CN106880520A - A kind of tea oil elite hair conditioner and preparation method thereof - Google Patents
A kind of tea oil elite hair conditioner and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/63—Steroids; Derivatives thereof
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
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Abstract
The invention belongs to daily chemical product field, a kind of tea oil elite hair conditioner and preparation method thereof is disclosed.The tea oil elite hair conditioner is made up of the following component counted by weight：10~30 parts of tea oil sucrose ester, 2~10 parts of Australia tea tree oil, 2~10 parts of stop dysentery grass oil, 1~5 part of tea sapogenol linoleate, 1~3 part of soybean lecithin, 0.5~2 part of cholesterol, 40~83.5 parts of deionized water.Method is：Tea oil sucrose ester and tea sapogenol linoleate are first prepared, then Australia tea tree oil, stop dysentery grass oil, soybean lecithin and cholesterol are well mixed, as A phases；Tea oil sucrose ester, tea sapogenol linoleate and deionized water are well mixed, as B phases；A is added in B phases, high speed homogenization emulsification obtains tea oil elite hair conditioner.Hair conditioner of the present invention has good affinity to scalp and hair, and nutritional ingredient can be made to enter deep layer scalp and hair follicle, preferably plays and nourishes and antibacterial action.
Description
Technical field
The invention belongs to daily chemical product field, and in particular to a kind of tea oil hair conditioner and preparation method thereof.
Background technology
The diaphragm that hair top layer is made up of the oil layer of a layer of complete hair scale piece and naturally secret, excessive hair washing,
Hair-waving, hair dyeing destroy this layer of diaphragm, increasingly highlight the problems such as make withered, short-tempered hair, bifurcated, hair loss, itching of the scalp, separately
Outer scalp bacterium and the breeding of fungi, result in a large amount of dandruffs and produce, and be also the one of the main reasons of alopecia.Hair conditioner be then
It is applied on hair after hair washing, is cleaned after certain hour, protective layer is formed on hair and scalp, is risen and nourish and protective effect.
Hair products in the market are numerous, but contain chemical addition agent mostly, or even contain chemicals, are unfavorable for
Environmental protection, while long-term use can be remained on skin, there is potential potential safety hazard to human body.Plant extracts is used as hair care
Product gradually rises, and to human body and Environmental security, but directly uses plant extracts, is difficult to be absorbed by scalp, it is also difficult to play
Nourish the effect of hair.
Tea oil is because containing polyunsaturated fatty acid, vitamin and mineral matter etc., being conducive to hair to protect.Application number
201410682433.X, 201610507342.1 patent application disclose a kind of hair conditioner, using tea oil as one of which group
Point.But tea oil, directly as hair products, the adhesive force to scalp and hair is smaller, it is difficult to play it and nourish and protection work
With.
The content of the invention
In order to overcome the shortcoming and deficiency of prior art, primary and foremost purpose of the invention is to provide a kind of tea oil hair care to produce
Product.The present invention is played good antibacterial, is protected by tea oil sucrose ester, tea sapogenol linoleate compatibility natural antibacterial essential oil
It is wet, the effect of protection scalp and hair.
Preparation method another object of the present invention is to provide above-mentioned tea oil elite hair conditioner.The present invention by tea oil and
The structure of modification of Tea Saponin, strengthens to scalp and hair affinity；By nanometer emulsified preparation, nutritional ingredient is conducive to enter head
Skin and hair follicle, preferably play a role.
The purpose of the present invention is achieved through the following technical solutions：
A kind of tea oil elite hair conditioner, is made up of following component by weight：
10~30 parts of tea oil sucrose ester, 2~10 parts of Australia tea tree oil, 2~10 parts of stop dysentery grass oil, tea sapogenol linoleic acid
1~5 part of ester, 1~3 part of soybean lecithin, 0.5~2 part of cholesterol, 40~83.5 parts of deionized water.
The tea oil elite hair conditioner, is preferably made up of the component of following weight portion：
20 parts of tea oil sucrose ester, 5 parts of Australia tea tree oil, 5 parts of stop dysentery grass oil, 3 parts of tea sapogenol linoleate, soybean ovum
Phosphatidase 2 part, 1 part of cholesterol, 64 parts of deionized water.
The tea oil sucrose ester is prepared by the following method and obtains：Tea-seed oil is mixed with sucrose, potassium carbonate is added, in
110~140 DEG C of insulation reactions, using water wash, stratification, except sub-cloud, obtains tea oil sucrose ester.
