CN103554961A - Formula and production method for preparing brown wheat straw dye - Google Patents

Formula and production method for preparing brown wheat straw dye Download PDF

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CN103554961A
CN103554961A CN 201310548688 CN201310548688A CN103554961A CN 103554961 A CN103554961 A CN 103554961A CN 201310548688 CN201310548688 CN 201310548688 CN 201310548688 A CN201310548688 A CN 201310548688A CN 103554961 A CN103554961 A CN 103554961A
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formula
production
method
straw
preparing
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CN 201310548688
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马文侠
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哈尔滨市工艺美术有限责任公司
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Abstract

The invention relates to a formula and a production method for preparing brown wheat straw dye. The formula is characterized by adopting dry hibiscus mutabilis, isatis tinctoria, alumen, areca-nut, an iron-ion compound solution and mineral water as main raw materials. The production method comprises the following main steps of sorting, cutting, drying, soaking, boiling, mixing, precipitating, dying and forming a finished product. The invention relates to the formula and the production method for preparing the brown wheat straw dye which is pure natural, pollution-free, environment-friendly and free from toxic and side effects on the human body and prepared by from the pure natural plants.

Description

一种制备褐色麦秸秆染料的配方及生产方法 Formulation and production process for preparing a dye brown wheat straw

[0001] 技术领域: [0001] Technical Field:

本发明涉一种植物染料,特别是涉及一种制备褐色麦秸杆染料的配方及生产方法背景技术: The present invention relates to a plant dyes, in particular, it relates to the formulation and production method for preparing BACKGROUND wheat straw brown dye:

现有技术中,将制作麦秸画的主要原料麦秸杆染成褐色的方法有很多种,但多数染料均为化学染料,染出的褐色不纯正,容易退色,不仅不环保,部分染料在染制的过程中甚至会产生有毒气体,威胁人体的健康。 The prior art, the main raw material for the production of wheat straw paintings straw dyed brown There are many ways, but most are dyes chemical dye, dyed brown is not pure, easy to fade, not only environmentally friendly, part of the dye in the dye process system even produces toxic gases, threat to human health.

[0002]因而,在麦秸画制作领域缺乏一种将麦秸杆染成不同颜色的植物染料,特别是将麦秸杆染成褐色的纯天然植物染料,它染出的褐色麦秸杆不仅色彩纯正,用其材料制出的麦秸画光鲜亮丽,不易退色,而且绿色环保,作品长时间散发出植物清香,有易人的身心健康,程度不同的解决了其它有毒有害化学染料在染制过程中对人们身体造成的威害。 [0002] Thus, the lack of a straw produced in the field of wheat straw paintings will be dyed different colors of vegetable dyes, especially the wheat straw dyed brown natural plant dyes, dye it a brown color not only wheat straw pure, with its materials out of the straw painting glamorous, easy to fade, and the green, works long exudes fragrance of plants, have changed hands physical and mental health, the extent of different solutions other toxic chemical dyes in dyed process Viagra on people caused by the body harm.

[0003] 发明内容: [0003] SUMMARY OF THE INVENTION:

本发明的目的在于提供一种纯天然、无污染、绿色环保、对人身体无毒副作用的用纯天然植物配制成的一种制备褐色麦秸杆染料的配方及生产方法 Object of the present invention is to provide a natural, pollution, environmental protection, toxic side effects on human health formulations are formulated with a natural plant into a brown dye of wheat straw and production methods

本发明的目的是这样实现的。 Object of the present invention is implemented. 它是由下述重量配的原料制成的,芙蓉花干10-30份、菘蓝10-30份、白矾10-30份、槟榔10-30份、铁离子化合物溶液5-15份、矿泉水30-80份。 It is composed of the following weight distribution of the raw material, 10-30 parts of dried hibiscus flower, Isatis 10-30 parts, 10-30 parts of alum, betel 10-30 parts, 5-15 parts of a solution of iron compounds, mineral 30 to 80 parts water.

[0004] 制备本发明褐色麦秸杆染料的配方优选重量配比范围是,其中各种原料的重量配比是,芙蓉花干10-25份、菘蓝10-25份、白矾10-25份、槟榔10-25份、铁离子化合物溶液5-13份、矿泉水30-70份。 [0004] Formulations of the present invention preferably range of the ratio by weight of a brown dye preparation are wheat straw, wherein the weight ratio of the various feedstocks are, hibiscus 10-25 dry parts, Isatis 10-25 parts, 10-25 parts of alum betel 10-25 parts, 5-13 parts of a solution of a compound of iron ions, 30-70 parts mineral.

