CN105919910B - The preparation method of native fibroin facial mask - Google Patents
The preparation method of native fibroin facial mask Download PDFInfo
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Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Dermatology (AREA)
- Zoology (AREA)
- Cosmetics (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The present invention relates to cosmetic field, the preparation method of specifically a kind of native fibroin facial mask, processing step are as follows: (1) after the matured silkworm defecation of silkworm is complete, put it to spinning on the net, matured silkworm is allowed uniformly to spit 5-8 layers of silk on the net in spinning；(2) after the spinning of band matured silkworm, by silk dust and sundries remove, and by silk from the online removing of spinning；(3) silk that removing obtains is cut out by the shape of facial mask, obtains facial mask shape silk；(4) facial mask shape silk is placed in the device that energy water steams, is steamed silk 3-5 minutes using water vapour, the temperature of water vapour is maintained between 100 DEG C -105 DEG C；(5) the facial mask shape silk steamed by water is put into microwave sterilization machine and is carried out microwave disinfection 5-6 minutes；(6) the facial mask shape silk after sterilization is carried out packaging according to traditional facial mask technology of the package can be obtained pure mulberry silk protein facial mask.Facial mask processing flow of the invention is short, it is not easy to damage silk, and skin effect is good.
Description
Technical field
The present invention relates to cosmetic field, the preparation method of specifically a kind of native fibroin facial mask.
Background technique
Silk is a kind of natural protein fibre, is all natural fiber cottons, hair, silk, unique filament fiber in fiber crops,
The silk length that a first-class cocoon energy reel silk from cocoons obtains can reach a km, therefore the silk of filament structure is commonly used to the high-grade clothes of production
Dress and silk goods, and the leftover bits and pieces that silk generates in silk reeling process is cut into staple fiber and carries out silk spinning processing again, makes thin,tough silk
Textile fabric (short silk fiber).The section of natural silk is triangle, is to be binded by two monofilament by silk gum, albumen
Matter composition is fibroin and two kinds of silk gum, and fibroin accounts for about 70% or so the center for being distributed in silk, and silk gum accounts for 30% or so, and silk gum is structure
At the protein of silk fiber outer tissue, silk gum plays a part of protection and bonding to the fibroin of package inside it.Fibroin
Albumen includes 18 kinds of amino acid such as lysine, histidine, cystine, asparatate and various trace elements, can increase skin
The water content of cuticula promotes collagen synthesis, enhances the tension and elasticity of skin, have with human skin stronger affine
Power, it is easy to be absorbed by human skin.Silk gum is a kind of globular preteins, by 18 kinds of serine, asparatate and glutamic acid etc.
Amino acid composition, sericin has the characteristic inhibited tyrosinase activity, therefore can prevent the formation of melanin in skin, beauty
Pale skin prevents injury of the daylight middle-ultraviolet lamp to skin, therefore sericin is a kind of natural cosmetics ingredient of preciousness.
With the improvement of living standards, facial mask has become the indispensable skin care products of modern from original luxury consumer goods.And silkworm
Silk is used as a kind of natural animal protein, has very big similitude with human skin, for relatively other albumen, be also easier to by
Absorption of human body plays the role of whitening, moisturizing.In addition, the more tyrosine of content and phenylalanine etc. are to ultraviolet light in silk
With good absorption effect, has effects that sun-proof skin care.Therefore, silk also becomes the very popular face mask substrate material of facial mask circle.
