CN105919910A - Preparation method of natural fibroin mask - Google Patents

Preparation method of natural fibroin mask Download PDF

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Publication number
CN105919910A
CN105919910A CN201610273950.0A CN201610273950A CN105919910A CN 105919910 A CN105919910 A CN 105919910A CN 201610273950 A CN201610273950 A CN 201610273950A CN 105919910 A CN105919910 A CN 105919910A
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silk
silkworm
mask
silks
facial film
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CN201610273950.0A
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CN105919910B (en
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韦有任
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Shanghai Tieman Biotechnology Co., Ltd.
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韦有任
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES
    • A61K8/00Cosmetics or similar toilet preparations
    • A61K8/18Cosmetics or similar toilet preparations characterised by the composition
    • A61K8/96Cosmetics or similar toilet preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/98Cosmetics or similar toilet preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/987Cosmetics or similar toilet preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES
    • A61K8/00Cosmetics or similar toilet preparations
    • A61K8/18Cosmetics or similar toilet preparations characterised by the composition
    • A61K8/30Cosmetics or similar toilet preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILET PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL, OR TOILET PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/805Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95

Abstract

The invention relates to the field of cosmetics and concretely relates to a preparation method of a natural fibroin mask. The method comprises 1, after matured silkworms for spitting silk defecation, putting the matured silkworms on a silk spitting net so that the matured silkworms uniformly spit 5-8 layers of silks on the silk spitting net, 2, after the matured silkworms finish silk spitting, removing dust and impurities on the silks and separating the silks from the silk spitting net, 3, cutting the separated silks according to a mask shape to obtain mask-shaped silks, 4, arranging the mask-shaped silks on the position for water steaming and steaming the silks through vapor at a temperature of 100-105 DEG C for 3-5min, 5, putting the steamed mask-shaped silks into a microwave sterilization machine and carrying out microwave sterilization for 5-6min, and 6, packaging the mask-shaped silks subjected to sterilization through a traditional mask packaging technology to obtain a pure fibroin mask. The preparation method has short mask processing processes, does not damage silks and has good skin care effects.