[0005] 制备本发明褐色麦秸杆染料的最佳重量配比范围是,其中各种原料的重量配比是:芙蓉花干15份、菘蓝15份、白矾15份、槟榔15份、柘黄15份、铁离子化合物溶液7份、矿泉水60份。 [0005] The optimum range of the ratio by weight of wheat straw brown dye preparation of the present invention, wherein the weight ratio of the various starting materials are: 15 parts by dry hibiscus, Isatis 15 parts, 15 parts of alum, 15 parts of betel, Zhe yellow 15 parts, 7 parts of iron compound solution, 60 parts of mineral water. ` `

[0006] 将上述各组份制成本发明褐色麦秸杆染料的生产方法,主要工艺流程为:选料、切料、烘干、浸泡、热煮、混合、沉淀、染色、成品,具体操作方法依次按下列步骤:A、选料、按原料重量配比,挑选符合国家卫生和质量标准的芙蓉花干、菘蓝、白矾、槟榔、铁离子化合物溶液、矿泉水备用、切料、将选出的原料除分别切成块状;C、烘干、将切成块状原料分别置于烘干炉中干化,温度控制在100-120°C,时间30分钟,蒸发原料水份、灭菌;D、浸泡、将烘干后的原料置于装有矿泉水的储槽中浸泡,温度为室20°C,时间2 - 3小时;E、热煮、将泡过的原料从水中捞出,放到陶器里热煮,时间6小时,煮出色素溶液;F、混合、将色素液侵入20%铁离子化合物溶液里,时间4-8小时,制成混合溶液;G、沉淀、将混合溶液凉至20°C,沉淀出纯净褐色素溶液、染色、将100 [0006] The cost of the components prepared above method for producing the invention's dye brown wheat straw, the main process are: choice of materials, cutting, drying, soaking, heat cooking, mixing, sedimentation, dyed, finished, the specific operation the method of the following steps in sequence: a, choice of materials, weight ratio of raw materials, selection of hibiscus flower dry compliance with national health and quality standards, Isatis, alum, betel nut, iron compound solution, mineral reserve, cutting, will be selected from the group in addition to the raw materials are cut into pieces; C, and drying the cut block material were placed in the drying oven temperature was controlled at 100-120 ° C, for 30 minutes, water was evaporated material, off bacteria; D, soaking, after drying the raw material placed in the reservoir with the mineral water soaking, room temperature 20 ° C, time 2 - 3 hours; E, boiled with water, soaked feedstock from water fishing out into the hot cooking of pottery, 6 hours, cook dye solution; F, mixing the dye solution of 20% ferric ions invade compound solution, and the time 4-8 hours, to prepare a mixed solution; G, precipitation, the mixed solution to cool to 20 ° C, the solution was precipitated pure brown pigment, dye, 100 升纯净褐色素溶液的温度渐渐升到80°C以上,将经过杀菌、脱硫、蒸煮处理后的麦秸杆浸泡其中,恒温静置12-14小时,期间将麦秸杆上下翻动,使麦秸杆充分吸收褐色素溶液,均匀染色;1、固色、将染色后的麦秸杆放入加入白矾粉沫的溶液中,浸泡3-6小时,使麦秸杆充分固色后捞出,淋干,在室温中慢慢干燥成褐色麦秸杆成品。 Liters of purified brown pigment temperature of the solution gradually rose to above 80 ° C, the pasteurized, desulfurization, after retorting soaked wheat straw wherein temperature was allowed to stand 12-14 hours, during which the turning down of wheat straw, wheat straw so brown pigment was fully absorbed lever, even dyeing; 1, fixing, the dyed wheat straw were added into a solution of alum powder, soaked 3-6 hours, the wheat straw was sufficiently remove fixation, pour dry, brown wheat straw was slowly dried at room temperature in the finished product.