The tea-seed oil is (2~6) with the mass ratio of sucrose：1, the addition of the potassium carbonate is the 1 of tea seed oil quality
~5%, the time of the insulation reaction is 3~8h；The consumption of the water is 0.5~3 times of tea seed oil quality.
The tea sapogenol linoleate is prepared by the following method and obtains：Tea Saponin is mixed with linoleic acid, is added
Dicyclohexylcarbodiimide (DCC) and DMAP (DMAP), in 80~110 DEG C of insulation reactions, with water wash, stand
Layering, except sub-cloud, obtains tea sapogenol linoleate.
The Tea Saponin and linoleic acid in mass ratio 1：(1~5), the addition of the dicyclohexylcarbodiimide is tea soap
The 20~50% of quality amount, the addition of the DMAP is the 5~20% of Tea Saponin quality；The insulation reaction
Time be 3~8h, the consumption of the water is 0.5~3 times of linoleic acid quality.
The preparation method of the tea oil elite hair conditioner, comprises the following steps：
(1) Australia tea tree oil, stop dysentery grass oil, soybean lecithin and cholesterol are well mixed, as A phases；By tea oil sugarcane
Sugar ester, tea sapogenol linoleate and deionized water are well mixed, used as B phases；
(2) A is added in B phases, high speed homogenization emulsification obtains nanosizing tea oil elite hair conditioner.
The rotating speed of the high speed homogenization is 5000~20000 turns/min, and the time of the emulsifying is 20~60min.
The particle diameter of particle is 200~500nm in the nanosizing tea oil elite hair conditioner, and the particle is oil-in-water
Grain.
The tea oil elite hair conditioner, the effect of scalp and hair follicle is nourished with antibacterial and deep layer.
The tea-seed oil is the tea-seed oil of oil tea.
Principle：Tea oil is made sucrose ester by the present invention by ester-interchange method, improves the hydrophily of tea oil；Tea Saponin is led to
Over-churning method is made tea sapogenol linoleate, improves the lipophile of Tea Saponin；Australia tea tree oil and stop dysentery grass oil are
Natural antibacterial essential oil, can effectively suppress scalp bacterium and fungi, by tea oil sucrose ester, tea sapogenol linoleate and Australia tea
Tree oil, stop dysentery grass oil are made nano-particle, easily infiltrate through in scalp and hair, rise and preferably nourish and antibacterial action.
The present invention has the following advantages and effect relative to prior art：
(1) improved tea oil, Tea Saponin and Australia tea tree oil, stop dysentery grass oil compatibility, both effective trophonema hair, prevented again
Skin of head bacterium and fungi grow, and anti-alopecia-stopping and hair are withered and yellow.
(2) nanosizing tea oil elite hair conditioner prepared by the present invention, is conducive to going deep into scalp and hair follicle, is more beneficial for nutrition
Absorb and deep layer antibacterial；
(3) preparation process is simple of the present invention, is easy to industrialized production.
Specific embodiment
With reference to embodiment, the present invention is described in further detail, but embodiments of the present invention not limited to this.
Australia tea tree oil is oily by Australia tea tree steam distillation in the present embodiment, purchased from Guangzhou Wen Ling trade Co., Ltds；Stop dysentery grass oil
It is stop dysentery grass steam distillation oil, purchased from Jishui County book on Chinese herbal medicine medicinal flavours oil factory.
Embodiment 1
A kind of tea oil elite hair conditioner, is made up of following component by weight：
20 parts of tea oil sucrose ester, 5 parts of Australia tea tree oil, 5 parts of stop dysentery grass oil, 3 parts of tea sapogenol linoleate, soybean ovum
Phosphatidase 2 part, 1 part of cholesterol, 64 parts of deionized water；
The preparation method of the tea oil elite hair conditioner, comprises the following steps：
(1) prepared by tea oil sucrose ester：Tea-seed oil and sucrose in mass ratio 2：1 mixing, adds the carbonic acid of tea seed oil quality 1%
Potassium, is heated to 140 DEG C, is incubated 8h, then with the water wash of 0.5 times of tea seed oil quality, stratification (time of standing is 1h) is removed
Sub-cloud, obtains final product tea oil sucrose ester；
(2) prepared by tea sapogenol linoleate：Tea Saponin and linoleic acid in mass ratio 1：1 mixing, adds Tea Saponin matter
The dicyclohexylcarbodiimide (DCC) of amount 50% and the DMAP (DMAP) of Tea Saponin quality 20%, are heated to 80
DEG C, it is incubated 3h, then with the water wash of 3 times of linoleic acid quality, stratification (time of standing is 1h), except sub-cloud, obtains final product tea
Sapogenol linoleate；
(3) Australia tea tree oil, stop dysentery grass oil, soybean lecithin and cholesterol are well mixed, as A phases；By tea oil sugarcane
Sugar ester, tea sapogenol linoleate and deionized water are well mixed, used as B phases；A is added in B phases, 5000 turns/min is equal
Matter emulsifies 60min, obtains nanosizing tea oil elite hair conditioner.
