CN104894746B - A kind of manufacture method of the continuous piece of silkworm - Google Patents

A kind of manufacture method of the continuous piece of silkworm Download PDF

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Publication number
CN104894746B
CN104894746B CN201510371073.6A CN201510371073A CN104894746B CN 104894746 B CN104894746 B CN 104894746B CN 201510371073 A CN201510371073 A CN 201510371073A CN 104894746 B CN104894746 B CN 104894746B
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pelettes
continuous piece
silk
continuous
silk floss
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CN104894746A (en
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潘大东
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GUANGXI LI SHENG COCOON SILK CO Ltd
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GUANGXI LI SHENG COCOON SILK CO Ltd
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Abstract

The present invention disclose a kind of manufacture method of silkworm silk floss piece, and the manufacture method of the continuous piece is through the following steps that to realize:→ pelettes reprocess → plays silk floss and → boils silk floss → rinsing and dehydration → dipping softening agent → cleaning and dewatering → dries for pelettes pretreatment.Pelettes is directly processed into continuous piece by the present invention, and easy to operate, production cost is low, is adapted to industrialized production, and the impurity that continuous piece is mingled with is less, and deoiling effect is good, adds softening agent and causes continuous piece soft texture, color is pure white, quality is high.

Description

A kind of manufacture method of the continuous piece of silkworm
Technical field
The present invention relates to textile engineering technical field, more particularly, to a kind of manufacture method of the continuous piece of silkworm.
Background technology
The scrotiform protective layer in silkworm pupa time, includes pupal cell, and protective layer includes the parts such as husks, cocoon layer and pelettes.Cocoon layer can With filature, the waste silk after husks and reel silk from cocoons system can make silk flosssilk wadding and silk spinning raw material.After matured silkworm is placed on small straw bundles to spin cocoons, the husks of loose unrest is made in first spinning, Then cephalothorax starts to swing regularly, the wire ring spued in~shape or ∞ fonts, and 15-25 wire ring of product is into 1 silk piece.Through After constantly changing position, many overlapping silk pieces are formed, are adhered by silk gum, constitute the cocoon with many micro-pores between fibre Layer.Fibre on cocoon layer claims silk, and after outer and inner completion cocoon layer, silkworm body is reduced significantly, and swings slow, spinning loses rule Property, the very thin silk layer of loose unrest is finally formed in cocoon layer inner chamber, claims pelettes, that is, completes spinning and cocoons process.
Natural silk silk floss is, by silk floss stripping machine dissociation silk, to obtain being cleaned after silk floss, by chemical drugs by silk cocoon Agent is added and boiled in continuous pot, the part silk gum in silk floss, pupal fat is separated, then is cleaned, is dried, obtains silk continuous.In tradition Silk floss process, be to be put into silk floss piecewise to boil in continuous pot (cement pit or container) and add chemical agent and steam, Picked up piecewise again after certain time.
The preparation method that open source literature also reports silk floss, such as:
Chinese patent:Silk floss manufacture craft under high altitude environment, application number:201310333650.3, apply (patent right) People:Yunnan Hai Run Silk qualities Co., Ltd, summary:The invention belongs to the manufacture technology field that silk silk floss makes, and in particular to The technology that a kind of silk floss under high altitude environment makes.Being improved to for this manufacture craft, 1. makes continuous:Beat the temperature of continuous solution Boiling point should be reached, the every silk floss weight in wet base got is controlled under Suitable solutions assistant concentration;2. soak:Control and boil silk floss every time Amount, then clear water immersion, centre needs to change water once, is dehydrated;3. silk floss is boiled:It is heated up to after boiling, when the boiling that closes the lid is suitable Between;4. it is dehydrated:First it is dehydrated, is soaked by two clear water reserviors segmentations, then be dehydrated;5. bleach:It is put into Bellmer liquid, is heated up to spy Constant temperature degree, soaks, dehydration, clear water immersion, then is dehydrated;6. dry:Dried in the interior of lucifuge to moisture content 9 ± 1%.The present invention The silk floss color of making is fair and clear, glossiness is good, soft, smell is small, and silk gum melts mistake rate and diminished.
Chinese patent:A kind of manufacture method of pelettes silk quilt, application number:201410585989.7, apply (patent right) People:Nafuer Garment Ornament Co., Ld., Nantong, summary:The invention discloses a kind of technique that pelettes is processed into silk quilt, this hair Bright method mainly beats the step such as expanded including buck spray, rolling, cutting, immersion, degreasing degumming, bleaching, drying, bullet Suddenly, pelettes can be directly processed into by the method for the present invention by silk quilt, easy to operate, smooth, production cost is low, be adapted to Industrialized production;The silk quilt uniform specification of production, silk quilt impurity is few, grease removal effect is good, and silk quilt is soft, color Pure white, quality is high.
But studied through the present inventor and find that the manufacture method of silk floss or silk quilt in document disclosed above is numerous and diverse, and production It is of long duration, add cost.
