CN103053628B - A kind of plant source fire ant bait agent - Google Patents
A kind of plant source fire ant bait agent Download PDFInfo
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- CN103053628B CN103053628B CN201210080051.0A CN201210080051A CN103053628B CN 103053628 B CN103053628 B CN 103053628B CN 201210080051 A CN201210080051 A CN 201210080051A CN 103053628 B CN103053628 B CN 103053628B
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Abstract
The present invention relates to red fire ant technical field of pharmaceuticals, specifically a kind of bait formulation type red fire ant medicine.The active ingredient of the bait formulation is the extract of cattail platymiscium typha angustifolia (T.angustifolia L.) complete stool, can be the one or more in root extract or stem extraction or flower extract, can be ethanol extract or petroleum ether layer extract or ethyl acetate layer extract in extract, its mass percent is 0.02%~5%.The active component of the bait formulation extracts from natural plants, in the environment can be degradable after, does not have residual contamination.The bait formulation has slow cytotoxicity, and it can lure red fire ant worker ant to be moved back to ant nest, and the habit by mutually being fed between red fire ant individual, its toxicity is delivered into queen and other individuals, so as to reach the preventive effect for killing full nest red fire ant.
Description
Technical field
The present invention relates to red fire ant technical field of pharmaceuticals, specific to a kind of bait formulation red fire ant medicine of safety and environmental protection.
Technical background
S.invicta Buren (Solenopsis invicta) belongs to Hymenoptera (Hymenoptera) Formicidae (Formicidae)
Myrmicinae (Myrmicinae) Solenopsis (Solenopsis), Parana (Parana) basin of South America is originated in,
Including states such as Brazil, Paraguay, Argentina.2003, China Taiwan reported that discovery has a red fire ant invasion first, in September, 2004,
Find that the ground such as red fire ant epidemic situation, Guangxi, Hunan, Fujian, Hong Kong, Macao also finds that invasion is red in succession first in Wuchuan City, Guangdong Province
Fiery ant.
Period poison bait control red fire ant effect is good, and time and labour saving is laborsaving, is suitable for the Solenopsis invicta of large area, is current
The means of prevention carried out energetically.But the period poison bait red fire ant cycle is longer, take effect slowly, and the environmental condition launched to poison bait will
Ask higher.Red fire ant category social insect, different individuals has the different divisions of labor in society in a complete nest group.Queen is
The individual uniquely multiplied in ant nest with reproductive function, guarantee ant colony existence；Worker ant maintains the whole daily routines of ant nest, bag
Include it is outgoing look for food, the defence of nest body, the function such as the nursing of queen and the young；Young ant is particularly liquefaction of the 4 age children ants to food
Have the function that irreplaceable；Aner is only responsible for mating, and nuptial flight post-coitum is death.Have between red fire ant difference nest group compatible
Property, prevented and kill off during the chemical prevention of red fire ant not thoroughly, its nubbin will be reassembled into new nest body and be able to after
It is continuous to live and reproduce.In order to reach full nest death or the completely purpose of control red fire ant, it is necessary to queen and other reproduction ants are killed,
Inclusive pupa.Pointed out according to researchs such as StringerI, a kind of insecticide of effectively poison bait must is fulfilled for following condition：A) exist
More than 10-100 times dosage range has slow cytotoxicity；B) toxic agent can quickly be passed in ant colony by cross report
Pass, and can kill by medicine ant；C) there is no avoidance effect to worker ant of looking for food；D) easily preparation is made with food and other carriers.And
Bait as red fire ant trapping must also is fulfilled for following requirement：1) bait must be cheap material；2) bait
It is processed and easily makes certain formulation；3) bait can easily be used with traditional dispenser equipment；4) bait drops after applying
Rain, do not influence gathering effect；5) bait is to people and animals, wild animal and aquatile safety；6) milk in herbivore, in meat with
And it can not be accumulated in vegetables.Red fire ant poison bait is typically made up of toxic agent and attractant two parts.Period poison bait red fire ant is to utilize
The food of red fire ant hobby adds attractant as carrier, and the stomach poison and insect growth of sustained release are then added in bait
Conditioning agent.Develop at present mainly has hydramethylnon, fenoxycarb, pyriproxyfen, methoprene, Avermectin for the toxic agent of Solenopsis invicta
Element, sulfluramid, ethiprole, boric acid etc., and the corn particle that attractant is mainly soybean oil and degreasing is ground.
Period poison bait red fire ant is started from the 1960s, state big by United States Department of Agriculture, Auburn University and Mississippi
Propose and apply to put into practice first.Reported for work currently with the research of botanical pesticide preventing and treating red fire ant is less at home and abroad, bear
Loyal China have studied influence of the nimbin to red fire ant virgin's queen fecundity, and Zhang Songsheng has applied for that rotenone, matrine, goat's horn are turned round
Glucoside, coniine, jervine etc. are therein a kind of or the preventing and treating fire ant bait agent patent of mutual mixture, Liu Na have studied photoactivation agriculture
Behavioral toxicology of the medicine α-terthienyl to red fire ant.A kind of trichome plant of having reported for work such as Styrsky JD can indirectly increase
The natural enemy of more red fire ants.
Chemical pesticide bait formulation insecticidal constituent only has one or two kinds of, and composition is single, and long-term use of red fire ant is also easy to produce anti-
Property, and residues of pesticides largely are also easy to produce using chemical pesticide, pollution is produced to environment.Rotenone, matrine, goat's horn turn round glucoside,
The plant sources such as coniine, jervine, which kill ant active component, has acute toxic action or preventive effect unobvious to red fire ant.
