CN104479465A - Preparation method of natural edible film formers for ecological body painting pigments - Google Patents
Preparation method of natural edible film formers for ecological body painting pigments Download PDFInfo
- Publication number
- CN104479465A CN104479465A CN201410809492.9A CN201410809492A CN104479465A CN 104479465 A CN104479465 A CN 104479465A CN 201410809492 A CN201410809492 A CN 201410809492A CN 104479465 A CN104479465 A CN 104479465A
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- CN
- China
- Prior art keywords
- film forming
- protein
- forming matter
- ecological body
- specially
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D103/00—Coating compositions based on starch, amylose or amylopectin or on their derivatives or degradation products
- C09D103/02—Starch; Degradation products thereof, e.g. dextrin
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D105/00—Coating compositions based on polysaccharides or on their derivatives, not provided for in groups C09D101/00 or C09D103/00
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Medicinal Preparation (AREA)
Abstract
The invention relates to a preparation method of natural edible film formers for ecological body painting pigments. The preparation method comprises steps as follows: (1) a polysaccharide substance, a plasticizer and an enhancer are stirred and gelatinized in a certain ratio at a certain temperature for a certain period, and then a natural edible film former for water-based painting pigments is prepared through vacuum degassing; (2) natural vegetable oil is used as a solvent, and a certain amount of lipids are dissolved to be used as an oil phase; the polysaccharide substance, a protein substance, the plasticizer, the enhancer and the like are added to an aqueous phase; then the aqueous phase is dropwise added to the oil phase for emulsification, and a natural edible film former for oil-based painting pigments is prepared.
Description
Technical field
The present invention relates to a kind of preparation method of the edible natural film forming matter for ecological body paint, the exploitation of environment-friendly type art painting can be widely used in, and environmental protection, the production of nontoxic, natural coating for wall surface and application.
Background technology
The material that tradition colored drawing uses is acrylic paints, oil colour and moisture pigment etc. mostly, and wherein the use of acrylic paints is maximum.Its main film forming substance is acrylate and acrylic copolymeric resin, and the arguement in recent years for acrylic paints security becomes focus, comprises the stimulation to human body skin and mucous membrane, repeatedly contacts the chronic toxicity and carinogenicity that cause and the harm to environment.
In natural colored drawing coating, generally all adopt natural Plants and Animals lipid acid and natural resin, processing modified through different process, obtain more satisfactory natural filmogen material, even reach edible rank.Edible film is for raw material with edible natural material (as polysaccharide, protein, lipoid etc.), by in molecule and molecular interaction and the some strength that has that formed has the film of network structure, optionally choke, resistance is provided to wet, hinder content diffusion and deaden the several functions such as the objectionable impurities of external environment, and there is good physical and mechanical properties, thus as the main component of body painting coating, and can serve as effective carrier for other compositions in coating.
Summary of the invention
The present invention relates to a kind of preparation method of the edible natural film forming matter for ecological body paint, described preparation method comprises the steps: that (1) polysaccharose substance, softening agent and toughener stir gelatinization according to certain proportioning under certain temperature, and held for some time; Then vacuum outgas, i.e. the edible natural film forming matter of obtained water-based coloured drawing pigment; (2) be solvent with crude vegetal, dissolve a certain amount of lipoid as oil phase; Polysaccharose substance, protein matter, softening agent and toughener etc. are added in aqueous phase; Then aqueous phase is dropwise joined emulsification in oil phase, i.e. the edible natural film forming matter of obtained oiliness coloured drawing pigment.
For an ecological body paint's edible natural film forming matter, it is characterized in that described polysaccharose substance is specially one or more mixtures of tapioca (flour), W-Gum, yam starch, gum arabic, yellow collagen, chitin, chitosan etc.
A kind of edible natural film forming matter for ecological body paint, it is characterized in that described protein substance is based on animal protein isolate or plant separation protein, is specially one or more mixtures of collagen protein, gelatin, soybean protein, mucedin, casein etc.
For an ecological body paint's edible natural film forming matter, it is characterized in that described lipid material is specially one or more mixtures of gutta-percha, beeswax, carnauba wax, insect wax, Jojoba oil, phosphatide etc.
For an ecological body paint's edible natural film forming matter, it is characterized in that described softening agent is glycerine; Toughener is specially one or more mixtures of sodium alginate (Alg-Na), Xylo-Mucine (CMC-Na), methylcellulose gum (MC) etc.
Embodiment
Embodiment 1
(1) take 2.0g tapioca (flour), be placed in the there-necked flask with whipping appts, and add 40mL deionized water, under normal temperature, stir into starch milk.
(2) in the obtained starch milk of step (1), add 6mL CMC-Na solution successively, 1.2mL glycerine solution and 4mL xanthan gum solution, and fully stir, at gelatinization point 69 DEG C, be incubated 3h.
