CN105639400A - Banana peel antioxidant additive and preparation method thereof - Google Patents
Banana peel antioxidant additive and preparation method thereof Download PDFInfo
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- CN105639400A CN105639400A CN201511011327.XA CN201511011327A CN105639400A CN 105639400 A CN105639400 A CN 105639400A CN 201511011327 A CN201511011327 A CN 201511011327A CN 105639400 A CN105639400 A CN 105639400A
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- 239000003963 antioxidant agent Substances 0.000 title claims abstract description 23
- 238000002360 preparation method Methods 0.000 title claims abstract description 9
- 241000234295 Musa Species 0.000 title abstract 4
- 235000018290 Musa x paradisiaca Nutrition 0.000 title abstract 4
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 claims abstract description 18
- LXNHXLLTXMVWPM-UHFFFAOYSA-N pyridoxine Chemical compound CC1=NC=C(CO)C(CO)=C1O LXNHXLLTXMVWPM-UHFFFAOYSA-N 0.000 claims abstract description 16
- 229930003427 Vitamin E Natural products 0.000 claims abstract description 9
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 claims abstract description 9
- 235000019154 vitamin C Nutrition 0.000 claims abstract description 9
- 239000011718 vitamin C Substances 0.000 claims abstract description 9
- 235000019165 vitamin E Nutrition 0.000 claims abstract description 9
- 239000011709 vitamin E Substances 0.000 claims abstract description 9
- 229940046009 vitamin E Drugs 0.000 claims abstract description 9
- FPIPGXGPPPQFEQ-UHFFFAOYSA-N 13-cis retinol Natural products OCC=C(C)C=CC=C(C)C=CC1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-UHFFFAOYSA-N 0.000 claims abstract description 8
- FPIPGXGPPPQFEQ-BOOMUCAASA-N Vitamin A Natural products OC/C=C(/C)\C=C\C=C(\C)/C=C/C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-BOOMUCAASA-N 0.000 claims abstract description 8
- FPIPGXGPPPQFEQ-OVSJKPMPSA-N all-trans-retinol Chemical compound OC\C=C(/C)\C=C\C=C(/C)\C=C\C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-OVSJKPMPSA-N 0.000 claims abstract description 8
- MKJXYGKVIBWPFZ-UHFFFAOYSA-L calcium lactate Chemical compound [Ca+2].CC(O)C([O-])=O.CC(O)C([O-])=O MKJXYGKVIBWPFZ-UHFFFAOYSA-L 0.000 claims abstract description 8
- 235000011086 calcium lactate Nutrition 0.000 claims abstract description 8
- 229960002401 calcium lactate Drugs 0.000 claims abstract description 8
- 239000001527 calcium lactate Substances 0.000 claims abstract description 8
- 235000003891 ferrous sulphate Nutrition 0.000 claims abstract description 8
- 239000011790 ferrous sulphate Substances 0.000 claims abstract description 8
- 235000013923 monosodium glutamate Nutrition 0.000 claims abstract description 8
- RADKZDMFGJYCBB-UHFFFAOYSA-N pyridoxal hydrochloride Natural products CC1=NC=C(CO)C(C=O)=C1O RADKZDMFGJYCBB-UHFFFAOYSA-N 0.000 claims abstract description 8
- 235000019155 vitamin A Nutrition 0.000 claims abstract description 8
- 239000011719 vitamin A Substances 0.000 claims abstract description 8
- 235000019158 vitamin B6 Nutrition 0.000 claims abstract description 8
- 239000011726 vitamin B6 Substances 0.000 claims abstract description 8
- 235000019166 vitamin D Nutrition 0.000 claims abstract description 8
- 239000011710 vitamin D Substances 0.000 claims abstract description 8
- 229940045997 vitamin a Drugs 0.000 claims abstract description 8
- 229940011671 vitamin b6 Drugs 0.000 claims abstract description 8
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 24
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 18
- 230000003078 antioxidant effect Effects 0.000 claims description 18
- 235000006708 antioxidants Nutrition 0.000 claims description 18
- 239000000243 solution Substances 0.000 claims description 18
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 16
- 238000000605 extraction Methods 0.000 claims description 12