The content of the invention
It is easy it is an object of the invention to provide a kind of method, the continuous piece making method of silkworm of low production cost, fully profit Pelettes raw material is used, this boils continuous technique for use, effectively increases the quality index such as strength, cleaning and the cleaning of continuous piece;By to pupa A series of processing of lining, obtain the continuous piece that color is fair and clear, glossiness is high and soft, improve the value of substandard goods.
The present invention uses following technical proposals:
The manufacture method of the continuous piece of silkworm a kind of is through the following steps that to realize:
Silk floss → rinsing and dehydration → dipping softening agent → cleaning and dewatering are boiled in pelettes pretreatment → pelettes reprocess → plays silk floss → → dry.
Specifically include following steps:
1)Pelettes is pre-processed:According to 1:80-90 immersion ratio, pelettes is immersed in treatment fluid, is soaked at 40-50 DEG C 40-50min, wherein described treatment fluid is tea bran water, mass concentration is 15-20%;There is abundant thick egg inside tea bran water In vain, and the nutriment such as several amino acids, dirt-removing power is strong, and silk is injured without chemical analysis, is optimal clear of the Nature One of clean dose;
2)Pelettes is reprocessed:Pelettes is put into silk floss machine, NaOH solution is directly sprayed on pelettes, wherein the NaOH The concentration expressed in percentage by weight of solution is 0.4-0.5%, and temperature is 60-70 DEG C;Using spray mode pelettes can be made to be acted on equal by alkali Even, silk layer becomes more loose, is conducive to the silk of pelettes on silk floss machine cylinder;
3)Play silk floss:Step 2 will be passed through)Treated pelettes is transported to beat in continuous machine and carries out playing silk floss, and it is every that control is got Piece silk floss weight in wet base is in 2-2.5Kg;
4)Boil silk floss:According to 1:40-50 bath raio, the continuous piece extracted is put into and boiled in continuous liquid, is kept at 90 DEG C -100 DEG C Micro-boiling state 90-100 minutes, boils the following ingredients that continuous liquid represents by following concentration expressed in percentage by weight and constitutes wherein described:5%- 15% NaOH, 5%-15% hydrogen peroxide;1%-8% textile soap, 1%-5% sodium metasilicate, surplus is water;
5)Rinsing and dehydration:By step 4)Continuous piece be put into water and rinse repeatedly, until the pH value of continuous piece is in neutrality, then It is 27% that continuous piece after rinsing, which is dehydrated to water content,;
6)Impregnate softening agent:By above-mentioned steps 5)Continuous piece after cleaning and dewatering is put into softening pond and carries out dipping softening, continuous piece It is 1 with the aqueous solution weight ratio in pond:8-10;The described aqueous solution is by 2-5% surfactant, 2-3% sodium metasilicate and 2- 5% hydrogen peroxide is prepared;Wherein surfactant is:Triethyl citrate, neopelex and laurel alcohol ether phosphate Any of potassium;
7)Cleaning and dewatering:By above-mentioned steps 6)Continuous piece after dipping softening agent is pulled out and fully rinsed well, reagent removal, is taken off Water;
8)Dry:By above-mentioned steps 7)Continuous piece after cleaning and dewatering is dried in the interior of lucifuge to regain 7-10%.
Compared with prior art, the positive effect of the present invention is:
1st, silkworm pelettes is directly processed into continuous piece, and easy to operate, production cost is low, is adapted to industrialized production, and continuous piece is mingled with Impurity it is less, deoiling effect is good, adds softening agent and causes continuous piece soft texture, color is pure white, quality is high.
2nd, add tea bran water to pre-process pelettes, soak 40-50min at 40-50 DEG C, pupa can be removed well The greasy dirt of lining, and certain degumming effect can be played, silk is not injured also;There is abundant crude protein inside tea bran water, and The nutriments such as several amino acids, dirt-removing power is strong, and silk is injured without chemical analysis, be the optimal cleaning agent of the Nature it One.
3rd, the softening agent that the present invention is configured enables to continuous piece soft, it is not easy to lump, so as to greatly improve final products The quality of silk quilt.
Embodiment
The present invention is expanded on further with reference to specific embodiment.It should be understood that these embodiments are merely to illustrate this hair Bright rather than limitation the scope of the present invention.In addition, it is to be understood that after the content of the invention lectured has been read, this area skill Art personnel can make various changes or modifications to the present invention, and these equivalent form of values equally fall within the application appended claims institute The scope of restriction.
Embodiment 1
A kind of manufacture method of the continuous piece of silkworm, it comprises the following steps:
1)Pelettes is pre-processed:According to 1:80 immersion ratio, pelettes is immersed in treatment fluid, 40min is soaked at 40 DEG C, Wherein described treatment fluid is tea bran water, and mass concentration is 15%;
2)Pelettes is reprocessed:Pelettes is put into silk floss machine, NaOH solution is directly sprayed on pelettes, wherein the NaOH The concentration expressed in percentage by weight of solution is 0.4%, and temperature is 60 DEG C;
3)Play silk floss:Step 2 will be passed through)Treated pelettes is transported to beat in continuous machine and carries out playing silk floss, controls every got Silk floss weight in wet base is in 2Kg;