[0007] 本发明的生产方法优点在于:1、选择原料,配方科学,色彩纯正;2、产品中不添加防腐剂,化工原料,纯天然,对人体无任何伤害,用其原料制成的麦秸画作品不仅散发植物香气,而且抗腐蚀;3原料来源广泛,加工艺线路短,产品易加工制造。 [0007] A production process of the present invention is that the advantages of: 1, selection of raw materials, formulation science, pure color; 2, the product does not add preservatives, chemical raw materials, natural, without any harm to the human body, with its raw material of straw paintings not only exudes the aroma of the plant, and corrosion resistance; 3 wide range of sources of raw materials, plus short-circuit the process, the product is easy to manufacturing.

具体实施方式 detailed description

[0008] 下面结合具体实施例对本发明作进一步的说明: [0008] The following embodiments in conjunction with specific embodiments of the present invention is further described:

实施例1: Example 1:

制备本发明褐色麦秸杆染料的配方重量配比范围是:芙蓉花干10-30份、菘蓝10-30份、白矾10-30份、槟榔10-30份、铁离子化合物溶液5-15份、矿泉水30-80份。 Formulation ratio by weight of wheat straw brown dye preparation scope of the present invention are: 10-30 parts of dried hibiscus flowers, Isatis 10-30 parts, 10-30 parts of alum, 10-30 parts of betel nut, iron compound solution 5-15 parts, 30-80 parts of mineral water.

[0009] 实施例2: [0009] Example 2:

制备本发明褐色麦秸杆染料的配方优选重量配比范围是:芙蓉花干10-25份、菘蓝10-25份、白矾10-25份、槟榔10-25份、铁离子化合物溶液5_13份、矿泉水30-70份。 The preferred weight ratio range of formulations prepared wheat straw brown dyes of the present invention are: 10-25 parts of dried hibiscus flowers, Isatis 10-25 parts, 10-25 parts of alum, betel 10-25 parts, parts of iron compound solution 5_13 , mineral water 30-70 parts.

[0010] 实施例3: [0010] Example 3:

制备本发明褐色麦秸杆染料的配方最佳重量配比范围是:芙蓉花干15份、菘蓝15份、白矾15份、槟榔15份、柘黄15份、铁离子化合物溶液7份、矿泉水60份。 Formulation optimum range of the ratio by weight of wheat straw as a brown dye of the invention is: 15 parts dry hibiscus, Isatis 15 parts, 15 parts of alum, betel nut 15 parts, 15 parts of yellow Zhe, 7 parts of iron compound solution, mineral 60 parts of water.

[0011] 将上述各组份制成本发明褐色麦秸杆染料的生产方法,主要工艺流程为:选料、切料、烘干、浸泡、热煮、混合、沉淀、染色、成品,具体操作方法依次按下列步骤:A、选料、按原料重量配比,挑选符合国家卫生和质量标准的芙蓉花干、菘蓝、白矾、槟榔、铁离子化合物溶液、矿泉水备用、切料、将选出的原料除分别切成块状;C、烘干、将切成块状原料分别置于烘干炉中干化,温度控制在100-120°C,时间30分钟,蒸发原料水份、灭菌;D、浸泡、将烘干后的原料置于装有矿泉水的储槽中浸泡,温度为室20°C,时间2 - 3小时;E、热煮、将泡过的原料从水中捞出,放到陶器里热煮,时间6小时,煮出色素溶液;F、混合、将色素液侵入20%铁离子化合物溶液里,时间4-8小时,制成混合溶液;G、沉淀、将混合溶液凉至20°C,沉淀出纯净褐色素溶液、染色、将100 [0011] The cost of the components prepared above method for producing the invention's dye brown wheat straw, the main process are: choice of materials, cutting, drying, soaking, heat cooking, mixing, sedimentation, dyed, finished, the specific operation the method of the following steps in sequence: a, choice of materials, weight ratio of raw materials, selection of hibiscus flower dry compliance with national health and quality standards, Isatis, alum, betel nut, iron compound solution, mineral reserve, cutting, will be selected from the group in addition to the raw materials are cut into pieces; C, and drying the cut block material were placed in the drying oven temperature was controlled at 100-120 ° C, for 30 minutes, water was evaporated material, off bacteria; D, soaking, after drying the raw material placed in the reservoir with the mineral water soaking, room temperature 20 ° C, time 2 - 3 hours; E, boiled with water, soaked feedstock from water fishing out into the hot cooking of pottery, 6 hours, cook dye solution; F, mixing the dye solution of 20% ferric ions invade compound solution, and the time 4-8 hours, to prepare a mixed solution; G, precipitation, the mixed solution to cool to 20 ° C, the solution was precipitated pure brown pigment, dye, 100 升纯净褐色素溶液的温度渐渐升到80°C以上,将经过杀菌、脱硫、蒸煮处理后的麦秸杆浸泡其中,恒温静置12-14小时,期间将麦秸杆上下翻动,使麦秸杆充分吸收褐色素溶液,均匀染色;1、固色、将染色后的麦秸杆放入加入白矾粉沫的溶液中,浸泡3-6小时,使麦秸杆充分固色后捞出,淋干,在室温中慢慢干燥成褐色麦秸杆成品。 Liters of purified brown pigment temperature of the solution gradually rose to above 80 ° C, the pasteurized, desulfurization, after retorting soaked wheat straw wherein temperature was allowed to stand 12-14 hours, during which the turning down of wheat straw, wheat straw so brown pigment was fully absorbed lever, even dyeing; 1, fixing, the dyed wheat straw were added into a solution of alum powder, soaked 3-6 hours, the wheat straw was sufficiently remove fixation, pour dry, brown wheat straw was slowly dried at room temperature in the finished product.