- 239000007788 liquid Substances 0.000 claims description 12
- 238000001035 drying Methods 0.000 claims description 10
- 238000004458 analytical method Methods 0.000 claims description 9
- 229920002538 Polyethylene Glycol 20000 Polymers 0.000 claims description 8
- 238000001953 recrystallisation Methods 0.000 claims description 8
- 238000004440 column chromatography Methods 0.000 claims description 7
- PXEDJBXQKAGXNJ-QTNFYWBSSA-L disodium L-glutamate Chemical compound [Na+].[Na+].[O-]C(=O)[C@@H](N)CCC([O-])=O PXEDJBXQKAGXNJ-QTNFYWBSSA-L 0.000 claims description 7
- BAUYGSIQEAFULO-UHFFFAOYSA-L iron(2+) sulfate (anhydrous) Chemical compound [Fe+2].[O-]S([O-])(=O)=O BAUYGSIQEAFULO-UHFFFAOYSA-L 0.000 claims description 7
- 229910000359 iron(II) sulfate Inorganic materials 0.000 claims description 7
- 229940073490 sodium glutamate Drugs 0.000 claims description 7
- 239000002594 sorbent Substances 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 5
- 238000003756 stirring Methods 0.000 claims description 5
- 238000000034 method Methods 0.000 claims description 2
- 239000011259 mixed solution Substances 0.000 claims description 2
- 230000000694 effects Effects 0.000 abstract description 4
- 230000000050 nutritive effect Effects 0.000 abstract description 3
- 230000010100 anticoagulation Effects 0.000 abstract description 2
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 abstract 2
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 abstract 1
- 206010028980 Neoplasm Diseases 0.000 abstract 1
- 229930003268 Vitamin C Natural products 0.000 abstract 1
- 229930003316 Vitamin D Natural products 0.000 abstract 1
- QYSXJUFSXHHAJI-XFEUOLMDSA-N Vitamin D3 Natural products C1(/[C@@H]2CC[C@@H]([C@]2(CCC1)C)[C@H](C)CCCC(C)C)=C/C=C1\C[C@@H](O)CCC1=C QYSXJUFSXHHAJI-XFEUOLMDSA-N 0.000 abstract 1
- 230000003064 anti-oxidating effect Effects 0.000 abstract 1
- 239000008280 blood Substances 0.000 abstract 1
- 210000004369 blood Anatomy 0.000 abstract 1
- 210000002865 immune cell Anatomy 0.000 abstract 1
- LPUQAYUQRXPFSQ-DFWYDOINSA-M monosodium L-glutamate Chemical compound [Na+].[O-]C(=O)[C@@H](N)CCC(O)=O LPUQAYUQRXPFSQ-DFWYDOINSA-M 0.000 abstract 1
- 239000004223 monosodium glutamate Substances 0.000 abstract 1
- 239000000047 product Substances 0.000 abstract 1
- 239000002994 raw material Substances 0.000 abstract 1
- 230000001988 toxicity Effects 0.000 abstract 1
- 231100000419 toxicity Toxicity 0.000 abstract 1
- 150000003710 vitamin D derivatives Chemical class 0.000 abstract 1
- 229940046008 vitamin d Drugs 0.000 abstract 1
- 230000000996 additive effect Effects 0.000 description 6
- 235000013305 food Nutrition 0.000 description 6
- 239000000654 additive Substances 0.000 description 5
- 238000001914 filtration Methods 0.000 description 3
- 239000000126 substance Substances 0.000 description 2
- BHPQYMZQTOCNFJ-UHFFFAOYSA-N Calcium cation Chemical compound [Ca+2] BHPQYMZQTOCNFJ-UHFFFAOYSA-N 0.000 description 1
- 230000000259 anti-tumor effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229910001424 calcium ion Inorganic materials 0.000 description 1
- 238000004587 chromatography analysis Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000001627 detrimental effect Effects 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 235000013373 food additive Nutrition 0.000 description 1
- 239000002778 food additive Substances 0.000 description 1
- 235000019261 food antioxidant Nutrition 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 210000003205 muscle Anatomy 0.000 description 1
- 230000004118 muscle contraction Effects 0.000 description 1
- 231100000957 no side effect Toxicity 0.000 description 1
- 230000036542 oxidative stress Effects 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/34—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
- A23L3/3454—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
- A23L3/3463—Organic compounds; Microorganisms; Enzymes
