CN104903983A - 一种电容器级钽铌合金丝及其制造方法 - Google Patents
一种电容器级钽铌合金丝及其制造方法 Download PDFInfo
- Publication number
- CN104903983A CN104903983A CN201380069773.9A CN201380069773A CN104903983A CN 104903983 A CN104903983 A CN 104903983A CN 201380069773 A CN201380069773 A CN 201380069773A CN 104903983 A CN104903983 A CN 104903983A
- Authority
- CN
- China
- Prior art keywords
- tantalum
- niobium alloy
- minutes
- niobium
- alloy silk
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- RHDUVDHGVHBHCL-UHFFFAOYSA-N niobium tantalum Chemical compound [Nb].[Ta] RHDUVDHGVHBHCL-UHFFFAOYSA-N 0.000 title claims abstract description 58
- 229910001257 Nb alloy Inorganic materials 0.000 title claims abstract description 57
- 239000003990 capacitor Substances 0.000 title claims abstract description 23
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 10
- GUVRBAGPIYLISA-UHFFFAOYSA-N tantalum atom Chemical compound [Ta] GUVRBAGPIYLISA-UHFFFAOYSA-N 0.000 claims abstract description 25
- 238000005245 sintering Methods 0.000 claims abstract description 16
- 239000002019 doping agent Substances 0.000 claims abstract description 12
- GUCVJGMIXFAOAE-UHFFFAOYSA-N niobium atom Chemical compound [Nb] GUCVJGMIXFAOAE-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000012535 impurity Substances 0.000 claims abstract description 7
- 239000000126 substance Substances 0.000 claims abstract description 7
- 239000000203 mixture Substances 0.000 claims abstract description 6
- 239000010955 niobium Substances 0.000 claims abstract description 5
- 238000000034 method Methods 0.000 claims description 25
- 238000000137 annealing Methods 0.000 claims description 16
- 239000000843 powder Substances 0.000 claims description 15
- 238000002156 mixing Methods 0.000 claims description 11
- 230000008569 process Effects 0.000 claims description 5
- 238000002791 soaking Methods 0.000 claims description 5
- 238000002844 melting Methods 0.000 claims description 4
- 230000008018 melting Effects 0.000 claims description 4
- 239000011812 mixed powder Substances 0.000 claims description 4
- 238000005096 rolling process Methods 0.000 claims description 4
- 229910052710 silicon Inorganic materials 0.000 claims description 4
- 239000010703 silicon Substances 0.000 claims description 4
- 229910052684 Cerium Inorganic materials 0.000 claims description 3
- ZMIGMASIKSOYAM-UHFFFAOYSA-N cerium Chemical compound [Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce][Ce] ZMIGMASIKSOYAM-UHFFFAOYSA-N 0.000 claims description 3
- 150000001875 compounds Chemical class 0.000 claims description 3
- 229910052732 germanium Inorganic materials 0.000 claims description 3
- GNPVGFCGXDBREM-UHFFFAOYSA-N germanium atom Chemical compound [Ge] GNPVGFCGXDBREM-UHFFFAOYSA-N 0.000 claims description 3
- 238000012545 processing Methods 0.000 claims description 3
- 229910052727 yttrium Inorganic materials 0.000 claims description 3
- VWQVUPCCIRVNHF-UHFFFAOYSA-N yttrium atom Chemical compound [Y] VWQVUPCCIRVNHF-UHFFFAOYSA-N 0.000 claims description 3
- ZSLUVFAKFWKJRC-IGMARMGPSA-N 232Th Chemical compound [232Th] ZSLUVFAKFWKJRC-IGMARMGPSA-N 0.000 claims description 2
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 claims description 2
- BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 claims description 2
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 2
- 229910052776 Thorium Inorganic materials 0.000 claims description 2
- 229910052787 antimony Inorganic materials 0.000 claims description 2
- WATWJIUSRGPENY-UHFFFAOYSA-N antimony atom Chemical compound [Sb] WATWJIUSRGPENY-UHFFFAOYSA-N 0.000 claims description 2
- 229910052785 arsenic Inorganic materials 0.000 claims description 2
- RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic atom Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 claims description 2
- 229910052796 boron Inorganic materials 0.000 claims description 2
- 238000005242 forging Methods 0.000 claims description 2
- 229910052735 hafnium Inorganic materials 0.000 claims description 2
- VBJZVLUMGGDVMO-UHFFFAOYSA-N hafnium atom Chemical compound [Hf] VBJZVLUMGGDVMO-UHFFFAOYSA-N 0.000 claims description 2
- 229910052746 lanthanum Inorganic materials 0.000 claims description 2
- FZLIPJUXYLNCLC-UHFFFAOYSA-N lanthanum atom Chemical compound [La] FZLIPJUXYLNCLC-UHFFFAOYSA-N 0.000 claims description 2
- 238000003754 machining Methods 0.000 claims description 2
- 238000003801 milling Methods 0.000 claims description 2
- 229910052711 selenium Inorganic materials 0.000 claims description 2
- 239000011669 selenium Substances 0.000 claims description 2
- 238000007493 shaping process Methods 0.000 claims description 2
- 229910052714 tellurium Inorganic materials 0.000 claims description 2
- PORWMNRCUJJQNO-UHFFFAOYSA-N tellurium atom Chemical compound [Te] PORWMNRCUJJQNO-UHFFFAOYSA-N 0.000 claims description 2
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims 1
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 claims 1
- 229910052698 phosphorus Inorganic materials 0.000 claims 1
- 239000011574 phosphorus Substances 0.000 claims 1
- 229910052719 titanium Inorganic materials 0.000 claims 1
- 239000010936 titanium Substances 0.000 claims 1
- 229910052726 zirconium Inorganic materials 0.000 claims 1
- 229910052715 tantalum Inorganic materials 0.000 abstract description 6
- 230000008901 benefit Effects 0.000 abstract description 3
- 229910052758 niobium Inorganic materials 0.000 abstract description 3
- 230000009286 beneficial effect Effects 0.000 abstract description 2
- 239000002994 raw material Substances 0.000 abstract 1
- 239000000463 material Substances 0.000 description 6
- 238000005452 bending Methods 0.000 description 4
- 230000000052 comparative effect Effects 0.000 description 3
- 239000007789 gas Substances 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- 239000004744 fabric Substances 0.000 description 2
- 230000006872 improvement Effects 0.000 description 2
- 239000011261 inert gas Substances 0.000 description 2
- 229910052756 noble gas Inorganic materials 0.000 description 2
- 238000003825 pressing Methods 0.000 description 2
- 241000208340 Araliaceae Species 0.000 description 1
- 241000792859 Enema Species 0.000 description 1
- 241001412225 Firmiana simplex Species 0.000 description 1
- 235000005035 Panax pseudoginseng ssp. pseudoginseng Nutrition 0.000 description 1
- 235000003140 Panax quinquefolius Nutrition 0.000 description 1
- 239000005030 aluminium foil Substances 0.000 description 1
- 229910052786 argon Inorganic materials 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000011449 brick Substances 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 238000004891 communication Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000013872 defecation Effects 0.000 description 1
- -1 drink Chemical compound 0.000 description 1
- 239000007920 enema Substances 0.000 description 1
- 229940095399 enema Drugs 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 235000008434 ginseng Nutrition 0.000 description 1
- 238000010348 incorporation Methods 0.000 description 1
- 230000001939 inductive effect Effects 0.000 description 1
- 238000003780 insertion Methods 0.000 description 1
- 230000037431 insertion Effects 0.000 description 1
- 238000013508 migration Methods 0.000 description 1
