CN104922243B - The method that rose pollen is prepared from the rose waste liquid after extraction essential oil - Google Patents
The method that rose pollen is prepared from the rose waste liquid after extraction essential oil Download PDFInfo
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Abstract
The present invention relates to rose waste liquid technical field, is a kind of method that rose pollen is prepared in rose waste liquid after essential oil is extracted；Carry out in the steps below：The first step, the rose waste liquid after appropriate extraction essential oil is taken to be stood, by the isolated lower floor's mixed liquor of supernatant liquor after standing；The rose pollen and existing fresh rose flower pollen that the present invention is prepared from the rose waste liquid after extraction essential oil are consistent；The yield of the rose pollen obtained by the present invention is 6.2% to 6.5%, realizing turns waste into wealth the rose waste liquid after extraction essential oil, rose pollen resource is set to have obtained effective utilization, the price of every 500 grams of the rose pollen obtained by the present invention is 100 yuan to 130 yuan, adds the economic benefit of enterprise；Supernatant liquor after lower floor's mixed liquor is stood in the present invention simultaneously can be used as beverage additive or oral solution additive after separation, so that water resource has obtained effective utilization, reduce production cost.
Description
Technical field
The present invention relates to rose waste liquid technical field, is to prepare rose in a kind of rose waste liquid after essential oil is extracted
The method of flower pollen.
Background technology
Rose（Scientific name：Rosa rugosa）, original producton location China；Category Rosales, rose family machaka, the more acupunctures of branch bar,
Imparipinnate leaf, 5 to 9, leaflet, ellipse, there is side thorn.Petal obovate, polyphyll to half polyphyll, flower have aubergine, white
Color, fruiting period August to September, oblate spheroid.When rose is as crops, its flower is mainly used in food and refines essence attar of rose, rose
Rare oil is applied to the industry such as cosmetics, food, fine chemistry industry.Contain 300 various chemical components in rose, such as alcohol of fragrance,
Aldehyde, aliphatic acid, phenol and oil and fat containing essence, often eat in rose product with the awake stomach of soft liver, promoting blood circulation of having a respite, beautifying face and moistering lotion, make us
God is refreshing.
Pollen is the distinctive structure of seed plant, male gametophyte early stage developed equivalent to a microspore and by it.Flower
Powder is mostly spherical, and equatorial axis is longer than the referred to as oblate spheroid of pole axis；Especially flat is referred to as peroblate；On the contrary, pole axis be longer than it is red
Being referred to as road axle is long spherical, and especially long is referred to as perprolate.Pollen, can be rounded in polar view finding equatorial limb, has angle
Shape, tool splintery etc..Face is seen under the line, and pollen profile can rounded, oval, rhombus, square etc..Pollen size is because of kind
Category is different and different, and change is very big.
Pollen wall is generally divided into two layers, i.e. outer wall and inwall.The composition of inwall is mainly pecto-cellulose, resistance is poor,
Easily rotted in earth's surface, handle through soda acid and then decompose；And outer wall main component is sporopollenin, anticorrosive and anti acid alkali performance can be strong,
Still remained intact through millions upon millions of years in the earth formation, so Study of Pollens form, the structure of Main Basiss outer wall.Pollen surface is smooth
Or the various decorative patterns of tool, the type of decorative pattern are different because kind is different.Main decorative pattern has graininess, netted, cerebelloid
Etc..
Rich in several amino acids, vitamin A, vitamin C, vitamin E and trace elements of selenium, phosphatide, nucleic acid in pollen
Deng composition.Pollen has ease constipation, resistance building, skin moistening and whitening, antifatigue, blood-nourishing tonifying Qi and other effects.Work(of the pollen to stomach and intestine
There can be good activation, can whet the appetite, so as to have additional nutrients, be become thin available for treatment.It can also by brain centres,
The functional rehabilitation of each organ of human body is balanced and is coordinated, make bracing up for people, it is happy, and being capable of dispelling fatigue.
But get rid of illness and take care of health, should not eat more it is noted that although pollens nutrition enriches.
Contain substantial amounts of rose pollen in waste liquid after the existing extracted essential oil of new fresh-rose, typically will extraction essence
Rose waste liquid after oil directly discharges without any processing, causes the waste of rose pollen and water resource.
