CN105919910A - Preparation method of natural fibroin mask - Google Patents

Preparation method of natural fibroin mask Download PDF

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CN105919910A
CN105919910A CN201610273950.0A CN201610273950A CN105919910A CN 105919910 A CN105919910 A CN 105919910A CN 201610273950 A CN201610273950 A CN 201610273950A CN 105919910 A CN105919910 A CN 105919910A
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韦有任
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Shanghai Tieman Biotechnology Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/98Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/987Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/805Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
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  • Cosmetics (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)

Abstract

The invention relates to the field of cosmetics, in particular to a preparation method of a natural fibroin mask, which comprises the following process steps: (1) after the mature silkworms of the mulberry silkworms defecate, putting the mature silkworms on a silking net, and enabling the mature silkworms to evenly spit 5-8 layers of silks on the silking net; (2) after the silking of the matured silkworms is finished, removing dust and sundries on the silks, and peeling the silks from the silking net; (3) cutting the peeled silk according to the shape of the mask to obtain mask-shaped silk; (4) placing the facial mask-shaped silk in a device capable of steaming with water, steaming the silk for 3-5 minutes by using water vapor, wherein the temperature of the water vapor is kept between 100 ℃ and 105 ℃; (5) placing the steamed facial mask-shaped silk into a microwave sterilization machine for microwave sterilization for 5-6 minutes; (6) and packaging the sterilized facial mask-shaped silk according to a traditional facial mask packaging process to obtain the pure mulberry silk protein facial mask. The facial mask provided by the invention is short in processing flow, silk is not easy to damage, and the skin care effect is good.

Description

天然蚕丝蛋白面膜的制备方法 Preparation method of natural silk protein facial mask

技术领域 technical field

本发明涉及化妆品领域,具体是一种天然蚕丝蛋白面膜的制备方法。 The invention relates to the field of cosmetics, in particular to a preparation method of a natural silk protein facial mask.

背景技术 Background technique

蚕丝是一种天然的蛋白质纤维,是所有天然纤维棉、毛、丝、麻中唯一的长丝纤维,上好的一粒茧能缫得的茧丝长度可达到一千米,因此长丝结构的蚕丝通常用来制作高档服装和丝织品,而蚕丝在缫丝过程中产生的下脚料被切断成短纤维再进行绢纺加工,制作绢纺面料(蚕丝短纤维)。天然蚕丝的截面为三角形,是由两根单丝依靠丝胶黏合而成,其蛋白质组成是丝素和丝胶两种,丝素约占70%左右分布在蚕丝的中心,丝胶占30%左右,丝胶是构成蚕丝纤维外层组织的蛋白质,丝胶对包裹在其内部的丝素起着保护和粘接的作用。丝素蛋白包括赖氨酸、组氨酸、胱氨酸、天门冬氨酸等18种氨基酸和多种微量元素,能增加皮肤角质层的含水量,促进胶原蛋白合成,增强皮肤的张力和弹性,与人体皮肤有较强的亲和力,很容易被人体肌肤吸收。丝胶是一种球状蛋白,由丝氨酸、天门冬氨酸和谷氨酸等18种氨基酸组成,丝胶蛋白具有抑制酪氨酸酶活性的特性,因此能阻止皮肤中黑色素的形成,美白皮肤,防止日光中紫外线对皮肤的伤害,因此丝胶蛋白是一种宝贵的天然化妆品配料。 Silk is a natural protein fiber and the only filament fiber among all natural fibers cotton, wool, silk, and hemp. A good cocoon can be reeled to a length of one kilometer, so the filament structure High-quality silk is usually used to make high-end clothing and silk fabrics, while the leftovers produced during the silk reeling process are cut into short fibers and then processed into silk spinning to make silk spinning fabrics (short silk fibers). The cross section of natural silk is triangular, and it is made of two monofilaments bonded by sericin. Its protein composition is silk fibroin and sericin. About 70% of silk fibroin is distributed in the center of silk, and sericin accounts for 30%. Left and right, sericin is a protein that constitutes the outer layer of silk fiber, and sericin plays a role in protecting and bonding the silk fibroin wrapped inside it. Silk fibroin includes 18 kinds of amino acids such as lysine, histidine, cystine and aspartic acid and various trace elements, which can increase the water content of the stratum corneum of the skin, promote the synthesis of collagen, and enhance the tension and elasticity of the skin , has a strong affinity with human skin and is easily absorbed by human skin. Sericin is a globular protein composed of 18 kinds of amino acids such as serine, aspartic acid and glutamic acid. Sericin protein has the property of inhibiting tyrosinase activity, so it can prevent the formation of melanin in the skin, whiten the skin, Prevents the skin from being damaged by ultraviolet rays in the sun, so sericin is a valuable natural cosmetic ingredient.