- 230000005012 migration Effects 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 239000000829 suppository Substances 0.000 description 1
- 238000001291 vacuum drying Methods 0.000 description 1
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
- H01G9/00—Electrolytic capacitors, rectifiers, detectors, switching devices, light-sensitive or temperature-sensitive devices; Processes of their manufacture
- H01G9/004—Details
- H01G9/008—Terminals
- H01G9/012—Terminals specially adapted for solid capacitors
Landscapes
- Engineering & Computer Science (AREA)
- Power Engineering (AREA)
- Microelectronics & Electronic Packaging (AREA)
- Powder Metallurgy (AREA)
Abstract
本发明提供了一种满足电解电容器阳极引线使用要求的钽铌合金丝及其制造方法。其特征在于:该钽铌合金丝化学成分(重量)百分比为钽0.1-99.9%,有益掺杂物0.001-0.2%,余量为铌和不可避免的杂质。通过本发明的钽铌合金丝及其制备方法,有效地改善了钽铌合金丝的高温性能和抗脆性,提高了其高温烧结后的折丝性能,同时也具备常规钽铌合金丝原料成本低,单位重量有效使用长度长等优点。
Description
PCT国内申请,说明书已公开。
Claims (1)
- PCT国内申请,权利要求书已公开。
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
PCT/CN2013/071876 WO2014131151A1 (zh) | 2013-02-26 | 2013-02-26 | 一种电容器级钽铌合金丝及其制造方法 |
Publications (1)
Publication Number | Publication Date |
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CN104903983A true CN104903983A (zh) | 2015-09-09 |
Family
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Family Applications (1)
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CN201380069773.9A Pending CN104903983A (zh) | 2013-02-26 | 2013-02-26 | 一种电容器级钽铌合金丝及其制造方法 |
Country Status (2)
Country | Link |
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CN (1) | CN104903983A (zh) |
WO (1) | WO2014131151A1 (zh) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109675956A (zh) * | 2018-12-28 | 2019-04-26 | 宁夏东方钽业股份有限公司 | 一种小规格超导铌棒的制备方法 |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US10134530B2 (en) | 2016-02-17 | 2018-11-20 | Kemet Electronics Corporation | Anode lead wires for improved solid electrolytic capacitors |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH0653087A (ja) * | 1992-07-27 | 1994-02-25 | Nippon Steel Corp | コンデンサ用電極材料の製造方法 |
CN1437753A (zh) * | 2000-06-21 | 2003-08-20 | H.C.施塔克股份有限公司 | 电容器粉末 |
CN1623215A (zh) * | 2002-01-24 | 2005-06-01 | H.C.施塔克公司 | 拉伸强度和硬度改进的电容器级引线 |
CN101243539A (zh) * | 2005-08-12 | 2008-08-13 | W.C.贺利氏股份有限公司 | 特别是基于铌的、用于单侧插座灯的导线和框架及其生产方法和使用 |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
BE668967A (zh) * | 1964-08-31 | |||
US4245275A (en) * | 1978-06-23 | 1981-01-13 | Mepco/Electra, Inc. | Refractory metal alloy case capacitor |
-
2013
- 2013-02-26 CN CN201380069773.9A patent/CN104903983A/zh active Pending
- 2013-02-26 WO PCT/CN2013/071876 patent/WO2014131151A1/zh active Application Filing
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH0653087A (ja) * | 1992-07-27 | 1994-02-25 | Nippon Steel Corp | コンデンサ用電極材料の製造方法 |
CN1437753A (zh) * | 2000-06-21 | 2003-08-20 | H.C.施塔克股份有限公司 | 电容器粉末 |
CN1623215A (zh) * | 2002-01-24 | 2005-06-01 | H.C.施塔克公司 | 拉伸强度和硬度改进的电容器级引线 |
CN101243539A (zh) * | 2005-08-12 | 2008-08-13 | W.C.贺利氏股份有限公司 | 特别是基于铌的、用于单侧插座灯的导线和框架及其生产方法和使用 |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109675956A (zh) * | 2018-12-28 | 2019-04-26 | 宁夏东方钽业股份有限公司 | 一种小规格超导铌棒的制备方法 |
Also Published As
Publication number | Publication date |
---|---|
WO2014131151A1 (zh) | 2014-09-04 |
WO2014131151A8 (zh) | 2015-07-02 |
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PB01 | Publication | ||
C10 | Entry into substantive examination | ||
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RJ01 | Rejection of invention patent application after publication | ||
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Application publication date: 20150909 |