The content of the invention
Technical problem solved by the invention be to provide it is a kind of red fire ant is not likely to produce drug-fast, trapping effect is good
, and the fire ant bait agent of the environmentally friendly type without residues of pesticides.
The present invention is realized by following technical scheme：
Kill ant active component：The extract of typha angustifolia (T.angustifolia L.) complete stool, can be root extract,
One or more in stem extraction, flower extract, leaf extract, can be ethanol extract, petroleum ether extraction in extract
One or more in thing, ethyl acetate layer extract, its mass percent are 0.02%~5%；
Bait：Tea seed cake, the mass percent of its total content Gu bait formulation is 30%~50%
Feeding attractants：Flavoring apple essence or sucrose sugar or one kind in honey or its mixture, its total content Gu bait formulation
Mass percent is 44.5%~69.48%
Preservative：0.5% sorbic acid
The present invention has following remarkable result than prior art：
The active ingredient of the fire ant bait agent of the present invention is to extract and obtain from a kind of brand-new vegetable material, is had no at present
Any relevant plant extracts is to reporting for work in terms of Solenopsis invicta.The day that bait, the active insecticidal components of the bait formulation take
Right plant, it is thus possible to degrade in natural environment, do not remain, destruction will not be polluted to environment.The activity of the bait formulation
Composition is complicated typha angustifolia primary extract, thus red fire ant will not develop immunity to drugs to it.
Tea seed cake is added in the bait of the bait formulation simultaneously, tea seed cake there can not only be attracting action to red fire ant, and right
Red fire ant also has certain toxic effect, is a kind of synergist, while tea seed cake or a kind of organic fertilizer, to being destroyed by red fire ant
Lawn have and expedite the emergence of long and repair.
The active insecticidal components of the bait formulation have good chronic toxic effect to red fire ant, can be by red fire ant
After ant nest is carried back in worker ant feeding, the effect killed is produced to whole nest red fire ant.
Embodiment
Plant source type fire ant bait agent is described in detail below by embodiment.
Typha angustifolia active component separating and extracting process
Typha angustifolia root, stem, flower, root flower, rhizome, scape dry powder are weighed respectively, and the ethanol for adding 5 times of volumes (W/W) enters
Row extraction, places in lucifuge shady place, extracts 24h every time, during which stirs 5 times, extracts 3 times, extract solution is merged, and filters, warp
Rotary Evaporators are concentrated under reduced pressure into dry, obtain typha angustifolia alcohol extracts, are placed in 4 DEG C of refrigerators and save backup.
Extraction is distributed using liquid liquid, by typha angustifolia root, stem, flower, root flower, rhizome, a small amount of methanol of scape extract
After dissolving, add a certain amount of water and fully shake up, be completely dissolved it, load separatory funnel, add isometric petroleum ether, shake
It is even, extract 3 times, obtain petroleum ether layer extract.Same method is extracted with ethyl acetate 3 times again, obtains ethyl acetate layer extract.
Finally remaining is water layer extract.Each several part extract is concentrated to dryness, weighs and is preserved after in 4 DEG C of refrigerators.
The typha angustifolia root petroleum ether extract fire ant bait agent of embodiment 1
Active insecticidal components are typha angustifolia root ligroin extraction in the fire ant bait agent that the present embodiment provides, according to matter
100 parts of meters of fraction are measured, the active insecticidal components take 0.02 part, and feeding inducing substance is honey, flavoring apple essence, sucrose (honey: apple
Fruity essence: sucrose=1: 0.3: 1.5) mixture takes 50, and bait tea seed cake takes 49.5 parts, and sorbic acid takes 0.5 as anti-corrosion composition
Part.
The typha angustifolia rhizome petroleum ether extract fire ant bait agent of embodiment 2
Active insecticidal components are typha angustifolia rhizome ligroin extraction in the fire ant bait agent that the present embodiment provides, according to
100 parts of meters of mass fraction, the active insecticidal components take 5 parts, and feeding inducing substance is honey, flavoring apple essence, sucrose (honey: apple
Fruity essence: sucrose=1: 0.6: 3) mixture takes 60, and bait tea seed cake takes 34.5 parts, and sorbic acid takes 0.5 part as anti-corrosion composition.
The typha angustifolia root of embodiment 3 spends petroleum ether extract fire ant bait agent
Active insecticidal components are that typha angustifolia root spends ligroin extraction in the fire ant bait agent that the present embodiment provides, according to
100 parts of meters of mass fraction, the active insecticidal components take 3 parts, and feeding inducing substance is honey, flavoring apple essence, sucrose (honey: apple
Fruity essence: sucrose=1: 0.3: 2) mixture takes 65, and bait tea seed cake takes 31.5 parts, and sorbic acid takes 0.5 part as anti-corrosion composition.
The typha angustifolia of embodiment 4 spends petroleum ether extract fire ant bait agent
Active insecticidal components are that typha angustifolia spends ligroin extraction in the fire ant bait agent that the present embodiment provides, according to matter
100 parts of meters of fraction are measured, the active insecticidal components take 5 parts, and feeding inducing substance is honey, flavoring apple essence, sucrose (honey: apple
Essence: sucrose=1: 0.6: 1.5) mixture takes 50, and bait tea seed cake takes 44.5 parts, and sorbic acid takes 0.5 part as anti-corrosion composition.