Description

The preparation method of native fibroin facial film
Technical field
The present invention relates to cosmetic field, the preparation method of a kind of native fibroin facial film.
Background technology
Silkworm silk is a kind of natural protein fibre, it it is unique filament fiber in all natural fibers cotton, hair, silk, fiber crops, the silk length that a first-class cocoon energy reel silk from cocoons obtains can reach a km, therefore the silkworm silk of filament structure is commonly used to make high-grade clothing and silk, and the leftover bits and pieces that silkworm silk produces in silk reeling process is cut into chopped fiber and carries out silk spinning processing again, make spun silk fabric (short silk fiber).The cross section of natural silk is triangle; it is to be relied on sericin to bind by two monofilament to form; its protein composition is fibroin and sericin two kinds; fibroin accounts for about 70% center being distributed in silkworm silk; sericin accounts for about 30%; sericin is the protein constituting silk fiber outer tissue, and sericin plays protection and bonding effect to the fibroin wrapped up therein.Fibroin albumen includes 18 kinds of aminoacid and the various trace elements such as lysine, histidine, cystine, aspartic acid, the water content of keratodermatitis can be increased, promote collagen protein synthesis, strengthen tension force and the elasticity of skin, stronger affinity is had, it is easy to absorbed by human skin with human body skin.Sericin is a kind of globular preteins, it is made up of 18 kinds of aminoacid such as serine, aspartic acid and glutamic acid, sericin has the characteristic of suppression tyrosinase activity, therefore melanic formation in skin can be stoped, skin whitening, preventing the injury to skin of the daylight middle-ultraviolet lamp, therefore sericin is the natural cosmetics dispensing of a kind of preciousness.
Along with living standard improves, facial film has become the indispensable skin care products of modern from original luxury consumer goods.And silkworm silk is as a kind of natural animal protein, with human body skin, there is the biggest similarity, relatively for other albumen, be also more easy to be absorbed by the body, play the effect of whitening, moisturizing.It addition, the tyrosine that in silkworm silk, content is more and phenylalanine etc. have good Absorption to ultraviolet, there is sun-proof skin care effect.Therefore, silkworm silk also becomes the face mask substrate material that facial film circle is very popular.
Presently commercially available silk mask mainly uses the manufacturing process of non-woven fabrics, and the production technology of non-woven fabrics is complex: mainly use silk spinning raw material (i.e. leftover bits and pieces in filature, waste silk, bourette etc.), spun lacing (or acupuncture) production line is entered after remove impurity, cut-out, degumming (or solid glue) refine, combing, addition antistatic additive, regulation and control humiture.These silk spinning raw material major parts are through physics repeatedly, chemical action (high temperature, high pressure, chemical assistant), although sericin is still withed a hook at the end, but albumen is through degeneration renaturation process repeatedly, and the activity of major part sericin is lost already, it is impossible to reach preferable cosmetic result.In Bombyx bombycis forms the traditional handicraft of face mask substrate material, Bombyx bombycis all has to pass through high temperature steaming (decatize), during this, sericin can run off and degeneration in a large number, cause significant wastage, its skin effect is the most undesirable, and the silk mask formed is due to sericin loss, loosely organized, during use yielding, use inconvenience.It addition, the silk non-woven fabric that current spun lacing (or acupuncture) line is produced is the most thick and heavy, causing silk mask and the right difference of skin paste, using effect is undesirable, loses its skin-friendly.Therefore, the silk mask that a kind of skin effect is good, the always direction of row insider research are the most simply obtained.Open source literature also reports some silk masks, such as:
1, Chinese patent: a kind of Bombyx bombycis produces method and the silk mask of silk mask base fabric, application number: 201510040948.4, the applying date: 2015.01.27, applicant: Southwest University, address: 400715 sky, the It In Beibei, Chongqing means of livelihood 2, inventor: Xia Qingyou, Xi Xinghang, poplar are worn, summary: a kind of Bombyx bombycis of this disclosure of the invention produces the method for silk mask base fabric, completes in accordance with the following steps: (1), wash cocoon: Bombyx bombycis clear water is washed away dust and foreign material;(2), moistening: the Bombyx bombycis after cleaning is soaked in water and makes its abundant moistening;(3), caustic dip: the Bombyx bombycis after moistening is uniformly put into steaming kier, be able to the aqueous alkali spray Bombyx bombycis of moistening Bombyx bombycis so that Bombyx bombycis is the most wetted;(4), decatize: make sericin complete swelling with steamed Bombyx bombycis;(5), clean: with the steamed Bombyx bombycis of clean water;(6), stripping cocoon: by Pupa bombycis peel-away removal;(7), the Bombyx bombycis of peel-away removal Pupa bombycis is made arc silkworm silk nethike embrane;(8), silkworm silk nethike embrane is passed through bleaching, is finally punched into type obtains silk mask base fabric with glacial acetic acid solution neutralization, drying.This invention can be maximally maintained the activity of sericin.Technological process is simple, can make full use of the nutrient substance of silkworm silk, be the whitening of pure natural, moisturizing, crease-resistant, uv-resistant product.