4)Boil silk floss:According to 1:40 bath raio, the continuous piece extracted is put into and boiled in continuous liquid, and micro-boiling state is kept at 90 DEG C 90 minutes, boil the following ingredients that continuous liquid represents by following concentration expressed in percentage by weight wherein described and constitute:5% NaOH, 5% dioxygen Water;1% textile soap, 1% sodium metasilicate, surplus is water;
5)Rinsing and dehydration:By step 4)Continuous piece be put into water and rinse repeatedly, until the pH value of continuous piece is in neutrality, then It is 27% that continuous piece after rinsing, which is dehydrated to water content,;
6)Impregnate softening agent:By above-mentioned steps 5)Continuous piece after cleaning and dewatering is put into softening pond and carries out dipping softening, continuous piece It is 1 with the aqueous solution weight ratio in pond:8;The described aqueous solution is by 2% surfactant, 2% sodium metasilicate and 2% hydrogen peroxide Prepare;Wherein surfactant is triethyl citrate;
7)Cleaning and dewatering:By above-mentioned steps 6)Continuous piece after dipping softening agent is pulled out and fully rinsed well, reagent removal, is taken off Water;
8)Dry:By above-mentioned steps 7)Continuous piece after cleaning and dewatering is dried in the interior of lucifuge to regain 7%.
Embodiment 2
A kind of manufacture method of the continuous piece of silkworm, it comprises the following steps:
1)Pelettes is pre-processed:According to 1:85 immersion ratio, pelettes is immersed in treatment fluid, 45min is soaked at 45 DEG C, Wherein described treatment fluid is tea bran water, and mass concentration is 18%;
2)Pelettes is reprocessed:Pelettes is put into silk floss machine, NaOH solution is directly sprayed on pelettes, wherein the NaOH The concentration expressed in percentage by weight of solution is 0.5%, and temperature is 65 DEG C;
3)Play silk floss:Step 2 will be passed through)Treated pelettes is transported to beat in continuous machine and carries out playing silk floss, controls every got Silk floss weight in wet base is in 2.2Kg;
4)Boil silk floss:According to 1:45 bath raio, the continuous piece extracted is put into and boiled in continuous liquid, and micro-boiling state is kept at 95 DEG C 95 minutes, boil the following ingredients that continuous liquid represents by following concentration expressed in percentage by weight wherein described and constitute:10% NaOH, 10% dioxygen Water;5% textile soap, 3% sodium metasilicate, surplus is water;
5)Rinsing and dehydration:By step 4)Continuous piece be put into water and rinse repeatedly, until the pH value of continuous piece is in neutrality, so It is 27% that the continuous piece after rinsing, which is dehydrated to water content, afterwards;
6)Impregnate softening agent:By above-mentioned steps 5)Continuous piece after cleaning and dewatering is put into softening pond and carries out dipping softening, continuous piece It is 1 with the aqueous solution weight ratio in pond:9;The described aqueous solution is by 3% surfactant, 3% sodium metasilicate and 3% hydrogen peroxide Prepare;Wherein surfactant is neopelex;
7)Cleaning and dewatering:By above-mentioned steps 6)Continuous piece after dipping softening agent is pulled out and fully rinsed well, reagent removal, is taken off Water;
8)Dry:By above-mentioned steps 7)Continuous piece after cleaning and dewatering is dried in the interior of lucifuge to regain 8%.
Embodiment 3
A kind of manufacture method of the continuous piece of silkworm, it comprises the following steps:
1)Pelettes is pre-processed:According to 1:90 immersion ratio, pelettes is immersed in treatment fluid, 40- is soaked at 50 DEG C 50min, wherein described treatment fluid is tea bran water, mass concentration is 20%;
2)Pelettes is reprocessed:Pelettes is put into silk floss machine, NaOH solution is directly sprayed on pelettes, wherein the NaOH The concentration expressed in percentage by weight of solution is 0.5%, and temperature is 70 DEG C;
3)Play silk floss:Step 2 will be passed through)Treated pelettes is transported to beat in continuous machine and carries out playing silk floss, controls every got Silk floss weight in wet base is in 2.5Kg;
4)Boil silk floss:According to 1:50 bath raio, the continuous piece extracted is put into and boiled in continuous liquid, and micro-boiling shape is kept at 100 DEG C State 100 minutes, boils the following ingredients that continuous liquid represents by following concentration expressed in percentage by weight and constitutes wherein described:15% NaOH, 15% Hydrogen peroxide;8% textile soap, 5% sodium metasilicate, surplus is water;
5)Rinsing and dehydration:By step 4)Continuous piece be put into water and rinse repeatedly, until the pH value of continuous piece is in neutrality, so It is 27% that the continuous piece after rinsing, which is dehydrated to water content, afterwards;
6)Impregnate softening agent:By above-mentioned steps 5)Continuous piece after cleaning and dewatering is put into softening pond and carries out dipping softening, continuous piece It is with the aqueous solution weight ratio in pond:1:10;The described aqueous solution is by 5% surfactant, 3% sodium metasilicate and 5% dioxygen Water is prepared;Wherein surfactant is laurel alcohol ether phosphate potassium;
7)Cleaning and dewatering:By above-mentioned steps 6)Continuous piece after dipping softening agent is pulled out and fully rinsed well, reagent removal, is taken off Water;
8)Dry:By above-mentioned steps 7)Continuous piece after cleaning and dewatering is dried in the interior of lucifuge to regain 10%.
Application Example
Compared with the continuous piece of silkworm of the prior art, the continuous piece of silkworm of the invention is in oil content, nasal receptor and whiteness etc. Aspect has different degrees of raising(Refer to following table):

