CN104773997B - A kind of preparation method for twisting tire ceramic antique bricks - Google Patents
A kind of preparation method for twisting tire ceramic antique bricks Download PDFInfo
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- CN104773997B CN104773997B CN201510150405.8A CN201510150405A CN104773997B CN 104773997 B CN104773997 B CN 104773997B CN 201510150405 A CN201510150405 A CN 201510150405A CN 104773997 B CN104773997 B CN 104773997B
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Abstract
The present invention relates to a kind of preparation method for twisting tire ceramic antique bricks, its step is as follows：1) raw material is crushed respectively, crosses 250 mesh sieves, and be well mixed, obtain compound；2) compound is placed in vacuum deairing machine the pugging that adds water, obtains uniform mud bar, blank is obtained after ageing；3) blank is divided into n parts (n >=2), a copy of it is designated as blank 1, remaining blank adds different colorant puggings respectively, obtains colored mud bar, blank 2 is obtained after ageing ..., n (n >=2)；4) with mixing pugging machine by blank 1 and blank 2 ..., n is stranded, obtains colour mixture mud bar；5) colour mixture mud bar is put into gypsum mold, is molded using plastic compression method, obtains green compact；6) apply clear frit after green compact are dried, then be placed in fired in roller kilns after obtain twisting tire ceramic antique bricks.Present invention process is simple, and firing temperature is low, and prepared strand tire ceramic antique bricks good decorating effect, water absorption rate are low.
Description
Technical field
The present invention relates to a kind of preparation method for twisting tire ceramic antique bricks.
Background technology
With the continuous improvement of living standard, people for the building and ornament materials such as Ceramic Tiles requirement also more and more higher,
Health, environmental protection, the Ceramic Tiles of good texture are welcome by consumption market deeply.Antique Imitation Tiles are imbued with individuality formation because of its decoration, contain history
And the art of culture, increasingly liked by people.The production of general high-grade ceramic Antique Imitation Tiles need to carry out incrustation to it
(the problems such as needing to consider glaze fit), then kiln-firing are formed.Color glaze is not applied in preparation, which or not can be presented the ceramics of antique effect
Antique Imitation Tiles, can simplify the technological process of ceramic antique bricks, significant to preparing for ceramic antique bricks.
Twist tire skill and appear in the Tang Dynasty, prosperous in the Song dynasty, it is using being interlinked to the outside in preparing by hand, with grain decorating effect
The skill and technique of fruit ceramics.Ceramic is drastically increased by the texture structure and color change that twist the acquisition of tire skill
Artistic decorative effect.Chinese patent CN101722788A discloses a kind of using tire skill is twisted, and prepares what is be interlinked to the outside with
The texture of determination and the strand tire porcelain of pattern.It uses artisan craftsmanship, with the tire soil mutually stranded shaping of multiple color, will carry face
The mud section splicing of texture between form and aspect, which turns into, determines pattern, and firing 8~10h in 1280~1300 DEG C has prepared with birds
The strand tire porcelain of pattern.Chinese patent CN 103057343A disclose a kind of artisan craftsmanship for twisting the natural decorative pattern of tire artistic porcelain and made
Method.It uses multiple color color mud, is molded after kneading by throwing, and roasting has prepared class agate effect and marble certainly
The strand tire porcelain of right line.
European patent EP 1731330A3 discloses a kind of method for preparing ceramic antique bricks, uses clay, flux, quartz
Ceramic Tiles green compact are prepared, green surface is imposed on as base glaze for 30% quartzy slurry using water content, is filled using inorganic color
Decorations, ceramic antique bricks are prepared for by secondary.Its need to carry out secondary firing and first firing temperature it is higher (900~
1000℃).Chinese patent CN103073263A discloses a kind of method that utilization various solid wastes manufacture ceramic antique bricks,
Water absorption rate ＜ 0.5% ceramic antique bricks are produced using useless mud, useless brick, polishing slag and flyash etc., production cost is low, but its
There is level to match somebody with somebody to powder to require, and firing range is narrower, is 1185~1195 DEG C.
The content of the invention
The technical problems to be solved by the invention are to twist tire pottery there is provided one kind for above shortcomings in the prior art
The preparation method of porcelain Antique Imitation Tiles, the ceramic antique bricks with alternate streak decoration effect are prepared by twisting tire technique.