Claims (4)

  1. 1.一种制备褐色麦秸杆染料的配方,其特征在于:它是由下述重量配比的原料制成的,芙蓉花干10-30份、菘蓝10-30份、白矾10-30份、槟榔10-30份、铁离子化合物溶液5_15份、矿泉水30-80份。 Formulation A brown dye preparation wheat straw, characterized in that: it is made by the following ratio by weight of the raw material, 10-30 parts of dried hibiscus flower, Isatis parts 10-30, 10-30 alum parts, 10-30 parts betel nut, iron parts 5_15 compound solution, 30 to 80 parts of mineral water.
  2. 2.一种制备褐色麦秸杆染料的配方,其特征在于:其中各种原料的重量配比是, 芙蓉花干10-25份、菘蓝10-25份、白矾10-25份、槟榔10-25份、铁离子化合物溶液5-13份、矿泉水30-70份。 A formulation was prepared wheat straw brown dye, wherein: wherein the weight ratio of the various raw materials is 10-25 parts dry hibiscus, Isatis 10-25 parts, 10-25 parts of alum, betel nut 10 -25 parts, 5-13 parts of a solution of iron compound, 30-70 parts of mineral water.
  3. 3.一种制备褐色麦秸杆染料的配方,其特征在于:其中各种原料的重量配比是, 芙蓉花干15份、菘蓝15份、白矾15份、槟榔15份、铁离子化合物溶液7份、矿泉水60份。 3. A process for preparing the formulation wheat straw brown dye, wherein: wherein the weight ratio of the various raw materials, the hibiscus 15 dry parts, 15 parts Isatis, alum 15 parts, 15 parts of betel nut, iron compound solution 7 parts, 60 parts of mineral water.
  4. 4.根据权利要求1-3所述的一种制备褐色麦秸杆染料配方的生产方法,其特征在于:主要工艺流程为:选料、切料、烘干、浸泡、热煮、混合、沉淀、染色、成品,具体操作方法依次按下列步骤:A、选料、按原料重量配比,挑选符合国家卫生和质量标准的芙蓉花干、菘蓝、白矾、槟榔、铁离子化合物溶液、矿泉水备用、切料、将选出的原料除分别切成块状;C、烘干、将切成块状原料分别置于烘干炉中干化,温度控制在100-120°C,时间30分钟,蒸发原料水份、灭菌;D、浸泡、将烘干后的原料置于装有矿泉水的储槽中浸泡,温度为室20°C,时间2 — 3小时;E、热煮、将泡过的原料从水中捞出,放到陶器里热煮,时间6小时,煮出色素溶液;F、混合、将色素液侵入20%铁离子化合物溶液里,时间4-8小时,制成混合溶液;G、沉淀、将混合溶液凉至20°C,沉淀出纯净褐 The production method of a wheat straw brown 1-3 for preparing a dye formulation as claimed in claim, wherein: Main process: material selection, cutting, drying, soaking, heat cooking, mixing, sedimentation , dyed, finished, the specific operation method of the following steps in sequence: a, choice of materials, weight ratio of raw materials, selection of hibiscus flower dry compliance with national health and quality standards, Isatis, alum, betel nut, iron compound solution, mineral water standby, cutting, respectively, the selected raw materials other cut block; C, and drying the cut block material were placed in the drying oven temperature was controlled at 100-120 ° C, 30 minutes evaporated material moisture sterilization; D, soaking, after drying the raw material placed in the reservoir with the mineral water soaking, room temperature 20 ° C, time 2 - 3 hours; E, boiled with water, the bubble remove water from the feedstock, into the hot cooking of pottery, 6 hours, cook dye solution; F, mixing the dye solution of 20% ferric ions invade compound solution, and the time 4-8 hours, to prepare a mixed solution; G, the precipitate, the mixed solution to cool to 20 ° C, the brown precipitate out pure 素溶液;H、染色、将100升纯净褐色素溶液的温度渐渐升到80°C以上,将经过杀菌、脱硫、蒸煮处理后的麦秸杆浸泡其中,恒温静置12-14小时,期间将麦秸杆上下翻动,使麦秸杆充分吸收褐色素溶液,均匀染色;1、固色、将染色后的麦秸杆放入加入白矾粉沫的溶液中,浸泡3-6小时,使麦秸杆充分固色后捞出,淋干,在室温中慢慢干燥成褐色麦秸杆成`品。 