Hair conditioner proterties prepared by the present embodiment is emulsion liquid, with natural tea extract salted cake fried in sesame oil taste, quickly divide after use
The hair tip and scalp are dissipated to, back luminance is washed submissive.
Embodiment 2
A kind of tea oil elite hair conditioner, is made up of following component by weight：
10 parts of tea oil sucrose ester, 2 parts of Australia tea tree oil, 2 parts of stop dysentery grass oil, 1 part of tea sapogenol linoleate, soybean ovum
Phosphatidase 1 part, 0.5 part of cholesterol, 83.5 parts of deionized water.
The preparation method of the tea oil elite hair conditioner, comprises the following steps：
(1) prepared by tea oil sucrose ester：Tea-seed oil and sucrose in mass ratio 6：1 mixing, adds the carbonic acid of tea seed oil quality 5%
Potassium, is heated to 110 DEG C, is incubated 8h, then with the water wash of 3 times of tea seed oil quality, stratification (time of standing is 2h) is removed
Lower floor, obtains final product tea oil sucrose ester；
(2) prepared by tea sapogenol linoleate：Tea Saponin and linoleic acid in mass ratio 1：5 mixing, add Tea Saponin matter
The dicyclohexylcarbodiimide (DCC) of amount 20% and the DMAP (DMAP) of Tea Saponin quality 5%, are heated to 110
DEG C, it is incubated 3h, then with the water wash of 3 times of linoleic acid quality, stratification (time of standing is 2h), except sub-cloud, obtains final product tea
Sapogenol linoleate；
(3) Australia tea tree oil, stop dysentery grass oil, soybean lecithin and cholesterol are well mixed, as A phases；By tea oil sugarcane
Sugar ester, tea sapogenol linoleate and deionized water are well mixed, used as B phases；A is added in B phases, 20000 turns/min
Emulsifying 20min, obtains nanosizing tea oil elite hair conditioner.
Hair conditioner proterties prepared by the present embodiment is emulsion liquid, with natural tea extract salted cake fried in sesame oil taste, it is quick after use
The hair tip and scalp are dispersed to, back luminance is washed submissive.
Embodiment 3
A kind of tea oil elite hair conditioner, is made up of following component by weight：
30 parts of tea oil sucrose ester, 10 parts of Australia tea tree oil, 10 parts of stop dysentery grass oil, 5 parts of tea sapogenol linoleate, soybean
3 parts of lecithin, 2 parts of cholesterol, 40 parts of deionized water.
The preparation method of the tea oil elite hair conditioner, comprises the following steps：
(1) prepared by tea oil sucrose ester：Tea-seed oil and sucrose in mass ratio 3：1 mixing, adds the carbonic acid of tea seed oil quality 2%
Potassium, is heated to 120 DEG C, is incubated 6h, then with the water wash of 1 times of tea seed oil quality, stratification (time of standing is 3h) is removed
Lower floor, obtains final product tea oil sucrose ester；
(2) prepared by tea sapogenol linoleate：Tea Saponin and linoleic acid in mass ratio 1：2 mixing, add Tea Saponin matter
The dicyclohexylcarbodiimide (DCC) of amount 30% and the DMAP (DMAP) of Tea Saponin quality 10%, are heated to 100
DEG C, it is incubated 4h, then with the water wash of 2 times of linoleic acid quality, stratification (time of standing is 3h), except sub-cloud, obtains final product tea
Sapogenol linoleate；
(3) Australia tea tree oil, stop dysentery grass oil, soybean lecithin and cholesterol are well mixed, as A phases；By tea oil sugarcane
Sugar ester, tea sapogenol linoleate and deionized water are well mixed, used as B phases；A is added in B phases, 10000 turns/min
Emulsifying 60min, obtains nanosizing tea oil elite hair conditioner.