The typha angustifolia stem petroleum ether extract fire ant bait agent of embodiment 5
Active insecticidal components are typha angustifolia stem ligroin extraction in the fire ant bait agent that the present embodiment provides, according to matter
100 parts of meters of fraction are measured, the active insecticidal components take 5 parts, and feeding inducing substance is honey, flavoring apple essence, sucrose (honey: apple
Essence: sucrose=1: 0.6: 3) mixture takes 50, and bait tea seed cake takes 44.5 parts, and sorbic acid takes 0.5 part as anti-corrosion composition.
The typha angustifolia scape petroleum ether extract fire ant bait agent of embodiment 6
Active insecticidal components are typha angustifolia scape ligroin extraction in the fire ant bait agent that the present embodiment provides, according to
100 parts of meters of mass fraction, the active insecticidal components take 0.02 part, and feeding inducing substance is honey, flavoring apple essence, sucrose (honey
: flavoring apple essence: sucrose=1: 1: 2) mixture takes 54, and bait tea seed cake takes 45.5 parts, and sorbic acid takes 0.5 part as anti-corrosion composition.
The typha angustifolia root ethanol extract fire ant bait agent of embodiment 7
Active insecticidal components are typha angustifolia root ethanol extract in the fire ant bait agent that the present embodiment provides, according to quality
100 parts of meters of fraction, the active insecticidal components take 3 parts, and feeding inducing substance is honey, flavoring apple essence, sucrose (honey: apple is fragrant
Essence: sucrose=1: 1: 3) mixture takes 69, and bait tea seed cake takes 27.5 parts, and sorbic acid takes 0.5 part as anti-corrosion composition.
The typha angustifolia rhizome ethanol extract fire ant bait agent of embodiment 8
Active insecticidal components are typha angustifolia rhizome ethanol extract in the fire ant bait agent that the present embodiment provides, according to matter
100 parts of meters of fraction are measured, the active insecticidal components take 0.02 part, and feeding inducing substance is honey, flavoring apple essence, sucrose (honey: apple
Fruity essence: sucrose=1: 1: 2) mixture takes 55, and bait tea seed cake takes 44.5 parts, and sorbic acid takes 0.5 part as anti-corrosion composition.
The typha angustifolia root of embodiment 9 spends ethanol extract fire ant bait agent
Active insecticidal components are that typha angustifolia root spends ethanol extract in the fire ant bait agent that the present embodiment provides, according to matter
100 parts of meters of fraction are measured, the active insecticidal components take 5 parts, and feeding inducing substance is honey, flavoring apple essence, sucrose (honey: apple
Essence: sucrose=1: 0.3: 1.5) mixture takes 50, and bait tea seed cake takes 44.5 parts, and sorbic acid takes 0.5 part as anti-corrosion composition.
The typha angustifolia of embodiment 10 spends ethanol extract fire ant bait agent
Active insecticidal components are that typha angustifolia spends ethanol extract in the fire ant bait agent that the present embodiment provides, according to quality
100 parts of meters of fraction, the active insecticidal components take 5 parts, and feeding inducing substance is honey, flavoring apple essence, sucrose (honey: apple is fragrant
Essence: sucrose=1: 0.6: 1.5) mixture takes 50, and bait tea seed cake takes 44.5 parts, and sorbic acid takes 0.5 part as anti-corrosion composition.
The typha angustifolia stem ethanol extract fire ant bait agent of embodiment 11
Active insecticidal components are typha angustifolia stem ethanol extract in the fire ant bait agent that the present embodiment provides, according to quality
100 parts of meters of fraction, the active insecticidal components take 3 parts, and feeding inducing substance is honey, flavoring apple essence, sucrose (honey: apple is fragrant
Essence: sucrose=1: 1: 2.5) mixture takes 45, and bait tea seed cake takes 51.5 parts, and sorbic acid takes 0.5 part as anti-corrosion composition.
The typha angustifolia scape ethanol extract fire ant bait agent of embodiment 12
Active insecticidal components are typha angustifolia scape ethanol extract in the fire ant bait agent that the present embodiment provides, according to matter
100 parts of meters of fraction are measured, the active insecticidal components take 0.02 part, and feeding inducing substance is honey, flavoring apple essence, sucrose (honey: apple
Fruity essence: sucrose=1: 1: 2) mixture takes 54, and bait tea seed cake takes 45.5 parts, and sorbic acid takes 0.5 part as anti-corrosion composition.
The typha angustifolia root acetic acid ethyl ester extract fire ant bait agent of embodiment 13
Active insecticidal components are typha angustifolia root acetic acid ethyl ester extract in the fire ant bait agent that the present embodiment provides, according to
100 parts of meters of mass fraction, the active insecticidal components take 0.02 part, and feeding inducing substance is honey, flavoring apple essence, sucrose (honey
: flavoring apple essence: sucrose=1: 0.3: 1.5) mixture takes 50, and bait tea seed cake takes 49.5 parts, and sorbic acid takes as anti-corrosion composition
0.5 part.