Presently commercially available silk mask mainly uses the manufacturing process of non-woven fabrics, and the production technology of non-woven fabrics is more
It is complicated: mainly to use silk spinning raw material (leftover bits and pieces, waste silk, bourette i.e. in filature etc.), by removal of impurities, cutting, degumming are (or solid
Glue) it refines, comb, entering spun lacing (or needle thorn) production line after addition antistatic agent, regulation temperature and humidity.The big portion of these silk spinning raw materials
Divide and have been subjected to multiple physics, chemical action (high temperature, high pressure, chemical assistant), although silk gum is still withed a hook at the end, albumen is through excessive
The activity of secondary denaturation renaturation process, most of sericin is lost already, is unable to reach ideal cosmetic result.In silk cocoon shape
At in the traditional handicraft of face mask substrate material, silk cocoon all has to pass through thermophilic digestion (decatize), during this silk gum can be largely lost and
Denaturation, cause significant wastage, skin effect is also undesirable, and formed silk mask due to silk gum be lost, it is loosely organized, make
It is inconvenient for use with easily-deformable in the process.In addition, the silk non-woven fabric that current spun lacing (or needle thorn) line is produced is generally thicker
Weight, leads to silk mask and the right difference of skin paste, using effect is undesirable, loses its skin-friendly.Therefore, how simply to obtain
A kind of silk mask that skin effect is good is always the direction of row insider research.Open source literature also reports some silks
Facial mask, such as:
1, Chinese patent: a kind of method and silk mask with silk cocoon production silk mask base fabric, application number:
201510040948.4, the applying date: 2015.01.27, applicant: Southwest University, address: 400715 It In Beibei, Chongqings are born
Road 2, inventor: Xia Qingyou, Xi Xinghang, poplar are worn, abstract: the disclosure of the invention is a kind of to produce silk mask base fabric with silk cocoon
Method, in accordance with the following steps complete: (1), wash cocoon: silk cocoon washed away into dust and sundries with clear water；(2), it soaks: after cleaning
Silk cocoon be soaked in water and soak it sufficiently；(3), caustic dip: being uniformly put into steaming kier for the silk cocoon after wetting, be able to soak silk cocoon
Buck spray silk cocoon so that silk cocoon is wetted again；(4), decatize: make silk gum complete swelling with steamed silk cocoon；(5),
Cleaning: steamed silk cocoon is cleaned with clear water；(6), peeling: by silkworm chrysalis peel-away removal；(7), by the silk cocoon system of peel-away removal silkworm chrysalis
Camber silk nethike embrane；(8), silk nethike embrane is neutralized by bleaching, with glacial acetic acid solution, drying is finally punched into type and obtains silkworm
Silk mask substrate.The invention can be maximally maintained the activity of sericin.Process flow is simple, can make full use of silk
Nutriment is pure natural whitening, moisturizing, crease-resistant, anti-UV product.
2, Chinese patent: the method for making high activity silk mask with silk cocoon, application number: 201510181125.3, application
Day: 2015.04.17, applicant: Chongqing Hangfan Silk Technology Development Co., Ltd., address: 400030 Shapingba District, Chongqing Cities
The main road Feng Tian 18, inventor: Xi Xinghang, Xi Lan, Zhao Ping, poplar are worn, abstract: the disclosure of the invention is a kind of made of silk cocoon it is high living
Property silk mask method, it is characterised in that: complete in accordance with the following steps: (1) washing cocoon: with clear water wash away dust on silk cocoon and
Sundries；(2) molten cocoon: the silk cocoon after cleaning is put into the protein enzyme solution that concentration is 0.1%~5% and is impregnated, keeps silk gum abundant
Swelling, cocoon layer are opened；(3) peeling: tearing cocoon layer, removes silkworm chrysalis；(4) it forms a film: the silk cocoon for removing silkworm chrysalis is covered in arch mold
On, silk nethike embrane is made；(5) dry: naturally dry or low temperature drying (6) punch forming.The invented technology process is short, production
Simply, full process stream Cheng Jun is handled at low temperature, does not need dipping by lye, does not need thermophilic digestion, so that protein active is maximum
The reservation of limit, so that silk gum invariance is not lost, facial mask is compact to spend, easy to use.
It has been investigated that the document of report disclosed above, is all that silk cocoon is used to prepare as raw material when preparing silk mask,
Processing flow is long, is easy to damage silk, is not able to maintain required native protein.
Summary of the invention
The object of the present invention is to provide a kind of processing flow is short, it is not easy to damage silk, and the pure silkworm that skin effect is good
Silk-fibroin facial mask and preparation method thereof.