The content of the invention
The invention provides the method that rose pollen is prepared in the rose waste liquid after a kind of essential oil from extraction, overcome
The deficiency of above-mentioned prior art, its can effectively solve it is existing extraction essential oil after rose waste liquid without it is any processing directly row
The problem of putting and causing the waste of rose pollen and water resource, the present invention are advantageous to improve the added value and one of rose industry
The exploitation of series of products, pollution is reduced, while be advantageous to environmental protection.
The technical scheme is that realized by following measures：In a kind of rose waste liquid after essential oil from extraction
The method for preparing rose pollen, is carried out in the steps below：The first step, the rose waste liquid after appropriate extraction essential oil is taken to carry out quiet
Put, after supernatant liquor is separated after standing, obtain lower floor's mixed liquor；Second step, lower floor's mixed liquor is stood,
After supernatant liquor is separated after standing, secondary lower floor's mixed liquor is obtained；3rd step, edible wine is added in secondary lower floor's mixed liquor
After essence, tune pH is settled after being 9 to 11, and pollen liquid is obtained after sedimentation；4th step, deionized water is added in pollen liquid and is mixed
Conjunction uniformly obtains mixed liquor, and mixed liquor is stood, and after supernatant liquor is separated after standing, obtains lower floor's mixed liquor three times；The
Five steps, three times lower floor's mixed liquor filter cake is obtained after screen filtration, filter cake is placed in baking oven and is dried to constant weight, obtains rose
Pollen.
Here is the further optimization and/or improvements to foregoing invention technical scheme：
Rose waste liquid after said extracted essential oil obtains as follows：New fresh-rose is gathered, in new fresh-rose
It is middle to add new fresh-rose 3 again to the deionized water of 4 times of quality, refluxing extraction is carried out while stirring after being heated to boiling, is flowed back
3h to 5h is extracted, stir speed (S.S.) is 150 revs/min to 180 revs/min, evaporates excess through 300 mesh to 500 after refluxing extraction essential oil
Obtain extracting the rose waste liquid after essential oil after mesh sieve net filtration.
In the above-mentioned first step, it is 12h to 24h to extract the time that the rose waste liquid after essential oil is stood.
In above-mentioned second step, the time that lower floor's mixed liquor is stood is 12h to 24h.
In above-mentioned 3rd step, the addition of edible alcohol is 2 times to 3 times of secondary lower floor's mixeding liquid volume；Under secondary
It is 2h to 3h that edible alcohol sedimentation time after pH is reconciled is added in layer mixed liquor.
In above-mentioned 4th step, the addition of deionized water is 1 times to 2 times of pollen liquid volume；The time that mixed liquor is stood
For 5min to 10min.
In above-mentioned 5th step, the aperture of screen cloth is 300 mesh to 500 mesh；The temperature that filter cake is dried in an oven be 60 DEG C extremely
65℃。
Above-mentioned rose is colored Damask Rose or purple branch rose or brackish water rose or rose.
The rose pollen and existing fresh rose flower pollen phase that the present invention is prepared from the rose waste liquid after extraction essential oil
Unanimously；The yield of the rose pollen obtained by the present invention is 6.2% to 6.5%, is realized the rose after extraction essential oil
Waste liquid is turned waste into wealth, and rose pollen resource has been obtained effective utilization, every 500 grams of the rose pollen obtained by the present invention
Price be 100 yuan to 130 yuan, add the economic benefit of enterprise；After lower floor's mixed liquor is stood in the present invention simultaneously
Supernatant liquor can be used as beverage additive or oral solution additive after separation, so that water resource has obtained effective utilization, drop
Low production cost.
Brief description of the drawings
Accompanying drawing 1 is the electron microscope that existing Damascus fresh flower pollen amplifies 3500 times.
Accompanying drawing 2 is the electron microscope that existing Damascus fresh flower pollen amplifies 4000 times.
The rose pollen amplification 4000 that accompanying drawing 3 is prepared for the present invention from the damascene rose waste liquid after extraction essential oil
Electron microscope again.
The rose pollen amplification 4300 that accompanying drawing 4 is prepared for the present invention from the damascene rose waste liquid after extraction essential oil
Electron microscope again.
Embodiment
The present invention is not limited by following embodiments, can technique according to the invention scheme and actual conditions it is specific to determine
Embodiment.