- A23L3/3526—Organic compounds containing nitrogen
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L3/00—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
- A23L3/34—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
- A23L3/3454—Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
- A23L3/3598—Apparatus for preserving using solids
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
- Y02A40/90—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in food processing or handling, e.g. food conservation
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Microbiology (AREA)
- Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
Abstract
The invention discloses a banana peel antioxidant additive and a preparation method thereof. The banana peel antioxidant additive comprises the following components: a banana peel extract product, monosodium glutamate, ferrous sulphate, calcium lactate, vitamin A, vitamin E, vitamin C, vitamin D and vitamin B6. The antioxidant additive has the advantages of natural raw materials without toxicity and side-effects, high nutritive value, and wide application; the antioxidant additive has the effects of anticoagulation, blood fat reduction, immune cell enhancement, tumor resistance, and antioxidation.
Description
Technical field
The invention belongs to technical field of food additives, it is specifically related to a kind of anti-oxidant interpolation of Pericarpium Musae and its preparation method.
Background technology
Existing food oxydating resistance additive mainly contains chemistry food oxydating resistance additive and the big class of whole food antioxidant addn two, wherein, chemistry food oxydating resistance additive effect is good, but there is shortcoming, life-time service or the excessive amounts such as toxic side effect in various degree and health is caused damage. Artificial chemistry food oxydating resistance additive refers to obtained by artificial chemical synthesis process. Meanwhile, a large amount of research reports is pointed out, nearly all chemical food oxydating resistance additive all can not provide nutritive substance to human body, and some chemistry food oxydating resistance additive even can be detrimental to health.
Summary of the invention
It is an object of the invention to overcome prior art defect, it is provided that a kind of Pericarpium Musae antioxidant addn.
Another object of the present invention is to provide the preparation method of this Pericarpium Musae antioxidant addn.
The technical scheme of the present invention is as follows:
A kind of Pericarpium Musae antioxidant addn, comprises the component of following weight part:
Pericarp of Fructus Musae extract 90-100 weight part
Sodium Glutamate 0.3-0.5 weight part
Ferrous sulfate 0.01-0.02 weight part
Calcium lactate 0.01-0.02 weight part
Vitamin A 0.4-0.6 weight part
Vitamin-E 0.1-0.3 weight part
Vitamins C 1-3 weight part
Vitamins D 0.1-0.2 weight part
Vitamin B6 0.01-0.02 weight part
Another technical scheme of the present invention is as follows:
A preparation method for above-mentioned Pericarpium Musae antioxidant addn, comprises the steps:
(1) by Pericarpium Musae successively after aqueous ethanolic solution thermal backflow lixiviate, extracted with diethyl ether, the analysis of PEG 20000 chromatography column layer, the analysis of Silon layer, eluant ethanol recrystallization and drying, obtained described pericarp of Fructus Musae extract;
(2) by above-mentioned pericarp of Fructus Musae extract 90-100 weight part, Sodium Glutamate 0.3-0.5 weight part, ferrous sulfate 0.01-0.02 weight part, calcium lactate 0.01-0.02 weight part, vitamin A 0.4-0.6 weight part, vitamin-E 0.1-0.3 weight part, vitamins C 1-3 weight part, vitamins D 0.1-0.2 weight part, vitamin B6 0.01-0.02 weight part mixing and stirring, namely obtains described Pericarpium Musae antioxidant addn after dry.