In order to solve the above technical problems, the technical scheme that the present invention is provided is：
A kind of preparation method for twisting tire ceramic antique bricks is provided, its step is as follows：
1) raw material is crushed respectively, crosses 250 mesh sieves, and be well mixed, obtain compound, the raw material includes following weight
The material component of content：Diopside 23~35%, kaolin 35~45%, attaclay 5~15%, feldspar 7~11%, quartz
Sand 8~13%；
2) by step 1) gained compound is placed in vacuum deairing machine the pugging that adds water, and the quality of water is the 10 of mixture quality
~13%, uniform mud bar is obtained, blank is obtained after ageing；
3) by step 2) gained blank be divided into n parts (n >=2), a copy of it is designated as blank 1, and remaining blank adds difference respectively
Colorant pugging, obtain colored mud bar, blank 2 obtained after ageing ..., n (n >=2)；
4) with mixing pugging machine by step 3) gained blank 1 and blank 2 ..., n (n >=2) is stranded, obtains colour mixture mud bar；
5) by step 4) gained colour mixture mud bar be put into gypsum mold, using plastic compression method be molded, obtain green compact；
6) by step 5) gained green compact apply clear frit after drying, then be placed in fired in roller kilns after obtain twisting tire ceramic antique
Brick.
By such scheme, step 1) the kaolin iron-holder be less than 1.6wt%；The attaclay iron-holder is less than
1.2wt%.
By such scheme, step 2) a diameter of 20~30mm of mud bar, length is 200~300mm；Step 3) band
A diameter of 20~the 30mm of color mud bar, length is 200~300mm.
By such scheme, step 2) and step 3) digestion time be 48~72h.
By such scheme, step 3) colorant be manganese red, cobalt blue and chrome green in one kind, colorant quality be respective blanks
The 2~4% of quality, colorant average grain diameter is 1~10 μm.
By such scheme, step 4) a diameter of 40~60mm of colour mixture mud bar, length is 200~300mm.
By such scheme, step 5) green surface for square, the square length of side be 300~400mm.
By such scheme, step 5) the plastic compression method molding technological condition is：Application pressure is 7~8MPa, dwell time
For 5s.
By such scheme, step 6) drying condition be 100 DEG C at dry 24h；The firing condition be 1150~
1250 DEG C of 20~24h of firing.
The present invention also provides the strand tire ceramic antique bricks prepared according to the above method, and it meets standard GB/T/T
The requirement of BIa classes Imitation Rock Porcelain Tiles in 4100-2006.
The beneficial effects of the present invention are：1st, the present invention will twist tire technique and be used to prepare architectural pottery Antique Imitation Tiles, shaping side
Method is simple, and firing temperature is low (1150~1250 DEG C), and technological process is short, and largely avoid conventionally spray-dried and brought
Dust pollution, environment-friendly effect is obvious；2nd, the ceramic antique bricks prepared by the present invention have alternate texture, elegant in appearance,
Natural antique effect is good, and water absorption rate is low (water absorption rate ＜ 0.5%), is porcelain ceramic antique bricks.
Brief description of the drawings
Fig. 1 is that the embodiment of the present invention 1 prepares the schematic diagram for twisting tire ceramic antique bricks.
Embodiment
To make those skilled in the art more fully understand technical scheme, the present invention is made below in conjunction with the accompanying drawings into
One step is described in detail.
Kaolin iron-holder used by the embodiment of the present invention is 1.5wt%, and attaclay iron-holder used is 1.1wt%.