随着生活水平提高,面膜已从原来的奢侈消费品变为现代人的必备保养品。而蚕丝作为一种天然动物蛋白质,与人体皮肤具有很大的相似性,相对其它蛋白来说,也更易被人体吸收,起到美白、保湿的作用。另外,蚕丝中含量较多的酪氨酸和苯丙氨酸等对紫外线具有很好的吸收作用,具有防晒护肤功效。因此,蚕丝也成为面膜界广受欢迎的面膜基材。 With the improvement of living standards, facial masks have changed from an original luxury consumer product to an essential skin care product for modern people. Silk, as a natural animal protein, has a great similarity with human skin. Compared with other proteins, it is easier to be absorbed by the human body, and plays the role of whitening and moisturizing. In addition, the tyrosine and phenylalanine contained in silk have a good absorption effect on ultraviolet rays, and have the effect of sun protection and skin care. Therefore, silk has also become a popular mask substrate in the mask industry.

目前市售的蚕丝面膜主要采用无纺布的生产制造工艺,而无纺布的生产工艺较为复杂:主要采用绢纺原料(即缫丝中的下脚料、废丝、落绵等),经过除杂,切断、脱胶(或固胶)精炼、梳理、加入抗静电剂、调控温湿度后进入水刺(或针刺)生产线。这些绢纺原料大部分已经过多次的物理、化学作用(高温、高压、化学助剂),丝胶虽然仍有保留,但蛋白经过多次的变性复性过程,大部分丝胶蛋白的活性早已丧失,无法达到理想的美容效果。在蚕茧形成面膜基材的传统工艺中,蚕茧都必须经过高温蒸煮(汽蒸),此过程中丝胶会大量流失和变性,造成极大浪费,其护肤效果也不理想,且形成的蚕丝面膜由于丝胶流失,结构松散,使用过程中易变形,使用不便。另外,目前的水刺(或针刺)线生产出的蚕丝无纺布普遍较厚重,导致蚕丝面膜与皮肤贴合度差,使用效果不理想,丧失其亲肤性。因此,如何简单的获得一种护肤效果好的蚕丝面膜,一直是行业内人士研究的方向。公开文献也报道了一些蚕丝面膜,例如: Currently commercially available silk masks mainly use the manufacturing process of non-woven fabrics, and the production process of non-woven fabrics is more complicated: mainly use silk spinning raw materials (ie leftovers in silk reeling, waste silk, cotton, etc.), after removing Miscellaneous, cutting, degumming (or glue fixing) refining, carding, adding antistatic agent, adjusting temperature and humidity, and then entering the spunlace (or acupuncture) production line. Most of these silk spinning raw materials have undergone multiple physical and chemical actions (high temperature, high pressure, chemical additives). Although sericin is still retained, the protein has undergone multiple denaturation and refolding processes, and most of the activity of sericin protein It has long been lost and cannot achieve the desired cosmetic effect. In the traditional process of silkworm cocoons forming mask substrates, silkworm cocoons must be cooked at high temperature (steaming). During this process, a large amount of sericin will be lost and denatured, resulting in great waste, and its skin care effect is not ideal, and the formed silk mask Due to the loss of sericin, the structure is loose, easy to deform during use, and inconvenient to use. In addition, the silk non-woven fabric produced by the current spunlace (or acupuncture) line is generally thick and heavy, resulting in poor adhesion between the silk mask and the skin, unsatisfactory use effect, and loss of its skin-friendliness. Therefore, how to simply obtain a silk mask with good skin care effect has been the research direction of people in the industry always. Public literature also reports some silk facial masks, such as:

1、中国专利:一种用蚕茧生产蚕丝面膜基布的方法及蚕丝面膜,申请号 :201510040948.4,申请日:2015.01.27,申请人:西南大学,地址:400715 重庆市北碚区天生路 2 号,发明人:夏庆友、席星航、杨佩,摘要:该发明公开了一种用蚕茧生产蚕丝面膜基布的方法,按照如下步骤完成:(1)、洗茧:将蚕茧用清水洗去灰尘和杂物;(2)、润湿:将清洗后的蚕茧用水浸泡使其充分润湿;(3)、浸碱:将润湿后的蚕茧均匀放入蒸桶,用恰能润湿蚕茧的碱水喷淋蚕茧,使得蚕茧再次被润湿;(4)、汽蒸:用蒸汽蒸蚕茧使得丝胶完全溶胀;(5)、清洗:用清水清洗蒸好的蚕茧;(6)、剥茧:将蚕蛹剥离去掉;(7)、将剥离去掉蚕蛹的蚕茧制成弧形蚕丝网膜;(8)、将蚕丝网膜经过漂白、用冰醋酸溶液中和、烘干最后冲压成型得到蚕丝面膜基布。该发明能最大程度的保持丝胶蛋白的活性。工艺流程简单,能充分利用蚕丝的营养物质,是纯天然的美白、保湿、抗皱、抗 UV 产品。 1. Chinese patent: a method for producing silk mask base fabrics from silkworm cocoons and silk masks, application number: 201510040948.4, application date: 2015.01.27, applicant: Southwest University, address: No. 2, Tiansheng Road, Beibei District, Chongqing, 400715, Inventors: Xia Qingyou, Xi Xinghang, Yang Pei, Abstract: This invention discloses a method of using silkworm cocoons to produce silk mask base fabric, which is completed according to the following steps: (1) Cocoon washing: wash the silkworm cocoons with clean water to remove dust and sundries (2), wetting: soak the silkworm cocoons after cleaning in water to make them fully wet; (3), soaking in alkali: put the moistened silkworm cocoons evenly into the steaming bucket, spray them with alkaline water that can just wet the silkworm cocoons Drenching the silkworm cocoons to moisten the silkworm cocoons again; (4), steaming: steaming the silkworm cocoons to make the sericin fully swell; (5), cleaning: cleaning the steamed silkworm cocoons with clear water; (6), peeling cocoons: removing the silkworm chrysalis (7), the cocoons of silkworm chrysalis that have been stripped off are made into an arc-shaped silk mesh; (8), the silk mesh is bleached, neutralized with glacial acetic acid solution, dried, and finally stamped to obtain a silk mask base cloth. The invention can maintain the activity of sericin to the greatest extent. The technological process is simple, and the nutrients of silk can be fully utilized. It is a pure natural whitening, moisturizing, anti-wrinkle, and anti-UV product.

2、中国专利:用蚕茧制作高活性蚕丝面膜的方法,申请号:201510181125.3,申请日:2015.04.17,申请人:重庆航凡蚕丝技术开发有限公司,地址:400030 重庆市沙坪坝区凤天大道18号,发明人:席星航、席兰、赵萍、杨佩,摘要:该发明公开了一种用蚕茧制作高活性蚕丝面膜的方法,其特征在于:按照如下步骤完成:(1)洗茧:用清水洗去蚕茧上的灰尘和杂物;(2)溶茧:将清洗后的蚕茧放入浓度为0.1%~5%的蛋白酶溶液中浸泡,使丝胶充分溶胀,茧层打开;(3)剥茧:撕开茧层,去掉蚕蛹;(4)成膜:将去掉蚕蛹的蚕茧套在拱形模具上,制成蚕丝网膜;(5)干燥 :自然晾干或低温烘干(6)冲压成型。该发明工艺流程短,制作简单,全工艺流程均在低温下处理,不需要碱液浸泡,不需要高温蒸煮,使得蛋白活性最大限度的保留,使得丝胶不变性不流失,面膜紧致度好,使用方便。 2. Chinese patent: Method for making highly active silk mask with silkworm cocoons, application number: 201510181125.3, application date: 2015.04.17, applicant: Chongqing Hangfan Silk Technology Development Co., Ltd., address: 400030 Fengtian Avenue 18, Shapingba District, Chongqing No., Inventors: Xi Xinghang, Xi Lan, Zhao Ping, Yang Pei, Abstract: This invention discloses a method for making a highly active silk mask with silkworm cocoons, which is characterized in that: it is completed according to the following steps: (1) Cocoon washing: Clean water to wash away dust and sundries on silkworm cocoons; (2) cocoon melting: soak the washed silkworm cocoons in a protease solution with a concentration of 0.1% to 5%, so that the sericin is fully swollen and the cocoon layer is opened; (3) Cocoon peeling: tearing the cocoon layer and removing the silkworm chrysalis; (4) film formation: putting the silkworm cocoon with the removed silkworm chrysalis on the arched mold to make a silk mesh film; (5) drying: drying naturally or at low temperature (6) Stamping. The invention has a short technological process and is easy to manufacture. The whole technological process is processed at low temperature without lye soaking or high-temperature cooking, so that the activity of the protein is preserved to the maximum extent, the sericin does not lose its denaturation, and the firmness of the mask is good. , easy to use.

