CN104922243A - Method for preparing rosa rugosa pollen from waste liquid of rosa rugosa subjected to essential oil extraction - Google Patents
Method for preparing rosa rugosa pollen from waste liquid of rosa rugosa subjected to essential oil extraction Download PDFInfo
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Abstract
The invention discloses a method for preparing rosa rugosa pollen from waste liquid of rosa rugosa subjected to essential oil extraction, relating to the technical field of waste liquid of rosa rugosa. The method comprises the following steps: 1, taking an appropriate amount of waste liquid of rosa rugosa subjected to essential oil extraction, standing, and then separating supernatant liquid to obtain primary lower-layer mixed liquid; the rosa rugosa pollen prepared from the waste liquid of rosa rugosa subjected to essential oil extraction is consistent with existing rosa rugosa pollen; the yield of the rosa rugosa pollen obtained by using the method disclosed by the invention is 6.2% to 6.5%, the waste liquid of rosa rugosa subjected to essential oil extraction is made to be profitable, so that rosa rugosa pollen resources are effectively utilized; every 500g of rosa rugosa pollen obtained by using the method disclosed by the invention sells for 100 Yuan to 130 Yuan, and therefore the economic benefit of enterprises is increased; in the meantime, the supernatant liquid obtained after standing of the primary lower-layer mixed liquid is separated and then acts as a beverage additive or an oral solution additive, and therefore water resources are effectively utilized and the production cost is reduced.
Description
Technical field
the present invention relates to Flos Rosae Rugosae waste liquid technical field, is a kind of method preparing Flos Rosae Rugosae pollen from the Flos Rosae Rugosae waste liquid after extraction quintessence oil.
Background technology
flos Rosae Rugosae (formal name used at school:rosa rugosa
), original producton location China; Belong to Rosales, Rosaceae machaka, branch bar spininess stings, imparipinnate leaf, 5 to 9, lobule, oval, has limit to sting.Petal obovate, polyphyll to half polyphyll, flower has aubergine, white, and really August phase is to JIUYUE, oblate spheroid.When Flos Rosae Rugosae is as crops, its flower is mainly used in food and refines essence Oleum Rosae Rugosae, and Oleum Rosae Rugosae is applied to the industry such as cosmetics, food, fine chemistry industry.Containing 300 various chemical components in Flos Rosae Rugosae, as the alcohol of fragrance, aldehyde, fatty acid, phenol and containing the oil of essence and fat, to wake up stomach with easing the affected liver in normal food Flos Rosae Rugosae goods, have a respite and invigorate blood circulation, looks improving and the skin nourishing, make us refreshing refreshing.
pollen is the distinctive structure of seed plant, the male gametophyte in early stage being equivalent to a sporidiole and being grown by it.Pollen mostly is spherical, and what equatorial axis was longer than pole axis is called oblate spheroid; Flat is especially called peroblate; On the contrary, what pole axis was longer than equatorial axis is called long ball shape, and long is especially called perprolate.Pollen, can be rounded at polar view finding equatorial limb, tool horn shape, tool splintery etc.Face is seen under the line, and pollen profile can rounded, oval, rhombus, square etc.Pollen size is different because kind is different, alters a great deal.
pollen wall is divided into two-layer usually, i.e. outer wall and inwall.The composition mainly pecto-cellulose of inwall, resistance is poor, easily rot on earth's surface, then decomposes through acid-alkali treatment; And outer wall main component is sporopollenin, anticorrosive and anti acid alkali performance can be strong, still remains intact in the earth formation through millions upon millions of year, so Study of Pollens form, and the structure of Main Basis outer wall.Pollen smooth surface or the various decorative pattern of tool, the type of decorative pattern is different because kind is different.Main decorative pattern has graininess, netted, cerebelloid etc.
the composition such as several amino acids, vitamin A, vitamin C, vitamin E and trace element-selenium, phospholipid, nucleic acid is rich in pollen.Pollen has intestine moistening, builds up resistance, skin moistening and whitening, resisting fatigue, nourish blood the effects such as QI invigorating.The function of pollen to gastrointestinal has good activation, can appetite strengthening, thus has additional nutrients, and can be used for treatment and becomes thin.It is also by brain centres, makes the functional rehabilitation balance of each organ of human body and coordinates, and makes bracing up of people, happy, and can allaying tiredness.Although but it is noted that pollens nutrition enriches, get rid of illness and take care of health, unsuitable polyphagia.
containing a large amount of Flos Rosae Rugosae pollen in the waste liquid of existing new fresh-rose after extracting quintessence oil, normally the Flos Rosae Rugosae waste liquid after extraction quintessence oil is directly discharged without any process, cause the waste of Flos Rosae Rugosae pollen and water resource.