Hair conditioner proterties prepared by the present embodiment is emulsion liquid, with natural tea extract salted cake fried in sesame oil taste, it is quick after use
The hair tip and scalp are dispersed to, back luminance is washed submissive.
Embodiment 4
A kind of tea oil elite hair conditioner, is made up of following component by weight：
15 parts of tea oil sucrose ester, 5 parts of Australia tea tree oil, 3 parts of stop dysentery grass oil, 3 parts of tea sapogenol linoleate, soybean ovum
Phosphatidase 2 part, 1 part of cholesterol, 71 parts of deionized water.
The preparation method of the tea oil elite hair conditioner, comprises the following steps：
(1) prepared by tea oil sucrose ester：Tea-seed oil and sucrose in mass ratio 4：1 mixing, adds the carbonic acid of tea seed oil quality 3%
Potassium, is heated to 130 DEG C, is incubated 5h, then with the water wash of 2 times of tea seed oil quality, stratification (time of standing is 2h) is removed
Lower floor, obtains final product tea oil sucrose ester；
(2) prepared by tea sapogenol linoleate：Tea Saponin and linoleic acid in mass ratio 1：4 mixing, add Tea Saponin matter
The dicyclohexylcarbodiimide (DCC) of amount 40% and the DMAP (DMAP) of Tea Saponin quality 15%, are heated to 90
DEG C, it is incubated 6h, then with the water wash of 3 times of linoleic acid quality, stratification (time of standing is 3h), except sub-cloud, obtains final product tea
Sapogenol linoleate；
(3) Australia tea tree oil, stop dysentery grass oil, soybean lecithin and cholesterol are well mixed, as A phases；By tea oil sugarcane
Sugar ester, tea sapogenol linoleate and deionized water are well mixed, used as B phases；A is added in B phases, 15000 turns/min
Emulsifying 30min, obtains nanosizing tea oil elite hair conditioner.
Hair conditioner proterties prepared by the present embodiment is emulsion liquid, with natural tea extract salted cake fried in sesame oil taste, it is quick after use
The hair tip and scalp are dispersed to, back luminance is washed submissive.
Embodiment 5
A kind of tea oil elite hair conditioner, is made up of following component by weight：
25 parts of tea oil sucrose ester, 7 parts of Australia tea tree oil, 5 parts of stop dysentery grass oil, 2 parts of tea sapogenol linoleate, soybean ovum
Phosphatidase 1 part, 0.5 part of cholesterol, 59.5 parts of deionized water.
The preparation method of the tea oil elite hair conditioner, comprises the following steps：
(1) prepared by tea oil sucrose ester：Tea-seed oil and sucrose in mass ratio 5：1 mixing, adds the carbonic acid of tea seed oil quality 2%
Potassium, is heated to 130 DEG C, is incubated 7h, then with the water wash of 1.5 times of tea seed oil quality, stratification (time of standing is 1h) is removed
Sub-cloud, obtains final product tea oil sucrose ester；
(2) prepared by tea sapogenol linoleate：Tea Saponin and linoleic acid in mass ratio 1：4 mixing, add Tea Saponin matter
The dicyclohexylcarbodiimide (DCC) of amount 25% and the DMAP (DMAP) of Tea Saponin quality 12%, are heated to 105
DEG C, it is incubated 7h, then with the water wash of 2.5 times of linoleic acid quality, stratification (time of standing is 2h), except sub-cloud, is obtained final product
Tea sapogenol linoleate；
(3) Australia tea tree oil, stop dysentery grass oil, soybean lecithin and cholesterol are well mixed, as A phases；By tea oil sugarcane
Sugar ester, tea sapogenol linoleate and deionized water are well mixed, used as B phases；A is added in B phases, 10000 turns/min
Emulsifying 40min, obtains nanosizing tea oil elite hair conditioner.
Hair conditioner proterties prepared by the present embodiment is emulsion liquid, with natural tea extract salted cake fried in sesame oil taste, it is quick after use
The hair tip and scalp are dispersed to, back luminance is washed submissive.
Embodiment 6
A kind of tea oil elite hair conditioner, is made up of following component by weight：
30 parts of tea oil sucrose ester, 6 parts of Australia tea tree oil, 5 parts of stop dysentery grass oil, 4 parts of tea sapogenol linoleate, soybean ovum
Phosphatidase 3 part, 1 part of cholesterol, 51 parts of deionized water.