经研究发现,上述公开报道的文献,在制备蚕丝面膜时都是用蚕茧作为原料制备,加工流程长,容易损伤蚕丝,不能保持所需的天然蛋白。 After research, it is found that the above-mentioned publicly reported documents all use silkworm cocoons as raw materials when preparing silk facial masks. The processing flow is long, the silk is easily damaged, and the required natural protein cannot be maintained.

发明内容 Contents of the invention

本发明的目的是提供一种加工流程短,不容易损伤蚕丝,且护肤效果好的纯桑蚕丝蛋白面膜及其制备方法。 The purpose of the present invention is to provide a pure mulberry silk protein mask with short processing flow, not easy to damage silk, and good skin care effect and its preparation method.

为了实现上述目的,本发明采取的技术方案是: In order to achieve the above object, the technical scheme that the present invention takes is:

一种天然蚕丝蛋白面膜的制备方法,其采用以下步骤: A preparation method of natural silk protein facial mask, which adopts the following steps:

(1)待桑蚕的熟蚕排便完后,将其放到吐丝网上,让熟蚕在吐丝网上均匀的吐5-8层丝;将熟蚕放到吐丝网上前,必须待其排便完,才能放到吐丝网上,让其吐丝,可避免熟蚕在吐丝前排便污染吐丝网,从而污染蚕丝;蚕宝宝到了五龄末期,就逐渐体现出老熟的特征:先是排出的粪便由硬变软,由墨绿色变成叶绿色;食欲减退,食桑量下降;前部消化管空虚,胸部呈透明状;继而完全停食,体驱缩短,腹部也趋向透明,蚕体头胸部昂起,口吐丝缕,左右上下摆动寻找营茧场所,这样的蚕就称为熟蚕。 (1) After the cooked silkworms have defecated, put them on the silk spinning net, and let the cooked silkworms spit 5-8 layers of silk evenly on the silk spinning net; before putting the cooked silkworms on the silk spinning net, they must wait After defecating, put it on the silk-spinning net and let it spin silk, which can prevent cooked silkworms from polluting the silk-spinning net by defecation before spinning, and thus contaminate the silk; silkworm babies gradually show the characteristics of maturity when they reach the end of the fifth instar: first, they excrete The feces in the feces changed from hard to soft, from dark green to leaf green; appetite decreased, and the amount of food eaten decreased; the front part of the digestive tract was empty, and the chest became transparent; and then completely stopped eating, the body shortened, and the abdomen also tended to be transparent. The chest is lifted up, the mouth spits out silk threads, and it swings up and down to find a place for cocooning. Such silkworms are called cooked silkworms.

