CN104830154A - Water-soluble protective ink and preparation method thereof - Google Patents
Water-soluble protective ink and preparation method thereof Download PDFInfo
- Publication number
- CN104830154A CN104830154A CN201510236810.1A CN201510236810A CN104830154A CN 104830154 A CN104830154 A CN 104830154A CN 201510236810 A CN201510236810 A CN 201510236810A CN 104830154 A CN104830154 A CN 104830154A
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- China
- Prior art keywords
- water
- ink
- sodium hydroxide
- acrylic resin
- talcum powder
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/10—Printing inks based on artificial resins
- C09D11/106—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- C09D11/107—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds from unsaturated acids or derivatives thereof
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention provides water-soluble protective ink and a preparation method thereof. The water-soluble protective ink comprises the following raw materials in parts by weight: 35-40 parts of water-based acrylic resin, 25-30 parts of talcum powder, 2-2.5 parts of sodium hydroxide, 2-2.5 parts of a defoaming agent and 25-30 parts of water. The water-soluble protective ink disclosed by the invention has the advantages that the raw materials are readily available, the preparation process is simple and pungent smell is avoided.
Description
Technical field
The present invention relates to the technical field of protection ink, especially, relate to a kind of water-soluble protection ink and preparation method thereof.
Background technology
Water-soluble protection ink is a kind of printing ink on the glass surface, and energy available protecting glass surface, reduces and scratch.It is generally soluble in water, or is soluble in alkalescent water, but existing water-soluble protection printing ink to manufacture raw material is complicated, and cost of manufacture is higher, with irritating smell.
Such as, disclose a kind of formula in printing-ink of Chinese patent 201410627076.7 1 kinds of resistances to chemical attack and preparation method thereof, be made up of the raw material of following weight part:: ketone resin 15-18, ethyl p-hydroxybenzoate 3-5, propylene glycol phenylate 10-13, edible ethanol 25-35, Dodecyl Polyglucosides 6-9, Z 250 0.2-0.4, dibutyl tin laurate 0.1-0.3, W-Gum 1-3, barnyard grass stalk 7-9, Herba Lysimachiae foenumgraeci quintessence oil 0.03-0.06, Syzygium aromaticum stem oil 3-4, light calcium carbonate 4-7, talcum powder 3-6, pigment dyestuff 4-6, auxiliary agent 5-8; Described auxiliary agent is made up of following raw materials in part by weight: tree ash 5-8, irgasfos 168 0.3-0.6, permeate agent SF-1020.2-0.5, Magnesium Stearate 0.4-0.7, isocaprylic acid zinc 0.6-0.9, lauryl alcohol phosphoric acid ester potassium 1.1-2.1, tributyl phosphate 6-9, N-BUTYL ACETATE 7-10, benzylideneacetone 1-2, paraffin 3-4, paste dryer 2-3, peanut oil 2.3-3.5, propyl methocel 0.03-0.06, polybutene 2.1-3.6, propylene glycol 4-7.
Summary of the invention
The object of the invention is to provide a kind of water-soluble protection ink and preparation method thereof, to solve the technical problem of existing water-soluble protection printing ink to manufacture raw material complexity.
For achieving the above object, the invention provides a kind of water-soluble protection ink, comprise the raw material of following weight part:
Water-borne acrylic resin 35-40 part, talcum powder 25-30 part, sodium hydroxide 2-2.5 part, defoamer 2-2.5 part, water 25-30 part.
Preferably, described ink is only composed of the following components: water-borne acrylic resin 35-40 part, talcum powder 25-30 part, sodium hydroxide 2-2.5 part, defoamer 2-2.5 part, water 25-30 part; Without other components.
Preferably, the raw material of following weight part is comprised: water-borne acrylic resin 36-38 part, talcum powder 26-29 part, sodium hydroxide 2.1-2.3 part, defoamer 2.1-2.2 part, water 26-28 part.
Preferably, the raw material of following weight part is also comprised: osmanthus flower fragrance 5-8 part.
Preferably, described ink is only composed of the following components: water-borne acrylic resin 35-40 part, talcum powder 25-30 part, sodium hydroxide 2-2.5 part, defoamer 2-2.5 part, water 25-30 part, osmanthus flower fragrance 5-8 part; Without other components.
Preferably, sodium hydroxide is solid state.
Preferably, in said components ratio, the weight ratio of described water-borne acrylic resin and sodium hydroxide is 14.5-19:1.
According to the preparation method of above-mentioned water-soluble protection ink, comprise step:
A, according to respective weight ratio, by sodium hydroxide water dissolution, then mix disperseing machine with water-borne acrylic resin, dispersing speed is 200-600 rev/min, adds talcum powder during dispersion in batches;
B, add talcum powder after, the rotating speed of dispersion machine is adjusted to 600-1000 rev/min, dispersion 0.5-1 hour;
C, dispersing speed are adjusted to 200-600 rev/min, add defoamer; Obtain water-based ink.