To achieve the goals above, the technical solution adopted by the present invention is that:
A kind of preparation method of native fibroin facial mask, uses following steps:
(1) it after the matured silkworm defecation of silkworm is complete, puts it to spinning on the net, matured silkworm is allowed uniformly to spit 5-8 on the net in spinning
Layer silk；Before matured silkworm is put into spinning on the net, it is necessary to it is complete to its defecation, it can just be put into spinning on the net, it is allowed to spin, can avoid matured silkworm
The defecation pollution spinning net before spinning, to pollute silk；Silkworm just gradually embodies aging spy to five latter stages in age
Sign: the excrement being discharged before this becomes leaf green from hard to soft, by blackish green；Appetite stimulator, food mulberry amount decline；Front digest tube is empty
Void, chest are transparent；Then to stop eating completely, body, which drives, to be shortened, and abdomen also tends to transparent, and silkworm body cephalothorax is held high, mouth spinning thread,
Left and right, which is swung up and down, finds cocooning place, and such silkworm is known as matured silkworm.
(2) after the spinning of band matured silkworm, by silk dust and sundries remove, and by silk from the online removing of spinning；
(3) silk that removing obtains is cut out by the shape of facial mask, obtains facial mask shape silk；
(4) facial mask shape silk is placed in the device that energy water steams, is steamed silk 3-5 minutes using water vapour, by silk-fibroin
It is exuded to silk table face, the temperature of water vapour is maintained between 100 DEG C -105 DEG C；
(5) the facial mask shape silk steamed by water is put into microwave sterilization machine and is carried out microwave disinfection 5-6 minutes；It is micro- in progress
Facial mask shape silk is needed to carry out having detected whether silk-fibroin exudation before wave sterilization, have silk-fibroin exudation can carry out microwave disinfection；
Guarantee that the time of storage reaches 3-5 months or more
(6) the facial mask shape silk after sterilization is carried out packaging according to traditional facial mask technology of the package can be obtained pure mulberry silk
Protein facial mask.
The mesh width of the described spinning net is 1-3 millimeters, the net that spins with a thickness of 0.5-1 millimeters.
Microwave sterilization machine can be bought in Guangzhou Fu Tao microwave equipment Co., Ltd, address: be thanked in Baiyun District, Guangzhou City Taihe county town
Family village Ta Kwu Ling street 13, network address: http://www.gzfutao.com；The output microwave power of microwave sterilization machine: 40KW, function
Rate is adjustable.
The invention has the benefit that
1, the preparation method processing flow of native fibroin facial mask of the invention is short, it is not easy to silk is damaged, from matured silkworm
Spinning starts from, and artificially breaks the normal habit that silkworms spin silk, changes traditional cluster that silkworm cocooning needs and has condition, instead of with plane
The spinning net of shape makes matured silkworm in the online spinning of spinning, directly forms planar silk bunches of threads, rather than the cocoon of ellipse
Son, then by silk bunches of threads by cutting out up to facial mask shape silk, with processing flow, short, long filament does not fall bits, does not damage silkworm
The good characteristics such as silk.
2, traditional silk refining procedure is all to remove silk gum and be discharged into environment, wastes valuable silk gum money
Source, pollution environment, while also having a degree of damage to silk itself, pure mulberry silk protein facial mask provided by the invention is with ripe
The plane silk that curley waste goes out is as raw material, in order to increase its hydrophily, improve pliability, uses unique water and steams method for silk-fibroin
It is exuded to silk table face, the precious sericin not being denaturalized is preserved, silk-fibroin meets slow release after water, to play
The effect of beauty.
3, preparation process of the invention does not need the processing of lye, does not need the conventional process work of the silks such as bleaching, neutralization
Skill, greatly ensure that the activity of fibroin, not will cause silk-fibroin loss, is able to maintain the distinctive filament structure of silk, obtains
The facial mask gas permeability arrived is splendid, is unlikely to deform in use process, easy to use.
Specific embodiment
Below with reference to embodiment, the technical solution in invention is clearly and completely described, described embodiment is only
It is only a part of the invention, instead of all the embodiments.