The typha angustifolia rhizome acetic acid ethyl ester extract fire ant bait agent of embodiment 14
Active insecticidal components are typha angustifolia rhizome acetic acid ethyl ester extract in the fire ant bait agent that the present embodiment provides, and are pressed
According to 100 parts of mass fraction meter, the active insecticidal components take 5 parts, feeding inducing substance be honey, flavoring apple essence, sucrose (honey:
Flavoring apple essence: sucrose=1: 0.6: 3) mixture takes 60, and bait tea seed cake takes 34.5 parts, and sorbic acid takes 0.5 as anti-corrosion composition
Part.
The typha angustifolia root of embodiment 15 spends acetic acid ethyl ester extract fire ant bait agent
Active insecticidal components are that typha angustifolia root spends acetic acid ethyl ester extract in the fire ant bait agent that the present embodiment provides, and are pressed
According to 100 parts of meters of mass fraction, the active insecticidal components take 0.02 part, and feeding inducing substance is honey, flavoring apple essence, sucrose (honeybee
Honey: flavoring apple essence: sucrose=1: 0.8: 2) mixture takes 45, and bait tea seed cake takes 54.5 parts, and sorbic acid takes as anti-corrosion composition
0.5 part.
The typha angustifolia of embodiment 16 spends acetic acid ethyl ester extract fire ant bait agent
Active insecticidal components are that typha angustifolia spends acetic acid ethyl ester extract in the fire ant bait agent that the present embodiment provides, according to
100 parts of meters of mass fraction, the active insecticidal components take 3 parts, and feeding inducing substance is honey, flavoring apple essence, sucrose (honey: apple
Fruity essence: sucrose=1: 0.6: 2) mixture takes 45, and bait tea seed cake takes 51.5 parts, and sorbic acid takes 0.5 part as anti-corrosion composition.
The typha angustifolia stem acetic acid ethyl ester extract fire ant bait agent of embodiment 17
Active insecticidal components are typha angustifolia stem acetic acid ethyl ester extract in the fire ant bait agent that the present embodiment provides, according to
100 parts of meters of mass fraction, the active insecticidal components take 5 parts, and feeding inducing substance is honey, flavoring apple essence, sucrose (honey: apple
Fruity essence: sucrose=1: 0.6: 3) mixture takes 50, and bait tea seed cake takes 44.5 parts, and sorbic acid takes 0.5 part as anti-corrosion composition.
The typha angustifolia scape acetic acid ethyl ester extract fire ant bait agent of embodiment 18
Active insecticidal components are typha angustifolia scape acetic acid ethyl ester extract in the fire ant bait agent that the present embodiment provides, and are pressed
According to 100 parts of mass fraction meter, the active insecticidal components take 3 parts, feeding inducing substance be honey, flavoring apple essence, sucrose (honey:
Flavoring apple essence: sucrose=1: 1: 3) mixture takes 65, and bait tea seed cake takes 31.5 parts, and sorbic acid takes 0.5 part as anti-corrosion composition.
Each active ingredient of the typha angustifolia petroleum ether layer extract fire ant bait agent of embodiment 19~30 and content list
Each active ingredient of the typha angustifolia ethanol extract fire ant bait agent of embodiment 31~42 and content list
Each active ingredient of the typha angustifolia ethyl acetate layer extract fire ant bait agent of embodiment 43~54 and content list
Field test
Test site：Select Agricultural University Of South China Zengcheng farm
Test method：Each bait formulation handles 3 nest active mounds, and carries out sign with small red flag.In August, 2011 is rushed for trying
Test ground dispenser.According to ant nest size, ant nest surface and around uniformly spread fertilizer over the fields poison bait 10g in the range of 10~50cm.
Do not rained in 24h after dispenser.Before dispenser, set 10 per cell and lure measuring point, make bait with ham sausage, ham sausage is cut into thickness
About 0.3~0.5 thin slice, the special plastic for being positioned over diameter 2.5cm and having cavity, which lures, to be surveyed in bottle, and it is 1h to lure the survey time.Will
Whole lure in bottle 75% alcohol of input collects red fire ant, and records the red fire ant quantity respectively trapped a little.30 days after dispenser, same
Method traps red fire ant worker ant.Control is used as using the ham sausage of not dosing.
Bait formulation prevention effect evaluation method：
Worker ant decline rate (%)=(be averaged ant number after 1- medicines before the average ant number/medicine of bait on bait) × 100.