Embodiment 1
A kind of manufacture method for twisting tire ceramic antique bricks, step is as follows：
1) by raw material according to mass percent：Diopside 35%, kaolin 41%, attaclay 6%, feldspar 7%, quartz
The ratio feeding of sand 11%, is crushed respectively, crosses 250 mesh sieves, and is well mixed, and obtains compound；
2) by step 1) gained compound is placed in vacuum deairing machine the pugging that adds water, and amount of water is mixture quality
12%, obtain blank (Φ 20mm, length 300mm) after obtaining uniform mud bar, ageing 48h；
3) by step 2) gained blank be divided into 2 parts, a copy of it is designated as blank 1, another additional 3% zaffre
(1 μm of colorant average grain diameter) pugging, blank 2 (Φ 20mm, length 300mm) is obtained after obtaining colored mud bar, ageing 48h；
4) with mixing pugging machine by step 3) gained blank 1 and blank 2 it is stranded, obtain colour mixture mud bar (Φ 40mm, length
300mm)；
5) by step 4) gained colour mixture mud bar be put into gypsum mold (internal diameter size is 300*300mm), using plastic compression method
Shaping, obtaining green compact by 500t hydraulic presses application 8MPa pressure, after pressurize 5s, (green surface is square, square side
A length of 300mm)；
6) by step 5) gained green compact are placed in drying box in applying clear frit after 100 DEG C of dry 24h, then be placed in roller kilns
Fired in 1150 DEG C and the strand tire ceramic antique bricks with blue white alternate decorative stripe are obtained after 22h.It is the present embodiment as shown in Figure 1
Prepare the schematic diagram for twisting tire ceramic antique bricks.
After tested, ceramic antique bricks water absorption rate of the invention is 0.39%, is porcelain tile；Bending strength is 52MPa, symbol
Close the requirement of BIa class Imitation Rock Porcelain Tiles in standard GB/T/T 4100-2006.
Embodiment 2
A kind of manufacture method for twisting tire ceramic antique bricks, step is as follows：
1) by raw material according to mass percent：Diopside 28%, kaolin 39%, attaclay 9%, feldspar 11%, stone
The ratio feeding of sand 13%, is crushed respectively, crosses 250 mesh sieves, and is well mixed, and obtains compound；
2) by step 1) gained compound part is placed in vacuum deairing machine the pugging that adds water, and amount of water is mixture quality
13%, obtain blank (Φ 30mm, length 200mm) after obtaining uniform mud bar, ageing 52h；
3) by step 2) gained blank be divided into 2 parts, a copy of it is designated as blank 1, another additional 4% manganese red colorant
(10 μm of colorant average grain diameter) pugging, blank 2 (Φ 30mm, length 200mm) is obtained after obtaining colored mud bar, ageing 52h；
4) with mixing pugging machine by step 3) the gained blank 2 of blank 1 is stranded, obtains colour mixture mud bar (Φ 60mm, length
200mm)；
5) by step 4) gained colour mixture mud bar be put into gypsum mold, using plastic compression method be molded, by 500t hydraulic presses
Apply and green compact are obtained after 8MPa pressure, pressurize 5s (green surface is square, and the square length of side is 400mm)；
6) by step 5) gained green compact are placed in drying box in applying clear frit after 100 DEG C of dry 24h, then be placed in roller kilns
The strand tire ceramic antique bricks with decorative stripe red and white are obtained after firing 24h in 1250 DEG C.
After tested, ceramic antique bricks water absorption rate of the invention is 0.27%, is porcelain tile；Bending strength is 64MPa, symbol
Close the requirement of BIa class Imitation Rock Porcelain Tiles in standard GB/T/T 4100-2006.
Embodiment 3
A kind of manufacture method for twisting tire ceramic antique bricks, step is as follows：
1) by raw material according to mass percent：Diopside 23%, kaolin 45%, attaclay 13%, feldspar 9%, stone
The ratio feeding of sand 10%, is crushed respectively, crosses 250 mesh sieves, and is well mixed, and obtains compound；
2) by step 1) gained compound is placed in vacuum deairing machine the pugging that adds water, and amount of water is mixture quality
13%, obtain blank (Φ 20mm, length 300mm) after obtaining uniform mud bar, ageing 64h；
3) by step 2) gained blank be divided into 2 parts, a copy of it is designated as blank 1, another additional 2% chrome green colorant
(colorant average grain diameter is 5 μm) pugging, blank 2 (Φ 20mm, length 300mm) is obtained after obtaining colored mud bar, ageing 64h；
4) with mixing pugging machine by step 3) the gained blank 2 of blank 1 and 3 is stranded, obtains colour mixture mud bar (Φ 40mm, length
300mm)；
5) by step 4) gained colour mixture mud bar be put into gypsum mold, using plastic compression method be molded, by 500t hydraulic presses
Apply and green compact are obtained after 7MPa pressure, pressurize 5s (green surface is square, and the square length of side is 300mm)；
6) by step 5) gained green compact are placed in drying box in applying clear frit after 100 DEG C of dry 24h, then be placed in roller kilns
Fired in 1190 DEG C and the strand tire ceramic antique bricks with green white alternate decorative stripe are obtained after 21h.