2, Chinese patent: the method making high activity silk mask with Bombyx bombycis, application number: 201510181125.3, the applying date: 2015.04.17, applicant: Chongqing Hangfan Silk Technology Development Co., Ltd., address: 400030 Feng Tian Road, Shapingba District, Chongqing City 18, inventor: Xi Xinghang, Xi Lan, Zhao Ping, poplar are worn, summary: a kind of Bombyx bombycis of this disclosure of the invention makes the method for high activity silk mask, it is characterised in that: complete in accordance with the following steps: (1) washes cocoon: the dust washing away on Bombyx bombycis with clear water and foreign material;(2) molten cocoon: the Bombyx bombycis after cleaning is put in the protein enzyme solution that concentration is 0.1%~5% and soaked, and makes sericin the most swelling, and cocoon layer is opened;(3) stripping cocoon: tear cocoon layer, remove Pupa bombycis;(4) film forming: be enclosed within arch mould by the Bombyx bombycis removing Pupa bombycis, makes silkworm silk nethike embrane;(5) it is dried: naturally dry or oven drying at low temperature (6) punch forming.This invented technology flow process is short, makes simple, and full process stream Cheng Jun processes at low temperatures, it is not necessary to dipping by lye, it is not necessary to high temperature steaming so that protein active retains to greatest extent so that sericin invariance does not runs off, and facial film degree of compacting is good, easy to use.
It has been investigated that, the document of report disclosed above, is all to prepare as raw material with Bombyx bombycis when preparing silk mask, and work flow is long, easily damages silkworm silk, it is impossible to the native protein needed for holding.
Summary of the invention
It is an object of the invention to provide a kind of work flow short, it is not easy to damage silkworm silk, and the good pure mulberry silk protein facial mask of skin effect and preparation method thereof.
To achieve these goals, the present invention adopts the technical scheme that:
A kind of preparation method of native fibroin facial film, it uses following steps:
(1) after the matured silkworm defecation of Bombyxmori Linnaeus is complete, put it to weave silk online, allow matured silkworm tell 5-8 layer silk uniformly on the net weaving silk;Matured silkworm is put into before weaving silk on the net, it is necessary to treat that its defecation is complete, just can be put into and weave silk on the net, allow it weave silk, matured silkworm defecation before weaving silk can be avoided to pollute net of weaving silk, thus pollute silkworm silk;Silkworm, to five latter stages in age, the most gradually embodies aging feature: the feces discharged before this from hard to soft, is become leaf green by blackish green;Loss of appetite, food Mulberry amount declines;Anterior digestive tube is hollow, the transparent shape of chest;Stopping eating the most completely, body drives shortening, and abdominal part also tends to transparent, and silkworm body cephalothorax is held high, and mouth is weaved silk in detail, and left and right swings up and down searching cocooning place, and such silkworm is known as matured silkworm.
(2), after band matured silkworm weaves silk end, the dust on silkworm silk and foreign material are removed, and by silkworm silk from online stripping of weaving silk;
(3) silkworm silk stripping obtained is cut out by the shape of facial film, obtains facial film shape silkworm silk;
(4) being placed on by facial film shape silkworm silk in the device that energy water steams, utilize water vapour to be steamed 3-5 minute by silkworm silk, fibroin is exuded to a surface, the temperature of water vapour is maintained between 100 DEG C-105 DEG C;
(5) the facial film shape silkworm silk steamed through water is put in microwave sterilization machine carries out microwave disinfection 5-6 minute;Need facial film shape silkworm silk to carry out having detected whether that fibroin oozes out before carrying out microwave disinfection, have what fibroin oozed out can carry out microwave disinfection;Ensure that the time stored reaches more than 3-5 month.
(6) carry out packing according to traditional facial film technology of the package by the facial film shape silkworm silk after sterilization and i.e. can get pure mulberry silk protein facial mask.
The mesh width of described net of weaving silk is 1-3 millimeter, and the thickness of net of weaving silk is 0.5-1 millimeter.
Microwave sterilization machine can be bought in Guangzhou Fu Tao microwave equipment company limited, address: Ta Kwu Ling street, the Xie Jia village, Taihe county town, Baiyun District, Guangzhou City 13, network address: http://www.gzfutao.com;The output microwave power of microwave sterilization machine: 40KW, power adjustable.
The invention have the benefit that
1, the preparation method work flow of the native fibroin facial film of the present invention is short, it is not easy to damage silkworm silk, weave silk from matured silkworm and start from, artificially break the normal habit that silkworms spin silk, change the tradition bunch tool condition that silkworm cocooning needs, replace with plane net of weaving silk, matured silkworm is made to weave silk on the net weaving silk, directly form plane silkworm silk bunches of threads, rather than the callus of ellipse, then silkworm silk bunches of threads is i.e. obtained facial film shape silkworm silk through cutting out, have that work flow is short, long filament does not fall bits, do not damages the good characteristics such as silkworm silk.
2, traditional silkworm silk refining procedure is all to be removed by sericin and be discharged in environment, the sericin resource of waste preciousness, pollution environment, silkworm silk itself also there is a certain degree of damage simultaneously, the plane silk that the pure mulberry silk protein facial mask that the present invention provides spues using matured silkworm is as raw material, in order to increase its hydrophilic, improve pliability, fibroin is exuded to a surface by the water steaming method that have employed uniqueness, the precious sericin not having degeneration is preserved, fibroin slowly discharges after meeting water, thus plays the effect of beauty treatment.