The typha angustifolia extract fire ant bait agent field efficiency test of table 1
| Handle bait formulation | Repeat | Worker ant average correction decline rate (%) | SE |
| Embodiment 1 | 3 | 81.35 | 2.10 |
| Embodiment 2 | 3 | 100.00 | 0.00 |
| Embodiment 3 | 3 | 100.00 | 0.00 |
| Embodiment 4 | 3 | 100.00 | 0.00 |
| Embodiment 5 | 3 | 94.79 | 1.08 |
| Embodiment 6 | 3 | 79.25 | 2.86 |
| Embodiment 7 | 3 | 68.49 | 4.41 |
| Embodiment 8 | 3 | 48.63 | 4.03 |
| Embodiment 9 | 3 | 100.00 | 0.00 |
| Embodiment 10 | 3 | 100.00 | 0.00 |
| Embodiment 11 | 3 | 47.48 | 4.70 |
| Embodiment 12 | 3 | 38.37 | 3.14 |
| Embodiment 13 | 3 | 78.97 | 2.85 |
| Embodiment 14 | 3 | 100.00 | 0.00 |
| Embodiment 15 | 3 | 73.57 | 1.75 |
| Embodiment 16 | 3 | 100.00 | 0.00 |
| Embodiment 17 | 3 | 78.93 | 6.14 |
| Embodiment 18 | 3 | 76.99 | 5.15 |
| Embodiment 19 | 3 | 100.00 | 0.00 |
| Embodiment 20 | 3 | 100.00 | 0.00 |
| Embodiment 21 | 3 | 69.14 | 3.75 |
| Embodiment 22 | 3 | 100.00 | 0.00 |
| Embodiment 23 | 3 | 83.73 | 3.94 |
| Embodiment 24 | 3 | 100.00 | 0.00 |
| Embodiment 25 | 3 | 89.98 | 1.75 |
| Embodiment 26 | 3 | 100.00 | 0.00 |
| Embodiment 27 | 3 | 67.28 | 1.94 |
| Embodiment 28 | 3 | 68.90 | 5.82 |
| Embodiment 29 | 3 | 100.00 | 0.00 |
| Embodiment 30 | 3 | 100.00 | 0.00 |
| Embodiment 31 | 3 | 54.51 | 2.97 |
| Embodiment 32 | 3 | 89.95 | 0.53 |
| Embodiment 33 | 3 | 86.87 | 1.86 |
| Embodiment 34 | 3 | 57.81 | 4.40 |
| Embodiment 35 | 3 | 77.33 | 0.49 |
| Embodiment 36 | 3 | 84.04 | 1.86 |
| Embodiment 37 | 3 | 69.40 | 1.66 |
| Embodiment 38 | 3 | 88.20 | 0.43 |
| Embodiment 39 | 3 | 42.49 | 4.67 |
| Embodiment 40 | 3 | 77.16 | 2.09 |
| Embodiment 41 | 3 | 75.13 | 5.62 |
| Embodiment 42 | 3 | 53.52 | 3.55 |
| Embodiment 43 | 3 | 100.00 | 0.00 |
| Embodiment 44 | 3 | 100.00 | 0.00 |
| Embodiment 45 | 3 | 67.85 | 4.65 |
| Embodiment 46 | 3 | 93.32 | 1.94 |
| Embodiment 47 | 3 | 100.00 | 0.00 |
| Embodiment 48 | 3 | 100.00 | 0.00 |
| Embodiment 49 | 3 | 84.04 | 1.63 |
| Embodiment 50 | 3 | 100.00 | 0.00 |
| Embodiment 51 | 3 | 43.68 | 1.25 |
| Embodiment 52 | 3 | 62.02 | 3.05 |
| Embodiment 53 | 3 | 57.37 | 6.23 |
| Embodiment 54 | 3 | 94.78 | 0.96 |
Claims (1)
1. a kind of plant source fire ant bait agent, component and proportioning are as follows according to 100 parts of meters of mass fraction：
Active insecticidal components are typha angustifolia rhizome petroleum ether extract in fire ant bait agent, should according to 100 parts of meters of mass fraction
Active insecticidal components take 5 parts, and feeding inducing substance takes 60 parts, feeding inducing substance be honey, flavoring apple essence, sucrose composition it is mixed
Compound, feeding inducing substance proportioning is honey: flavoring apple essence: sucrose=1: 0.6: 3, bait tea seed cake takes 34.5 parts, and sorbic acid is made
For anti-corrosion composition, 0.5 part is taken；Or
Active insecticidal components are typha angustifolia rhizome petroleum ether layer extract in fire ant bait agent, are counted for 100 parts according to mass fraction,
The active insecticidal components take 3 parts, and feeding inducing substance takes 68 parts, and feeding inducing substance is honey, flavoring apple essence, sucrose composition
Mixture, feeding inducing substance proportioning is honey: flavoring apple essence: sucrose=1: 0.9: 1.5, bait tea seed cake takes 28.5 parts, sorb
Acid is used as anti-corrosion composition, takes 0.5 part；Or
Active insecticidal components are that typha angustifolia root spends petroleum ether layer extract in fire ant bait agent, are counted for 100 parts according to mass fraction,
The active insecticidal components take 5 parts, and feeding inducing substance takes 50 parts, and feeding inducing substance is honey, flavoring apple essence, sucrose composition
Mixture, feeding inducing substance proportioning is honey: flavoring apple essence: sucrose=1: 0.3: 1.5, bait tea seed cake takes 44.5 parts, sorb
Acid is used as anti-corrosion composition, takes 0.5 part；Or
Active insecticidal components are that typha angustifolia root spends petroleum ether extract in fire ant bait agent, should according to 100 parts of meters of mass fraction
Active insecticidal components take 3 parts, and feeding inducing substance takes 65 parts, feeding inducing substance be honey, flavoring apple essence, sucrose composition it is mixed
Compound, feeding inducing substance proportioning is honey: flavoring apple essence: sucrose=1: 0.3: 2, bait tea seed cake takes 31.5 parts, and sorbic acid is made
For anti-corrosion composition, 0.5 part is taken；Or
Active insecticidal components are that typha angustifolia spends petroleum ether extract in fire ant bait agent, and according to 100 parts of meters of mass fraction, this is killed
Worm active component takes 5 parts, and feeding inducing substance takes 50 parts, and feeding inducing substance is the mixing of honey, flavoring apple essence, sucrose composition
Thing, feeding inducing substance proportioning is honey: flavoring apple essence: sucrose=1: 0.6: 1.5, bait tea seed cake takes 44.5 parts, and sorbic acid is made
For anti-corrosion composition, 0.5 part is taken；Or
Active insecticidal components are that typha angustifolia spends petroleum ether layer extract in fire ant bait agent, should according to 100 parts of meters of mass fraction
