CN104674355A - Preparation method of tussore non-woven fabric mask - Google Patents

Preparation method of tussore non-woven fabric mask Download PDF

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Publication number
CN104674355A
CN104674355A CN201510023843.8A CN201510023843A CN104674355A CN 104674355 A CN104674355 A CN 104674355A CN 201510023843 A CN201510023843 A CN 201510023843A CN 104674355 A CN104674355 A CN 104674355A
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CN
China
Prior art keywords
temperature
silk
kilograms
kilogram
preparation
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201510023843.8A
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Chinese (zh)
Inventor
慕德明
慕程程
吴春华
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
DANDONG ZHONGTIAN TUSSAH BIOLOGICAL TECHNOLOGY Co Ltd
Original Assignee
DANDONG ZHONGTIAN TUSSAH BIOLOGICAL TECHNOLOGY Co Ltd
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Application filed by DANDONG ZHONGTIAN TUSSAH BIOLOGICAL TECHNOLOGY Co Ltd filed Critical DANDONG ZHONGTIAN TUSSAH BIOLOGICAL TECHNOLOGY Co Ltd
Priority to CN201510023843.8A priority Critical patent/CN104674355A/en
Publication of CN104674355A publication Critical patent/CN104674355A/en
Pending legal-status Critical Current

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Classifications

    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01CCHEMICAL OR BIOLOGICAL TREATMENT OF NATURAL FILAMENTARY OR FIBROUS MATERIAL TO OBTAIN FILAMENTS OR FIBRES FOR SPINNING; CARBONISING RAGS TO RECOVER ANIMAL FIBRES
    • D01C3/00Treatment of animal material, e.g. chemical scouring of wool
    • D01C3/02De-gumming silk
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/0212Face masks
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/98Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/987Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01CCHEMICAL OR BIOLOGICAL TREATMENT OF NATURAL FILAMENTARY OR FIBROUS MATERIAL TO OBTAIN FILAMENTS OR FIBRES FOR SPINNING; CARBONISING RAGS TO RECOVER ANIMAL FIBRES
    • D01C3/00Treatment of animal material, e.g. chemical scouring of wool
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/10General cosmetic use

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Public Health (AREA)
  • Animal Behavior & Ethology (AREA)
  • Veterinary Medicine (AREA)
  • General Health & Medical Sciences (AREA)
  • Zoology (AREA)
  • Epidemiology (AREA)
  • Birds (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Textile Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Animal Husbandry (AREA)
  • Molecular Biology (AREA)
  • Dermatology (AREA)
  • Cosmetics (AREA)
  • Chemical Or Physical Treatment Of Fibers (AREA)

Abstract

The invention discloses a preparation method of a tussore non-woven fabric mask, relating to the technical field of skin care products. The preparation method comprises a sophistication process and a degumming process, wherein the temperature of the sophistication process is controlled at 120-128 DEG C; the sophistication process is carried out in a pressure dissolved air tank; the pressure is 0.15-0.2MPa; when the temperature of the silk fibers is 60-70 DEG C, sericin is dissolved, when the temperature is 95-98 DEG C, sericin is quickly dissolved, and when the temperature is 120-128 DEG C, sericin is fully expanded, so that the optimum flexibility of the silk fibers is obtained. The comfort level for skin exposure of a human body is enhanced. Neutral protease is adopted to degum and remove cocoons, the silk is degummed slowly, mildly and uniformly; the quality and performance of the silk fibers are perfectly retained; the mask in application give full play to health care, skincare and beatifying functions and the like.

