CN104938528A - Termite attracticide and preparation method - Google Patents
Termite attracticide and preparation method Download PDFInfo
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Abstract
The invention provides a termite attracticide, which comprises the following raw materials: paper, chlorfenapyr, ivermectin, asparaginic acid, chitosan, saccharose, pollen pini and diatom powder, and further comprises tea tree root powder and bismuth oxyhalide. The invention further discloses a preparation method of the termite attracticide. The method comprises the following steps: mixing and spraying raw materials on paper; preparing into the required shape; and drying to obtain the termite attracticide. By virtue of the formula, the dosage of a chemical agent is greatly reduced; and the security threats to the environment and human are reduced.
Description
Technical field
The present invention relates to termite control field, be specifically related to a kind of attracticide and preparation method of control termites.
Background technology
Termite, as global insect, relates to the various aspects such as building construction, farm-forestry crop, reservoir dam, storage goods and materials, underground cables to the loss that national economy causes.All there is termite damage most province ,city and area of China, endangers more serious more southward.Along with the quickening of mankind's town and country construction, Material Transportation are more frequent and the impact of the factor such as climate warming, termite damage is day by day serious and extensively paid attention to by people, actively develops preventing and controlling and effectively can alleviate loss because termite damage causes.
For a long time, termite control uses high poison and the great insecticide of environmental pollution mostly, as Niran, mirex, aldrin, dieldrin, heptachlor etc.Although these medical treatment effects are very remarkable, the chemical substance long-term existence of a large amount of high malicious high residue, in environment, has great potential risk to people and animals, and termite swarming being entered to building is also helpless.Along with China fulfils " Convention of Stockholm " comprehensively, termite control is eliminated the medicament of high malicious high residue gradually and is actively found substitute products.
The termiticides that current China uses mainly contains chlopyrifos, sumicidin, decis, Biphenthrin, cypermethrin, permethrin, Imidacloprid, ethiprole, Hydramethylnon Bait, HEXAFLUMURON, vikane etc.Go out bait formulation, paste, the Er slice of controlling use of termite is input, and the former medicine of vikane is used for the airtight stifling of the stifling of odontoterme the ants main way and building ant evil, pulvis for spreading in building and timber.The application process of the formulation medicament such as suspending agent, missible oil, microemulsion, aqueous emulsion, water dispersible granules agent of termite prevention has the immersion of soil treatment (sprinkling), timber, sprays and smear etc.
Although toxicity is lower comparatively speaking, residual life is shorter for surrogate-data technique, long-term a large amount of use is still to environment and the human health particularly larger hidden danger of groundwater environment existence.Trapping system (Monitoring and Controlling technology) is because its low toxicity, dosage are few and can effectively control termite damage and be widely used gradually, its principle utilizes the material of termite eating to make bait, take after the worker ant of looking for food of some is lured dust spraying or throw in poison bait, after returning nest group with malicious termite, transmit mutually by trophallaxis and grooming behavior the effect finally reaching and kill whole nest termite.Trapping system greatly reduces the usage amount of chemical agent, meets the target of Ecological Civilization Construction, will promote the upgrading of China's termite control technology and theory.But in actual applications, still there is following problem:
(1) first lure collection termite to dust again, spray or throw in poison bait, need running check whether to lure to collect to arrive sufficient amount
Termite, can greatly increase cost of labor and cause interference to termite foraging activity, affect gathering effect;
(2) for pesticide control, need select to termite without anti-repelling properties or the very weak slow medicament of anti-repelling properties, and take measures to prevent poison bait from occurring going mouldy, rotting within comparatively short-term.
Chlorfenapyr is Phenylpyrazole insecticides, and insecticidal spectrum is wide, and within the scope of finite concentration, not having anti-repelling properties to termite, and have transferability, is that the medicament of killing of active ingredient also has report with chlorfenapyr.As: invention people is woods wild goose, He Liwen etc., publication number CN 102948419A, publication date on March 6th, 2013; Invention people is woods wild goose, Chen Danqi etc., publication number CN 102860306A, publication date on January 9th, 2013.
Ivermectin is the semi-synthetic macrolides multi-component antibiotic produced by Avid kyowamycin streptomyces avermitilis fermentation, has transferability, better to termite control effects, is that the medicament of killing of active ingredient also has report with ivermectin.As: invention people is Guo Jianqiang, Lei Agui etc., publication number CN1299597A, 20 days June calendar year 2001 of publication date; Invent that the artificial money palm is clear, Guo Jianqiang, publication number 104430412A, publication date on March 25th, 2015.