Active insecticidal components take 3 parts, and feeding inducing substance takes 45 parts, feeding inducing substance be honey, flavoring apple essence, sucrose composition it is mixed
Compound, feeding inducing substance proportioning is honey: flavoring apple essence: sucrose=1: 0.6: 2, bait tea seed cake takes 51.5 parts, and sorbic acid is made
For anti-corrosion composition, 0.5 part is taken；Or
Active insecticidal components are typha angustifolia root petroleum ether layer extract in fire ant bait agent, should according to 100 parts of meters of mass fraction
Active insecticidal components take 5 parts, and feeding inducing substance takes 45 parts, feeding inducing substance be honey, flavoring apple essence, sucrose composition it is mixed
Compound, feeding inducing substance proportioning is honey: flavoring apple essence: sucrose=1: 0.6: 2, bait tea seed cake takes 49.5 parts, and sorbic acid is made
For anti-corrosion composition, 0.5 part is taken；Or
Active insecticidal components are typha angustifolia root petroleum ether layer extract in fire ant bait agent, should according to 100 parts of meters of mass fraction
Active insecticidal components take 3 parts, and feeding inducing substance takes 69 parts, feeding inducing substance be honey, flavoring apple essence, sucrose composition it is mixed
Compound, feeding inducing substance proportioning is honey: flavoring apple essence: sucrose=1: 1: 3, bait tea seed cake takes 27.5 parts, sorbic acid conduct
Anti-corrosion composition, take 0.5 part；Or
Active insecticidal components are typha angustifolia stem petroleum ether layer extract in fire ant bait agent, should according to 100 parts of meters of mass fraction
Active insecticidal components take 5 parts, and feeding inducing substance takes 50 parts, feeding inducing substance be honey, flavoring apple essence, sucrose composition it is mixed
Compound, feeding inducing substance proportioning is honey: flavoring apple essence: sucrose=1: 0.6: 3, bait tea seed cake takes 44.5 parts, and sorbic acid is made
For anti-corrosion composition, 0.5 part is taken；Or
Active insecticidal components are typha angustifolia scape petroleum ether layer extract in fire ant bait agent, are counted for 100 parts according to mass fraction,
The active insecticidal components take 5 parts, and feeding inducing substance takes 46 parts, and feeding inducing substance is honey, flavoring apple essence, sucrose composition
Mixture, feeding inducing substance proportioning is honey: flavoring apple essence: sucrose=1: 1: 1.5, bait tea seed cake takes 48.5 parts, sorbic acid
As anti-corrosion composition, 0.5 part is taken；Or
Active insecticidal components are typha angustifolia scape petroleum ether layer extract in fire ant bait agent, are counted for 100 parts according to mass fraction,
The active insecticidal components take 3 parts, and feeding inducing substance takes 65 parts, and feeding inducing substance is honey, flavoring apple essence, sucrose composition
Mixture, feeding inducing substance proportioning is honey: flavoring apple essence: sucrose=1: 1: 3, bait tea seed cake takes 31.5 parts, and sorbic acid is made
For anti-corrosion composition, 0.5 part is taken；Or
Active insecticidal components are that typha angustifolia root spends ethanol extract in fire ant bait agent, and according to 100 parts of meters of mass fraction, this is killed
Worm active component takes 5 parts, and feeding inducing substance takes 50 parts, and feeding inducing substance is the mixing of honey, flavoring apple essence, sucrose composition
Thing, feeding inducing substance proportioning is honey: flavoring apple essence: sucrose=1: 0.3: 1.5, bait tea seed cake takes 44.5 parts, and sorbic acid is made
For anti-corrosion composition, 0.5 part is taken；Or
Active insecticidal components are that typha angustifolia root spends ethanol extract in fire ant bait agent, and according to 100 parts of meters of mass fraction, this is killed
Worm active component takes 3 parts, and feeding inducing substance takes 65 parts, and feeding inducing substance is the mixing of honey, flavoring apple essence, sucrose composition
Thing, feeding inducing substance proportioning is honey: flavoring apple essence: sucrose=1: 0.3: 2, bait tea seed cake takes 31.5 parts, sorbic acid conduct
Anti-corrosion composition, take 0.5 part；Or
Active insecticidal components are that typha angustifolia spends ethanol extract in fire ant bait agent, according to 100 parts of meters of mass fraction, the desinsection
Active component takes 3 parts, and feeding inducing substance takes 45 parts, and feeding inducing substance is the mixing of honey, flavoring apple essence, sucrose composition
Thing, feeding inducing substance proportioning is honey: flavoring apple essence: sucrose=1: 0.6: 2, bait tea seed cake takes 51.5 parts, sorbic acid conduct
Anti-corrosion composition, take 0.5 part；Or
Active insecticidal components are that typha angustifolia spends ethanol extract in fire ant bait agent, according to 100 parts of meters of mass fraction, the desinsection
Active component takes 5 parts, and feeding inducing substance takes 50 parts, and feeding inducing substance is the mixing of honey, flavoring apple essence, sucrose composition
Thing, feeding inducing substance proportioning is honey: flavoring apple essence: sucrose=1: 0.6: 1.5, bait tea seed cake takes 44.5 parts, and sorbic acid is made