(2)带熟蚕吐丝结束后,将蚕丝上的灰尘和杂物去除,并将蚕丝从吐丝网上剥离; (2) After the silk spinning with cooked silkworms is finished, remove the dust and sundries on the silk, and peel off the silk from the silk spinning net;

(3)将剥离得到的蚕丝按面膜的形状剪裁,得到面膜形蚕丝; (3) Cut the stripped silk according to the shape of the mask to obtain mask-shaped silk;

(4)将面膜形蚕丝放在能水蒸的装置中,利用水蒸汽将蚕丝蒸3-5分钟,将丝蛋白渗出到丝表面,水蒸汽的温度保持在100℃-105℃之间; (4) Put the mask-shaped silk in a device capable of steaming water, steam the silk for 3-5 minutes with water vapor, and exude silk protein to the surface of the silk, and keep the temperature of the water vapor between 100°C and 105°C;

(5)将经过水蒸的面膜形蚕丝放到微波杀菌机中进行微波杀菌5-6分钟;在进行微波杀菌前需面膜形蚕丝进行检测是否有丝蛋白渗出,有丝蛋白渗出的即可进行微波杀菌;保证储存的时间达到3-5个月以上. (5) Put the steamed mask-shaped silk in a microwave sterilizer for microwave sterilization for 5-6 minutes; before microwave sterilization, the mask-shaped silk needs to be tested for silk protein exudation, and silk protein exudation is immediately It can be sterilized by microwave; the storage time is guaranteed to be more than 3-5 months.

(6)将杀菌后的面膜形蚕丝按照传统的面膜包装工艺进行包装即可得到纯桑蚕丝蛋白面膜。 (6) Pack the sterilized mask-shaped silk according to the traditional mask packaging process to obtain a pure mulberry silk protein mask.

所述的吐丝网的网眼宽度为1-3毫米,吐丝网的厚度为0.5-1毫米。 The mesh width of the spinning net is 1-3 mm, and the thickness of the spinning net is 0.5-1 mm.

微波杀菌机可在广州福滔微波设备有限公司购买,地址:广州市白云区太和镇谢家庄打鼓岭街13号,网址:http://www.gzfutao.com;微波杀菌机的输出微波功率:40KW,功率可调。 Microwave sterilizer can be purchased at Guangzhou Futao Microwave Equipment Co., Ltd. Address: No. 13, Daguling Street, Xiejiazhuang, Taihe Town, Baiyun District, Guangzhou City, website: http://www.gzfutao.com; output microwave power of microwave sterilizer: 40KW, adjustable power.

本发明的有益效果为: The beneficial effects of the present invention are:

1、本发明的天然蚕丝蛋白面膜的制备方法加工流程短,不容易损伤蚕丝,从熟蚕吐丝开始制作,人为打破蚕吐丝的正常习性,改变蚕营茧需要的传统簇具条件,代替以平面状的吐丝网,使熟蚕在吐丝网上吐丝,直接形成平面状的蚕丝长丝片,而不是椭圆形的茧子,然后将蚕丝长丝片经过剪裁即得面膜形蚕丝,具有加工流程短、长丝不掉屑、不损伤蚕丝等优良特性。 1. The preparation method of the natural silk protein facial mask of the present invention has a short processing flow and is not easy to damage silk. It is produced from cooked silkworm silk spinning, artificially breaks the normal habit of silkworm silk spinning, changes the traditional cluster conditions required by silkworm cocoons, and replaces Using a planar silk-spinning net, the cooked silkworms spin silk on the silk-spinning net to directly form a planar silk filament sheet instead of an oval cocoon, and then cut the silk filament sheet to obtain a mask-shaped silk, which has The processing flow is short, the filament does not shed crumbs, and does not damage silk and other excellent characteristics.

2、传统的蚕丝精炼工序是将丝胶全部去除并排放到环境中,浪费宝贵的丝胶资源、污染环境,同时对蚕丝本身也有一定程度的损伤,本发明提供的纯桑蚕丝蛋白面膜以熟蚕吐出的平面丝作为原料,为了增加其亲水性、改善柔软度,采用了独特的水蒸法将丝蛋白渗出到丝表面,将珍贵的没有变性的丝胶蛋白保存下来,丝蛋白遇水后缓慢释放,从而起到美容的效果。 2. The traditional silk refining process removes all sericin and discharges it into the environment, which wastes valuable sericin resources and pollutes the environment. At the same time, it also damages the silk itself to a certain extent. The pure mulberry silk protein mask provided by the invention is made of cooked The flat silk extruded by silkworms is used as raw material. In order to increase its hydrophilicity and improve softness, a unique steaming method is used to exude silk protein onto the surface of the silk, so as to preserve the precious undenatured sericin. Slowly released after water, so as to play a cosmetic effect.