Summary of the invention
the invention provides a kind of method preparing Flos Rosae Rugosae pollen from the Flos Rosae Rugosae waste liquid after extraction quintessence oil; overcome the deficiency of above-mentioned prior art; Flos Rosae Rugosae waste liquid after it effectively can solve existing extraction quintessence oil directly discharges without any process and causes the problem of the waste of Flos Rosae Rugosae pollen and water resource; the present invention is conducive to improving the added value of Flos Rosae Rugosae industry and the exploitation of a series of product; decreasing pollution, is conducive to protection of the environment simultaneously.
technical scheme of the present invention is realized by following measures: a kind of method preparing Flos Rosae Rugosae pollen from the Flos Rosae Rugosae waste liquid after extraction quintessence oil, carry out in the steps below: the first step, the Flos Rosae Rugosae waste liquid got after appropriate extraction quintessence oil leaves standstill, after the supernatant being separated after leaving standstill, obtain lower floor's mixed liquor; Second step, leaves standstill lower floor's mixed liquor, after the supernatant being separated, obtains secondary lower floor mixed liquor after leaving standstill; 3rd step, after adding edible ethanol, adjusts pH to carry out sedimentation after 9 to 11, obtains pollen liquid after sedimentation in secondary lower floor mixed liquor; 4th step, adds deionized water in pollen liquid and mix homogeneously obtains mixed liquor, and mixed liquor leaves standstill, and after the supernatant being separated, obtains three lower floor's mixed liquors after leaving standstill; 5th step, three times lower floor's mixed liquor obtains filter cake after screen filtration, filter cake is placed in baking oven and dries to constant weight, obtain Flos Rosae Rugosae pollen.
here is the further optimization and/or improvements to foregoing invention technical scheme:
flos Rosae Rugosae waste liquid after said extracted quintessence oil obtains as follows: gather new fresh-rose, the deionized water of new fresh-rose 3 doubly to 4 times quality is added in new fresh-rose, reflux, extract, is carried out while stirring after being heated to boiling, reflux, extract, 3h to 5h, stir speed (S.S.) is 150 revs/min to 180 revs/min, heats up in a steamer excess after 300 order to 500 eye mesh screens filter, obtain the Flos Rosae Rugosae waste liquid after extracting quintessence oil after reflux, extract, quintessence oil.
in the above-mentioned first step, the time of extracting the Flos Rosae Rugosae waste liquid after quintessence oil standing is 12h to 24h.
in above-mentioned second step, the time that lower floor's mixed liquor leaves standstill is 12h to 24h.
in above-mentioned 3rd step, the addition of edible ethanol is 2 times of secondary lower floor mixeding liquid volume to 3 times; In secondary lower floor mixed liquor, add edible ethanol sedimentation time after pH reconciles is 2h to 3h.
in above-mentioned 4th step, the addition of deionized water is 1 times of pollen liquid volume to 2 times; The time that mixed liquor leaves standstill is 5min to 10min.
in above-mentioned 5th step, the aperture of screen cloth is 300 order to 500 orders; The temperature that filter cake is dried in an oven is 60 DEG C to 65 DEG C.
above-mentioned Flos Rosae Rugosae is Damascus Flos Rosae Rugosae flower or purple branch Flos Rosae Rugosae or Rosa setate X R. rugosa or Flos Rosae Rugosae.
the present invention from extract the Flos Rosae Rugosae pollen prepared the Flos Rosae Rugosae waste liquid after quintessence oil and existing fresh rose flower pollen consistent; The yield of the Flos Rosae Rugosae pollen obtained by the present invention is 6.2% to 6.5%, achieve the Flos Rosae Rugosae waste liquid after by extraction quintessence oil to turn waste into wealth, Flos Rosae Rugosae pollen resource is made to obtain effective utilization, the price of every 500 grams of the Flos Rosae Rugosae pollen obtained by the present invention is 100 yuan to 130 yuan, adds the economic benefit of enterprise; Simultaneously in the present invention lower floor's mixed liquor leave standstill after the supernatant after being separated, can be used as beverage additive or oral liquid additive, thus make water resource obtain effective utilization, reduce production cost.