Embodiment 1
Pure mulberry silk protein facial mask can be made using following steps completion:
(1) it after the matured silkworm defecation of silkworm is complete, puts it to spinning on the net, matured silkworm is allowed uniformly to spit 5 layers on the net in spinning
Silk；
(2) after the spinning of band matured silkworm, by silk dust and sundries remove, and by silk from the online removing of spinning；
(3) silk that removing obtains is cut out by the shape of facial mask, obtains facial mask shape silk；
(4) facial mask shape silk is placed in the device that energy water steams, silk is steamed 3 minutes using water vapour, silk-fibroin is seeped
Silk table face is arrived out, and the temperature of water vapour is maintained at 100 DEG C -105 DEG C；
(5) the facial mask shape silk steamed by water is put into microwave sterilization machine and is carried out microwave disinfection 5 minutes；Export microwave function
Rate 40KW；
(6) the facial mask shape silk after sterilization is carried out packaging according to traditional facial mask technology of the package can be obtained pure mulberry silk
Protein facial mask.
The mesh width of the described spinning net is 1 millimeter, the net that spins with a thickness of 0.5-1 millimeters.
Embodiment 2
Pure mulberry silk protein facial mask can be made using following steps completion:
(1) it after the matured silkworm defecation of silkworm is complete, puts it to spinning on the net, matured silkworm is allowed uniformly to spit 6 layers on the net in spinning
Silk；
(2) after the spinning of band matured silkworm, by silk dust and sundries remove, and by silk from the online removing of spinning；
(3) silk that removing obtains is cut out by the shape of facial mask, obtains facial mask shape silk；
(4) facial mask shape silk is placed in the device that energy water steams, silk is steamed 4 minutes using water vapour, silk-fibroin is seeped
Silk table face is arrived out, and the temperature of water vapour is maintained at 100 DEG C -105 DEG C；
(5) the facial mask shape silk steamed by water is put into microwave sterilization machine and is carried out microwave disinfection 5.5 minutes；
(6) the facial mask shape silk after sterilization is carried out packaging according to traditional facial mask technology of the package can be obtained pure mulberry silk
Protein facial mask.
The mesh width of the described spinning net is 2 millimeters, the net that spins with a thickness of 0.5-1 millimeters.
Embodiment 3
Pure mulberry silk protein facial mask can be made using following steps completion:
(1) it after the matured silkworm defecation of silkworm is complete, puts it to spinning on the net, matured silkworm is allowed uniformly to spit 7 layers on the net in spinning
Silk；
(2) after the spinning of band matured silkworm, by silk dust and sundries remove, and by silk from the online removing of spinning；
(3) silk that removing obtains is cut out by the shape of facial mask, obtains facial mask shape silk；
(4) facial mask shape silk is placed in the device that energy water steams, silk is steamed 5 minutes using water vapour, silk-fibroin is seeped
Silk table face is arrived out, and the temperature of water vapour is maintained at 100 DEG C -105 DEG C；
(5) the facial mask shape silk steamed by water is put into microwave sterilization machine and is carried out microwave disinfection 6 minutes；
(6) the facial mask shape silk after sterilization is carried out packaging according to traditional facial mask technology of the package can be obtained pure mulberry silk
Protein facial mask.
The mesh width of the described spinning net is 3 millimeters, the net that spins with a thickness of 0.5-1 millimeters.
The product of above-described embodiment is supplied to 20 25-35 years old female volunteers and uses, originally they skin is thick on the face
Rough dimness, some go back spottiness, use pure mulberry silk protein facial mask of the invention later, will after wash clean face before sleeping every night
On its architrave, patch 15 minutes or more every time, 20 experimenters have 19 skins after one month to start to become ruddy gloss, spot
Also thin out.
Application Example
1, Guangxi Zhang, female, 30 years old, people from Nanning, child seven months, after Zhang's pregnancy is given birth to a child, skin became thick on the face
Rough dim and have stigma, she introduces through friend and has used pure mulberry silk protein facial mask of the invention, sleeps preceding wash clean every night
By on pure mulberry silk protein facial mask architrave after face, paste 15-20 minutes every time, Zhang becomes ruddy light using skin after one month
Pool, spot is also thin out, does not almost see spottiness after two months.