Chlorfenapyr and ivermectin under low concentration to termite without obvious repellent action, and toxic action is comparatively slow, has transitivity; Shitosan, can be degradable as natural polysaccharide, environmental sound, and its large quantity research as slow releasing carrier of medication is reported as and the invention provides reference; By adding bait, embedding substance, suitable carrier and anticorrosive mildewproof measure, overcoming that termite bait formulation is perishable, mouldy, allure is strong, can not keep the weakness such as long-acting, will be the direction of termite control bait formulation research and development.
Summary of the invention
The consumption that the object of the invention is to exist according to existing termiticide is large, security risk is high, and the problem such as bait formulation allure is more weak, the lasting period is shorter, provides that a kind of consumption is few, environmentally safe and can keep long-acting termiticides.
Another object of the present invention is to the preparation method that above-mentioned control termites medicament is provided.
The present invention will be achieved through the following technical solutions above-mentioned purpose:
A kind of termite-killing trapping medicament, described termite-killing trapping medicament comprises the raw material composition of following weight portion: paper 30-50 part, chlorfenapyr 0.001-0.01 part, ivermectin 0.001-0.01 part, asparatate 0.001-0.01 part, shitosan 10-20 part, sucrose 10-30 part, pollen pini 5-20 part, diatom powder 5-10 part.
More preferably, a kind of termite-killing trapping medicament, described termite-killing trapping medicament comprises the raw material composition of following weight portion: 40 parts, paper, chlorfenapyr 0.0057 part, ivermectin 0.0023 part, asparatate 0.0035 part, shitosan 14 parts, sucrose 27 parts, pollen pini 14 parts, diatom powder 5 parts.
Described paper is wood pulp paper, paper sheet thickness 0.01-0.1mm, long 100-400mm, wide 50-200mm.
Described pollen pini is the dry pollen of pine genus plant, and granularity crosses 40-80 order.
Described diatom powder is the fine particle of tripoli class ore fine finishining, and granularity crosses 40-120 order.
Described paper can also replace with bagasse or crops straw, and after wherein bagasse, crops straw are crushed to 1-10mm, methyl alcohol extracts obtained.
The medicament of above-mentioned control termites also comprises tea root powder 5-15 part, BiOX 0.1-1 part, that is: paper 30-50 part, chlorfenapyr 0.001-0.01 part, ivermectin 0.001-0.01 part, asparatate 0.001-0.01 part, shitosan 10-20 part, sucrose 10-30 part, pollen pini 5-20 part, diatom powder 5-10 part, tea root powder 5-15 part, BiOX 0.1-1 part.
More preferably the medicament of control termites also comprises 10.5 parts, tea root powder, BiOX 0.45 part, that is: 40 parts, paper, chlorfenapyr 0.0057 part, ivermectin 0.0023 part, asparatate 0.0035 part, shitosan 14 parts, sucrose 27 parts, pollen pini 14 parts, diatom powder 5 parts, 10.5 parts, tea root powder, BiOX 0.45 part.
Described BiOX is bismuth oxybromide.
The present invention also provides a kind of preparation method of termite-killing trapping medicament, comprises the steps:
1) take the former powder of raw material chlorfenapyr by proportioning, the former powder of ivermectin, shitosan, asparatate, sucrose, pollen pini, diatom powder add the mixing of appropriate distilled water, heating stirs;
2) by step 1) in mixture hairbrush be painted on paper or with high-pressure spray gun and be evenly sprayed at paper, brushing dose is the one side fully filling paper;
3) by step 2) in brushed admixing medical solutions the scraps of paper make pellet or sheet or column, the constant temperature oven drying being placed in 35-50 DEG C is anhydrated, and drying time is not less than 48h; Or take vacuum cooling drying to anhydrate, termiticides of the present invention can be obtained.
Above-mentioned steps 1)-3) all carry out under the illumination condition of 10-50lux.