Embodiment 1, the method that rose pollen should be prepared from the rose waste liquid after extraction essential oil, enters in the steps below
OK：The first step, take the rose waste liquid after appropriate extraction essential oil to be stood, after supernatant liquor is separated after standing, obtain one
Secondary lower floor's mixed liquor；Second step, lower floor's mixed liquor is stood, after supernatant liquor is separated after standing, obtained secondary
Lower floor's mixed liquor；3rd step, after adding edible alcohol in secondary lower floor's mixed liquor, tune pH is settled after being 9 to 11, is settled
After obtain pollen liquid；4th step, added in pollen liquid deionized water and it is well mixed obtain mixed liquor, mixed liquor carries out quiet
Put, after supernatant liquor is separated after standing, obtain lower floor's mixed liquor three times；5th step, lower floor's mixed liquor is through screen filtration three times
After obtain filter cake, filter cake is placed in baking oven and is dried to constant weight, obtains rose pollen.The purity of edible alcohol is preferably 95%；
In 3rd step, pH value can be adjusted by 0.1mol/L sodium hydroxides.Supernatant liquor warp after lower floor's mixed liquor standing
It can be used as beverage additive or oral solution additive after separation, so that water resource has obtained effective utilization, reduce and be produced into
This.
Embodiment 2, as the optimization of above-described embodiment, extract the rose waste liquid after essential oil and obtain as follows：Adopt
Collect new fresh-rose, new fresh-rose 3 is added in new fresh-rose again to the deionized water of 4 times of quality, after being heated to boiling
Refluxing extraction, refluxing extraction 3h to 5h are carried out while stirring, and stir speed (S.S.) is 150 revs/min to 180 revs/min, refluxing extraction
Excess is evaporated after essential oil to obtain extracting the rose waste liquid after essential oil after 300 mesh to 500 mesh sieve net filtrations.The container of refluxing extraction
It can be double-deck back flow reaction kettle.
Embodiment 3, as the optimization of above-described embodiment, in the first step, extract that the rose waste liquid after essential oil stands when
Between be 12h to 24h.
Embodiment 4, as the optimization of above-described embodiment, in second step, the time that lower floor's mixed liquor is stood for 12h extremely
24h。
Embodiment 5, as the optimization of above-described embodiment, in the 3rd step, the addition of edible alcohol is the mixing of secondary lower floor
2 times to 3 times of liquid product；It is 2h to 3h that edible alcohol sedimentation time after pH is reconciled is added in secondary lower floor's mixed liquor.
Embodiment 6, as the optimization of above-described embodiment, in the 4th step, the addition of deionized water is the 1 of pollen liquid volume
Again to 2 times；The time that mixed liquor is stood is 5min to 10min.
Embodiment 7, as the optimization of above-described embodiment, in the 5th step, the aperture of screen cloth is 300 mesh to 500 mesh；Filter cake exists
The temperature dried in baking oven is 60 DEG C to 65 DEG C.
Embodiment 8, as the optimization of above-described embodiment, rose is colored Damask Rose or purple branch rose or misery
Rose or rose.
Embodiment 9, the method that rose pollen should be prepared from the rose waste liquid after extraction essential oil, enters in the steps below
OK：The first step, take the rose waste liquid after appropriate extraction essential oil to stand 12h, after supernatant liquor is separated after standing, obtain once
Lower floor's mixed liquor；Second step, lower floor's mixed liquor is stood into 15h, after supernatant liquor is separated after standing, obtains secondary lower floor
Mixed liquor；3rd step, after adding edible alcohol in secondary lower floor's mixed liquor, tune pH carries out sedimentation 2h, edible wine after being 9 to 11
The addition of essence is 2 times of secondary lower floor's mixeding liquid volume, and pollen liquid is obtained after sedimentation；4th step, add and go in pollen liquid
Ionized water and it is well mixed obtain mixed liquor, the addition of deionized water is 1 times of pollen liquid volume, and mixed liquor stands 5min,
After supernatant liquor is separated after standing, lower floor's mixed liquor three times is obtained；5th step, three times screen cloth of lower floor's mixed liquor through 300 mesh
Filter cake is obtained after filtering, filter cake is placed in baking oven and is dried to constant weight in the case where temperature is 60 DEG C, obtains rose pollen.Using weight
Amount（W/W）Determine yield of the rose pollen in its rose waste liquid after extracting essential oil；The rose that the present embodiment obtains
The yield of pollen is 6.2%.
