CN104909363A - 一种网络状纳米结构碳材料的制备方法 - Google Patents
一种网络状纳米结构碳材料的制备方法 Download PDFInfo
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- CN104909363A CN104909363A CN201510253797.0A CN201510253797A CN104909363A CN 104909363 A CN104909363 A CN 104909363A CN 201510253797 A CN201510253797 A CN 201510253797A CN 104909363 A CN104909363 A CN 104909363A
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Cited By (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106082193A (zh) * | 2016-06-14 | 2016-11-09 | 陕西科技大学 | 一种以藻类植物为碳源制备多级结构碳材料的方法 |
CN106345409A (zh) * | 2016-09-27 | 2017-01-25 | 芜湖美智空调设备有限公司 | 一种高效吸附甲醛的活性炭材料的制备方法 |
CN106563816A (zh) * | 2016-10-26 | 2017-04-19 | 陕西科技大学 | 一种多孔碳负载石墨烯包覆纳米镍颗粒吸波材料的制备方法 |
CN108002382A (zh) * | 2017-11-29 | 2018-05-08 | 同济大学 | 氮掺杂多孔碳负载Fe2O3复合材料的制备方法 |
CN109360739A (zh) * | 2018-12-17 | 2019-02-19 | 中南林业科技大学 | 负载镍/氧化镍的碳纳米纤维电极材料的制备方法 |
CN111285688A (zh) * | 2020-02-10 | 2020-06-16 | 北方民族大学 | 生物质碳膜及其制备方法和应用 |
CN111732097A (zh) * | 2020-06-17 | 2020-10-02 | 武汉大学 | 大比表面积石墨化炭的制备方法及应用 |
CN113122184A (zh) * | 2021-05-11 | 2021-07-16 | 盐城工学院 | 一种生物质多孔碳吸波材料的制备方法 |
CN114744175A (zh) * | 2021-04-21 | 2022-07-12 | 卡本斯科普有限公司 | 组合物、石墨粉末、阳极粉末及其生产方法 |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102583333A (zh) * | 2012-01-18 | 2012-07-18 | 黑龙江大学 | 以玉米秸秆为碳源合成多孔纳米石墨片的方法 |
CN103346025A (zh) * | 2013-06-26 | 2013-10-09 | 西北师范大学 | 用紫菜制备超级电容器电极材料的方法 |
CN103771408A (zh) * | 2013-12-30 | 2014-05-07 | 上海交通大学 | 基于海藻的超级电容器用活性炭的制备方法 |
CN104518226A (zh) * | 2013-09-29 | 2015-04-15 | 中国科学院大连化学物理研究所 | 一种锂·空气或锂氧电池正极用多孔碳材料 |
CN104518219A (zh) * | 2013-09-29 | 2015-04-15 | 中国科学院大连化学物理研究所 | 多孔碳材料在锂-亚硫酰氯电池正极中的应用 |
-
2015
- 2015-05-18 CN CN201510253797.0A patent/CN104909363B/zh active Active
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102583333A (zh) * | 2012-01-18 | 2012-07-18 | 黑龙江大学 | 以玉米秸秆为碳源合成多孔纳米石墨片的方法 |
CN103346025A (zh) * | 2013-06-26 | 2013-10-09 | 西北师范大学 | 用紫菜制备超级电容器电极材料的方法 |
CN104518226A (zh) * | 2013-09-29 | 2015-04-15 | 中国科学院大连化学物理研究所 | 一种锂·空气或锂氧电池正极用多孔碳材料 |
CN104518219A (zh) * | 2013-09-29 | 2015-04-15 | 中国科学院大连化学物理研究所 | 多孔碳材料在锂-亚硫酰氯电池正极中的应用 |
CN103771408A (zh) * | 2013-12-30 | 2014-05-07 | 上海交通大学 | 基于海藻的超级电容器用活性炭的制备方法 |
Cited By (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106082193A (zh) * | 2016-06-14 | 2016-11-09 | 陕西科技大学 | 一种以藻类植物为碳源制备多级结构碳材料的方法 |
CN106082193B (zh) * | 2016-06-14 | 2018-03-16 | 陕西科技大学 | 一种以藻类植物为碳源制备多级结构碳材料的方法 |
CN106345409A (zh) * | 2016-09-27 | 2017-01-25 | 芜湖美智空调设备有限公司 | 一种高效吸附甲醛的活性炭材料的制备方法 |
CN106345409B (zh) * | 2016-09-27 | 2018-04-03 | 芜湖美智空调设备有限公司 | 一种高效吸附甲醛的活性炭材料的制备方法 |
CN106563816A (zh) * | 2016-10-26 | 2017-04-19 | 陕西科技大学 | 一种多孔碳负载石墨烯包覆纳米镍颗粒吸波材料的制备方法 |
CN108002382A (zh) * | 2017-11-29 | 2018-05-08 | 同济大学 | 氮掺杂多孔碳负载Fe2O3复合材料的制备方法 |
CN109360739A (zh) * | 2018-12-17 | 2019-02-19 | 中南林业科技大学 | 负载镍/氧化镍的碳纳米纤维电极材料的制备方法 |
CN109360739B (zh) * | 2018-12-17 | 2020-11-10 | 中南林业科技大学 | 负载镍/氧化镍的碳纳米纤维电极材料的制备方法 |
CN111285688A (zh) * | 2020-02-10 | 2020-06-16 | 北方民族大学 | 生物质碳膜及其制备方法和应用 |
CN111732097A (zh) * | 2020-06-17 | 2020-10-02 | 武汉大学 | 大比表面积石墨化炭的制备方法及应用 |
CN114744175A (zh) * | 2021-04-21 | 2022-07-12 | 卡本斯科普有限公司 | 组合物、石墨粉末、阳极粉末及其生产方法 |
CN113122184A (zh) * | 2021-05-11 | 2021-07-16 | 盐城工学院 | 一种生物质多孔碳吸波材料的制备方法 |
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