CN103409811B - Silk floss manufacture craft under high altitude environment - Google Patents
Silk floss manufacture craft under high altitude environment Download PDFInfo
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- CN103409811B CN103409811B CN201310333650.3A CN201310333650A CN103409811B CN 103409811 B CN103409811 B CN 103409811B CN 201310333650 A CN201310333650 A CN 201310333650A CN 103409811 B CN103409811 B CN 103409811B
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Abstract
The invention belongs to the manufacture technology field that silk silk floss makes, be specifically related to a kind of technology that silk floss makes under high altitude environment.Being improved to of this manufacture craft, 1. silk floss processed: the temperature of beating continuous solution should reach boiling point, control the every sheet silk floss weight in wet base got under Suitable solutions assistant concentration; 2. soak: control well and boil continuous amount at every turn, then clear water soaks, and centre needs to change water once, dehydration; 3. silk floss is boiled: heat to boiling, cover lid boiling suitable time; 4. dewater: first dewater, soak through two clear water reserviors segmentations, then dewater; 5. bleach: put into Bellmer liquid, heat to specified temp, soak, dehydration, clear water soaks, then dewaters; 6. dry: dry to moisture content 9 ± 1% in the indoor of lucifuge.The silk floss color that the present invention makes is fair and clear, glossiness good, soft, smell is little, and silk gum melts mistake rate and diminishes.
Description
Technical field
The invention belongs to the manufacture technology field that silk silk floss makes, be specifically related to a kind of technology that silk floss makes under high altitude environment.
Background technology
Climate of Yunnan is suitable for, and it's like spring all the year round, is to produce the large province of cocoon, and being again that silk floss quilt consumption is large economizes, and pure natural cocoon silk quilt is liked by the Yunnan people deeply.Make raw material---the silk floss of cocoon silk quilt, be pure natural silk fiber, this fiber is made up of silk gum and fibroin, belongs to long fiber class.A lot of Chan Can districts height above sea level in Yunnan is between 1800 ~ 2200 meters, and in silk floss production process, Chan Can district is by the impact of high altitude low air pressure, and boiled water temperature is less than 100 DEG C, and the easy yellowing of silk floss of production, feel are hardened or embrittlement, have a strong impact on silk floss quality.
Summary of the invention
The easy yellowing of silk floss that the object of the invention is to produce according to high altitude localities, feel is hardened or embrittlement, problem of low grade, and provide silk floss manufacture craft under a kind of high altitude environment of improvement, the method can form stable production.
Solving the technical scheme that technical problem of the present invention takes is: the system that mainly contains is continuous, soak, boil silk floss, dehydration, bleach, to dry etc. on the conventional silk floss manufacture craft basis of operation composition, carry out following improvement, 1. silk floss processed: the temperature of beating continuous solution should reach boiling point, it is 0.03 ± 0.005wt% that solution allocates concentration after special assistant into, and the every sheet silk floss weight in wet base got is at 2.4 ~ 2.8Kg; 2. soak: every 39 ~ 41 of the silk floss accomplished fluently boils once, clear water soaks 22 ~ 26 hours, and centre needs to change water once, dehydration; 3. silk floss is boiled: heat to boiling, cover lid boiling 3 ~ 12 hours; 4. dewater: first dewater, soak 11 ~ 13 hours through two clear water reserviors segmentations, then dewater; 5. bleach: put into Bellmer liquid, heat to 58 ~ 62 DEG C, soak 1.5 ~ 2.5 hours, dehydration, clear water soaks, then dewaters; 6. dry: dry to moisture content 9 ± 1wt% in the indoor of lucifuge.
Technical scheme of the present invention also comprises: 1. make in continuous operation, and the silk floss under cutting should be placed in netted sack and prepare to soak; 2. boil in continuous operation, the proportioning of boiling continuous liquid is add in every 1000Kg water to boil continuous special agent, i.e. hydrogen peroxide 15Kg, waterglass 11Kg, soda ash 1Kg, and deoil clever 1.0Kg; 3., in bleaching process, the proportioning of bleaching liquid is add bleaching special agent in every 900Kg water, spun silk softener 1Kg, glacial acetic acid 0.5Kg, silk impregnating agent 6Kg.
Boiling in continuous operation, should be dipped into boil below continuous liquid by boiling in continuous pond the continuous sheet floated in time; In the continuous operation of system, silk floss weight is beat continuous solution 10.5%.