Embodiment 10, the method that rose pollen should be prepared from the rose waste liquid after extraction essential oil, in the steps below
Carry out：The first step, take the rose waste liquid after appropriate extraction essential oil to stand 24h, after supernatant liquor is separated after standing, obtain one
Secondary lower floor's mixed liquor；Second step, a lower floor mixed liquor is stood into 24h, after supernatant liquor is separated after standing, obtain it is secondary under
Layer mixed liquor；3rd step, after adding edible alcohol in secondary lower floor's mixed liquor, tune pH carries out sedimentation 3h after being 9 to 11, eats
The addition of alcohol is 3 times of secondary lower floor's mixeding liquid volume, and pollen liquid is obtained after sedimentation；4th step, is added in pollen liquid
Deionized water and it is well mixed obtain mixed liquor, the addition of deionized water is 2 times of pollen liquid volume, and mixed liquor is stood
8min, after supernatant liquor is separated after standing, obtain lower floor's mixed liquor three times；5th step, lower floor's mixed liquor is through 500 purposes three times
Filter cake is obtained after screen filtration, filter cake is placed in baking oven and is dried to constant weight in the case where temperature is 65 DEG C, obtains rose pollen.Adopt
Use weight（W/W）Determine yield of the rose pollen in its rose waste liquid after extracting essential oil；The rose that the present embodiment obtains
The yield of rare pollen is 6.5%.
Checking test
Test foundation：People's Republic of China (PRC) national metrological verification regulations JJG550-88（SEM）
Test organization：Xinjiang Medicine University's Electron Microscopy Room
Tester：Japanese JEOLSM-630LV ESEMs
Method of testing：Choose the rose pollen that the present invention is prepared from the Damask Rose flower waste liquid after extraction essential oil
Powder, cloth is uniformly removed on the sample carrier of double faced adhesive tape is stained with, Damask Rose flower pollen is uniformly adhered in adhesive tape table
Face, after by Damask Rose flower pollen put spraying plating golden film 3min to 4min in vacuum evaporating instrument, be placed in Japanese JEOLSM-
Observe and take pictures under 630LV type ESEMs, see Fig. 3 and Fig. 4, Electronic Speculum operating voltage is 15KV；Through generally observing, selection has
The representational visual field, amplify 3500 times to 4300 times observation pollen grain configurations, and carry out microscopic photography.Take its representative
Property pollen grain 10, variation amplitude is represented with minimum value to maximum, measurement pollen grain pole axis is long, equator axial length, record
Maximum and minimum value, average value is calculated, represent pollen.
Test result：Existing Damask Rose fresh flower pollen grain typically exhibit it is spherical or length it is spherical, equatorial view is ellipse
Circle, polar view three split circular, slightly triangular in shape, and germinal aperature is trench, there is 3 hole ditches, sample room difference unobvious；Pollen
The most linear markings for rule of grain surface texture, or irregular brain line.Damask Rose of the present invention after essential oil is extracted
The rose pollen for preparing is presented spherical in flower waste liquid, equatorial view ellipse, polar view three split it is circular, slightly triangular in shape,
Germinal aperature is trench, there is 3 hole ditches, the most linear markings for rule of pollen grain surface texture, according to drawing for pollen
Divider then, Damask Rose flower pollen grain equator axial length between 10um between 30um, belonging to small-sized pollen grain, and
P/E value also close to；Table 1 is Damask Rose of the existing Damask Rose fresh flower pollen with the present invention after essential oil is extracted
The rose pollen-morphological characteristics prepared in flower waste liquid compare list, and this is can be seen that from table 1, Fig. 1, Fig. 2, Fig. 3 and Fig. 4
The Damask Rose flower pollen and existing Damascus that invention is prepared from the Damask Rose flower waste liquid after extraction essential oil
Fresh rose flower pollen is consistent.
In summary, the rose pollen and existing rose that the present invention is prepared from the rose waste liquid after extraction essential oil are fresh
Flower pollen is consistent；The yield of the rose pollen obtained by the present invention is 6.2% to 6.5%, is realized after extraction essential oil
Rose waste liquid turn waste into wealth, rose pollen resource has been obtained effective utilization, pass through the obtained rose of the present invention
The price that every 500 grams of powder is 100 yuan to 130 yuan, adds the economic benefit of enterprise；Lower floor's mixed liquor in the present invention simultaneously
Supernatant liquor after standing can be used as beverage additive or oral solution additive after separation, so that water resource has obtained effectively
Utilize, reduce production cost.