Preferably, while adding defoamer in step C, add osmanthus flower fragrance.
Preferably, step is comprised after step C:
D, by scattered water-based ink three-roller grinding 2-4 time;
E, be disperse 0.5-1 hour in the dispersion machine of 200-600 rev/min at rotating speed by ground water-based ink.
The present invention has following beneficial effect:
The object that the present invention protects ink to add sodium hydroxide is modified aqueous acrylic acid resin, forms carboxylic acid sodium (sodium salt), strengthens the solubization of water-soluble protection oil; Ink ink is stablized, reduces print surface residual toxicity.
Water-soluble protection printing ink to manufacture raw material of the present invention is simple and easy to get, and printing ink to manufacture technique is simple, has no irritating odor, and slightly sweet osmanthus delicate fragrance.
Except object described above, feature and advantage, the present invention also has other object, feature and advantage.The present invention is further detailed explanation below.
Embodiment
Below embodiments of the invention are described in detail, but the multitude of different ways that the present invention can limit according to claim and cover is implemented.
This application provides a kind of water-soluble protection ink, comprise the raw material of following weight part:
Water-borne acrylic resin 35-40 part, talcum powder 25-30 part, sodium hydroxide 2-2.5 part, defoamer 2-2.5 part, water 25-30 part.
Preparation method: by 2-2.5 part sodium hydroxide 25-30 part water dissolution, then mix disperseing machine with 25-30 part water-borne acrylic resin, dispersing speed is 200-600 rev/min, add 25-30 part talcum powder during dispersion in batches, after adding talcum powder, the rotating speed of dispersion machine is adjusted to 600-1000 rev/min, disperses after 0.5-1 hour, dispersing speed is adjusted to 200-600 rev/min, adds 2-2.5 defoamer and 5-8 part osmanthus flower fragrance; Obtain water-based ink.
By scattered water-based ink three-roller grinding 2-4 time; Be disperse 0.5-1 hour in the dispersion machine of 200-600 rev/min at rotating speed by ground water-based ink.
Wherein, sodium hydroxide is the solid-state shapes such as pellet, sheet, bulk or granule, is easy to preserve.Defoamer is used for eliminating the foam in water color ink, can be commercially available general types.
Contriver finds in practice, and when the weight ratio of water-borne acrylic resin and sodium hydroxide is 14.5-19:1, ink protected effect is better.
For making ink fragrant, improving the pleasurable sensation of user, appropriate osmanthus flower fragrance can be added.
Specific embodiment component proportion can see table, and preparation method is all with above-mentioned.
The finished product obtained by above-described embodiment adopts screen painting, and spread upon sapphire surface, ink thickness is 6 ~ 12 μm, and being interrupted baking time is 60 ~ 90 minutes, and storing temperature is 180 ~ 220 DEG C.Then be immersed in respectively in 60 DEG C of warm water and 60 DEG C of alkalescent waters (PH=12), result of implementation is as shown in the table:
Usually time is shorter, illustrates that the cleaning difficulty of this ink is less; And usually time is too short, then illustrates that its water-absorbent is excessive, be unfavorable for that actual process is produced, the usually time (60 DEG C of warm water) of high-quality ink is generally about 2min on the market.Learn from upper table; this application claims the usually time (60 DEG C of warm water) of the ink of protection mostly between 45-80S, relatively commercial ink, had both reduced cleaning difficulty; being unlikely to again to carry out just producing obscission because absorbing water in process in follow-up production, polluting.
The foregoing is only the preferred embodiments of the present invention, be not limited to the present invention, for a person skilled in the art, the present invention can have various modifications and variations.Within the spirit and principles in the present invention all, any amendment done, equivalent replacement, improvement etc., all should be included within protection scope of the present invention.
Claims (9)
1. a water-soluble protection ink, is characterized in that, comprises the raw material of following weight part:
Water-borne acrylic resin 35-40 part, talcum powder 25-30 part, sodium hydroxide 2-2.5 part, defoamer 2-2.5 part, water 25-30 part.
2. a water-soluble protection ink, is characterized in that, described ink is composed of the following components:
Water-borne acrylic resin 35-40 part, talcum powder 25-30 part, sodium hydroxide 2-2.5 part, defoamer 2-2.5 part, water 25-30 part.
3. the water-soluble protection ink of one according to claim 1, is characterized in that, comprise the raw material of following weight part: water-borne acrylic resin 36-38 part, talcum powder 26-29 part, sodium hydroxide 2.1-2.3 part, defoamer 2.1-2.2 part, water 26-28 part.
4. the water-soluble protection ink of one according to claim 1, is characterized in that, also comprise the raw material of following weight part: osmanthus flower fragrance 5-8 part.