The present invention also provides the preparation method of another kind of termite-killing trapping medicament, comprises the steps:
1) take the former powder of raw material chlorfenapyr by proportioning, the former powder of ivermectin, shitosan, asparatate, sucrose, pollen pini, diatom powder add the mixing of appropriate distilled water, heating stirs;
2) by the bagasse pulverized or crops straw and tea root powder, after BiOX mixing, add suitable quantity of water stir after with step 1) in pastel mix, flood 10-24h;
3) by step 2) in mixture make pellet or sheet or column or Powdered, the constant temperature oven drying being placed in 35-50 DEG C is anhydrated, and drying time is not less than 48h; Or take vacuum cooling drying to anhydrate, termiticides of the present invention can be obtained.
Above-mentioned steps 1)-3) all carry out under the illumination condition of 10-50lux.
The medicine of the control termites obtained by preparation method of the present invention, also can be added termite bait and make bait formulation bag, also can directly be invested in termite activity place, compared with prior art, and beneficial effect of the present invention:
(1) the present invention is compared with traditional chemical control, greatly reduces the usage amount of chemical agent, reduces the security threat to environment, human health;
(2) medicament of control termites provided by the invention, active drug composition is chlorfenapyr and ivermectin mixture, can strengthen drug effect, stops pesticide resistance, improves control efficiency;
(3) the present invention uses sucrose, shitosan in formula, stronger allure is had to termite, after sugar being dissolved simultaneously, its stickiness is utilized each component to be sticked together and stick on paper, strengthen the stability of each component, shitosan is generally used as slow releasing carrier of medication, can extend the lasting period of each component of the present invention, asparatate can strengthen the food ingestion of termite, slows down the release of chlorfenapyr and ivermectin medicament simultaneously;
(4) the present invention is with pollen pini, diatom powder for component, and pollen pini has stronger allure to termite, and diatom powder has disinfection, anti-mildew effect, can extend the lasting period of medicament of the present invention;
(5) medicament provided by the invention can overcome existing medicament and knocks down fireballing shortcoming to termite, is convenient to the virulence transmission of termite to medicament, realizes killing termite colony;
(6) tea root powder, the interpolation of BiOX promotes the attractant effect of termite, each component lasting period extends the positive role served.
(7) compared with existing medicament, medicament dosage provided by the invention is few, and cost is lower, applied widely.
Embodiment
Below the invention will be further described for experiment and example, but do not do pro forma restriction to the present invention.
Embodiment 1
A kind of control termites medicament and preparation method, comprise the steps:
1) take the former powder of raw material chlorfenapyr by proportioning, the former powder of ivermectin, shitosan, asparatate, sucrose, pollen pini, diatom powder add the mixing of appropriate distilled water, heating stirs;
2) by step 1) in mixture hairbrush be painted on paper or with high-pressure spray gun and be evenly sprayed at paper, brushing dose is the one side fully filling paper;
3) by step 2) in brushed admixing medical solutions the scraps of paper make pellet or sheet or column, the constant temperature oven drying being placed in 35-50 DEG C is anhydrated, and drying time is not less than 48h; Or take vacuum cooling drying to anhydrate, termiticides of the present invention can be obtained.
Above-mentioned steps 1)-3) all carry out under the illumination condition of 10lux.
The present invention also provides the preparation method of another kind of termite-killing trapping medicament, comprises the steps:
1) take the former powder of raw material chlorfenapyr by proportioning, the former powder of ivermectin, shitosan, asparatate, sucrose, pollen pini, diatom powder add the mixing of appropriate distilled water, heating stirs;
2) by the bagasse pulverized or crops straw and tea root powder, after BiOX mixing, add suitable quantity of water stir after with step 1) in pastel mix, flood 10-24h;
3) by step 2) in mixture make pellet or sheet or column or Powdered, the constant temperature oven drying being placed in 35-50 DEG C is anhydrated, and drying time is not less than 48h; Or take vacuum cooling drying to anhydrate, termiticides of the present invention can be obtained.
Above-mentioned steps 1)-3) all carry out under the illumination condition of 10lux.
Laboratory test
Formula 1: 40 parts, paper, chlorfenapyr 0.0057 part, ivermectin 0.0023 part, shitosan 14 parts, asparatate 0.0035 part, sucrose 27 parts, pollen pini 14 parts, diatom powder 5 parts.
Formula 2: 40 parts, paper, chlorfenapyr 0.01 part, ivermectin 0.001 part, shitosan 14 parts, asparatate 0.008 part, sucrose 27 parts, pollen pini 14 parts, diatom powder 5 parts.