Above technical characteristic constitutes embodiments of the invention, and it has stronger adaptability and implementation result, can basis
The non-essential technical characteristic of increase and decrease is actually needed, to meet the needs of different situations.
Claims (65)
1. the method for rose pollen is prepared in the rose waste liquid after a kind of essential oil from extraction, it is characterised in that in the steps below
Carry out：The first step, take the rose waste liquid after appropriate extraction essential oil to be stood, after supernatant liquor is separated after standing, obtain
Lower floor's mixed liquor；Second step, lower floor's mixed liquor is stood, after supernatant liquor is separated after standing, obtains two
Secondary lower floor's mixed liquor；3rd step, after adding edible alcohol in secondary lower floor's mixed liquor, tune pH is settled after being 9 to 11, is sunk
Pollen liquid is obtained after drop；4th step, added in pollen liquid deionized water and it is well mixed obtain mixed liquor, mixed liquor carries out quiet
Put, after supernatant liquor is separated after standing, obtain lower floor's mixed liquor three times；5th step, lower floor's mixed liquor is through screen filtration three times
After obtain filter cake, filter cake is placed in baking oven and is dried to constant weight, obtains rose pollen.
2. preparing the method for rose pollen in the rose waste liquid after the essential oil according to claim 1 from extraction, it is special
Sign is that the rose waste liquid after extraction essential oil obtains as follows：New fresh-rose is gathered, is added in new fresh-rose
To the deionized water of 4 times of quality, refluxing extraction, refluxing extraction 3h are carried out after being heated to boiling again while stirring for new fresh-rose 3
To 5h, stir speed (S.S.) is 150 revs/min to 180 revs/min, evaporates excess through 300 mesh to 500 eye mesh screens after refluxing extraction essential oil
Obtain extracting the rose waste liquid after essential oil after filtering.
3. the method for rose pollen is prepared in the rose waste liquid after the essential oil according to claim 1 or 2 from extraction, its
It is characterised by the first step, it is 12h to 24h to extract the time that the rose waste liquid after essential oil is stood.
4. the method for rose pollen is prepared in the rose waste liquid after the essential oil according to claim 1 or 2 from extraction, its
It is characterised by second step, the time that lower floor's mixed liquor is stood is 12h to 24h.
5. preparing the method for rose pollen in the rose waste liquid after the essential oil according to claim 3 from extraction, it is special
For sign in second step, the time that lower floor's mixed liquor is stood is 12h to 24h.
6. the method for rose pollen is prepared in the rose waste liquid after the essential oil according to claim 1 or 2 from extraction, its
It is characterised by the 3rd step, the addition of edible alcohol is 2 times to 3 times of secondary lower floor's mixeding liquid volume；Mixed in secondary lower floor
It is 2h to 3h to close addition edible alcohol sedimentation time after pH is reconciled in liquid.
7. preparing the method for rose pollen in the rose waste liquid after the essential oil according to claim 3 from extraction, it is special
For sign in the 3rd step, the addition of edible alcohol is 2 times to 3 times of secondary lower floor's mixeding liquid volume；Mixed in secondary lower floor
It is 2h to 3h that edible alcohol sedimentation time after pH is reconciled is added in liquid.
8. preparing the method for rose pollen in the rose waste liquid after the essential oil according to claim 4 from extraction, it is special
For sign in the 3rd step, the addition of edible alcohol is 2 times to 3 times of secondary lower floor's mixeding liquid volume；Mixed in secondary lower floor
It is 2h to 3h that edible alcohol sedimentation time after pH is reconciled is added in liquid.
9. preparing the method for rose pollen in the rose waste liquid after the essential oil according to claim 5 from extraction, it is special
For sign in the 3rd step, the addition of edible alcohol is 2 times to 3 times of secondary lower floor's mixeding liquid volume；Mixed in secondary lower floor
It is 2h to 3h that edible alcohol sedimentation time after pH is reconciled is added in liquid.
10. the method for rose pollen is prepared in the rose waste liquid after the essential oil according to claim 1 or 2 from extraction,
It is characterized in that in the 4th step, the addition of deionized water is 1 times to 2 times of pollen liquid volume；Mixed liquor stand time be
5min to 10min.