The present invention, owing to have adjusted portion of techniques and the parameter of conventional silk floss manufacture craft, therefore has following effect, and (1) color is more fair and more clear, glossiness better, feel is more soft, smell is little; (2) sericin degumming loss percentage diminishes, and the original technique of weight ratio slightly increases.
Detailed description of the invention
Embodiment 1:
1, system is continuous: the temperature of beating continuous solution should reach boiling point, and solution aid concentration is 0.01%, and the every sheet silk floss weight in wet base got is 2.4 kilograms, and the silk floss under cutting is placed in netted sack and prepares to soak.
2, soak: every 40 of the silk floss accomplished fluently boils once, and clear water soaks 22 hours, and centre needs to change water once, dehydration.
3, add in every 1000 kg of water and boil continuous special agent: 12 kilograms, hydrogen peroxide, waterglass 9 kilograms, soda ash 0.5 kilogram, spirit 0.5 kilogram of deoiling, heat to boiling, cover lid boiling 3 hours; Should be dipped into boil below continuous liquid by boiling in continuous pond the continuous sheet floated in time; In the continuous process of system, silk floss weight is beat continuous solution 10.5%.
4, dewater: first dewater, soak 1 hour through two clear water reserviors segmentations, then dewater.
5, bleach: add bleaching special agent in every 900 kg of water, spun silk softener 1 kilogram, 0.5 kilogram, glacial acetic acid, silk impregnating agent 6 kilograms, heat to 58 DEG C, soak 1.5 hours, dehydration, clear water soaks, then dewaters.
6, dry: dry to moisture content 8% in the indoor of lucifuge.
Make continuous effect:
1, white color, glossiness is general, and soft, smell is slightly;
2, sericin degumming loss percentage change is little, and often opening continuous weight increased by 10 grams more originally.
Embodiment 2:
1, system is continuous: the temperature of beating continuous solution should reach boiling point, and solution aid concentration is 0.02%, and the every sheet silk floss weight in wet base got is 2.4 kilograms, and the silk floss under cutting is placed in netted sack and prepares to soak.
2, soak: every 40 of the silk floss accomplished fluently boils once, and clear water soaks 23 hours, and centre needs to change water once, dehydration.
3, add in every 1000 kg of water and boil continuous special agent: 13 kilograms, hydrogen peroxide, waterglass 10 kilograms, soda ash 0.5 kilogram, spirit 0.5 kilogram of deoiling, heat to boiling, cover lid boiling 5 hours; Should be dipped into boil below continuous liquid by boiling in continuous pond the continuous sheet floated in time; In the continuous process of system, silk floss weight is beat continuous solution 10.5%.
4, dewater: first dewater, soak 1 hour through two clear water reserviors segmentations, then dewater.
5, bleach: add bleaching special agent in every 900 kg of water, spun silk softener 1 kilogram, 0.5 kilogram, glacial acetic acid, silk impregnating agent 6 kilograms, heat to 60 DEG C, soak 2 hours, dehydration, clear water soaks, then dewaters.
6, dry: dry to moisture content 9% in the indoor of lucifuge.
Make continuous effect:
1, white color, good luster, soft, smell is slightly;
2, sericin degumming loss percentage change is little, and often opening continuous weight increased by 12 grams more originally.
Embodiment 3:
1, system is continuous: the temperature of beating continuous solution should reach boiling point, and solution aid concentration is 0.03%, and the every sheet silk floss weight in wet base got is 2.4 kilograms, and the silk floss under cutting is placed in netted sack and prepares to soak.
2, soak: every 40 of the silk floss accomplished fluently boils once, and clear water soaks 24 hours, and centre needs to change water once, dehydration.
3, add in every 1000 kg of water and boil continuous special agent: 15 kilograms, hydrogen peroxide, waterglass 11 kilograms, soda ash 1 kilogram, spirit 1 kilogram of deoiling, heat to boiling, cover lid boiling 8 hours; Should be dipped into boil below continuous liquid by boiling in continuous pond the continuous sheet floated in time; In the continuous process of system, silk floss weight is beat continuous solution 10.5%.
4, dewater: first dewater, soak 1 hour through two clear water reserviors segmentations, then dewater.
5, bleach: add bleaching special agent in every 900 kg of water, spun silk softener 1 kilogram, 0.5 kilogram, glacial acetic acid, silk impregnating agent 6 kilograms, heat to 62 DEG C, soak 2.5 hours, dehydration, clear water soaks, then dewaters.