5. the water-soluble protection ink of one according to claim 1 and 2, is characterized in that, sodium hydroxide is solid state.
6. the water-soluble protection ink of one according to claim 1 and 2, is characterized in that, the weight ratio of described water-borne acrylic resin and sodium hydroxide is 14.5-19:1.
7. the preparation method of the water-soluble protection ink according to any one of claim 1-6, is characterized in that, comprise step:
A, according to respective weight ratio, by sodium hydroxide water dissolution, then mix in dispersion machine with water-borne acrylic resin, dispersing speed is 200-600 rev/min, adds talcum powder during dispersion in batches;
B, add talcum powder after, the rotating speed of dispersion machine is adjusted to 600-1000 rev/min, dispersion 0.5-1 hour;
C, dispersing speed are adjusted to 200-600 rev/min, add defoamer; Obtain water-based ink.
8. preparation method according to claim 7, is characterized in that, while adding defoamer, adds osmanthus flower fragrance in step C.
9. preparation method according to claim 7, is characterized in that, comprises step after step C:
D, by scattered water-based ink three-roller grinding 2-4 time;
E, be disperse 0.5-1 hour in the dispersion machine of 200-600 rev/min at rotating speed by ground water-based ink.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510236810.1A CN104830154A (en) | 2015-05-11 | 2015-05-11 | Water-soluble protective ink and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510236810.1A CN104830154A (en) | 2015-05-11 | 2015-05-11 | Water-soluble protective ink and preparation method thereof |
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| CN104830154A true CN104830154A (en) | 2015-08-12 |
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| CN201510236810.1A Pending CN104830154A (en) | 2015-05-11 | 2015-05-11 | Water-soluble protective ink and preparation method thereof |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105087162A (en) * | 2015-08-28 | 2015-11-25 | 上海应用技术学院 | Osmanthus flower essence for water-based ink and preparing method of osmanthus flower essence |
| CN105348959A (en) * | 2015-11-02 | 2016-02-24 | 蓝思科技（长沙）有限公司 | Fast-drying water-soluble glass protection glue and preparation method thereof |
| CN105368201A (en) * | 2015-11-02 | 2016-03-02 | 蓝思科技（长沙）有限公司 | Temperature resistance type water-soluble glass protection glue and preparation method |
| CN111690293A (en) * | 2020-05-27 | 2020-09-22 | 鹤山市科鼎功能材料有限公司 | Resin for washable glass temporary protection ink and preparation method thereof |
| CN114316675A (en) * | 2022-01-21 | 2022-04-12 | 东莞市蓝邦电子五金材料有限公司 | Water-based protective ink and construction process |
| CN114907718A (en) * | 2021-07-08 | 2022-08-16 | 佛山市三水峻丙涂料有限公司 | Water-based ink and application thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101092531A (en) * | 2007-07-19 | 2007-12-26 | 王兆进 | Low temperature solidified glass printing ink in single constituent |
-
2015
- 2015-05-11 CN CN201510236810.1A patent/CN104830154A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101092531A (en) * | 2007-07-19 | 2007-12-26 | 王兆进 | Low temperature solidified glass printing ink in single constituent |
Non-Patent Citations (1)
| Title |
|---|
| 曹欣祥: "水性油墨用水性丙烯酸树脂的制备及性能研究", 《中国优秀硕士学位论文全文数据库 工程科技I辑》 * |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105087162A (en) * | 2015-08-28 | 2015-11-25 | 上海应用技术学院 | Osmanthus flower essence for water-based ink and preparing method of osmanthus flower essence |
| CN105348959A (en) * | 2015-11-02 | 2016-02-24 | 蓝思科技（长沙）有限公司 | Fast-drying water-soluble glass protection glue and preparation method thereof |
| CN105368201A (en) * | 2015-11-02 | 2016-03-02 | 蓝思科技（长沙）有限公司 | Temperature resistance type water-soluble glass protection glue and preparation method |
| CN105348959B (en) * | 2015-11-02 | 2017-12-29 | 蓝思科技（长沙）有限公司 | Quick-dry type water-soluble glass Protection glue and preparation method |
| CN111690293A (en) * | 2020-05-27 | 2020-09-22 | 鹤山市科鼎功能材料有限公司 | Resin for washable glass temporary protection ink and preparation method thereof |
| CN114907718A (en) * | 2021-07-08 | 2022-08-16 | 佛山市三水峻丙涂料有限公司 | Water-based ink and application thereof |
| CN114316675A (en) * | 2022-01-21 | 2022-04-12 | 东莞市蓝邦电子五金材料有限公司 | Water-based protective ink and construction process |
| CN114316675B (en) * | 2022-01-21 | 2023-08-04 | 东莞市蓝邦电子五金材料有限公司 | Water-based protective ink and construction process |
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Application publication date: 20150812 |