, add water furnishing pasty state, adds ethanol in proper amount and dilute hydrochloric acid, repeatedly to vibrate lixiviate through petroleum ether, leave standstill, take out petroleum ether layer, then the solvent in petroleum ether layer is evaporated, obtain slightly oil; Wherein, the addition of ethanol is 5% of pastel weight, and the addition of dilute hydrochloric acid is 0.01% of pastel weight.
B, refining: by above-mentioned thick oil decolorization, deodorize, obtains Princepia utilis oil.
The preparation method of essence compositions
By weight
(1) A phase: take deionized water 100 parts, glycerol 6 parts, carbomer 0.5 part, 0.1 part, EDTA tetra-sodium and EDETATE SODIUM 0.05 part, heating mixing, obtains aqueous phase;
(2) B phase: take Princepia utilis oil 5 parts, tea oil 3 parts, little marigold caul-fat 3 parts, linoleic acid 3 parts, dimethicone 5 parts, coenzyme Q10 3 parts, spermol 4 parts, lanoline 4 parts, tocopherol acetas 0.5 part and Sensiva SC50 1 part again, heating mixing, obtains oil phase;
(3) C phase: 1 part, essence;
(4) be added to described B in A phase, emulsifying, obtains emulsion;
(5) temperature of described emulsion is adjusted to 55 DEG C, adds methyl parahydroxybenzoate 0.05 part, ethylparaben 0.05 part; Mixing; Be cooled to 40 DEG C again, add C phase, mixing, is cooled to less than 35 DEG C, obtains final product.
Embodiment 3
The preparation of Princepia utilis oil
A, the thick oil of preparation: ground by Princepia utilis, add water furnishing pasty state, adds ethanol in proper amount and dilute hydrochloric acid, repeatedly to vibrate lixiviate through petroleum ether, leave standstill, take out petroleum ether layer, then the solvent in petroleum ether layer is evaporated, obtain slightly oil; Wherein, the addition of ethanol is 10% of pastel weight, and the addition of dilute hydrochloric acid is 0.05% of pastel weight.
B, refining: by above-mentioned thick oil decolorization, deodorize, obtains Princepia utilis oil.
The preparation method of essence compositions
By weight
(1) A phase: take deionized water 80 parts, glycerol 1 part, carbomer 0.1 part, 0.01 part, EDTA tetra-sodium and EDETATE SODIUM 0.01 part, heating mixing, obtains aqueous phase;
(2) B phase: take Princepia utilis oil 8 parts, tea oil 1 part, little marigold caul-fat 1 part, linoleic acid 1 part, dimethicone 3 parts, ubiquinone again
101 part, spermol 2 parts, lanoline 1 part, tocopherol acetas 0.1 part and Sensiva SC50 0.1 part, heating mixing, obtains oil phase;
(3) C phase: 0.1 part, essence;
(4) be added to described B in A phase, emulsifying, obtains emulsion;
(5) temperature of described emulsion is adjusted to 55 DEG C, adds methyl parahydroxybenzoate 0.01 part, ethylparaben 0.01 part; Mixing; Be cooled to 50 DEG C again, add C phase, mixing, is cooled to less than 35 DEG C, obtains final product.
Embodiment 4
The preparation of Princepia utilis oil
A, the thick oil of preparation: ground by Princepia utilis, add water furnishing pasty state, adds ethanol in proper amount and dilute hydrochloric acid, repeatedly to vibrate lixiviate through petroleum ether, leave standstill, take out petroleum ether layer, then the solvent in petroleum ether layer is evaporated, obtain slightly oil; Wherein, the addition of ethanol is 6% of pastel weight, and the addition of dilute hydrochloric acid is 0.02% of pastel weight.
B, refining: by above-mentioned thick oil decolorization, deodorize, obtains Princepia utilis oil.
The preparation method of essence compositions
By weight
(1) A phase: take deionized water 85 parts, glycerol 2 parts, carbomer 0.5 part, 0.05 part, EDTA tetra-sodium and EDETATE SODIUM 0.02 part, heating mixing, obtains aqueous phase;
(2) B phase: take Princepia utilis oil 6 parts, tea oil 2 parts, little marigold caul-fat 2 parts, linoleic acid 2 parts, dimethicone 4 parts, ubiquinone again
102.5 parts, spermol 3 parts, lanoline 1.5 parts, tocopherol acetas 0.25 part and Sensiva SC50 0.5 part, heating mixing, obtains oil phase;
(3) C phase: 0.3 part, essence;
(4) be added to described B in A phase, emulsifying, obtains emulsion;
(5) temperature of described emulsion is adjusted to 55 DEG C, adds methyl parahydroxybenzoate 0.01 part, ethylparaben 0.02 part; Mixing; Be cooled to 50 DEG C again, add C phase, mixing, is cooled to less than 35 DEG C, obtains final product.
For verifying technique effect of the present invention, the following experiment of special do:
One, experimental principle
With the actual test result of human body skin, verify the skin effect of essence compositions of the present invention.
Two, experimental technique
Tested number: 180 people; Age: 25 years old ~ 40 years old; Sex: female 150 people, male 30 people; Health status: subjects skin is healthy, without dermatosis and allergies.Above-noted persons are divided into three groups at random and do double-blind, blank group 1, distilled water; Matched group 2, is only Princepia utilis oil; Experimental group 3 is example 1 gained essence compositions.Above-mentioned three groups of crowds, carry out double-blind, and analyze statistical result.