Description

A kind of preparation method of tussah nonwoven fabric facial mask
Technical field:
The present invention relates to technical field of skin care, be specifically related to a kind of preparation method of tussah nonwoven fabric facial mask.
Background technology:
The silkworm section class of spontaneous growth in wild (toothed oak) Can Shi the Northeast mountain forest.Food mongolian oak leaf, therefore formal name used at school tussah.Wild silkworm has more active animal protein matter in natural silk and 18 seed amino acids.Its quality component is very close with human body skin structure.Therefore be described as human body Second Skin.Tussah is compared with mulberry silk, and maximum otherness is tussah fibre structure is loose structure.The distinctive hygroscopicity of its fiber, polywater, wet putting are more suitable for the preferred material as facial mask.Because tussah fibrous inside contains partial air, flexibility, elasticity are better, cool in summer and warm in winter.RGD tripeptides structure exclusive in tussah can, as medium, be the excellent acceptor of cell adherence.Cell is under the effect through RGD tripeptides, and the sericin in silk and fibroin albumen can promote that Fine born of the same parents absorb nutrition fully, strengthens cell activation.Effect that facial mask really embodies human body Second Skin is made with tussah.
Traditional handicraft natural silk degumming is unwinding, employing be chemicals, use caustic soda, brightening agent etc.Cause the protein in silk and amino acid to be subject to severe contamination and damage when natural silk degumming.When making facial mask, stimulating for avoiding producing human body skin, chemical technology again must be carried out by acid-base integration method again, just can reach pH value neutrality, meet national testing requirement.Therefore the sound development of the industry is greatly constrained.
Summary of the invention:
The object of this invention is to provide a kind of preparation method of tussah nonwoven fabric facial mask, it adopts neutral proteinase to come unstuck unwinding, when natural silk degumming, slow, gentle, even; Intact reservation is obtained to the quality of silk fiber and performance; Make it in the application of facial mask, give full play to the multiple efficacies such as due health care, skin care, beauty treatment.
In order to solve the problem existing for background technology, the present invention is by the following technical solutions: it comprises succinct technique and degumming tech, the temperature of described succinct technique controls between 120-128 degree, carry out in pressure air-dissolving tank, pressure is 0.15-0.2 MPa, silk fiber temperature be 60-70 spend time, silk gum starts to dissolve, rapid solution is formed when 95-98 spends, when 120-128 spends, silk fiber reaches abundant expansion, and then reaches the pliability of silk fiber the best, and elasticity is better, enhances the comfort level of contact human skin; Described degumming tech is: 1, feed intake silk fiber 100 kilograms; 2, neutral proteinase 5 kilograms is added; 3, add water 850-900 kilogram; 4, water temperature is controlled at 45-55 degree; 5, in the stainless cylinder of steel of insulation, keep liquid middling speed to circulate, under the condition of pH value 6.5, process 3 hours; 6, clean with full-automatic wash-out all-in-one and dewater; Keep water temperature 60-70 degree; Time is 10-20 minute; 7, naturally dry; 8, pack.
In the present invention the fibre strength of silk be 3.55g D, oil content is 0.21%, and pH value is 6.3-7.1, and cleanliness factor is 90 points.
Described neutral proteinase comprises 1 kilogram, 20,000 u lipase, 20,000 U amylase 1.5 kilograms, 20,000 U cellulase 2.5 kilograms, pectase 1 kilogram, 1 kilogram, brown sugar.
Beneficial effect of the present invention: it adopts neutral proteinase to come unstuck unwinding, when natural silk degumming, slow, gentle, even; Intact reservation is obtained to the quality of silk fiber and performance; Make it in the application of facial mask, give full play to the multiple efficacies such as due health care, skin care, beauty treatment.
Detailed description of the invention:
This detailed description of the invention is by the following technical solutions: it comprises succinct technique and degumming tech, the temperature of described succinct technique controls between 120-128 degree, carry out in pressure air-dissolving tank, pressure is 0.15-0.2 MPa, silk fiber temperature be 60-70 spend time, silk gum starts to dissolve, form rapid solution when 95-98 spends, when 120-128 spends, silk fiber reaches abundant expansion, and then reach the pliability of silk fiber the best, and elasticity is better.Enhance the comfort level of contact human skin; Described degumming tech is: 1, feed intake silk fiber 100 kilograms; 2, neutral proteinase 5 kilograms is added; 3, add water 850-900 kilogram; 4, water temperature is controlled at 45-55 degree; 5, in the stainless cylinder of steel of insulation, keep liquid middling speed to circulate, under the condition of pH value 6.5, process 3 hours; 6, clean with full-automatic wash-out all-in-one and dewater; Keep water temperature 60-70 degree; Time is 10-20 minute; 7, naturally dry; 8, pack.
In this detailed description of the invention the fibre strength of silk be 3.55g D, oil content is 0.21%, and pH value is 6.3-7.1, and cleanliness factor is 90 points.
Described neutral proteinase comprises 1 kilogram, 20,000 u lipase, 20,000 U amylase 1.5 kilograms, 20,000 U cellulase 2.5 kilograms, pectase 1 kilogram, 1 kilogram, brown sugar.
The beneficial effect of this detailed description of the invention: it adopts neutral proteinase to come unstuck unwinding, when natural silk degumming, slow, gentle, even; Intact reservation is obtained to the quality of silk fiber and performance; Make it in the application of facial mask, give full play to the multiple efficacies such as due health care, skin care, beauty treatment.
More than show and describe general principle of the present invention and principal character and advantage of the present invention.The technical staff of the industry should understand; the present invention is not restricted to the described embodiments; what describe in above-described embodiment and description just illustrates principle of the present invention; without departing from the spirit and scope of the present invention; the present invention also has various changes and modifications, and these changes and improvements all fall in the claimed scope of the invention.Application claims protection domain is defined by appending claims and equivalent thereof.