The preparation method of the tea oil elite hair conditioner, comprises the following steps：
(1) prepared by tea oil sucrose ester：Tea-seed oil and sucrose in mass ratio 3：1 mixing, adds the carbonic acid of tea seed oil quality 4%
Potassium, is heated to 115 DEG C, is incubated 4h, then with the water wash of 2.5 times of tea seed oil quality, stratification (time of standing is 3h) is removed
Sub-cloud, obtains final product tea oil sucrose ester；
(2) prepared by tea sapogenol linoleate：Tea Saponin and linoleic acid in mass ratio 1：3 mixing, add Tea Saponin matter
The dicyclohexylcarbodiimide (DCC) of amount 30% and the DMAP (DMAP) of Tea Saponin quality 15%, are heated to 95
DEG C, it is incubated 4.5h, then with the water wash of 2 times of linoleic acid quality, stratification (time of standing is 1h), except sub-cloud, is obtained final product
Tea sapogenol linoleate；
(3) Australia tea tree oil, stop dysentery grass oil, soybean lecithin and cholesterol are well mixed, as A phases；By tea oil sugarcane
Sugar ester, tea sapogenol linoleate and deionized water are well mixed, used as B phases；A is added in B phases, 20000 turns/min
Emulsifying 25min, obtains nanosizing tea oil elite hair conditioner.
Hair conditioner proterties prepared by the present embodiment is emulsion liquid, with natural tea extract salted cake fried in sesame oil taste, it is quick after use
The hair tip and scalp are dispersed to, back luminance is washed submissive.
The effect assessment of embodiment 7
The particle diameter of hair conditioner, antimycotic and hair care effect measure obtained in embodiment 1~6：
Experimental technique：
(1) droplet measurement：After sample is disperseed with suitable quantity of water, detected with Malvern nano particle size instrument, refraction coefficient is
1.33。
(2) fungistatic effect is determined：Using it is antibacterial it is around-France carry out fungistatic effect detection, bacterial strain uses therefor is Malassezia furfur mark
Quasi- bacterial strain, culture medium is agar medium.Sample addition is 1%, 37 DEG C of culture 24h.
(3) sensory effects scoring：The volunteer of 60 easy alopecias is divided into 6 groups, and the obtained shield of embodiment 1~6 is used respectively
Hair element 10 days, to its anticreep (≤25 points), comfortableness (≤25 points), compliance (≤25 points), (≤25 points) scorings of anti-bits property.
Experimental result is shown in Table 1.Result shows, hair conditioner particle diameter obtained in embodiment 1~6 is 200~450nm, with compared with
Good antibacterial action, hair care effect is better than commercially available domestic tea oil hair conditioner and Chinese medicine hair conditioner.
The antibiotic property of hair conditioner obtained in the embodiment 1~6 of table 1 and hair care effect evaluation (N=10)
Above-described embodiment is the present invention preferably implementation method, but embodiments of the present invention are not by above-described embodiment
Limitation, it is other it is any without departing from Spirit Essence of the invention and the change, modification, replacement made under principle, combine, simplification,
Equivalent substitute mode is should be, is included within protection scope of the present invention.
Claims (9)
1. a kind of tea oil elite hair conditioner, it is characterised in that：It is made up of the following component counted by weight：
10~30 parts of tea oil sucrose ester, 2~10 parts of Australia tea tree oil, 2~10 parts of stop dysentery grass oil, tea sapogenol linoleate 1
~5 parts, 1~3 part of soybean lecithin, 0.5~2 part of cholesterol, 40~83.5 parts of deionized water.
2. tea oil elite hair conditioner according to claim 1, it is characterised in that：By the following component group counted by weight
Into：
20 parts of tea oil sucrose ester, 5 parts of Australia tea tree oil, 5 parts of stop dysentery grass oil, 3 parts of tea sapogenol linoleate, soybean lecithin
2 parts, 1 part of cholesterol, 64 parts of deionized water.
3. tea oil elite hair conditioner according to claim 1 or claim 2, it is characterised in that：The tea oil sucrose ester is by with lower section
Method is prepared：Tea-seed oil is mixed with sucrose, potassium carbonate is added, in 110~140 DEG C of insulation reactions, using water wash, stood
Layering, except sub-cloud, obtains tea oil sucrose ester.
4. tea oil elite hair conditioner according to claim 3, it is characterised in that：The tea-seed oil is (2 with the mass ratio of sucrose
~6)：1, the addition of the potassium carbonate is the 1~5% of tea seed oil quality, and the time of the insulation reaction is 3~8h；It is described
The consumption of water is 0.5~3 times of tea seed oil quality.