3、本发明的制备过程不需要碱液的处理,不需要漂白、中和等蚕丝的传统处理工艺,极大的保证了蚕丝蛋白的活性,不会造成丝蛋白流失,能保持蚕丝特有的长丝结构,得到的面膜透气性极佳,使用过程中不易变形,使用方便。 3. The preparation process of the present invention does not require the treatment of lye, nor does it require the traditional silk processing techniques such as bleaching and neutralization, which greatly guarantees the activity of silk protein, does not cause the loss of silk protein, and can maintain the unique long-lasting properties of silk. Silk structure, the resulting mask has excellent air permeability, is not easy to deform during use, and is easy to use.

具体实施方式 detailed description

下面结合实施例,对发明中的技术方案进行清楚、完整地描述,所描述的实施例仅仅是本发明的一部分,而不是全部的实施例。 The technical solution in the invention is clearly and completely described below in conjunction with the embodiments, and the described embodiments are only a part of the present invention, not all embodiments.

实施例1 Example 1

采用以下步骤完成可制得纯桑蚕丝蛋白面膜: Use the following steps to complete the pure mulberry silk protein mask:

(1)待桑蚕的熟蚕排便完后,将其放到吐丝网上,让熟蚕在吐丝网上均匀的吐5层丝; (1) After the cooked silkworms have finished defecating, put them on the silk spinning net, and let the cooked silkworms spit 5 layers of silk evenly on the silk spinning net;

(2)带熟蚕吐丝结束后,将蚕丝上的灰尘和杂物去除,并将蚕丝从吐丝网上剥离; (2) After the silk spinning with cooked silkworms is finished, remove the dust and sundries on the silk, and peel off the silk from the silk spinning net;

(3)将剥离得到的蚕丝按面膜的形状剪裁,得到面膜形蚕丝; (3) Cut the stripped silk according to the shape of the mask to obtain mask-shaped silk;

(4)将面膜形蚕丝放在能水蒸的装置中,利用水蒸汽将蚕丝蒸3分钟,将丝蛋白渗出到丝表面,水蒸汽的温度保持在100℃-105℃; (4) Put the mask-shaped silk in a device capable of steaming water, steam the silk for 3 minutes with water vapor, and exude silk protein to the surface of the silk, and keep the temperature of the water vapor at 100°C-105°C;

(5)将经过水蒸的面膜形蚕丝放到微波杀菌机中进行微波杀菌5分钟;输出微波功率40KW; (5) Put the steamed mask-shaped silk in a microwave sterilizer for microwave sterilization for 5 minutes; the output microwave power is 40KW;

(6)将杀菌后的面膜形蚕丝按照传统的面膜包装工艺进行包装即可得到纯桑蚕丝蛋白面膜。 (6) Pack the sterilized mask-shaped silk according to the traditional mask packaging process to obtain a pure mulberry silk protein mask.

所述的吐丝网的网眼宽度为1毫米,吐丝网的厚度为0.5-1毫米。 The mesh width of the spinning net is 1 mm, and the thickness of the spinning net is 0.5-1 mm.

实施例2 Example 2

采用以下步骤完成可制得纯桑蚕丝蛋白面膜: Use the following steps to complete the pure mulberry silk protein mask:

(1)待桑蚕的熟蚕排便完后,将其放到吐丝网上,让熟蚕在吐丝网上均匀的吐6层丝; (1) After the cooked silkworms have finished defecating, put them on the silk spinning net, and let the cooked silkworms spit 6 layers of silk evenly on the silk spinning net;

(2)带熟蚕吐丝结束后,将蚕丝上的灰尘和杂物去除,并将蚕丝从吐丝网上剥离; (2) After the silk spinning with cooked silkworms is finished, remove the dust and sundries on the silk, and peel off the silk from the silk spinning net;

(3)将剥离得到的蚕丝按面膜的形状剪裁,得到面膜形蚕丝; (3) Cut the stripped silk according to the shape of the mask to obtain mask-shaped silk;

(4)将面膜形蚕丝放在能水蒸的装置中,利用水蒸汽将蚕丝蒸4分钟,将丝蛋白渗出到丝表面,水蒸汽的温度保持在100℃-105℃; (4) Put the mask-shaped silk in a device capable of steaming water, steam the silk for 4 minutes with water vapor, and exude silk protein to the surface of the silk, and keep the temperature of the water vapor at 100°C-105°C;