11. preparing the method for rose pollen in the rose waste liquid after the essential oil according to claim 3 from extraction, it is special
For sign in the 4th step, the addition of deionized water is 1 times to 2 times of pollen liquid volume；The time that mixed liquor is stood is 5min
To 10min.
12. preparing the method for rose pollen in the rose waste liquid after the essential oil according to claim 4 from extraction, it is special
For sign in the 4th step, the addition of deionized water is 1 times to 2 times of pollen liquid volume；The time that mixed liquor is stood is 5min
To 10min.
13. preparing the method for rose pollen in the rose waste liquid after the essential oil according to claim 5 from extraction, it is special
For sign in the 4th step, the addition of deionized water is 1 times to 2 times of pollen liquid volume；The time that mixed liquor is stood is 5min
To 10min.
14. preparing the method for rose pollen in the rose waste liquid after the essential oil according to claim 6 from extraction, it is special
For sign in the 4th step, the addition of deionized water is 1 times to 2 times of pollen liquid volume；The time that mixed liquor is stood is 5min
To 10min.
15. preparing the method for rose pollen in the rose waste liquid after the essential oil according to claim 7 from extraction, it is special
For sign in the 4th step, the addition of deionized water is 1 times to 2 times of pollen liquid volume；The time that mixed liquor is stood is 5min
To 10min.
16. preparing the method for rose pollen in the rose waste liquid after the essential oil according to claim 8 from extraction, it is special
For sign in the 4th step, the addition of deionized water is 1 times to 2 times of pollen liquid volume；The time that mixed liquor is stood is 5min
To 10min.
17. preparing the method for rose pollen in the rose waste liquid after the essential oil according to claim 9 from extraction, it is special
For sign in the 4th step, the addition of deionized water is 1 times to 2 times of pollen liquid volume；The time that mixed liquor is stood is 5min
To 10min.
18. the method for rose pollen is prepared in the rose waste liquid after the essential oil according to claim 1 or 2 from extraction,
It is characterized in that in the 5th step, the aperture of screen cloth is 300 mesh to 500 mesh；The temperature that filter cake is dried in an oven is 60 DEG C to 65
℃。
19. preparing the method for rose pollen in the rose waste liquid after the essential oil according to claim 3 from extraction, it is special
For sign in the 5th step, the aperture of screen cloth is 300 mesh to 500 mesh；The temperature that filter cake is dried in an oven is 60 DEG C to 65 DEG C.
20. preparing the method for rose pollen in the rose waste liquid after the essential oil according to claim 4 from extraction, it is special
For sign in the 5th step, the aperture of screen cloth is 300 mesh to 500 mesh；The temperature that filter cake is dried in an oven is 60 DEG C to 65 DEG C.
21. preparing the method for rose pollen in the rose waste liquid after the essential oil according to claim 5 from extraction, it is special
For sign in the 5th step, the aperture of screen cloth is 300 mesh to 500 mesh；The temperature that filter cake is dried in an oven is 60 DEG C to 65 DEG C.
22. preparing the method for rose pollen in the rose waste liquid after the essential oil according to claim 6 from extraction, it is special
For sign in the 5th step, the aperture of screen cloth is 300 mesh to 500 mesh；The temperature that filter cake is dried in an oven is 60 DEG C to 65 DEG C.
23. preparing the method for rose pollen in the rose waste liquid after the essential oil according to claim 7 from extraction, it is special
For sign in the 5th step, the aperture of screen cloth is 300 mesh to 500 mesh；The temperature that filter cake is dried in an oven is 60 DEG C to 65 DEG C.
24. preparing the method for rose pollen in the rose waste liquid after the essential oil according to claim 8 from extraction, it is special
For sign in the 5th step, the aperture of screen cloth is 300 mesh to 500 mesh；The temperature that filter cake is dried in an oven is 60 DEG C to 65 DEG C.
25. preparing the method for rose pollen in the rose waste liquid after the essential oil according to claim 9 from extraction, it is special
For sign in the 5th step, the aperture of screen cloth is 300 mesh to 500 mesh；The temperature that filter cake is dried in an oven is 60 DEG C to 65 DEG C.
26. the method for rose pollen is prepared in the rose waste liquid after the essential oil according to claim 10 from extraction, its
It is characterised by the 5th step, the aperture of screen cloth is 300 mesh to 500 mesh；The temperature that filter cake is dried in an oven is 60 DEG C to 65 DEG C.