6, dry: dry to moisture content 9% in the indoor of lucifuge.
Make continuous effect:
1, white color, good luster, soft, odorlessness;
2, sericin degumming loss percentage diminishes, and often opening continuous weight increased by 20 grams more originally.
Embodiment 4:
1, system is continuous: the temperature of beating continuous solution should reach boiling point, and solution aid concentration is 0.03%, and the every sheet silk floss weight in wet base got is 2.4 kilograms, and the silk floss under cutting is placed in netted sack and prepares to soak.
2, soak: every 40 of the silk floss accomplished fluently boils once, and clear water soaks 22 hours, and centre needs to change water once, dehydration.
3, add in every 1000 kg of water and boil continuous special agent: 15 kilograms, hydrogen peroxide, waterglass 11 kilograms, soda ash 1 kilogram, spirit 1 kilogram of deoiling, heat to boiling, cover lid boiling 5 hours; Should be dipped into boil below continuous liquid by boiling in continuous pond the continuous sheet floated in time; In the continuous process of system, silk floss weight is beat continuous solution 10.5%.
4, dewater: first dewater, soak 1 hour through two clear water reserviors segmentations, then dewater.
5, bleach: add bleaching special agent in every 900 kg of water, spun silk softener 1 kilogram, 0.5 kilogram, glacial acetic acid, silk impregnating agent 6 kilograms, heat to 62 DEG C, soak 2.5 hours, dehydration, clear water soaks, then dewaters.
6, dry: dry to moisture content 9.5% in the indoor of lucifuge.
Make continuous effect:
1, white color, glossiness is general, Boardy Feeling, and smell is slightly;
2, sericin degumming loss percentage diminishes, and often opening continuous weight increased by 5 grams more originally.
Embodiment 5:
1, system is continuous: the temperature of beating continuous solution should reach boiling point, and solution aid concentration is 0.03%, and the every sheet silk floss weight in wet base got is 2.6 kilograms, and the silk floss under cutting is placed in netted sack and prepares to soak.
2, soak: every 40 of the silk floss accomplished fluently boils once, and clear water soaks 26 hours, and centre needs to change water once, dehydration.
3, add in every 1000 kg of water and boil continuous special agent: 12 kilograms, hydrogen peroxide, waterglass 11 kilograms, soda ash 0.5 kilogram, spirit 1 kilogram of deoiling, heat to boiling, cover lid boiling 8 hours; Should be dipped into boil below continuous liquid by boiling in continuous pond the continuous sheet floated in time; In the continuous process of system, silk floss weight is beat continuous solution 10.5%.
4, dewater: first dewater, soak 1 hour through two clear water reserviors segmentations, then dewater.
5, bleach: add bleaching special agent in every 900 kg of water, spun silk softener 0.5 kilogram, 0.5 kilogram, glacial acetic acid, silk impregnating agent 4 kilograms, heat to 60 DEG C, soak 2.5 hours, dehydration, clear water soaks, then dewaters.
6, dry: dry to moisture content 9.5% in the indoor of lucifuge.
Make continuous effect:
1, white color, glossiness is general, and feel is slightly good, and smell slightly.
2, sericin degumming loss percentage diminishes, and often opening continuous weight increased by 12 grams more originally.
Embodiment 6:
1, system is continuous: the temperature of beating continuous solution should reach boiling point, and solution aid concentration is 0.03%, and the every sheet silk floss weight in wet base got is 2.4 kilograms, and the silk floss under cutting is placed in netted sack and prepares to soak;
2, soak: every 40 of the silk floss accomplished fluently boils once, and clear water soaks 22 hours, and centre needs to change water once, dehydration;
3, add in every 1000 kg of water and boil continuous special agent: 15 kilograms, hydrogen peroxide, waterglass 11 kilograms, soda ash 1 kilogram, spirit 1 kilogram of deoiling, heat to boiling, cover lid boiling 10 hours; Should be dipped into boil below continuous liquid by boiling in continuous pond the continuous sheet floated in time; In the continuous process of system, silk floss weight is beat continuous solution 10.5%.
4, dewater: first dewater, soak 2 hours through two clear water reserviors segmentations, then dewater.
5, bleach: add bleaching special agent in every 900 kg of water, spun silk softener 1 kilogram, 0.5 kilogram, glacial acetic acid, silk impregnating agent 6 kilograms, heat to 62 DEG C, soak 2.5 hours, dehydration, clear water soaks, then dewaters;
6, dry: dry to moisture content 9% in the indoor of lucifuge.