Accompanying drawing explanation
accompanying drawing 1 is the Electronic Speculum figure that existing Damascus flower pollen amplifies 3500 times.
accompanying drawing 2 is the Electronic Speculum figure that existing Damascus flower pollen amplifies 4000 times.
the accompanying drawing 3 Flos Rosae Rugosae pollen that to be the present invention prepare from the large horse scholar Flos Rosae Rugosae waste liquid after extracting quintessence oil amplifies the Electronic Speculum figure of 4000 times.
the accompanying drawing 4 Flos Rosae Rugosae pollen that to be the present invention prepare from the large horse scholar Flos Rosae Rugosae waste liquid after extracting quintessence oil amplifies the Electronic Speculum figure of 4300 times.
Detailed description of the invention
the present invention by the restriction of following embodiment, can not determine concrete embodiment according to technical scheme of the present invention and practical situation.
embodiment 1, should prepare the method for Flos Rosae Rugosae pollen from the Flos Rosae Rugosae waste liquid after extraction quintessence oil, carry out in the steps below: the first step, the Flos Rosae Rugosae waste liquid got after appropriate extraction quintessence oil leaves standstill, after the supernatant being separated after leaving standstill, obtain lower floor's mixed liquor; Second step, leaves standstill lower floor's mixed liquor, after the supernatant being separated, obtains secondary lower floor mixed liquor after leaving standstill; 3rd step, after adding edible ethanol, adjusts pH to carry out sedimentation after 9 to 11, obtains pollen liquid after sedimentation in secondary lower floor mixed liquor; 4th step, adds deionized water in pollen liquid and mix homogeneously obtains mixed liquor, and mixed liquor leaves standstill, and after the supernatant being separated, obtains three lower floor's mixed liquors after leaving standstill; 5th step, three times lower floor's mixed liquor obtains filter cake after screen filtration, filter cake is placed in baking oven and dries to constant weight, obtain Flos Rosae Rugosae pollen.The purity of edible ethanol is preferably 95%; In 3rd step, pH value regulates by 0.1mol/L sodium hydroxide.The supernatant after one time lower floor's mixed liquor leaves standstill can be used as beverage additive or oral liquid additive after being separated, thus makes water resource obtain effective utilization, reduces production cost.
embodiment 2, as the optimization of above-described embodiment, the Flos Rosae Rugosae waste liquid extracted after quintessence oil obtains as follows: gather new fresh-rose, the deionized water of new fresh-rose 3 doubly to 4 times quality is added in new fresh-rose, reflux, extract, is carried out while stirring after being heated to boiling, reflux, extract, 3h to 5h, stir speed (S.S.) is 150 revs/min to 180 revs/min, heats up in a steamer excess after 300 order to 500 eye mesh screens filter, obtain the Flos Rosae Rugosae waste liquid after extracting quintessence oil after reflux, extract, quintessence oil.The container of reflux, extract, can be double-deck backflow reactor.
embodiment 3, as the optimization of above-described embodiment, in the first step, the time of extracting the Flos Rosae Rugosae waste liquid after quintessence oil standing is 12h to 24h.
embodiment 4, as the optimization of above-described embodiment, in second step, the time that lower floor's mixed liquor leaves standstill is 12h to 24h.
embodiment 5, as the optimization of above-described embodiment, in the 3rd step, the addition of edible ethanol is 2 times of secondary lower floor mixeding liquid volume to 3 times; In secondary lower floor mixed liquor, add edible ethanol sedimentation time after pH reconciles is 2h to 3h.
embodiment 6, as the optimization of above-described embodiment, in the 4th step, the addition of deionized water is 1 times of pollen liquid volume to 2 times; The time that mixed liquor leaves standstill is 5min to 10min.