In a preferred embodiment of the invention, described step (1) comprises the steps:
A, aqueous ethanolic solution will be added after above-mentioned Pericarpium Musae drying and crushing in 50-60 DEG C of thermal backflow lixiviate 20-30 minute, and filter, obtain vat liquor;
B, above-mentioned vat liquor ether is extracted, obtain extraction liquid;
C, above-mentioned extraction liquid PEG 20000 post is carried out column chromatography, then it is the aqueous ethanolic solution wash-out of 10-20% by concentration, obtain first step elutriant;
D, above-mentioned first step elutriant Silon is carried out layer analysis as sorbent material, then with the mixed solution wash-out of aqueous acetic acid, obtain second stage elutriant;
E, above-mentioned second stage elutriant ethanol is carried out recrystallization, after dry, obtain described pericarp of Fructus Musae extract.
In a preferred embodiment of the invention, in the step a of described step (1), the concentration of aqueous ethanolic solution is 20-30%, and this aqueous ethanolic solution gross weight is 2-3 times of the Pericarpium Musae weight after drying and crushing.
In a preferred embodiment of the invention, in the steps d of described step (1), described Silon is 200 orders, and the concentration of described aqueous acetic acid is 1-2%.
The invention has the beneficial effects as follows:
1, containing Pericarpium Musae in the antioxidant addn of the present invention, drawing materials natural, nutritive value height, has no side effect, it is possible to anticoagulation and reducing blood-fat, enhancing immunocyte, antitumor, has good antioxygenation, applied range;
2, the vitamin-E in the antioxidant addn of the present invention is polyphenoils important in cytolemma and membrane stabilizer, maintaining the normal mechanism of muscle tissue and metabolism, particularly Power supply during Muscle contraction and calcium ion picked-up and release have important effect;
3, the vitamins C in the antioxidant addn of the present invention can obviously reduce exercise induced oxidative stress.
Embodiment
Below by way of embodiment, the technical scheme of the present invention is further detailed and describes.
Embodiment 1
(1) pericarp of Fructus Musae extract is prepared:
A, add 2L20% aqueous ethanolic solution by after 1kg Pericarpium Musae drying and crushing, in 50 DEG C of thermal backflow lixiviates 20 minutes, and filtering and concentrating, obtain vat liquor;
B, above-mentioned vat liquor ether is extracted, obtain extraction liquid;
C, above-mentioned extraction liquid PEG 20000 post is carried out column chromatography, then it is the aqueous ethanolic solution wash-out of 10% by concentration, obtain first step elutriant;
D, above-mentioned first step elutriant is carried out layer analysis with 200 object Silons as sorbent material, then with 1% aqueous acetic acid wash-out, obtain second stage elutriant;
E, above-mentioned second stage elutriant ethanol is carried out twice recrystallization, after dry, obtain described pericarp of Fructus Musae extract;
(2) by above-mentioned pericarp of Fructus Musae extract 90 weight part, Sodium Glutamate 0.3 weight part, ferrous sulfate 0.01 weight part, calcium lactate 0.01 weight part, vitamin A 0.4 weight part, vitamin-E 0.1 weight part, vitamins C 1 weight part, vitamins D 0.1 weight part, vitamin B6 0.01 weight part mixing and stirring, namely obtains described Pericarpium Musae antioxidant addn after dry.
Embodiment 2
(1) pericarp of Fructus Musae extract is prepared:
A, add 2.5L25% aqueous ethanolic solution by after 1kg Pericarpium Musae drying and crushing, in 55 DEG C of thermal backflow lixiviates 25 minutes, and filtering and concentrating, obtain vat liquor;
B, above-mentioned vat liquor ether is extracted, obtain extraction liquid;
C, above-mentioned extraction liquid PEG 20000 post is carried out column chromatography, then it is the aqueous ethanolic solution wash-out of 15% by concentration, obtain first step elutriant;
D, above-mentioned first step elutriant is carried out layer analysis with 200 object Silons as sorbent material, then with 1.5% aqueous acetic acid wash-out, obtain second stage elutriant;
E, above-mentioned second stage elutriant ethanol is carried out twice recrystallization, after dry, obtain described pericarp of Fructus Musae extract;
(2) by above-mentioned pericarp of Fructus Musae extract 95 weight part, Sodium Glutamate 0.4 weight part, ferrous sulfate 0.015 weight part, calcium lactate 0.015 weight part, vitamin A 0.5 weight part, vitamin-E 0.2 weight part, vitamins C 2 weight part, vitamins D 0.15 weight part, vitamin B6 0.015 weight part mixing and stirring, namely obtains described Pericarpium Musae antioxidant addn after dry.