5. tea oil elite hair conditioner according to claim 1 or claim 2, it is characterised in that：The tea sapogenol linoleate leads to
Following methods are crossed to prepare：Tea Saponin is mixed with linoleic acid, dicyclohexylcarbodiimide and DMAP is added,
In 80~110 DEG C of insulation reactions, with water wash, stratification, except sub-cloud, obtains tea sapogenol linoleate.
6. tea oil elite hair conditioner according to claim 5, it is characterised in that：The Tea Saponin and linoleic acid in mass ratio 1：
(1~5), the addition of the dicyclohexylcarbodiimide is the 20~50% of Tea Saponin quality, the DMAP
Addition for Tea Saponin quality 5~20%；The time of the insulation reaction is 3~8h, and the consumption of the water is linoleic acid
0.5~3 times of quality.
7. according to any one of claim 1~6 tea oil elite hair conditioner preparation method, it is characterised in that：Including as follows
Step：
(1) Australia tea tree oil, stop dysentery grass oil, soybean lecithin and cholesterol are well mixed, as A phases；By tea oil sucrose ester,
Tea sapogenol linoleate and deionized water are well mixed, used as B phases；
(2) A is added in B phases, high speed homogenization emulsification obtains nanosizing tea oil elite hair conditioner.
8. the preparation method of tea oil elite hair conditioner according to claim 7, it is characterised in that：The rotating speed of the high speed homogenization
It is 5000~20000 turns/min, the time of the emulsifying is 20~60min.
9. the preparation method of tea oil elite hair conditioner according to claim 7, it is characterised in that：The nanosizing tea oil elite
The particle diameter of particle is 200~500nm in hair conditioner.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107550794A (en) * | 2017-10-18 | 2018-01-09 | 湖南大三湘油茶生态产业有限公司 | Camellia oleifera fruit hair care and nourishing cream and preparation method thereof |
| CN109106650A (en) * | 2018-10-09 | 2019-01-01 | 赣州哈克生物科技有限公司 | A kind of tea oil essence hair conditioner and preparation method thereof |
| FR3083099A1 (en) * | 2018-06-29 | 2020-01-03 | L'oreal | COSMETIC COMPOSITION COMPRISING FATTY ACIDS, ANIONIC AND AMPHOTERIC SURFACTANTS, AND ESSENTIAL OILS, COSMETIC TREATMENT METHOD AND USE |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1965793A (en) * | 2006-11-07 | 2007-05-23 | 华南农业大学 | Hair conditioner and preparation process thereof |
| CN102030806A (en) * | 2010-10-21 | 2011-04-27 | 华南理工大学 | Tea saponin high-grade fatty ester as well as preparation method and application thereof |
| CN104473805A (en) * | 2014-11-24 | 2015-04-01 | 福建春辉生物工程有限公司 | Tea oil hair conditioner |
-
2017
- 2017-01-13 CN CN201710025867.6A patent/CN106880520A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1965793A (en) * | 2006-11-07 | 2007-05-23 | 华南农业大学 | Hair conditioner and preparation process thereof |
| CN102030806A (en) * | 2010-10-21 | 2011-04-27 | 华南理工大学 | Tea saponin high-grade fatty ester as well as preparation method and application thereof |
| CN104473805A (en) * | 2014-11-24 | 2015-04-01 | 福建春辉生物工程有限公司 | Tea oil hair conditioner |
Non-Patent Citations (1)
| Title |
|---|
| 韦巧艳: "《蔗糖脂肪酸酯在乳化抑菌方面的应用研究进展》", 《食品工业科技》 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107550794A (en) * | 2017-10-18 | 2018-01-09 | 湖南大三湘油茶生态产业有限公司 | Camellia oleifera fruit hair care and nourishing cream and preparation method thereof |
| FR3083099A1 (en) * | 2018-06-29 | 2020-01-03 | L'oreal | COSMETIC COMPOSITION COMPRISING FATTY ACIDS, ANIONIC AND AMPHOTERIC SURFACTANTS, AND ESSENTIAL OILS, COSMETIC TREATMENT METHOD AND USE |
| CN109106650A (en) * | 2018-10-09 | 2019-01-01 | 赣州哈克生物科技有限公司 | A kind of tea oil essence hair conditioner and preparation method thereof |
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