embodiment 7, as the optimization of above-described embodiment, in the 5th step, the aperture of screen cloth is 300 order to 500 orders; The temperature that filter cake is dried in an oven is 60 DEG C to 65 DEG C.
embodiment 8, as the optimization of above-described embodiment, Flos Rosae Rugosae is Damascus Flos Rosae Rugosae flower or purple branch Flos Rosae Rugosae or Rosa setate X R. rugosa or Flos Rosae Rugosae.
embodiment 9, should prepare the method for Flos Rosae Rugosae pollen, carry out in the steps below: the first step from the Flos Rosae Rugosae waste liquid after extraction quintessence oil, and the Flos Rosae Rugosae waste liquid got after appropriate extraction quintessence oil leaves standstill 12h, after the supernatant being separated, obtains lower floor's mixed liquor after leaving standstill; Second step, leaves standstill 15h by lower floor's mixed liquor, after the supernatant being separated, obtains secondary lower floor mixed liquor after leaving standstill; 3rd step, add edible ethanol in secondary lower floor mixed liquor after, adjust pH to carry out sedimentation 2h after 9 to 11, the addition of edible ethanol is 2 times of secondary lower floor mixeding liquid volume, obtains pollen liquid after sedimentation; 4th step, adds deionized water in pollen liquid and mix homogeneously obtains mixed liquor, and the addition of deionized water is 1 times of pollen liquid volume, and mixed liquor leaves standstill 5min, after the supernatant being separated, obtains three lower floor's mixed liquors after leaving standstill; 5th step, three times lower floor's mixed liquor obtains filter cake after 300 object screen filtrations, filter cake is placed in baking oven and dries to constant weight at temperature is 60 DEG C, obtain Flos Rosae Rugosae pollen.Employing weight (W/W) measures the yield in the Flos Rosae Rugosae waste liquid of Flos Rosae Rugosae pollen after it extracts quintessence oil; The yield of the Flos Rosae Rugosae pollen that the present embodiment obtains is 6.2%.
embodiment 10, should prepare the method for Flos Rosae Rugosae pollen from the Flos Rosae Rugosae waste liquid after extraction quintessence oil, carry out in the steps below: the first step, the Flos Rosae Rugosae waste liquid got after appropriate extraction quintessence oil leaves standstill 24h, after the supernatant being separated after leaving standstill, obtain lower floor's mixed liquor; Second step, leaves standstill 24h by lower floor's mixed liquor, after the supernatant being separated, obtains secondary lower floor mixed liquor after leaving standstill; 3rd step, add edible ethanol in secondary lower floor mixed liquor after, adjust pH to carry out sedimentation 3h after 9 to 11, the addition of edible ethanol is 3 times of secondary lower floor mixeding liquid volume, obtains pollen liquid after sedimentation; 4th step, adds deionized water in pollen liquid and mix homogeneously obtains mixed liquor, and the addition of deionized water is 2 times of pollen liquid volume, and mixed liquor leaves standstill 8min, after the supernatant being separated, obtains three lower floor's mixed liquors after leaving standstill; 5th step, three times lower floor's mixed liquor obtains filter cake after 500 object screen filtrations, filter cake is placed in baking oven and dries to constant weight at temperature is 65 DEG C, obtain Flos Rosae Rugosae pollen.Employing weight (W/W) measures the yield in the Flos Rosae Rugosae waste liquid of Flos Rosae Rugosae pollen after it extracts quintessence oil; The yield of the Flos Rosae Rugosae pollen that the present embodiment obtains is 6.5%.