For anti-corrosion composition, 0.5 part is taken；Or
Active insecticidal components are typha angustifolia root ethanol extract in fire ant bait agent, according to 100 parts of meters of mass fraction, the desinsection
Active component takes 5 parts, and feeding inducing substance takes 45 parts, and feeding inducing substance is the mixing of honey, flavoring apple essence, sucrose composition
Thing, feeding inducing substance proportioning is honey: flavoring apple essence: sucrose=1: 0.6: 2, bait tea seed cake takes 49.5 parts, sorbic acid conduct
Anti-corrosion composition, take 0.5 part；Or
Active insecticidal components are typha angustifolia stem ethanol extract in fire ant bait agent, according to 100 parts of meters of mass fraction, the desinsection
Active component takes 5 parts, and feeding inducing substance takes 50 parts, and feeding inducing substance is the mixing of honey, flavoring apple essence, sucrose composition
Thing, feeding inducing substance proportioning is honey: flavoring apple essence: sucrose=1: 0.6: 3, bait tea seed cake takes 44.5 parts, sorbic acid conduct
Anti-corrosion composition, take 0.5 part；Or
Active insecticidal components are typha angustifolia scape ethanol extract in fire ant bait agent, and according to 100 parts of meters of mass fraction, this is killed
Worm active component takes 5 parts, and feeding inducing substance takes 46 parts, and feeding inducing substance is the mixing of honey, flavoring apple essence, sucrose composition
Thing, feeding inducing substance proportioning is honey: flavoring apple essence: sucrose=1: 1: 1.5, bait tea seed cake takes 48.5 parts, sorbic acid conduct
Anti-corrosion composition, take 0.5 part；Or
Active insecticidal components are typha angustifolia rhizome ethanol extract in fire ant bait agent, and according to 100 parts of meters of mass fraction, this is killed
Worm active component takes 5 parts, and feeding inducing substance takes 60 parts, and feeding inducing substance is the mixing of honey, flavoring apple essence, sucrose composition
Thing, feeding inducing substance proportioning is honey: flavoring apple essence: sucrose=1: 0.6: 3, bait tea seed cake takes 34.5 parts, sorbic acid conduct
Anti-corrosion composition, take 0.5 part；Or
Active insecticidal components are typha angustifolia rhizome acetic acid ethyl ester extract in fire ant bait agent, are counted for 100 parts according to mass fraction,
The active insecticidal components take 3 parts, and feeding inducing substance takes 68 parts, and feeding inducing substance is honey, flavoring apple essence, sucrose composition
Mixture, feeding inducing substance proportioning is honey: flavoring apple essence: sucrose=1: 0.9: 1.5, bait tea seed cake takes 28.5 parts, sorb
Acid is used as anti-corrosion composition, takes 0.5 part；Or
Active insecticidal components are typha angustifolia rhizome acetic acid ethyl ester extract in fire ant bait agent, are counted for 100 parts according to mass fraction,
The active insecticidal components take 5 parts, and feeding inducing substance takes 60 parts, and feeding inducing substance is honey, flavoring apple essence, sucrose composition
Mixture, feeding inducing substance proportioning is honey: flavoring apple essence: sucrose=1: 0.6: 3, bait tea seed cake takes 34.5 parts, sorbic acid
As anti-corrosion composition, 0.5 part is taken；Or
Active insecticidal components are that typha angustifolia spends acetic acid ethyl ester extract in fire ant bait agent, should according to 100 parts of meters of mass fraction
Active insecticidal components take 3 parts, and feeding inducing substance takes 45 parts, feeding inducing substance be honey, flavoring apple essence, sucrose composition it is mixed
Compound, feeding inducing substance proportioning is honey: flavoring apple essence: sucrose=1: 0.6: 2, bait tea seed cake takes 51.5 parts, and sorbic acid is made
For anti-corrosion composition, 0.5 part is taken；Or
Active insecticidal components are that typha angustifolia spends acetic acid ethyl ester extract in fire ant bait agent, should according to 100 parts of meters of mass fraction
Active insecticidal components take 5 parts, and feeding inducing substance takes 50 parts, feeding inducing substance be honey, flavoring apple essence, sucrose composition it is mixed
Compound, feeding inducing substance proportioning is honey: flavoring apple essence: sucrose=1: 0.6: 1.5, bait tea seed cake takes 44.5 parts, sorbic acid
As anti-corrosion composition, 0.5 part is taken；Or
Active insecticidal components are typha angustifolia root acetic acid ethyl ester extract in fire ant bait agent, should according to 100 parts of meters of mass fraction
Active insecticidal components take 5 parts, and feeding inducing substance takes 45 parts, feeding inducing substance be honey, flavoring apple essence, sucrose composition it is mixed
Compound, feeding inducing substance proportioning is honey: flavoring apple essence: sucrose=1: 0.6: 2, bait tea seed cake takes 49.5 parts, and sorbic acid is made
For anti-corrosion composition, 0.5 part is taken；Or
Active insecticidal components are typha angustifolia root acetic acid ethyl ester extract in fire ant bait agent, should according to 100 parts of meters of mass fraction