(3) namely vacuum outgas 30min obtains the edible natural film forming matter of water-based coloured drawing pigment.
Embodiment 2
(1) in cable type extractor according, add appropriate Cortex Eucommiae, slowly drip sherwood oil, oil bath pan temperature is adjusted to 70 DEG C, reaction 12h.Extract and terminate the yellow liquid recrystallization obtained removing impurity to obtain transparent liquid, drying and volatilizing removing petroleum ether solvent, obtains white colloidal and gutta-percha.
(2) by 2.0g gutta-percha, 55mL sweet oil and 40mL linseed oil, be placed in the there-necked flask with whipping appts, fully stir at 60 DEG C, stirring velocity is 400r/min.
(3) by 80mL deionized water, 5g gum arabic, 5mL glycerine, 0.5g gelatin, 0.3gCMC-Na and 0.1g Alg-Na, be placed in the there-necked flask with whipping appts, fully stir at 60 DEG C, stirring velocity is 400r/min.
(4) carry out emulsification in utilize constant pressure funnel to be added drop-wise to by the mixing solutions that step (3) obtains mixing solutions that step (2) obtains, stirring velocity is 600r/min.
(5) dropwise, by emulsion homogeneous 5min under the stirring velocity of 200r/min, regulate its denseness, obtain the edible natural film forming matter of oiliness coloured drawing pigment.
Claims (4)
1., for an ecological body paint's edible natural film forming matter, it is characterized in that described polysaccharose substance is specially one or more mixtures of tapioca (flour), W-Gum, yam starch, gum arabic, yellow collagen, chitin, chitosan etc.
2. the edible natural film forming matter for ecological body paint, it is characterized in that described protein substance is based on animal protein isolate or plant separation protein, is specially one or more mixtures of collagen protein, gelatin, soybean protein, mucedin, casein etc.
3., for an ecological body paint's edible natural film forming matter, it is characterized in that described lipid material is specially one or more mixtures of gutta-percha, beeswax, carnauba wax, insect wax, Jojoba oil, phosphatide etc.
4., for an ecological body paint's edible natural film forming matter, it is characterized in that described softening agent is glycerine; Toughener is specially one or more mixtures of sodium alginate (Alg-Na), Xylo-Mucine (CMC-Na), methylcellulose gum (MC) etc.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410809492.9A CN104479465A (en) | 2014-12-23 | 2014-12-23 | Preparation method of natural edible film formers for ecological body painting pigments |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410809492.9A CN104479465A (en) | 2014-12-23 | 2014-12-23 | Preparation method of natural edible film formers for ecological body painting pigments |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104479465A true CN104479465A (en) | 2015-04-01 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410809492.9A Pending CN104479465A (en) | 2014-12-23 | 2014-12-23 | Preparation method of natural edible film formers for ecological body painting pigments |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104479465A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105238143A (en) * | 2015-11-19 | 2016-01-13 | 成都海娜文化传播有限公司 | Body painting pigment |
| CN111303674A (en) * | 2020-03-20 | 2020-06-19 | 宁波俊瑆玩具科技有限公司 | Human body colored drawing composition and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20040043134A1 (en) * | 2002-08-27 | 2004-03-04 | Corriveau Christine Leclair | Rolled edible thin film products and methods of making same |
| CN101899173A (en) * | 2010-07-16 | 2010-12-01 | 山东农业大学 | Edible starch-based food packaging film and preparation method thereof |
| CN103450506A (en) * | 2013-08-23 | 2013-12-18 | 吴江市英力达塑料包装有限公司 | Instant noodles seasoning packaging film and preparation method thereof |
| CN104151623A (en) * | 2014-07-29 | 2014-11-19 | 石芬 | Edible instant nutritional seasoning package film and preparation method thereof |
-
2014
- 2014-12-23 CN CN201410809492.9A patent/CN104479465A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20040043134A1 (en) * | 2002-08-27 | 2004-03-04 | Corriveau Christine Leclair | Rolled edible thin film products and methods of making same |
| CN101899173A (en) * | 2010-07-16 | 2010-12-01 | 山东农业大学 | Edible starch-based food packaging film and preparation method thereof |
| CN103450506A (en) * | 2013-08-23 | 2013-12-18 | 吴江市英力达塑料包装有限公司 | Instant noodles seasoning packaging film and preparation method thereof |
| CN104151623A (en) * | 2014-07-29 | 2014-11-19 | 石芬 | Edible instant nutritional seasoning package film and preparation method thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105238143A (en) * | 2015-11-19 | 2016-01-13 | 成都海娜文化传播有限公司 | Body painting pigment |
| CN111303674A (en) * | 2020-03-20 | 2020-06-19 | 宁波俊瑆玩具科技有限公司 | Human body colored drawing composition and preparation method thereof |
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Application publication date: 20150401 |
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