Embodiment 3
(1) pericarp of Fructus Musae extract is prepared:
A, add 3L30% aqueous ethanolic solution by after 1kg Pericarpium Musae drying and crushing, in 60 DEG C of thermal backflow lixiviates 30 minutes, and filtering and concentrating, obtain vat liquor;
B, above-mentioned vat liquor ether is extracted, obtain extraction liquid;
C, above-mentioned extraction liquid PEG 20000 post is carried out column chromatography, then it is the aqueous ethanolic solution wash-out of 20% by concentration, obtain first step elutriant;
D, above-mentioned first step elutriant is carried out layer analysis with 200 object Silons as sorbent material, then with 2% aqueous acetic acid wash-out, obtain second stage elutriant;
E, above-mentioned second stage elutriant ethanol is carried out twice recrystallization, after dry, obtain described pericarp of Fructus Musae extract;
(2) by above-mentioned pericarp of Fructus Musae extract 100 weight part, Sodium Glutamate 0.5 weight part, ferrous sulfate 0.02 weight part, calcium lactate 0.02 weight part, vitamin A 0.6 weight part, vitamin-E 0.3 weight part, vitamins C 3 weight part, vitamins D 0.2 weight part, vitamin B6 0.02 weight part mixing and stirring, namely obtains described Pericarpium Musae antioxidant addn after dry.
The above, be only the better embodiment of the present invention, therefore can not limit scope of the invention process according to this, and the equivalence namely done according to patent scope of the present invention and description changes and modifies, and all should still belong in the scope that the present invention is contained.
Claims (4)
1. a Pericarpium Musae antioxidant addn, it is characterised in that: the component comprising following weight part:
Pericarp of Fructus Musae extract 90-100 weight part
Sodium Glutamate 0.3-0.5 weight part
Ferrous sulfate 0.01-0.02 weight part
Calcium lactate 0.01-0.02 weight part
Vitamin A 0.4-0.6 weight part
Vitamin-E 0.1-0.3 weight part
Vitamins C 1-3 weight part
Vitamins D 0.1-0.2 weight part
Vitamin B6 0.01-0.02 weight part
The extracting method of above-mentioned pericarp of Fructus Musae extract is as follows:
A, add aqueous ethanolic solution in 50-60 DEG C of thermal backflow lixiviate 20-30 minute by crossing 100 eye mesh screens after above-mentioned Pericarpium Musae drying and crushing, and filter, obtain vat liquor;
B, above-mentioned vat liquor ether is extracted, obtain extraction liquid;
C, above-mentioned extraction liquid PEG 20000 post is carried out column chromatography, then it is the aqueous ethanolic solution wash-out of 10-20% by concentration, obtain first step elutriant;
D, above-mentioned first step elutriant Silon is carried out layer analysis as sorbent material, then use aqueous acetic acid wash-out, obtain second stage elutriant;
E, above-mentioned second stage elutriant ethanol is carried out recrystallization, after dry, obtain described pericarp of Fructus Musae extract.