3, the preparation process of the present invention need not the process of alkali liquor, need not the conventional processes of the silkworm silks such as bleaching, neutralization, ensure that the activity of fibroin greatly, do not result in fibroin to run off, the distinctive filament structure of silkworm silk can be kept, the facial film breathability obtained is splendid, is unlikely to deform during use, easy to use.
Detailed description of the invention
Below in conjunction with embodiment, being clearly and completely described the technical scheme in invention, described embodiment is only the part of the present invention rather than whole embodiments.
Embodiment 1
Following steps are used to complete to prepare pure mulberry silk protein facial mask:
(1) after the matured silkworm defecation of Bombyxmori Linnaeus is complete, put it to weave silk online, allow matured silkworm tell 5 layers of silk uniformly on the net weaving silk;
(2), after band matured silkworm weaves silk end, the dust on silkworm silk and foreign material are removed, and by silkworm silk from online stripping of weaving silk;
(3) silkworm silk stripping obtained is cut out by the shape of facial film, obtains facial film shape silkworm silk;
(4) being placed on by facial film shape silkworm silk in the device that energy water steams, utilize water vapour to be steamed 3 minutes by silkworm silk, fibroin is exuded to a surface, the temperature of water vapour is maintained at 100 DEG C-105 DEG C;
(5) the facial film shape silkworm silk steamed through water is put in microwave sterilization machine carries out microwave disinfection 5 minutes;Output microwave power 40KW;
(6) carry out packing according to traditional facial film technology of the package by the facial film shape silkworm silk after sterilization and i.e. can get pure mulberry silk protein facial mask.
The mesh width of described net of weaving silk is 1 millimeter, and the thickness of net of weaving silk is 0.5-1 millimeter.
Embodiment 2
Following steps are used to complete to prepare pure mulberry silk protein facial mask:
(1) after the matured silkworm defecation of Bombyxmori Linnaeus is complete, put it to weave silk online, allow matured silkworm tell 6 layers of silk uniformly on the net weaving silk;
(2), after band matured silkworm weaves silk end, the dust on silkworm silk and foreign material are removed, and by silkworm silk from online stripping of weaving silk;
(3) silkworm silk stripping obtained is cut out by the shape of facial film, obtains facial film shape silkworm silk;
(4) being placed on by facial film shape silkworm silk in the device that energy water steams, utilize water vapour to be steamed 4 minutes by silkworm silk, fibroin is exuded to a surface, the temperature of water vapour is maintained at 100 DEG C-105 DEG C;
(5) the facial film shape silkworm silk steamed through water is put in microwave sterilization machine carries out microwave disinfection 5.5 minutes;
(6) carry out packing according to traditional facial film technology of the package by the facial film shape silkworm silk after sterilization and i.e. can get pure mulberry silk protein facial mask.
The mesh width of described net of weaving silk is 2 millimeters, and the thickness of net of weaving silk is 0.5-1 millimeter.
Embodiment 3
Following steps are used to complete to prepare pure mulberry silk protein facial mask:
(1) after the matured silkworm defecation of Bombyxmori Linnaeus is complete, put it to weave silk online, allow matured silkworm tell 7 layers of silk uniformly on the net weaving silk;
(2), after band matured silkworm weaves silk end, the dust on silkworm silk and foreign material are removed, and by silkworm silk from online stripping of weaving silk;
(3) silkworm silk stripping obtained is cut out by the shape of facial film, obtains facial film shape silkworm silk;
(4) being placed on by facial film shape silkworm silk in the device that energy water steams, utilize water vapour to be steamed 5 minutes by silkworm silk, fibroin is exuded to a surface, the temperature of water vapour is maintained at 100 DEG C-105 DEG C;
(5) the facial film shape silkworm silk steamed through water is put in microwave sterilization machine carries out microwave disinfection 6 minutes;
(6) carry out packing according to traditional facial film technology of the package by the facial film shape silkworm silk after sterilization and i.e. can get pure mulberry silk protein facial mask.
The mesh width of described net of weaving silk is 3 millimeters, and the thickness of net of weaving silk is 0.5-1 millimeter.
The product of above-described embodiment be supplied to 20 example 25-35 year female volunteers use, originally they on the face pachylosis dim, have goes back spottiness, used the pure mulberry silk protein facial mask of the present invention later, sleep on its architrave every night after front wash clean face, every time patch more than 15 minutes, 20 example experimenters have 19 example after one month skin start to become ruddy gloss, speckle is the most thin out.
Application Example
1, Guangxi Zhang, female, 30 years old, people from Nanning, child seven months, after Zhang's pregnancy is given birth to a child, skin becomes coarse dimness and has stigma on the face, she introduces the pure mulberry silk protein facial mask employing the present invention through friend, sleeping on pure mulberry silk protein facial mask architrave every night after front wash clean face, patch 15-20 minute every time, after Zhang uses one month, skin becomes ruddy gloss, speckle is the most thin out, does not the most almost see spottiness.
2, Guangxi Chen, female, 33 years old, people from Nanning, Chen pendulum food stand originally, often stay up late, also have ignored and nurse skin on the face, skin becomes dark yellow on the face, and Chen changes one's profession, it also using a lot of skin care item, but skin is again without being improved, she introduces through friend and employs the pure mulberry silk protein facial mask of the present invention, sleeps on pure mulberry silk protein facial mask architrave every night after front wash clean face, patch 15-25 minute every time, after Chen uses one month, skin becomes pale gloss.