Su solution; H, dyeing, the temperature of 100 liters of purified brown pigment was gradually rise above 80 ° C, the pasteurized, desulfurization, after retorting soaked wheat straw wherein temperature was allowed to stand 12-14 hours, during wheat straw flip up and down the wheat straw brown pigment solution was fully absorbed, uniformly dyed; 1, fixing, the wheat straw was added into a solution of alum powder after dyeing, soaked 3-6 hours, the straw after sufficient fixing lever fish, pouring dry, brown wheat straw slowly dried to `product at room temperature.
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CN103804950A (en) * 2014-03-01 2014-05-21 哈尔滨市工艺美术有限责任公司 Dye capable of dyeing wheat straw into aged rose red and production method of dye
CN103804949A (en) * 2014-03-01 2014-05-21 哈尔滨市工艺美术有限责任公司 Dye for preparing bronze wheat straws and production method thereof
CN103804946A (en) * 2014-02-22 2014-05-21 哈尔滨市工艺美术有限责任公司 Formula and production method for preparing light khaki wheat straw dye
CN103804951A (en) * 2014-03-05 2014-05-21 哈尔滨市工艺美术有限责任公司 Wisteria-colored wheat straw dye and production method thereof
CN103804947A (en) * 2014-02-22 2014-05-21 哈尔滨市工艺美术有限责任公司 Formula and production method for preparing plum wheat straw dye
CN103819930A (en) * 2014-02-22 2014-05-28 哈尔滨市工艺美术有限责任公司 Formula for preparing plum red wheat straw dye and production method
CN103819932A (en) * 2014-03-05 2014-05-28 哈尔滨市工艺美术有限责任公司 Madder-red wheat straw dye and preparation method
CN103819931A (en) * 2014-02-26 2014-05-28 哈尔滨市工艺美术有限责任公司 Salmon wheat straw dye and production method
CN103834191A (en) * 2014-02-22 2014-06-04 哈尔滨市工艺美术有限责任公司 Formula and production method for preparing thistle purple wheat straw dye
CN103834193A (en) * 2014-02-27 2014-06-04 哈尔滨市工艺美术有限责任公司 Scarlet wheat straw dye and production method thereof
CN103834192A (en) * 2014-02-27 2014-06-04 哈尔滨市工艺美术有限责任公司 Ochre-yellow wheat straw dye and production method thereof
CN103865291A (en) * 2014-03-01 2014-06-18 哈尔滨市工艺美术有限责任公司 Navy-blue wheat straw dye and production method thereof
CN104085026A (en) * 2014-06-25 2014-10-08 安徽昌发实业有限公司 Betel juice-containing immersion liquid for reed modification, and use method thereof

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CN103773070A (en) * 2014-02-26 2014-05-07 哈尔滨市工艺美术有限责任公司 Light sky blue wheat straw dye and production method thereof
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CN103865291A (en) * 2014-03-01 2014-06-18 哈尔滨市工艺美术有限责任公司 Navy-blue wheat straw dye and production method thereof
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