Formula 3: 40 parts, paper, chlorfenapyr 0.001 part, ivermectin 0.01 part, shitosan 14 parts, sucrose 27 parts, pollen pini 14 parts, asparatate 0.0055 part, diatom powder 5 parts, 8 parts, tea root powder, bismuth oxybromide 0.22 part.
Formula 4: 40 parts, paper, chlorfenapyr 0.0057 part, ivermectin 0.0023 part, asparatate 0.0035 part, shitosan 14 parts, sucrose 27 parts, pollen pini 14 parts, diatom powder 5 parts, 10.5 parts, tea root powder, bismuth oxybromide 0.45 part.
Formula 5: 38 parts, paper, chlorfenapyr 0.0068 part, ivermectin 0.0045 part, asparatate 0.0018 part, shitosan 13 parts, sucrose 16 parts, pollen pini 14 parts, diatom powder 7 parts, 6.2 parts, tea root powder, bismuth oxybromide 0.24 part.
Eastern subterranean termite Reticulitermes speratus (Rolbe) is utilized to do effect experiment to the termite-killing trapping medicament of above 5 formulas in indoor, as follows in detail.
Test material and equipment: eastern subterranean termite R.speratus, pick up from Urban Area of Yichang City (30 ° 42 ' 13.6017 " N, 111 ° 16 ' 37.8733 " E), in 27 ± 1 DEG C, under 80 ± 5%RH dark condition raise one week for subsequent use.
Electronic analytical balance AL204 (plum Teller-towing force multiple instruments (Shanghai) Co., Ltd.), intelligent constant-temperature constant humidity cabinet HSX-350 (Shanghai Fuma Experiment Equipment Co., Ltd.).
Test method:
Indoor poison test
In the culture dish of diameter 9cm, bottom layer overlay fine sand (crossing 40 orders also moistening with 0.5ml distilled water), the sheet medicament that 0.50 ± more than 0.01g fills a prescription is taken with the electronic analytical balance that precision is 0.0001g, move into 50 healthy and strong eastern subterranean termite worker ants, cover culture dish lid and be placed in 27 ± 1 DEG C, under 80 ± 5%RH dark condition, observe that termite takes food, knocks down, death condition, with 0.5g filter paper for contrast.Each process repetition 3 times.During inspection, foot and feeler activity but normally can not creep and be judged to knock down, be then judged to be death without any reaction.After off-test, taken out by medicament, oven dry is weighed.
Result of the test
As can be seen from Table 1, the medicament of each formula is all lower to eastern subterranean termite rate of knockdown in 6 hours, and the worker ant rate of knockdown of 2 process of wherein filling a prescription is the highest, is 14.0%, and the rate of knockdown of formula 1,3,4 pairs of worker ants is significantly higher than formula 2,5.Process after 24 hours, the rate of knockdown of formula 2,5 pairs of worker ants is not yet more than 20%.As a child, the rate of knockdown of formula 1 pair of worker ant reaches 100%, is significantly higher than other process of respectively filling a prescription in process 48, is secondly formula 4, formula 3.
As can be seen from Table 2, the medicament of each formula is all lower to eastern subterranean termite worker ant lethality rate in 6 hours, and 2,5 process of wherein filling a prescription are all dead without worker ant.Process after 24 hours, formula 1-5 process worker ant lethality is all no more than 27.3%.Process after 48 hours, the lethality of formula 1 process worker ant reaches 100%, is significantly higher than other process of respectively filling a prescription, and is secondly formula 4, formula 3.The lethality of formula 1,3,4 process worker ant is significantly higher than formula 2,5.
As can be seen from Table 3, the food ingestion size of eastern subterranean termite worker ant to formula 1-5 is: formula 1> formula 4> formula 5> formula 3> formula 2, without significant difference between formula 1-5, the food ingestion of worker ant to formula 1-5 is all significantly higher than contrast.
Due to medicament be used as termite go out control time, first need termite to take food, then take back nest body and transmit mutually, therefore need termite to survive longer time.Arranging in formula 1 medicament 24 hours, worker ant rate of knockdown and lethality only have 33.3% and 27.3% respectively, and after 48 hours, termite rate of knockdown and lethality all reach 100%, are more suitable for producing termite control.Termite only needs the medicament taking food small amount simultaneously, can reach killing effect.Formula 4,3 medicaments of filling a prescription slightly are worse than formula 1 medicament in effect, and also reaching goes out preferably controls effect.