(5)将经过水蒸的面膜形蚕丝放到微波杀菌机中进行微波杀菌5.5分钟; (5) Put the steamed mask-shaped silk in a microwave sterilizer for microwave sterilization for 5.5 minutes;

(6)将杀菌后的面膜形蚕丝按照传统的面膜包装工艺进行包装即可得到纯桑蚕丝蛋白面膜。 (6) Pack the sterilized mask-shaped silk according to the traditional mask packaging process to obtain a pure mulberry silk protein mask.

所述的吐丝网的网眼宽度为2毫米,吐丝网的厚度为0.5-1毫米。 The mesh width of the spinning net is 2 mm, and the thickness of the spinning net is 0.5-1 mm.

实施例3 Example 3

采用以下步骤完成可制得纯桑蚕丝蛋白面膜: Use the following steps to complete the pure mulberry silk protein mask:

(1)待桑蚕的熟蚕排便完后,将其放到吐丝网上,让熟蚕在吐丝网上均匀的吐7层丝; (1) After the cooked silkworms have finished defecation, put them on the silk spinning net, and let the cooked silkworms spit 7 layers of silk evenly on the silk spinning net;

(2)带熟蚕吐丝结束后,将蚕丝上的灰尘和杂物去除,并将蚕丝从吐丝网上剥离; (2) After the silk spinning with cooked silkworms is finished, remove the dust and sundries on the silk, and peel off the silk from the silk spinning net;

(3)将剥离得到的蚕丝按面膜的形状剪裁,得到面膜形蚕丝; (3) Cut the stripped silk according to the shape of the mask to obtain mask-shaped silk;

(4)将面膜形蚕丝放在能水蒸的装置中,利用水蒸汽将蚕丝蒸5分钟,将丝蛋白渗出到丝表面,水蒸汽的温度保持在100℃-105℃; (4) Put the mask-shaped silk in a device capable of steaming water, steam the silk for 5 minutes with water vapor, and exude silk protein to the surface of the silk, and keep the temperature of the water vapor at 100°C-105°C;

(5)将经过水蒸的面膜形蚕丝放到微波杀菌机中进行微波杀菌6分钟; (5) Put the steamed mask-shaped silk in a microwave sterilizer for microwave sterilization for 6 minutes;

(6)将杀菌后的面膜形蚕丝按照传统的面膜包装工艺进行包装即可得到纯桑蚕丝蛋白面膜。 (6) Pack the sterilized mask-shaped silk according to the traditional mask packaging process to obtain a pure mulberry silk protein mask.

所述的吐丝网的网眼宽度为3毫米,吐丝网的厚度为0.5-1毫米。 The mesh width of the spinning net is 3 mm, and the thickness of the spinning net is 0.5-1 mm.

上述实施例的产品提供给20例25-35岁的女性志愿者使用,原来她们脸上皮肤粗糙暗淡,有的还有斑点,后来使用本发明的纯桑蚕丝蛋白面膜,每天晚上睡前洗干净脸后将其贴脸上,每次贴15分钟以上, 20例实验者有19例一个月后皮肤开始变得红润光泽,斑点也变淡了。 The product of the above-mentioned embodiment was provided to 20 female volunteers aged 25-35. They had rough and dull skin on their faces, and some had spots. Later, they used the pure mulberry silk protein mask of the present invention and washed it off every night before going to bed. Put it on the face after the face, and stick it for more than 15 minutes each time. 19 of the 20 experimenters had their skin begin to become rosy and shiny after one month, and the spots also faded.

应用实施例 application example

1、广西张某,女,30岁,南宁人,孩子七个月,张某怀孕生小孩后,脸上皮肤变得粗糙暗淡且有点斑,她经朋友介绍使用了本发明的纯桑蚕丝蛋白面膜,每天晚上睡前洗干净脸后将纯桑蚕丝蛋白面膜贴脸上,每次贴15-20分钟,张某使用一个月后皮肤变得红润光泽,斑点也变淡了,两个月后几乎看不出有斑点。 1. Zhang from Guangxi, female, 30 years old, from Nanning, the child is seven months old. After Zhang became pregnant and gave birth to a child, the skin on her face became rough and dull with spots. She was introduced by a friend to use the pure mulberry silk protein of the present invention. Mask, after washing the face before going to bed every night, put the pure mulberry silk protein mask on the face, each time for 15-20 minutes, Zhang's skin became rosy and shiny after using it for a month, and the spots also faded. After two months There are hardly any spots.