Make continuous effect:
1, white color, gloss is bright, soft, odorlessness;
2, sericin degumming loss percentage diminishes, and often opening continuous weight increased by 30 grams more originally.
Embodiment 7:
1, system is continuous: the temperature of beating continuous solution should reach boiling point, and solution aid concentration is 0.01%, and the every sheet silk floss weight in wet base got is 2.6 kilograms, and the silk floss under cutting is placed in netted sack and prepares to soak.
2, soak: every 40 of the silk floss accomplished fluently boils once, and clear water soaks 22 hours, and centre needs to change water once, dehydration.
3, add in every 1000 kg of water and boil continuous special agent: 8 kilograms, hydrogen peroxide, waterglass 5 kilograms, soda ash 1 kilogram, spirit 1 kilogram of deoiling, heat to boiling, cover lid boiling 10 hours; Should be dipped into boil below continuous liquid by boiling in continuous pond the continuous sheet floated in time; In the continuous process of system, silk floss weight is beat continuous solution 10.5%.
4, dewater: first dewater, soak 1 hour through two clear water reserviors segmentations, then dewater.
5, bleach: add bleaching special agent in every 900 kg of water, spun silk softener 1 kilogram, 0.5 kilogram, glacial acetic acid, silk impregnating agent 6 kilograms, heat to 62 DEG C, soak 1.5 hours, dehydration, clear water soaks, then dewaters.
6, dry: dry to moisture content 9% in the indoor of lucifuge.
Make continuous effect:
1, darker in color, low in glossiness, feel is coarse, scent of;
2, sericin degumming loss percentage diminishes, and often opening continuous weight increased by 20 grams more originally.
Embodiment 8:
1, system is continuous: the temperature of beating continuous solution should reach boiling point, and solution aid concentration is 0.02%, and the every sheet silk floss weight in wet base got is 2.8 kilograms, and the silk floss under cutting is placed in netted sack and prepares to soak.
2, soak: every 40 of the silk floss accomplished fluently boils once, and clear water soaks 24 hours, and centre needs to change water once, dehydration.
3, add in every 1000 kg of water and boil continuous special agent: 10 kilograms, hydrogen peroxide, waterglass 8 kilograms, soda ash 1 kilogram, spirit 1 kilogram of deoiling, heat to boiling, cover lid boiling 12 hours; Should be dipped into boil below continuous liquid by boiling in continuous pond the continuous sheet floated in time; In the continuous process of system, silk floss weight is beat continuous solution 10.5%.
4, dewater: first dewater, soak 2 hours through two clear water reserviors segmentations, then dewater.
5, bleach: add bleaching special agent in every 900 kg of water, spun silk softener 1 kilogram, 0.5 kilogram, glacial acetic acid, silk impregnating agent 6 kilograms, heat to 62 DEG C, soak 2 hours, dehydration, clear water soaks, then dewaters.
6, dry: dry to moisture content 9% in the indoor of lucifuge.
Make continuous effect:
1, white color, gloss is bright, soft, and smell is slightly;
2, sericin degumming loss percentage diminishes, and often opening continuous weight increased by 35 grams more originally.
Embodiment 9:
1, system is continuous: the temperature of beating continuous solution should reach boiling point, and solution aid concentration is 0.03%, and the every sheet silk floss weight in wet base got is 2.4 kilograms, and the silk floss under cutting is placed in netted sack and prepares to soak.
2, soak: every 40 of the silk floss accomplished fluently boils once, and clear water soaks 26 hours, and centre needs to change water once, dehydration.
3, add in every 1000 kg of water and boil continuous special agent: 15 kilograms, hydrogen peroxide, waterglass 10 kilograms, soda ash 1 kilogram, spirit 1 kilogram of deoiling, heat to boiling, cover lid boiling 12 hours; Should be dipped into boil below continuous liquid by boiling in continuous pond the continuous sheet floated in time; In the continuous process of system, silk floss weight is beat continuous solution 10.5%.
4, dewater: first dewater, soak 2 hours through two clear water reserviors segmentations, then dewater.
5, bleach: add bleaching special agent in every 900 kg of water, spun silk softener 1 kilogram, 0.5 kilogram, glacial acetic acid, silk impregnating agent 6 kilograms, heat to 62 DEG C, soak 2.5 hours, dehydration, clear water soaks, then dewaters.