demonstration test
test foundation: People's Republic of China (PRC) national metrological verification regulations JJG550-88(scanning electron microscope)
test organization: Xinjiang Medicine University's Electron Microscopy Room
test instrunment: Japanese JEOLSM-630LV scanning electron microscope
method of testing: choose the Flos Rosae Rugosae pollen powder that the present invention is prepared from the Damascus Flos Rosae Rugosae flower waste liquid after extraction quintessence oil, evenly remove cloth on the sample carrier being stained with double faced adhesive tape, Damascus Flos Rosae Rugosae flower pollen is made to stick to tape surface equably, after Damascus Flos Rosae Rugosae flower pollen to be put in vacuum evaporating instrument spraying plating gold film 3min to 4min, observe under being placed in Japanese JEOLSM-630LV type scanning electron microscope and take pictures, see Fig. 3 and Fig. 4, Electronic Speculum running voltage is 15KV; Through generally observing, choosing the representational visual field, amplifying 3500 times to 4300 times and observing pollen grain configuration, and carrying out microscopic photography.Get its representational pollen grain 10, represent variation amplitude with minima to maximum, measure pollen grain pole axis length, equator axial length, record maximum and minima, calculating mean value, represent pollen.
test result: existing Damascus Flos Rosae Rugosae flower pollen grain presents the spherical or long ball shape of class usually, equatorial view is oval, and polar view three splits circle, slightly triangular in shape, and germinal aperature is trench, and have 3 cylindrical void ditches, sample room difference is not obvious; Pollen grain superficial makings majority is the linear marking of rule, or irregular brain stricture of vagina.It is spherical that the Flos Rosae Rugosae pollen that the present invention is prepared from the Damascus Flos Rosae Rugosae flower waste liquid after extraction quintessence oil presents class, equatorial view is oval, polar view three splits circle, slightly triangular in shape, germinal aperature is trench, has 3 cylindrical void ditches, and pollen grain superficial makings majority is the linear marking of rule, according to the division rule of pollen, Damascus Flos Rosae Rugosae flower pollen grain equator axial length, all between 10um to 30um, belong to small-sized pollen grain, and the value of P/E is also close; The Flos Rosae Rugosae pollen-morphological characteristics comparison catalog that table 1 is prepared from the colored waste liquid of Damascus Flos Rosae Rugosae after extracting quintessence oil for existing Damascus Flos Rosae Rugosae flower pollen and the present invention, as can be seen from table 1, Fig. 1, Fig. 2, Fig. 3 and Fig. 4, the present invention from extract the Damascus Flos Rosae Rugosae flower pollen prepared the flower of the Damascus Flos Rosae Rugosae after quintessence oil waste liquid and existing Damascus Flos Rosae Rugosae flower pollen consistent.
in sum, the present invention from extract the Flos Rosae Rugosae pollen prepared the Flos Rosae Rugosae waste liquid after quintessence oil and existing fresh rose flower pollen consistent; The yield of the Flos Rosae Rugosae pollen obtained by the present invention is 6.2% to 6.5%, achieve the Flos Rosae Rugosae waste liquid after by extraction quintessence oil to turn waste into wealth, Flos Rosae Rugosae pollen resource is made to obtain effective utilization, the price of every 500 grams of the Flos Rosae Rugosae pollen obtained by the present invention is 100 yuan to 130 yuan, adds the economic benefit of enterprise; Simultaneously in the present invention lower floor's mixed liquor leave standstill after the supernatant after being separated, can be used as beverage additive or oral liquid additive, thus make water resource obtain effective utilization, reduce production cost.
above technical characteristic constitutes embodiments of the invention, and it has stronger adaptability and implementation result, can increase and decrease non-essential technical characteristic according to actual needs, meet the demand of different situations.
Claims (10)
1. from the Flos Rosae Rugosae waste liquid after extraction quintessence oil, prepare the method for Flos Rosae Rugosae pollen for one kind, it is characterized in that carrying out in the steps below: the first step, the Flos Rosae Rugosae waste liquid got after appropriate extraction quintessence oil leaves standstill, and after the supernatant being separated, obtains lower floor's mixed liquor after leaving standstill; Second step, leaves standstill lower floor's mixed liquor, after the supernatant being separated, obtains secondary lower floor mixed liquor after leaving standstill; 3rd step, after adding edible ethanol, adjusts pH to carry out sedimentation after 9 to 11, obtains pollen liquid after sedimentation in secondary lower floor mixed liquor; 4th step, adds deionized water in pollen liquid and mix homogeneously obtains mixed liquor, and mixed liquor leaves standstill, and after the supernatant being separated, obtains three lower floor's mixed liquors after leaving standstill; 5th step, three times lower floor's mixed liquor obtains filter cake after screen filtration, filter cake is placed in baking oven and dries to constant weight, obtain Flos Rosae Rugosae pollen.