Claims (2)

1. the preparation method of a native fibroin facial film, it is characterised in that: employing following steps:
(1) after the matured silkworm defecation of Bombyxmori Linnaeus is complete, put it to weave silk online, allow matured silkworm tell 5-8 layer silk uniformly on the net weaving silk;
(2), after band matured silkworm weaves silk end, the dust on silkworm silk and foreign material are removed, and by silkworm silk from online stripping of weaving silk;
(3) silkworm silk stripping obtained is cut out by the shape of facial film, obtains facial film shape silkworm silk;
(4) being placed on by facial film shape silkworm silk in the device that energy water steams, utilize water vapour to be steamed 3-5 minute by silkworm silk, fibroin is exuded to a surface, the temperature of water vapour is maintained between 100 DEG C-105 DEG C;
(5) the facial film shape silkworm silk steamed through water is put in microwave sterilization machine carries out microwave disinfection 5-6 minute;
(6) carry out packing according to traditional facial film technology of the package by the facial film shape silkworm silk after sterilization and i.e. can get pure mulberry silk protein facial mask.
The preparation method of native fibroin facial film the most according to claim 1, it is characterised in that: the mesh width of described net of weaving silk is 1-3 millimeter, and the thickness of net of weaving silk is 0.5-1 millimeter.
CN201610273950.0A 2016-04-28 2016-04-28 The preparation method of native fibroin facial mask Active CN105919910B (en)

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Cited By (6)

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CN106835507A (en) * 2017-03-29 2017-06-13 盐城工业职业技术学院 A kind of castor silkworm flat board wire production method and its a kind of facial mask
CN107012589A (en) * 2017-05-12 2017-08-04 广州雅南无纺布制品有限公司 A kind of silkworm carbon mask substrate and preparation method thereof
CN109661486A (en) * 2016-05-20 2019-04-19 塞里西娜公司 Nonwoven natural silk cloth and its manufacturing method
CN111166679A (en) * 2018-11-12 2020-05-19 焦伊斯恺化妆品株式会社 Method for manufacturing beauty mask using sheet containing unrefined silk
CN111939085A (en) * 2020-08-19 2020-11-17 浙江大学 Preparation method of silk mask and product
CN112941728A (en) * 2021-03-11 2021-06-11 汤贝特 Processing technology of natural fibroin mask

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CN104762756A (en) * 2015-04-24 2015-07-08 钱程 Natural silk facial mask base cloth and preparation method thereof
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Publication number Priority date Publication date Assignee Title
CN109661486A (en) * 2016-05-20 2019-04-19 塞里西娜公司 Nonwoven natural silk cloth and its manufacturing method
CN106835507A (en) * 2017-03-29 2017-06-13 盐城工业职业技术学院 A kind of castor silkworm flat board wire production method and its a kind of facial mask
CN106835507B (en) * 2017-03-29 2019-07-02 盐城工业职业技术学院 A kind of castor silkworm plate wire production method and its a kind of facial mask
CN107012589A (en) * 2017-05-12 2017-08-04 广州雅南无纺布制品有限公司 A kind of silkworm carbon mask substrate and preparation method thereof
CN111166679A (en) * 2018-11-12 2020-05-19 焦伊斯恺化妆品株式会社 Method for manufacturing beauty mask using sheet containing unrefined silk
CN111939085A (en) * 2020-08-19 2020-11-17 浙江大学 Preparation method of silk mask and product
CN111939085B (en) * 2020-08-19 2021-11-02 浙江大学 Preparation method of silk mask and product
CN112941728A (en) * 2021-03-11 2021-06-11 汤贝特 Processing technology of natural fibroin mask

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