6, dry: dry to moisture content 9% in the indoor of lucifuge.
Make continuous effect:
1, white color, gloss is bright, soft, odorlessness;
2, sericin degumming loss percentage diminishes, and often opening continuous weight increased by 50 grams more originally.
Silk floss under the high altitude environment prepared by above specific embodiments of the invention, quality all reaches Grade A, and the silk floss under the high altitude environment adopting routine techniques to prepare only has 76% to reach Grade A.
Claims (3)
1. silk floss manufacture craft under a high altitude environment, operation compositions such as mainly containing system silk floss, soak, boil silk floss, dehydration, bleach, dry, it is characterized in that: 1. silk floss processed: the temperature of beating continuous solution should reach boiling point, solution aid concentration is 0.03 ± 0.005wt%, and the every sheet silk floss weight in wet base got is at 2.4 ~ 2.8Kg; 2. soak: every 39 ~ 41 of the silk floss accomplished fluently boils once, clear water soaks 22 ~ 26 hours, and centre needs to change water once, dehydration; 3. silk floss is boiled: heat to boiling, cover lid boiling 3 ~ 12 hours; 4. dewater: first dewater, soak 11 ~ 13 hours through two clear water reserviors segmentations, then dewater; 5. bleach: put into Bellmer liquid, heat to 58 ~ 62 DEG C, soak 1.5 ~ 2.5 hours, dehydration, clear water soaks, then dewaters; 6. dry: dry to moisture content 9 ± 1% in the indoor of lucifuge.
2. by silk floss manufacture craft under high altitude environment according to claim 1, it is characterized in that: 1. make in continuous operation, the silk floss under cutting should be placed in netted sack and prepare to soak; 2. boil in continuous operation, the proportioning of boiling continuous liquid is add in every 1000Kg water to boil continuous special agent: i.e. hydrogen peroxide 15Kg, waterglass 11Kg, soda ash 1Kg, and deoil clever 1.0Kg; 3., in bleaching process, the proportioning of bleaching liquid is add bleaching special agent in every 900Kg water, spun silk softener 1Kg, glacial acetic acid 0.5Kg, silk impregnating agent 6Kg.
3. by silk floss manufacture craft under high altitude environment according to claim 2, it is characterized in that: boiling in continuous operation, should be dipped into boil boiling in continuous pond the continuous sheet floated below continuous liquid in time, and silk floss weight is 10.5% of dozen continuous solution.
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| CN201310333650.3A CN103409811B (en) | 2013-08-02 | 2013-08-02 | Silk floss manufacture craft under high altitude environment |
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| CN201310333650.3A CN103409811B (en) | 2013-08-02 | 2013-08-02 | Silk floss manufacture craft under high altitude environment |
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| CN103409811A CN103409811A (en) | 2013-11-27 |
| CN103409811B true CN103409811B (en) | 2015-11-04 |
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Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104894746B (en) * | 2015-06-30 | 2017-08-01 | 广西立盛茧丝绸有限公司 | A kind of manufacture method of the continuous piece of silkworm |
| CN105220243A (en) * | 2015-08-26 | 2016-01-06 | 广西八桂蚕坊丝绸有限公司 | The processing method of silkworm silk floss sheet |
| CN115162010B (en) * | 2022-06-22 | 2024-05-17 | 南充银海丝绸有限公司 | Silk floss grade-based silk floss sheet finished product processing method and silk quilt preparation method |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101100765A (en) * | 2007-07-25 | 2008-01-09 | 席星航 | Producing method for raw silk fixed gum softening |
| CN102965871A (en) * | 2012-12-19 | 2013-03-13 | 安徽源牌实业（集团）有限责任公司 | Production technique for colorful cocoon silk cotton |
| CN103005932A (en) * | 2012-12-14 | 2013-04-03 | 浙江理工大学 | Method for producing silk quilt by utilizing sericin |
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2013
- 2013-08-02 CN CN201310333650.3A patent/CN103409811B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101100765A (en) * | 2007-07-25 | 2008-01-09 | 席星航 | Producing method for raw silk fixed gum softening |
| CN103005932A (en) * | 2012-12-14 | 2013-04-03 | 浙江理工大学 | Method for producing silk quilt by utilizing sericin |
| CN102965871A (en) * | 2012-12-19 | 2013-03-13 | 安徽源牌实业（集团）有限责任公司 | Production technique for colorful cocoon silk cotton |
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