Claims (1)

1. a kind of manufacture method of the continuous piece of silkworm, it is characterised in that:The manufacture method of the continuous piece is through the following steps that come real Existing:
→ pelettes reprocess → plays silk floss and → boils silk floss → rinsing and dehydration → dipping softening agent → cleaning and dewatering → dries in the air for pelettes pretreatment It is dry;
Comprise the following steps that:
1)Pelettes is pre-processed:According to 1:80-90 immersion ratio, pelettes is immersed in treatment fluid, 40- is soaked at 40-50 DEG C 50min, wherein described treatment fluid is tea bran water, mass concentration is 15-20%;There is abundant crude protein inside tea bran water And several amino acids nutriment, dirt-removing power is strong, does not injure silk;
2)Pelettes is reprocessed:Pelettes is put into silk floss machine, NaOH solution is sprayed directly on pelettes, wherein the NaOH The concentration expressed in percentage by weight of solution is 0.4-0.5%, and temperature is 60-70 DEG C;Make pelettes by alkali even action, silk layer becomes more Plus it is loose, be conducive to the silk of pelettes on silk floss machine cylinder;
3)Play silk floss:Step 2 will be passed through)Treated pelettes is transported to beat in continuous machine and carries out playing silk floss, controls the every silk got Continuous weight in wet base is in 2-2.5Kg;
4)Boil silk floss:According to 1:40-50 bath raio, the continuous piece extracted is put into and boiled in continuous liquid, micro-boiling is kept at 90 DEG C -100 DEG C Rise state 90-100 minutes, boil the following ingredients that continuous liquid represents by following concentration expressed in percentage by weight wherein described and constitute:5%-15%'s NaOH, 5%-15% hydrogen peroxide;1%-8% textile soap, 1%-5% sodium metasilicate, surplus is water;
5)Rinsing and dehydration:By step 4)Continuous piece be put into water and rinse repeatedly, until the pH values of continuous piece are in neutral, then It is 27% that continuous piece after rinsing, which is dehydrated to water content,;
6)Impregnate softening agent:By above-mentioned steps 5)Continuous piece after cleaning and dewatering be put into softening pond carry out dipping softening, continuous piece with Aqueous solution weight ratio in pond is 1:8-10;The described aqueous solution is by 2-5% surfactant, 2-3% sodium metasilicate and 2-5% Hydrogen peroxide prepare;Wherein surfactant is triethyl citrate, neopelex and laurel alcohol ether phosphate potassium Any of;Add softening agent and cause continuous piece soft texture, it is not easy to lump, color is pure white, quality is high;
7)Cleaning and dewatering:By above-mentioned steps 6)Continuous piece after dipping softening agent, which is pulled out, fully to be rinsed well, reagent removal, dehydration ;
8)Dry:By above-mentioned steps 7)Continuous piece after cleaning and dewatering is dried in the interior of lucifuge to regain 7-10%.
CN201510371073.6A 2015-06-30 2015-06-30 A kind of manufacture method of the continuous piece of silkworm Expired - Fee Related CN104894746B (en)

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CN106263891B (en) * 2016-08-31 2018-02-27 广西桂华丝绸有限公司 A kind of eider down silk quilt and preparation method thereof
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CN113005529A (en) * 2021-03-05 2021-06-22 广西迎春丝绸有限公司 Method for refining pupa lining cotton dregs
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