Active insecticidal components take 3 parts, and feeding inducing substance takes 69 parts, feeding inducing substance be honey, flavoring apple essence, sucrose composition it is mixed
Compound, feeding inducing substance proportioning is honey: flavoring apple essence: sucrose=1: 1: 3, bait tea seed cake takes 27.5 parts, sorbic acid conduct
Anti-corrosion composition, take 0.5 part；Or
Active insecticidal components are that typha angustifolia root spends acetic acid ethyl ester extract in fire ant bait agent, are counted for 100 parts according to mass fraction,
The active insecticidal components take 5 parts, and feeding inducing substance takes 50 parts, and feeding inducing substance is honey, flavoring apple essence, sucrose composition
Mixture, feeding inducing substance proportioning is honey: flavoring apple essence: sucrose=1: 0.3: 1.5, bait tea seed cake takes 44.5 parts, sorb
Acid is used as anti-corrosion composition, takes 0.5 part；Or
Active insecticidal components are that typha angustifolia root spends acetic acid ethyl ester extract in fire ant bait agent, are counted for 100 parts according to mass fraction,
The active insecticidal components take 3 parts, and feeding inducing substance takes 65 parts, and feeding inducing substance is honey, flavoring apple essence, sucrose composition
Mixture, feeding inducing substance proportioning is honey: flavoring apple essence: sucrose=1: 0.3: 2, bait tea seed cake takes 31.5 parts, sorbic acid
As anti-corrosion composition, 0.5 part is taken；Or
Active insecticidal components are typha angustifolia stem acetic acid ethyl ester extract in fire ant bait agent, should according to 100 parts of meters of mass fraction
Active insecticidal components take 5 parts, and feeding inducing substance takes 50 parts, feeding inducing substance be honey, flavoring apple essence, sucrose composition it is mixed
Compound, feeding inducing substance proportioning is honey: flavoring apple essence: sucrose=1: 0.6: 3, bait tea seed cake takes 44.5 parts, and sorbic acid is made
For anti-corrosion composition, 0.5 part is taken；Or
Active insecticidal components are typha angustifolia scape acetic acid ethyl ester extract in fire ant bait agent, are counted for 100 parts according to mass fraction,
The active insecticidal components take 3 parts, and feeding inducing substance takes 65 parts, and feeding inducing substance is honey, flavoring apple essence, sucrose composition
Mixture, feeding inducing substance proportioning is honey: flavoring apple essence: sucrose=1: 1: 3, bait tea seed cake takes 31.5 parts, and sorbic acid is made
For anti-corrosion composition, 0.5 part is taken；Or
Active insecticidal components are typha angustifolia scape acetic acid ethyl ester extract in fire ant bait agent, are counted for 100 parts according to mass fraction,
The active insecticidal components take 5 parts, and feeding inducing substance takes 46 parts, and feeding inducing substance is honey, flavoring apple essence, sucrose composition
Mixture, feeding inducing substance proportioning is honey: flavoring apple essence: sucrose=1: 1: 1.5, bait tea seed cake takes 48.5 parts, sorbic acid
As anti-corrosion composition, 0.5 part is taken.
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| CN103349021B (en) * | 2013-07-29 | 2014-08-13 | 天津市蓟县绿普生蔬菜种植有限公司 | Crop gray mold prevention and treatment agent and preparation method thereof |
| CN103749555B (en) * | 2014-01-26 | 2016-06-15 | 华南农业大学 | A kind of toxic bait pesticide |
| CN111011367A (en) * | 2019-12-17 | 2020-04-17 | 安徽康宇生物科技工程有限公司 | Plant source bait for killing solenopsis invicta and preparation method thereof |
| CN113712049B (en) * | 2021-09-18 | 2022-11-15 | 华南农业大学 | Application of saponin extract in preventing and treating red imported fire ants |
| CN115413684B (en) * | 2022-09-22 | 2023-10-13 | 烟台固特丽生物科技股份有限公司 | Homopteran insect repellent prepared from typha extract |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6699489B1 (en) * | 2001-04-26 | 2004-03-02 | Richard Edward Driscoll, Sr. | Ecologically benign product for fire ant control |
| CN1810123A (en) * | 2006-01-20 | 2006-08-02 | 杨长举 | Botanical pesticide prepared with calamus |
| CN101189974A (en) * | 2007-11-30 | 2008-06-04 | 张颂声 | Safety environmental protection bait agent for red imported fire ant |
| CN101601395A (en) * | 2009-03-02 | 2009-12-16 | 深圳市捷立克卫生服务有限公司 | The bait for luring and killing red fire ants of improvement |
| CN101669528A (en) * | 2009-09-17 | 2010-03-17 | 惠州市南天生物科技有限公司 | Solenopsis invicta buren bait |
-
2012
- 2012-03-22 CN CN201210080051.0A patent/CN103053628B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6699489B1 (en) * | 2001-04-26 | 2004-03-02 | Richard Edward Driscoll, Sr. | Ecologically benign product for fire ant control |
| CN1810123A (en) * | 2006-01-20 | 2006-08-02 | 杨长举 | Botanical pesticide prepared with calamus |
| CN101189974A (en) * | 2007-11-30 | 2008-06-04 | 张颂声 | Safety environmental protection bait agent for red imported fire ant |
| CN101601395A (en) * | 2009-03-02 | 2009-12-16 | 深圳市捷立克卫生服务有限公司 | The bait for luring and killing red fire ants of improvement |
| CN101669528A (en) * | 2009-09-17 | 2010-03-17 | 惠州市南天生物科技有限公司 | Solenopsis invicta buren bait |
Non-Patent Citations (1)
| Title |
|---|
| 入侵红火蚁防治方法的研究进展;刘栋 等;《华中农业大学学报》;20050831;第24卷(第4期);第417～422页 * |
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