2, Guangxi Chen, female, 33 years old, people from Nanning, pendulum food was spread out Chen originally, is often stayed up late, is also had ignored nursing
Skin on the face, skin becomes dark yellow on the face, and Chen changes one's profession, and also uses many skin care item, but skin again without
Improved, she introduces through friend and has used pure mulberry silk protein facial mask of the invention, will after wash clean face before sleeping every night
On pure mulberry silk protein facial mask architrave, paste 15-25 minutes every time, Chen becomes pale gloss using skin after one month.
Claims (1)
1. a kind of preparation method of native fibroin facial mask, it is characterised in that: use following steps:
(1) after the matured silkworm defecation of silkworm is complete, spinning is put it on the net, the mesh width for the net that spins is 1-3 millimeters, and spin net
With a thickness of 0.5-1 millimeters, allow matured silkworm uniformly to spit 5-8 layers of silk on the net in spinning；Before matured silkworm is put into spinning on the net, it is necessary to
Its defecation is complete, can just be put into spinning on the net, it is allowed to spin, and can avoid matured silkworm defecation pollution spinning net before spinning；
(2) after to matured silkworm spinning, by silk dust and sundries remove, and by silk from the online removing of spinning；
(3) silk that removing obtains is cut out by the shape of facial mask, obtains facial mask shape silk；
(4) facial mask shape silk is placed in the device that energy water steams, silk is steamed 3-5 minutes using water vapour, silk-fibroin is oozed out
To silk table face, the temperature of water vapour is maintained between 100 DEG C -105 DEG C；
(5) the facial mask shape silk steamed by water is put into microwave sterilization machine and is carried out microwave disinfection 5-6 minutes；It is killed carrying out microwave
Facial mask shape silk is needed to carry out having detected whether silk-fibroin exudation before bacterium, have silk-fibroin exudation can carry out microwave disinfection；
(6) the facial mask shape silk after sterilization is carried out packaging according to traditional facial mask technology of the package can be obtained native fibroin
Facial mask.
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| CN201610273950.0A CN105919910B (en) | 2016-04-28 | 2016-04-28 | The preparation method of native fibroin facial mask |
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| CN201610273950.0A CN105919910B (en) | 2016-04-28 | 2016-04-28 | The preparation method of native fibroin facial mask |
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| CN105919910B true CN105919910B (en) | 2019-05-31 |
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Families Citing this family (8)
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|---|---|---|---|---|
| FR3051487B1 (en) * | 2016-05-20 | 2019-08-02 | Sericyne | NONWOVEN TEXTILE OF NATURAL SILK AND PROCESS FOR OBTAINING THE SAME |
| CN106835507B (en) * | 2017-03-29 | 2019-07-02 | 盐城工业职业技术学院 | A kind of castor silkworm plate wire production method and its a kind of facial mask |
| CN107012589A (en) * | 2017-05-12 | 2017-08-04 | 广州雅南无纺布制品有限公司 | A kind of silkworm carbon mask substrate and preparation method thereof |
| KR101966915B1 (en) * | 2018-11-12 | 2019-04-09 | 주식회사 조이스킨화장품 | Cosmetic pack manufacturing procedure using sheet comprising unrefined silk and cosmetic pack manufactured through the same procedure |
| CN111939085B (en) * | 2020-08-19 | 2021-11-02 | 浙江大学 | Preparation method of silk mask and product |
| JP7332564B2 (en) * | 2020-10-30 | 2023-08-23 | 山岸 幸一 | Multi-layer floss filter, manufacturing method thereof, silk filter mask using same, and manufacturing method thereof |
| CN112941728A (en) * | 2021-03-11 | 2021-06-11 | 汤贝特 | Processing technology of natural fibroin mask |
| CN114657697B (en) * | 2022-03-23 | 2023-04-07 | 盐城工业职业技术学院 | Preparation method of full-silk sericin cocoon flat-plate silk composite mask material |
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