27. the method for rose pollen is prepared in the rose waste liquid after the essential oil according to claim 11 from extraction, its
It is characterised by the 5th step, the aperture of screen cloth is 300 mesh to 500 mesh；The temperature that filter cake is dried in an oven is 60 DEG C to 65 DEG C.
28. the method for rose pollen is prepared in the rose waste liquid after the essential oil according to claim 12 from extraction, its
It is characterised by the 5th step, the aperture of screen cloth is 300 mesh to 500 mesh；The temperature that filter cake is dried in an oven is 60 DEG C to 65 DEG C.
29. the method for rose pollen is prepared in the rose waste liquid after the essential oil according to claim 13 from extraction, its
It is characterised by the 5th step, the aperture of screen cloth is 300 mesh to 500 mesh；The temperature that filter cake is dried in an oven is 60 DEG C to 65 DEG C.
30. the method for rose pollen is prepared in the rose waste liquid after the essential oil according to claim 14 from extraction, its
It is characterised by the 5th step, the aperture of screen cloth is 300 mesh to 500 mesh；The temperature that filter cake is dried in an oven is 60 DEG C to 65 DEG C.
31. the method for rose pollen is prepared in the rose waste liquid after the essential oil according to claim 15 from extraction, its
It is characterised by the 5th step, the aperture of screen cloth is 300 mesh to 500 mesh；The temperature that filter cake is dried in an oven is 60 DEG C to 65 DEG C.
32. the method for rose pollen is prepared in the rose waste liquid after the essential oil according to claim 16 from extraction, its
It is characterised by the 5th step, the aperture of screen cloth is 300 mesh to 500 mesh；The temperature that filter cake is dried in an oven is 60 DEG C to 65 DEG C.
33. the method for rose pollen is prepared in the rose waste liquid after the essential oil according to claim 17 from extraction, its
It is characterised by the 5th step, the aperture of screen cloth is 300 mesh to 500 mesh；The temperature that filter cake is dried in an oven is 60 DEG C to 65 DEG C.
34. the method for rose pollen is prepared in the rose waste liquid after the essential oil according to claim 1 or 2 from extraction,
It is characterized in that rose is colored Damask Rose or purple branch rose or brackish water rose or rose.
35. preparing the method for rose pollen in the rose waste liquid after the essential oil according to claim 3 from extraction, it is special
Sign is rose for Damask Rose is colored or purple branch rose or brackish water rose or rose.
36. preparing the method for rose pollen in the rose waste liquid after the essential oil according to claim 4 from extraction, it is special
Sign is rose for Damask Rose is colored or purple branch rose or brackish water rose or rose.
37. preparing the method for rose pollen in the rose waste liquid after the essential oil according to claim 5 from extraction, it is special
Sign is rose for Damask Rose is colored or purple branch rose or brackish water rose or rose.
38. preparing the method for rose pollen in the rose waste liquid after the essential oil according to claim 6 from extraction, it is special
Sign is rose for Damask Rose is colored or purple branch rose or brackish water rose or rose.
39. preparing the method for rose pollen in the rose waste liquid after the essential oil according to claim 7 from extraction, it is special
Sign is rose for Damask Rose is colored or purple branch rose or brackish water rose or rose.
40. preparing the method for rose pollen in the rose waste liquid after the essential oil according to claim 8 from extraction, it is special
Sign is rose for Damask Rose is colored or purple branch rose or brackish water rose or rose.
41. preparing the method for rose pollen in the rose waste liquid after the essential oil according to claim 9 from extraction, it is special
Sign is rose for Damask Rose is colored or purple branch rose or brackish water rose or rose.
42. the method for rose pollen is prepared in the rose waste liquid after the essential oil according to claim 10 from extraction, its
It is characterised by rose for Damask Rose is colored or purple branch rose or brackish water rose or rose.
43. the method for rose pollen is prepared in the rose waste liquid after the essential oil according to claim 11 from extraction, its
It is characterised by rose for Damask Rose is colored or purple branch rose or brackish water rose or rose.
44. the method for rose pollen is prepared in the rose waste liquid after the essential oil according to claim 12 from extraction, its
It is characterised by rose for Damask Rose is colored or purple branch rose or brackish water rose or rose.
45. the method for rose pollen is prepared in the rose waste liquid after the essential oil according to claim 13 from extraction, its
It is characterised by rose for Damask Rose is colored or purple branch rose or brackish water rose or rose.