Three, experimental result, in table 1
Table 1
Four, conclusion
According to the analysis of statistical data of above result of the test, use product of the present invention, the series of experiments that experimenter carries out is shown, this elite compositions is easily absorbed by the skin, make most subjects skin moist, wrinkle of skin obviously disappears, and compares blank group and matched group, has significant progress.
Finally it should be noted that, above embodiment is the unrestricted technical scheme of the present invention in order to explanation only, although with reference to above-described embodiment to invention has been detailed description, those skilled in the art are to be understood that, still can modify to the present invention or equivalent replacement, and not departing from any modification or partial replacement of the spirit and scope of the present invention, it all should be encompassed in right of the present invention.
Claims (4)
1. an essence compositions, is characterized in that, is made up of the material of following parts by weight: Princepia utilis oil 5 ~ 8 parts; Tea oil 1 ~ 3 part; Little marigold caul-fat 1 ~ 3 part; Glycerol 1 ~ 6 part; Linoleic acid 1 ~ 3 part; Dimethicone 3 ~ 5 parts; Coenzyme Q10 1 ~ 3 part; Spermol 2 ~ 4 parts; Lanoline 1 ~ 4 part; Tocopherol acetas 0.1 ~ 0.5 part; Methyl parahydroxybenzoate 0.01 ~ 0.05 part; Ethylparaben 0.01 ~ 0.05 part; Carbomer 0.1 ~ 0.5 part; 0.01 ~ 0.1 part, EDTA tetra-sodium; EDETATE SODIUM 0.01 ~ 0.05 part; Sensiva SC50 0.1 ~ 1 part; 0.1 ~ 1 part, essence; Deionized water 80 ~ 100 parts.
2. a kind of essence compositions according to claim 1, is characterized in that, be made up of the material of following parts by weight: Princepia utilis oil 6 parts; Tea oil 2 parts; Little marigold caul-fat 2 parts; Glycerol 2 parts; Linoleic acid 2 parts; Dimethicone 4 parts; Coenzyme Q10 2.5 parts; Spermol 3 parts; Lanoline 1.5 parts; Tocopherol acetas 0.25 part; Methyl parahydroxybenzoate 0.01 part; Ethylparaben 0.02 part; Carbomer 0.5 part; 0.05 part, EDTA tetra-sodium; EDETATE SODIUM 0.02 part; Sensiva SC50 0.5 part; 0.3 part, essence; Deionized water 85 parts.
3. a kind of essence compositions according to claim 1 or 2, it is characterized in that, the preparation method of described Princepia utilis oil comprises the following steps:
A, the thick oil of preparation: ground by Princepia utilis, add water furnishing pasty state, adds ethanol in proper amount and dilute hydrochloric acid, repeatedly to vibrate lixiviate through petroleum ether, leave standstill, take out petroleum ether layer, then the solvent in petroleum ether layer is evaporated, obtain slightly oil;
B, refining: by above-mentioned thick oil decolorization, deodorize, obtains Princepia utilis oil.
4., based on a preparation method for essence compositions described in claim 1 or 2, it is characterized in that, comprise the following steps:
(1) A phase: take deionized water, glycerol, carbomer, EDTA tetra-sodium and EDETATE SODIUM, heating mixing, obtains aqueous phase;
(2) B phase: take Princepia utilis oil, tea oil, little marigold caul-fat, linoleic acid, dimethicone, coenzyme Q10, spermol, lanoline, tocopherol acetas and Sensiva SC50 again, heating mixing, obtains oil phase;
(3) C phase: essence;
(4) be added to described B in A phase, emulsifying, obtains emulsion;
(5) temperature of described emulsion is adjusted to 55 ~ 60 DEG C, adds methyl parahydroxybenzoate, ethylparaben; Mixing; Be cooled to 40 ~ 50 DEG C again, add C phase, mixing, is cooled to less than 35 DEG C, obtains final product.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN109381362A (en) * | 2018-12-19 | 2019-02-26 | 浙江神首生物科技有限公司 | Shining life repair latex living of one kind and preparation method thereof |
| CN111110597A (en) * | 2020-03-19 | 2020-05-08 | 韩妍蜜化妆品(浙江)有限公司 | Skin-refreshing essence set |
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| CN1768729A (en) * | 2004-11-01 | 2006-05-10 | 天津市化妆品科学技术研究院有限公司 | Green bur cosmetic |
| CN101032459A (en) * | 2007-04-20 | 2007-09-12 | 东北林业大学 | Emulsion including coenzyme Q10 and vegetal marrow and preparing method thereof |
| CN102406576A (en) * | 2011-10-28 | 2012-04-11 | 何黎 | Prinsepia utilis Royle oil-containing functional skin care product and preparation method thereof |
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2015
- 2015-06-02 CN CN201510296193.4A patent/CN104940058A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1768729A (en) * | 2004-11-01 | 2006-05-10 | 天津市化妆品科学技术研究院有限公司 | Green bur cosmetic |
| CN101032459A (en) * | 2007-04-20 | 2007-09-12 | 东北林业大学 | Emulsion including coenzyme Q10 and vegetal marrow and preparing method thereof |
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Non-Patent Citations (1)
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109381362A (en) * | 2018-12-19 | 2019-02-26 | 浙江神首生物科技有限公司 | Shining life repair latex living of one kind and preparation method thereof |
| CN111110597A (en) * | 2020-03-19 | 2020-05-08 | 韩妍蜜化妆品(浙江)有限公司 | Skin-refreshing essence set |
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