CN104814883B - The method of high activity silk mask is made of Bombyx bombycis - Google Patents
The method of high activity silk mask is made of Bombyx bombycis Download PDFInfo
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- CN104814883B CN104814883B CN201510181125.3A CN201510181125A CN104814883B CN 104814883 B CN104814883 B CN 104814883B CN 201510181125 A CN201510181125 A CN 201510181125A CN 104814883 B CN104814883 B CN 104814883B
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Abstract
The invention discloses a kind of method that Bombyx bombycis makes high activity silk mask, it is characterized in that: complete in accordance with the following steps: (1) washes cocoon: wash away dust on Bombyx bombycis and foreign material with clear water; (2) molten cocoon: by cleaning after Bombyx bombycis put into concentration be 0.1% ~ 5% protein enzyme solution soak, make sericin fully swelling, cocoon layer is opened; (3) cocoon is shelled: tear cocoon layer, remove Pupa bombycis; (4) film forming: be enclosed within arch mould by the Bombyx bombycis removing Pupa bombycis, makes silkworm silk nethike embrane; (5) dry: naturally to dry or oven drying at low temperature (6) punch forming.Present invention process flow process is short, and make simple, full technological process processes all at low temperatures, does not need dipping by lye, does not need high temperature steaming, and protein active is retained to greatest extent, and sericin invariance is not run off, and facial film degree of compacting is good, easy to use.
Description
Technical field
The present invention relates to cosmetic field, is a kind of method that Bombyx bombycis makes high activity silk mask specifically.
Background technology
Facial film is the important class in current skin care item, and its major function is skin care, by the nutritional labeling of facial film itself, realizes the effects such as whitening, moisturizing, crease-resistant, slow down aging.
Silkworm silk, as a kind of natural animal protein, has very large similarity with human body skin, and other albumen, is also more easily absorbed by the body relatively, plays the effect of whitening, moisturizing.In addition, the tyrosine that in silkworm silk, content is more and phenylalanine etc. have good Absorption to ultraviolet, have sun-proof skin care effect.
But blemish in an otherwise perfect thing, fibroin is inactivation very easily, and after inactivation, its skin effect significantly reduces.Silk mask in the market, mostly adopt non-woven fabrics as base material, to the manufacture process of non-woven fabrics from cocoon drying, high temperature, soda acid, bleach etc. make fibroin there occurs irreversible degeneration already, and protein active greatly reduces.In the traditional handicraft of Bombyx bombycis forming surface film base material, Bombyx bombycis all has to pass through high temperature steaming (decatize), in this process, sericin can run off and degeneration in a large number, cause significant wastage, its skin effect is also undesirable, and the silk mask formed runs off due to sericin, loosely organized, yielding in use procedure, use inconvenience.
Summary of the invention
For existing problem, the object of the present invention is to provide a kind of method making high activity silk mask of Bombyx bombycis that greatly can keep fibroin activity.
To achieve these goals, technical scheme of the present invention is: a kind of Bombyx bombycis makes the method for high activity silk mask, it is characterized in that: comprised the steps:
(1) cocoon is washed: wash away dust on Bombyx bombycis and foreign material with clear water;
(2) molten cocoon: be the protein enzyme solution moistening of 0.1% ~ 5% by the Bombyx bombycis concentration after cleaning, make sericin fully swelling, cocoon layer is opened;
(3) film forming: the Bombyx bombycis removing Pupa bombycis is made silkworm silk nethike embrane;
(4) dry: naturally to dry or oven drying at low temperature;
(5) punch forming.
Adopt such scheme, the present invention does not adopt the molten cocoon of alkali liquor, adopts the molten cocoon of protease, the swelling rear Bombyx bombycis of sericin is non-yellowing, whiteness and the glossiness of fresh cocoon can be kept, make no longer to need the aftertreatment technologys such as bleaching, neutralization in subsequent technique, while keeping the activity of fibroin, shorten technique.
Secondly, processing procedure of the present invention is all process at low temperatures, do not need high temperature steaming (gas steaming), only when soaking with protease, can suitably heat, also can select just at room temperature to soak, even if the temperature of heating also higher than 60 DEG C, can not ensure that the activity of fibroin greatly.Avoid loss and the degeneration of the sericin caused because of high temperature steaming.