Claims (2)

1. the preparation method of a tussah nonwoven fabric facial mask, it is characterized in that it comprises succinct technique and degumming tech, the temperature of described succinct technique controls, between 120-128 degree, to carry out in pressure air-dissolving tank, pressure is 0.15-0.2 MPa, silk fiber temperature be 60-70 spend time, silk gum start dissolve, when 95-98 spends formed rapid solution, when 120-128 spends, silk fiber reaches abundant expansion, and then reaches the pliability of silk fiber the best, and elasticity is better.Enhance the comfort level of contact human skin; Described degumming tech is: (1), feed intake silk fiber 100 kilograms; (2) neutral proteinase 5 kilograms, is added; (3), add water 850-900 kilogram; (4) water temperature, is controlled at 45-55 degree; (5), in the stainless cylinder of steel of insulation keep liquid middling speed to circulate, under the condition of pH value 6.5, process 3 hours; (6), clean with full-automatic wash-out all-in-one and dewater; Keep water temperature 60-70 degree; Time is 10-20 minute; (7), naturally dry; (8), pack.
2. the preparation method of a kind of tussah nonwoven fabric facial mask according to claim, is characterized in that described neutral proteinase comprises 1 kilogram, 20,000 u lipase, 20,000 U amylase 1.5 kilograms, 20,000 U cellulase 2.5 kilograms, pectase 1 kilogram, 1 kilogram, brown sugar.
CN201510023843.8A 2015-01-19 2015-01-19 Preparation method of tussore non-woven fabric mask Pending CN104674355A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201510023843.8A CN104674355A (en) 2015-01-19 2015-01-19 Preparation method of tussore non-woven fabric mask

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201510023843.8A CN104674355A (en) 2015-01-19 2015-01-19 Preparation method of tussore non-woven fabric mask

Publications (1)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105088759A (en) * 2015-08-11 2015-11-25 陈丹儿 Preparing method for silk facial mask and facial mask
CN107489016A (en) * 2017-07-19 2017-12-19 苏州凯邦生物技术有限公司 A kind of biological enzyme silk fiber scouring agent
CN112587419A (en) * 2020-12-31 2021-04-02 广西八园农业科技有限公司 Preparation method of silk mask

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1160106A (en) * 1997-02-25 1997-09-24 俞祥根 Silk fiber pretreatment process and product thereof
WO2005032505A1 (en) * 2003-09-22 2005-04-14 Juvena (International) Ag Skin and hair care preparation containing a combination of protein hydrolysates
CN1800472A (en) * 2006-01-13 2006-07-12 席星航 Silk denaturated nonwoven fabric containing sericin, and its uses
CN103789846A (en) * 2014-01-20 2014-05-14 丹东中天柞蚕生物科技有限公司 Process method for refining neutral protease from tussah cocoon shell

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1160106A (en) * 1997-02-25 1997-09-24 俞祥根 Silk fiber pretreatment process and product thereof
WO2005032505A1 (en) * 2003-09-22 2005-04-14 Juvena (International) Ag Skin and hair care preparation containing a combination of protein hydrolysates
CN1800472A (en) * 2006-01-13 2006-07-12 席星航 Silk denaturated nonwoven fabric containing sericin, and its uses
CN103789846A (en) * 2014-01-20 2014-05-14 丹东中天柞蚕生物科技有限公司 Process method for refining neutral protease from tussah cocoon shell

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105088759A (en) * 2015-08-11 2015-11-25 陈丹儿 Preparing method for silk facial mask and facial mask
CN105088759B (en) * 2015-08-11 2016-08-24 席敏皓 The preparation method of a kind of silk facial film and facial film
CN107489016A (en) * 2017-07-19 2017-12-19 苏州凯邦生物技术有限公司 A kind of biological enzyme silk fiber scouring agent
CN112587419A (en) * 2020-12-31 2021-04-02 广西八园农业科技有限公司 Preparation method of silk mask

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Application publication date: 20150603

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