The table 1 different disposal time respectively fills a prescription to the rate of knockdown of eastern subterranean termite worker ant
Note: the different letter representations after same column numerical value (mean value ± SD) carry out significant difference after variance analysis (P < 0.05) through Duncan multiple comparison graph, lower same.
The table 2 different disposal time respectively fills a prescription the lethality of eastern subterranean termite worker ant
Table 3 eastern subterranean termite is to the food ingestion of different formulations medicament
Note: the different letter representations after colleague's numerical value (mean value ± SD) carry out significant difference after variance analysis (P < 0.05) through Duncan multiple comparison graph.
Indoor toxicity transmission is tested
In the culture dish of diameter 9cm, bottom layer overlay fine sand (crossing 40 orders also moistening with 0.5ml distilled water), the sheet medicament of 0.50 ± 0.01g formula 1 is taken with electronic balance, move into 50 healthy and strong eastern subterranean termite worker ants, cover culture dish lid and be placed in 27 ± 1 DEG C, under 80 ± 5%RH dark condition, observe that termite takes food, knocks down, death condition.When termite in culture dish knock down or death toll more than 20% time, the termite of wherein 10 still normal activities is proceeded to another and is placed with in the culture dish of 40 eastern subterranean termite worker ants and observes, raise 50 eastern subterranean termite worker ants for contrast with 0.5g filter paper.Each process repetition 3 times.Knock down with death determination standard the same, from proceed to band malicious termite time timing.
Result of the test
As can be seen from Table 4, taking food the poison of the band after medicament worker ant transferring to after in the worker ant with poison, the toxicity of medicament can be made to be transmitted by contacting with each other.After 48 hrs, worker ant rate of knockdown and lethality lower, but after 72 hours, worker ant is all dead.
Worker ant passes to other individualities again and causes it to be poisoned to death after taking food medicament provided by the invention, it is a process relatively slowly, under laboratory test environment, medicament provided by the invention can be contacted with each other by termite and transmits at least one times and can kill the individuality transmitted.But due to experimental enviroment limitation, termite certainly will contact frequently in narrow space, therefore need increase field test or prove effect of the present invention in actual applications.
Table 4 takes food rate of knockdown and the lethality of the rear worker ant of worker ant transfer of medicament
Effect of the present invention
The present invention is adopted to obtain the practice of medicament in termite control of control termites.
Implementation method: application comprises medicament of the present invention and processes the termite control business accepted, carried out paying a return visit check more than 1 time until ant evil is controlled within contracted scope to it in 6 months to 2 years.
Implementation result: take suitable method to carry out termite control according to actual conditions in each termite damage place, but all with prescription medicament provided by the invention for core technology.After administering, do not receive the complaint that service object finds termite damage again.Applicant takes the control efficiency of mode to the medicament of control termites provided by the invention of paying a return visit investigation to evaluate.Through observing, except having a small amount of termite activity during two test site checks, all the other 18 test site termite damages are all effectively controlled, without termite activity sign (table 5).
In summary, a kind of termite-killing trapping medicament provided by the invention, can make different dosage form according to actual conditions, is particularly suitable for termite and goes out and control.When arranging medicament provided by the invention, should ensure that the termite that quantity is many as far as possible takes food medicament provided by the invention.Should be arranged on the position that termite activity is frequent or possibility is movable, and attention is blocked, lucifuge, does not affect the normal foraging activity of termite.
Table 5 termite-killing trapping medicament implementation result
Note: make with medicament have the difformities such as sheet, pellet, column, every sheet (ball, post) numeration amount is 1.
Claims (10)
1. a termite-killing trapping medicament, it is characterized in that, the medicament of described control termites comprises the raw material composition of following weight portion: paper 30-50 part, chlorfenapyr 0.001-0.01 part, ivermectin 0.001-0.01 part, asparatate 0.001-0.01 part, shitosan 10-20 part, sucrose 10-30 part, pollen pini 5-20 part, diatom powder 5-10 part.
2. the termite-killing trapping medicament according to claim, it is characterized in that, the medicament of described control termites comprises the raw material composition of following weight portion: 40 parts, paper, chlorfenapyr 0.0057 part, ivermectin 0.0023 part, asparatate 0.0035 part, shitosan 14 parts, sucrose 27 parts, pollen pini 14 parts, diatom powder 5 parts.