Finally, silk mask of the present invention has the effect of frivolous recessiveness, and technological process is short, and manufacture method is simple, and the silk mask obtained is the long filament of directly garnetting from Bombyx bombycis, can not there is the phenomenon that short fiber drops.
In such scheme, in step (1): the dried cocoon that described Bombyx bombycis is fresh cocoon containing Pupa bombycis or dries at 60 DEG C.Namely Bombyx bombycis is the cocoon of the traditional ellipse containing Pupa bombycis, and dried cocoon easily preserves.
In such scheme, the method for film forming is: transferred in sericin aqueous solution by the Bombyx bombycis after swelling, gently tear Bombyx bombycis, remove Pupa bombycis with have gentle hands, be then enclosed within arch mould by the Bombyx bombycis removing Pupa bombycis, make silkworm silk nethike embrane.During film forming, we select to remove Pupa bombycis in sericin aqueous solution, decrease the loss of sericin, and after film forming, film has certain ability of anti-deformation due to the adhesion of sericin, and silk net membrane structure is compacted, can not be loose, uses more comfortable.
In such scheme: described Bombyx bombycis is the dull and stereotyped cocoon not containing Pupa bombycis.Silkworm weaves silk and knots into dull and stereotyped cocoon on a flat board.Dull and stereotyped cocoon, not containing Pupa bombycis, uses more convenient.Film forming is: the dull and stereotyped cocoon after swelling is put into sericin aqueous solution, gently tears cocoon layer with have gentle hands, the nethike embrane required for formation.Sericin can be avoided to run off.After film forming, film has certain ability of anti-deformation due to the adhesion of sericin, and silk net membrane structure is compacted, can not be loose, uses more comfortable.
As preferably: the mass concentration of described sericin aqueous solution is 0.5%-50%.Sericin is avoided to run off.
In such scheme, in step (2), the temperature of protein enzyme solution is 20-60 DEG C.Such Bombyx bombycis swelling effect is good, and keeps Bombyx bombycis to operate under lower than the condition of 60 DEG C all the time, makes the preservation that protein active is maximum.
In such scheme: described protease is one or more in alkaline protease or neutral protease.Preferred described protease is papain.
In such scheme: in step (2), Bombyx bombycis is put into protein enzyme solution and soaks, the time of immersion is 0.5-48h, soaks and adopts Dipping or Vaccum Permeating cocoon, bath raio 1:20 ~ 1:100.Vacuum is soaked and is made sericin more easily swelling.Finally make sericin fully swelling.
The invention has the beneficial effects as follows: the present invention utilizes Bombyx bombycis to make the silk mask obtained at low temperatures, does not need the process of alkali liquor, does not need the subsequent techniques such as bleaching, neutralization, ensure that the activity of fibroin greatly.Meanwhile, the present invention can avoid loss and the degeneration of sericin.Comparatively traditional handicraft is high for the silk mask protein active that the present invention obtains, and can better play the performance of natural amino acid moisturizing in silkworm silk, crease-resistant, uv-resistant, anti-inflammatory and anti-pock.In addition, operation is simple and feasible in the present invention, can keep the distinctive filament structure of silkworm silk, and obtained product is the facial film of " can breathe ", and breathability is splendid.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention will be further described:
The preparation of embodiment 1 silk mask, completes in accordance with the following steps:
(1) a certain amount of fresh cocoon (containing Pupa bombycis, oval) is chosen;
(2) cocoon is washed: wash away dust on Bombyx bombycis and foreign material with clear water.
(3) molten cocoon: it is the alkali protease2709 of 0.1% and the papain complex liquid of 0.1% that the Bombyx bombycis after cleaning is put into mass concentration, and bath raio 1:100, soaks 48h at 20-60 DEG C, and make sericin fully swelling, cocoon layer is opened.
(4) cocoon is shelled: transfer in clear water by the Bombyx bombycis after swelling, gently tear cocoon layer with have gentle hands, remove Pupa bombycis.
(5) film forming: the Bombyx bombycis 3 being removed Pupa bombycis is successively enclosed within arch mould, makes silkworm silk nethike embrane.Thickness as required, also can adopt one or more Bombyx bombycis to make one and to throw the net film.