46. the method for rose pollen is prepared in the rose waste liquid after the essential oil according to claim 14 from extraction, its
It is characterised by rose for Damask Rose is colored or purple branch rose or brackish water rose or rose.
47. the method for rose pollen is prepared in the rose waste liquid after the essential oil according to claim 15 from extraction, its
It is characterised by rose for Damask Rose is colored or purple branch rose or brackish water rose or rose.
48. the method for rose pollen is prepared in the rose waste liquid after the essential oil according to claim 16 from extraction, its
It is characterised by rose for Damask Rose is colored or purple branch rose or brackish water rose or rose.
49. the method for rose pollen is prepared in the rose waste liquid after the essential oil according to claim 17 from extraction, its
It is characterised by rose for Damask Rose is colored or purple branch rose or brackish water rose or rose.
50. the method for rose pollen is prepared in the rose waste liquid after the essential oil according to claim 18 from extraction, its
It is characterised by rose for Damask Rose is colored or purple branch rose or brackish water rose or rose.
51. the method for rose pollen is prepared in the rose waste liquid after the essential oil according to claim 19 from extraction, its
It is characterised by rose for Damask Rose is colored or purple branch rose or brackish water rose or rose.
52. the method for rose pollen is prepared in the rose waste liquid after the essential oil according to claim 20 from extraction, its
It is characterised by rose for Damask Rose is colored or purple branch rose or brackish water rose or rose.
53. the method for rose pollen is prepared in the rose waste liquid after the essential oil according to claim 21 from extraction, its
It is characterised by rose for Damask Rose is colored or purple branch rose or brackish water rose or rose.
54. the method for rose pollen is prepared in the rose waste liquid after the essential oil according to claim 22 from extraction, its
It is characterised by rose for Damask Rose is colored or purple branch rose or brackish water rose or rose.
55. the method for rose pollen is prepared in the rose waste liquid after the essential oil according to claim 23 from extraction, its
It is characterised by rose for Damask Rose is colored or purple branch rose or brackish water rose or rose.
56. the method for rose pollen is prepared in the rose waste liquid after the essential oil according to claim 24 from extraction, its
It is characterised by rose for Damask Rose is colored or purple branch rose or brackish water rose or rose.
57. the method for rose pollen is prepared in the rose waste liquid after the essential oil according to claim 25 from extraction, its
It is characterised by rose for Damask Rose is colored or purple branch rose or brackish water rose or rose.
58. the method for rose pollen is prepared in the rose waste liquid after the essential oil according to claim 26 from extraction, its
It is characterised by rose for Damask Rose is colored or purple branch rose or brackish water rose or rose.
59. the method for rose pollen is prepared in the rose waste liquid after the essential oil according to claim 27 from extraction, its
It is characterised by rose for Damask Rose is colored or purple branch rose or brackish water rose or rose.
60. the method for rose pollen is prepared in the rose waste liquid after the essential oil according to claim 28 from extraction, its
It is characterised by rose for Damask Rose is colored or purple branch rose or brackish water rose or rose.
61. the method for rose pollen is prepared in the rose waste liquid after the essential oil according to claim 29 from extraction, its
It is characterised by rose for Damask Rose is colored or purple branch rose or brackish water rose or rose.
62. the method for rose pollen is prepared in the rose waste liquid after the essential oil according to claim 30 from extraction, its
It is characterised by rose for Damask Rose is colored or purple branch rose or brackish water rose or rose.
63. the method for rose pollen is prepared in the rose waste liquid after the essential oil according to claim 31 from extraction, its
It is characterised by rose for Damask Rose is colored or purple branch rose or brackish water rose or rose.
64. the method for rose pollen is prepared in the rose waste liquid after the essential oil according to claim 32 from extraction, its
It is characterised by rose for Damask Rose is colored or purple branch rose or brackish water rose or rose.
65. the method for rose pollen is prepared in the rose waste liquid after the essential oil according to claim 33 from extraction, its
It is characterised by rose for Damask Rose is colored or purple branch rose or brackish water rose or rose.
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Non-Patent Citations (2)
| Title |
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| 玫瑰花的生药学研究初探;李明等;《中华中医药学刊》;20080131;第26卷(第1期);第109-112页 * |
| 花粉资源利用研究进展;杨晓宇等;《特产研究》;20031231(第4期);第52-55页 * |
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