2. the method preparing Flos Rosae Rugosae pollen from the Flos Rosae Rugosae waste liquid after extraction quintessence oil according to claim 1, it is characterized in that the Flos Rosae Rugosae waste liquid after extracting quintessence oil obtains as follows: gather new fresh-rose, the deionized water of new fresh-rose 3 doubly to 4 times quality is added in new fresh-rose, reflux, extract, is carried out while stirring after being heated to boiling, reflux, extract, 3h to 5h, stir speed (S.S.) is 150 revs/min to 180 revs/min, heats up in a steamer excess after 300 order to 500 eye mesh screens filter, obtain the Flos Rosae Rugosae waste liquid after extracting quintessence oil after reflux, extract, quintessence oil.
3. the method preparing Flos Rosae Rugosae pollen from the Flos Rosae Rugosae waste liquid after extraction quintessence oil according to claim 1 and 2, is characterized in that in the first step, and the time of extracting the Flos Rosae Rugosae waste liquid after quintessence oil standing is 12h to 24h.
4. according to claim 1 and 2ly it is characterized in that in second step from extracting the method preparing Flos Rosae Rugosae pollen the Flos Rosae Rugosae waste liquid after quintessence oil, the time that lower floor's mixed liquor leaves standstill is 12h to 24h.
5. according to claim 3ly it is characterized in that in second step from extracting the method preparing Flos Rosae Rugosae pollen the Flos Rosae Rugosae waste liquid after quintessence oil, the time that lower floor's mixed liquor leaves standstill is 12h to 24h.
6. the method preparing Flos Rosae Rugosae pollen from the Flos Rosae Rugosae waste liquid after extraction quintessence oil according to claim 1 and 2, it is characterized in that in the 3rd step, the addition of edible ethanol is 2 times of secondary lower floor mixeding liquid volume to 3 times; In secondary lower floor mixed liquor, add edible ethanol sedimentation time after pH reconciles is 2h to 3h.
7. the method preparing Flos Rosae Rugosae pollen from the Flos Rosae Rugosae waste liquid after extraction quintessence oil according to claim 3 or 4 or 5, it is characterized in that in the 3rd step, the addition of edible ethanol is 2 times of secondary lower floor mixeding liquid volume to 3 times; In secondary lower floor mixed liquor, add edible ethanol sedimentation time after pH reconciles is 2h to 3h.
8. the method preparing Flos Rosae Rugosae pollen from the Flos Rosae Rugosae waste liquid after extraction quintessence oil according to claim 1 or 2 or 3 or 4 or 5 or 6 or 7, it is characterized in that in the 4th step, the addition of deionized water is 1 times of pollen liquid volume to 2 times; The time that mixed liquor leaves standstill is 5min to 10min.
9. the method preparing Flos Rosae Rugosae pollen from the Flos Rosae Rugosae waste liquid after extraction quintessence oil according to claim 1 or 2 or 3 or 4 or 5 or 6 or 7 or 8, it is characterized in that in the 5th step, the aperture of screen cloth is 300 order to 500 orders; The temperature that filter cake is dried in an oven is 60 DEG C to 65 DEG C.
10. according to claim 1 or 2 or 3 or 4 or 5 or 6 or 7 or 8 or 9 from extracting the method preparing Flos Rosae Rugosae pollen the Flos Rosae Rugosae waste liquid after quintessence oil, it is characterized in that Flos Rosae Rugosae is Damascus Flos Rosae Rugosae flower or purple branch Flos Rosae Rugosae or Rosa setate X R. rugosa or Flos Rosae Rugosae.
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| CN103168844A (en) * | 2013-03-05 | 2013-06-26 | 蚌埠市福淋乳业有限公司 | Rose compound nutritive yoghourt |
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| JP2008115133A (en) * | 2006-11-07 | 2008-05-22 | Kinjirushi Kk | Atopic disease inhibiting composition |
| CN103168844A (en) * | 2013-03-05 | 2013-06-26 | 蚌埠市福淋乳业有限公司 | Rose compound nutritive yoghourt |
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