2、广西陈某某,女,33岁,南宁人,陈某某原来摆夜宵摊,经常熬夜,也忽略了护理脸上皮肤,脸上皮肤变得暗黄,陈某某改行了,其也使用了很多护肤品,但是皮肤还是没有得到改善,她经朋友介绍使用了本发明的纯桑蚕丝蛋白面膜,每天晚上睡前洗干净脸后将纯桑蚕丝蛋白面膜贴脸上,每次贴15-25分钟,陈某某使用一个月后皮肤变得白皙光泽。 2. Chen Moumou, female, 33 years old, from Nanning, Guangxi. Chen Moumou used to set up a supper stall, often stayed up late, and neglected to take care of the skin on his face. The skin on his face became dark yellow. She has used a lot of skin care products, but her skin has not been improved. She was introduced by a friend to use the pure mulberry silk protein mask of the present invention, and put the pure mulberry silk protein mask on her face every night after washing her face before going to bed. -25 minutes, Chen Moumou's skin became white and shiny after using it for a month.

Claims (2)

1.一种天然蚕丝蛋白面膜的制备方法,其特征在于:采用以下步骤: 1. a preparation method of natural silk protein facial mask, is characterized in that: adopt following steps: (1)待桑蚕的熟蚕排便完后,将其放到吐丝网上,让熟蚕在吐丝网上均匀的吐5-8层丝; (1) After the cooked silkworms have finished defecating, put them on the spinning net, and let the cooked silkworms spit 5-8 layers of silk evenly on the spinning net; (2)带熟蚕吐丝结束后,将蚕丝上的灰尘和杂物去除,并将蚕丝从吐丝网上剥离; (2) After the silk spinning with cooked silkworms is finished, remove the dust and sundries on the silk, and peel off the silk from the silk spinning net; (3)将剥离得到的蚕丝按面膜的形状剪裁,得到面膜形蚕丝; (3) Cut the stripped silk according to the shape of the mask to obtain mask-shaped silk; (4)将面膜形蚕丝放在能水蒸的装置中,利用水蒸汽将蚕丝蒸3-5分钟,将丝蛋白渗出到丝表面,水蒸汽的温度保持在100℃-105℃之间; (4) Put the mask-shaped silk in a device capable of steaming water, steam the silk for 3-5 minutes with water vapor, and exude silk protein to the surface of the silk, and keep the temperature of the water vapor between 100°C and 105°C; (5)将经过水蒸的面膜形蚕丝放到微波杀菌机中进行微波杀菌5-6分钟; (5) Put the steamed mask-shaped silk in a microwave sterilizer for microwave sterilization for 5-6 minutes; (6)将杀菌后的面膜形蚕丝按照传统的面膜包装工艺进行包装即可得到纯桑蚕丝蛋白面膜。 (6) Pack the sterilized mask-shaped silk according to the traditional mask packaging process to obtain a pure mulberry silk protein mask. 2.根据权利要求1所述的天然蚕丝蛋白面膜的制备方法,其特征在于:所述的吐丝网的网眼宽度为1-3毫米,吐丝网的厚度为0.5-1毫米。 2. the preparation method of natural silk protein facial mask according to claim 1 is characterized in that: the mesh width of described spinning net is 1-3 millimeter, and the thickness of spinning net is 0.5-1 millimeter.
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CN111939085A (en) * 2020-08-19 2020-11-17 浙江大学 Preparation method of silk mask and product
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CN112941728A (en) * 2021-03-11 2021-06-11 汤贝特 Processing technology of natural fibroin mask
CN114657697A (en) * 2022-03-23 2022-06-24 盐城工业职业技术学院 A kind of preparation method of whole sericin cocoon flat silk composite facial mask material
CN117089982A (en) * 2023-01-12 2023-11-21 西南大学 Production technology and application of silk non-woven fabric

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