3. termite-killing trapping medicament according to claim 1 and 2, is characterized in that, the medicament of this control termites also comprises tea root powder 5-15 part, BiOX 0.1-1 part.
4. termite-killing trapping medicament according to claim 1 and 2, is characterized in that, the medicament of this control termites also comprises 10.5 parts, tea root powder, BiOX 0.45 part.
5. the termite-killing trapping medicament according to claim 3 or 4, is characterized in that, described BiOX is bismuth oxybromide.
6. termite-killing trapping medicament according to claim 1 and 2, is characterized in that, described paper can also replace with bagasse or crops straw, and after wherein bagasse, crops straw are crushed to 1-10mm, methyl alcohol extracts obtained.
7. the termite-killing trapping medicament according to claim 1 or 2 or 6, it is characterized in that, described paper is wood pulp paper, paper sheet thickness 0.01-0.1mm, long 100-400mm, wide 50-200mm, described pollen pini is the dry pollen of pine genus plant, granularity crosses 40-80 order, and described diatom powder granularity crosses 40-120 order.
8. the preparation method of the termite-killing trapping medicament according to any one of claim 1-7, is characterized in that, comprise the steps:
1) take the former powder of raw material chlorfenapyr by proportioning, the former powder of ivermectin, shitosan, asparatate, sucrose, pollen pini, diatom powder add the mixing of appropriate distilled water, heating stirs;
2) be painted on paper or with high-pressure spray gun by the mixture hairbrush in step 1) and evenly spray on paper, admixing medical solutions brushing amount is fully to fill the one side of paper for the best;
3) by step 2) in brushed admixing medical solutions the scraps of paper make pellet or sheet or column, the constant temperature oven drying being placed in 35-50 DEG C is anhydrated, and drying time is not less than 48h; Or take vacuum cooling drying to anhydrate, termiticides of the present invention can be obtained.
9. the preparation method of the termite-killing trapping medicament according to any one of claim 1-7, is characterized in that, comprise the steps:
1) take the former powder of raw material chlorfenapyr by proportioning, the former powder of ivermectin, shitosan, asparatate, sucrose, pollen pini, diatom powder add the mixing of appropriate distilled water, heating stirs;
2) by the bagasse pulverized or crops straw and tea root powder, after BiOX mixing, add after suitable quantity of water stirs and mix with the pastel in step 1), flood 10-24h;
3) by step 2) in mixture make pellet or sheet or column or Powdered, the constant temperature oven drying being placed in 35-50 DEG C is anhydrated, and drying time is not less than 48h; Or take vacuum cooling drying to anhydrate, termiticides of the present invention can be obtained.
10. the preparation method of termite-killing trapping medicament according to claim 8 or claim 9, is characterized in that: step 1)-3) all carry out under the illumination condition of 10-50lux.
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| CN112400916A (en) * | 2020-12-09 | 2021-02-26 | 湖南科力除虫药械有限公司 | Termite trapping agent and preparation method and application thereof |
| CN113068711A (en) * | 2021-04-13 | 2021-07-06 | 安徽黑包公有害生物防控有限公司 | Ant prevention and treatment medicine and preparation method thereof |
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| CN105211064A (en) * | 2015-10-26 | 2016-01-06 | 广东省昆虫研究所 | A kind of termite bait formulation containing ethyl pleocidin |
| CN107347911A (en) * | 2017-08-29 | 2017-11-17 | 湖南淼农环保科技发展有限公司 | A kind of environment-friendly type medicament for preventing and treating termite and preparation method thereof |
| CN112400916A (en) * | 2020-12-09 | 2021-02-26 | 湖南科力除虫药械有限公司 | Termite trapping agent and preparation method and application thereof |
| CN113068711A (en) * | 2021-04-13 | 2021-07-06 | 安徽黑包公有害生物防控有限公司 | Ant prevention and treatment medicine and preparation method thereof |
| CN113068711B (en) * | 2021-04-13 | 2022-09-02 | 安徽黑包公有害生物防控有限公司 | Ant prevention and treatment medicine and preparation method thereof |
| CN113854319A (en) * | 2021-10-27 | 2021-12-31 | 温州绿亚科技服务有限公司 | Method for preventing and treating termite diseases and insect pests |
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| CN104938528B (en) | 2017-10-13 |
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