(6) dry: naturally to dry.
(7) punch forming.
The preparation of embodiment 2 silk mask, completes in accordance with the following steps:
(1) cocoon drying: fresh for 25kg cocoon is dried at 60 DEG C.
(2) cocoon is washed: wash away dust on Bombyx bombycis and foreign material with clear water.
(3) molten cocoon: the fresh cocoon after cleaning is put into vacuum tank, after evacuation, inject the neutral protein enzymatic solution that 500kg mass concentration is 5%, under room temperature, soak 48h, bath raio 1:20, make sericin fully swelling, cocoon layer is opened.
(4) cocoon is shelled: it is in the sericin aqueous solution of 0.5% that the Bombyx bombycis after swelling is transferred to mass concentration, gently tears cocoon layer, remove Pupa bombycis with have gentle hands.
(5) film forming: the Bombyx bombycis 5 being removed Pupa bombycis is successively enclosed within arch mould, makes silkworm silk nethike embrane.Thickness as required, also can adopt one or more Bombyx bombycis to make one and to throw the net film.
(6) dry: naturally to dry.
(7) punch forming.
The preparation of embodiment 3 silk mask, completes in accordance with the following steps:
(1) a certain amount of fresh cocoon is chosen.
(2) cocoon is washed: wash away dust on Bombyx bombycis and foreign material with clear water.
(3) molten cocoon: the Bombyx bombycis after cleaning is put into the papain solution that concentration is 2%, and soak 0.5h at 20-60 DEG C, bath raio 1:40, make sericin fully swelling, cocoon layer is opened.
(4) cocoon is shelled: it is in the sericin aqueous solution of 50% that the Bombyx bombycis after swelling is transferred to mass concentration, gently tears cocoon layer, remove Pupa bombycis with have gentle hands.
(5) film forming: the Bombyx bombycis 3 being removed Pupa bombycis is successively enclosed within arch mould, makes silkworm silk nethike embrane.Thickness as required, also can adopt one or more Bombyx bombycis to make nethike embrane.
(6) dry: naturally to dry or dry under lower than the low temperature of 60 DEG C.
(7) punch forming.
The preparation of embodiment 4 silk mask, completes in accordance with the following steps:
(1) a certain amount of dull and stereotyped cocoon is chosen;
(2) cocoon is washed: wash away dust on dull and stereotyped cocoon and foreign material with clear water.
(3) molten cocoon: the dull and stereotyped cocoon after cleaning is put into the alkali protease2709 that mass concentration is 0.5%, bath raio 1:50, and soak 2h at 20-60 DEG C, make sericin fully swelling, cocoon layer is opened.
(4) film forming: it is in the sericin aqueous solution of 20% that the dull and stereotyped cocoon after swelling is transferred to mass concentration, gently tears cocoon layer with have gentle hands, forms required nethike embrane.
(5) dry: naturally to dry or dry under lower than the low temperature of 60 DEG C.
(6) punch forming.
The facial film that the present invention obtains can be attached to after direct water-wet and use on the face, also can with other Protease Treatment liquid wetting, or encloses pearl film and make silk mask.
The present invention is not limited to above-mentioned specific embodiment, should be appreciated that those of ordinary skill in the art just design according to the present invention can make many modifications and variations without the need to creative work.In a word, all technical staff in the art, all should by the determined protection domain of claims under this invention's idea on the basis of existing technology by the available technical scheme of logical analysis, reasoning, or a limited experiment.
Claims (8)
1. make a method for high activity silk mask of Bombyx bombycis, it is characterized in that: comprised the steps:
(1) cocoon is washed: wash away dust on Bombyx bombycis and foreign material with clear water;
(2) molten cocoon: be the protein enzyme solution moistening of 0.1% ~ 5% by the Bombyx bombycis concentration after cleaning, make sericin fully swelling, cocoon layer is opened, and the temperature of protein enzyme solution is 20-60 DEG C;
(3) film forming: the Bombyx bombycis removing Pupa bombycis is made silkworm silk nethike embrane;
(4) dry: naturally to dry or oven drying at low temperature;
(5) punch forming; Described protease is one or more in alkaline protease or neutral protease.