2. the preparation method of a Pericarpium Musae antioxidant addn according to claim 1, it is characterised in that: comprise the steps:
(1) by Pericarpium Musae successively after aqueous ethanolic solution thermal backflow lixiviate, extracted with diethyl ether, PEG 20000 column chromatography, the analysis of Silon layer, eluant ethanol recrystallization and drying, obtained described pericarp of Fructus Musae extract, this step comprises the steps:
A, aqueous ethanolic solution will be added after above-mentioned Pericarpium Musae drying and crushing in 50-60 DEG C of thermal backflow lixiviate 20-30 minute, and filter, obtain vat liquor;
B, above-mentioned vat liquor ether is extracted, obtain extraction liquid;
C, above-mentioned extraction liquid PEG 20000 post is carried out column chromatography, then it is the aqueous ethanolic solution wash-out of 10-20% by concentration, obtain first step elutriant;
D, above-mentioned first step elutriant Silon is carried out layer analysis as sorbent material, then with the mixed solution wash-out of aqueous acetic acid, obtain second stage elutriant;
E, above-mentioned second stage elutriant ethanol is carried out recrystallization, after dry, obtain described pericarp of Fructus Musae extract;
(2) by above-mentioned pericarp of Fructus Musae extract 90-100 weight part, Sodium Glutamate 0.3-0.5 weight part, ferrous sulfate 0.01-0.02 weight part, calcium lactate 0.01-0.02 weight part, vitamin A 0.4-0.6 weight part, vitamin-E 0.1-0.3 weight part, vitamins C 1-3 weight part, vitamins D 0.1-0.2 weight part, vitamin B6 0.01-0.02 weight part mixing and stirring, namely obtains described Pericarpium Musae antioxidant addn after dry.
3. the preparation method of a kind of Pericarpium Musae antioxidant addn as claimed in claim 2, it is characterized in that: in the step a of described step (1), the concentration of aqueous ethanolic solution is 20-30%, and this aqueous ethanolic solution gross weight is 2-3 times of the Pericarpium Musae weight after drying and crushing.
4. the preparation method of a kind of Pericarpium Musae antioxidant addn as claimed in claim 2, it is characterised in that: in the steps d of described step (1), described Silon is 200 orders, and the concentration of described aqueous acetic acid is 1-2%.
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| CN201511011327.XA CN105639400A (en) | 2015-12-30 | 2015-12-30 | Banana peel antioxidant additive and preparation method thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105982287A (en) * | 2016-06-13 | 2016-10-05 | 湖北文理学院 | Special gynura bicolor seasoning for cooking bean curd |
| CN106036758A (en) * | 2016-06-13 | 2016-10-26 | 湖北文理学院 | Special condiment for cooked mutton with plantain herb |
| CN106071639A (en) * | 2016-06-13 | 2016-11-09 | 湖北文理学院 | A kind of Fructus Mangifera Indicae core antioxidant and preparation method thereof |
| CN106072606A (en) * | 2016-06-13 | 2016-11-09 | 湖北文理学院 | A kind of Pericarpium Vitis viniferae antioxidant and preparation method thereof |
| CN107006837A (en) * | 2017-03-27 | 2017-08-04 | 湖北文理学院 | A kind of mulberry leaf cyclodextrin antioxidant and preparation method thereof |
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|---|---|---|---|---|
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| CN102988627A (en) * | 2012-12-06 | 2013-03-27 | 上海中医药大学 | Preparation method of banana peel extract and application of banana peel extract |
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| CN102988627A (en) * | 2012-12-06 | 2013-03-27 | 上海中医药大学 | Preparation method of banana peel extract and application of banana peel extract |
| CN103445140A (en) * | 2013-07-15 | 2013-12-18 | 闽南师范大学 | Auricularia polytricha antioxidant additive and preparation method thereof |
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| CN105982287A (en) * | 2016-06-13 | 2016-10-05 | 湖北文理学院 | Special gynura bicolor seasoning for cooking bean curd |
| CN106036758A (en) * | 2016-06-13 | 2016-10-26 | 湖北文理学院 | Special condiment for cooked mutton with plantain herb |
| CN106071639A (en) * | 2016-06-13 | 2016-11-09 | 湖北文理学院 | A kind of Fructus Mangifera Indicae core antioxidant and preparation method thereof |
| CN106072606A (en) * | 2016-06-13 | 2016-11-09 | 湖北文理学院 | A kind of Pericarpium Vitis viniferae antioxidant and preparation method thereof |
| CN107006837A (en) * | 2017-03-27 | 2017-08-04 | 湖北文理学院 | A kind of mulberry leaf cyclodextrin antioxidant and preparation method thereof |
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