2. make the method for high activity silk mask according to claim 1 of Bombyx bombycis, it is characterized in that: in step (1): described Bombyx bombycis is the dried cocoon of fresh cocoon containing Pupa bombycis or oven dry at 60 DEG C.
3. the method for high activity silk mask is made according to claim 2 of Bombyx bombycis, it is characterized in that: the method for film forming is: the Bombyx bombycis after swelling is transferred in sericin aqueous solution, gently Bombyx bombycis is torn with have gentle hands, remove Pupa bombycis, then the Bombyx bombycis removing Pupa bombycis is enclosed within arch mould, makes silkworm silk nethike embrane.
4. make the method for high activity silk mask according to claim 1 of Bombyx bombycis, it is characterized in that: described Bombyx bombycis is the dull and stereotyped cocoon not containing Pupa bombycis.
5. make the method for high activity silk mask according to claim 4 of Bombyx bombycis, it is characterized in that: film forming is: the dull and stereotyped cocoon after swelling is put into sericin aqueous solution, gently tears cocoon layer with have gentle hands, the nethike embrane required for formation.
6. according to any one of claim 3 or 5, make the method for high activity silk mask of Bombyx bombycis, it is characterized in that: the mass concentration of described sericin aqueous solution is 0.5%-50%.
7. make the method for high activity silk mask according to claim 1 of Bombyx bombycis, it is characterized in that: described protease is papain.
8. the method for high activity silk mask is made according to claim 7 of Bombyx bombycis, it is characterized in that: in step (2), Bombyx bombycis is put into protein enzyme solution and soaks, soak and adopt Dipping or Vaccum Permeating cocoon; bath raio 1:20 ~ 1:100, the time of immersion is 0.5-48h.
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Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105326760A (en) * | 2015-11-30 | 2016-02-17 | 河池学院 | Soaking-free silkworm cocoon composition, preparation method and application of soaking-free silkworm cocoon composition in skin whitening |
| CN105919910B (en) * | 2016-04-28 | 2019-05-31 | 韦有任 | The preparation method of native fibroin facial mask |
| JP7332564B2 (en) | 2020-10-30 | 2023-08-23 | 山岸 幸一 | Multi-layer floss filter, manufacturing method thereof, silk filter mask using same, and manufacturing method thereof |
| CN112587419A (en) * | 2020-12-31 | 2021-04-02 | 广西八园农业科技有限公司 | Preparation method of silk mask |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1800473A (en) * | 2006-01-16 | 2006-07-12 | 唐懿 | Active sericin silk non-woven water jetting cloth process |
| CN103469313A (en) * | 2013-09-26 | 2013-12-25 | 大连工业大学 | Method for purely-neutral enzyme-degumming and reelability of tussah cocoons |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1800473A (en) * | 2006-01-16 | 2006-07-12 | 唐懿 | Active sericin silk non-woven water jetting cloth process |
| CN103469313A (en) * | 2013-09-26 | 2013-12-25 | 大连工业大学 | Method for purely-neutral enzyme-degumming and reelability of tussah cocoons |
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Effective date of registration: 20160216 Address after: 400038 No. 112, Fung Tin Road, Shapingba District, Chongqing, 17-5 Applicant after: Xi Minhao Address before: 400030, No. 18, Feng Tian Road, Shapingba District, Chongqing Applicant before: Chongqing Hangfan Silk Technology Development Co., Ltd. |
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Effective date of registration: 20170612 Address after: 400713 Chongqing city Beibei district on 128 Lilu Technology Innovation Center building B 505 Patentee after: Chongqing Sima Silk Technology Co. Ltd. Address before: 400038 No. 112, Fung Tin Road, Shapingba District, Chongqing, 17-5 Patentee before: Xi Minhao |
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Address after: No. 003-2, Gangbin Road, Shipan Industrial Park, Pingshan Town, Pingshan County, Yibin City, Sichuan Province, 645350 Patentee after: Sichuan Sima Silk Technology Co.,Ltd. Address before: 400713 505, building B, science and technology entrepreneurship center, 128 Anli Road, Beibei District, Chongqing Patentee before: CHONGQING SIMABO TECHNOLOGY Co.,Ltd. |