After tested, ceramic antique bricks water absorption rate of the invention is 0.23%, is porcelain tile；Bending strength is 67MPa, symbol
Close the requirement of BIa class Imitation Rock Porcelain Tiles in standard GB/T/T 4100-2006.
Embodiment 4
A kind of manufacture method for twisting tire ceramic antique bricks, step is as follows：
1) by raw material according to mass percent：Diopside 32%, kaolin 37%, attaclay 14%, feldspar 9%, stone
The ratio feeding of sand 8%, is crushed respectively, crosses 250 mesh sieves, and is well mixed, and obtains compound；
2) by step 1) gained compound is placed in vacuum deairing machine the pugging that adds water, and amount of water is mixture quality
11%, obtain blank (Φ 30mm, length 200mm) after obtaining uniform mud bar, ageing 72h；
3) by step 2) gained blank is divided into 3 parts, and a copy of it is designated as blank 1, the manganese red colorant (color of portion additional 2%
It is 1~10 μm to expect average grain diameter) pugging, blank 2 (Φ 30mm, length 200mm) is obtained after obtaining colored mud bar, ageing 72h, separately
Zaffre (colorant average grain diameter is 1~10 μm) pugging of outer portion additional 2%, is obtained after obtaining colored mud bar, ageing 72h
Blank 3 (Φ 30mm, length 200mm)；
4) with mixing pugging machine by step 3) gained blank 1 and blank 2 and blank 3 it is stranded, obtain colour mixture mud bar (Φ
60mm, length 200mm)；
5) by step 4) gained colour mixture mud bar be put into gypsum mold, using plastic compression method be molded, by 500t hydraulic presses
Apply and green compact are obtained after 7MPa pressure, pressurize 5s (green surface is square, and the square length of side is 300mm)；
6) by step 5) gained green compact are placed in drying box in applying clear frit after 100 DEG C of dry 24h, then be placed in roller kilns
Fired in 1200 DEG C and the strand tire ceramic antique bricks with green white alternate decorative stripe are obtained after 20h.
After tested, ceramic antique bricks water absorption rate of the invention is 0.15%, is porcelain tile；Bending strength is 66MPa, symbol
Close the requirement of BIa class Imitation Rock Porcelain Tiles in standard GB/T/T 4100-2006.
Each raw material cited by the present invention, and each raw material of the invention value interval up and down, and technological parameter (slurry
Moisture content, the mesh sieve of mud 250 are tailed over) bound, interval value can realize the present invention, it is numerous to list herein.
Claims (10)
1. a kind of preparation method for twisting tire ceramic antique bricks, it is characterised in that step is as follows：
1) raw material is crushed respectively, crosses 250 mesh sieves, and be well mixed, obtain compound, the raw material includes following weight content
Material component：Diopside 23~35%, kaolin 35~45%, attaclay 5~15%, feldspar 7~11%, quartz sand 8
~13%；
2) by step 1) gained compound is placed in vacuum deairing machine the pugging that adds water, the quality of water for mixture quality 10~
13%, uniform mud bar is obtained, blank is obtained after ageing；
3) by step 2) gained blank be divided into n parts, n >=2, a copy of it is designated as blank 1, and remaining blank adds different colorants respectively
Pugging, obtains colored mud bar, blank 2 is obtained after ageing ..., n；
4) with mixing pugging machine by step 3) gained blank 1 and blank 2 ..., n is stranded, obtains colour mixture mud bar；
5) by step 4) gained colour mixture mud bar be put into gypsum mold, using plastic compression method be molded, obtain green compact；
6) by step 5) gained green compact apply clear frit after drying, then be placed in fired in roller kilns after obtain twisting tire ceramic antique bricks.
2. the preparation method according to claim 1 for twisting tire ceramic antique bricks, it is characterised in that：Step 1) kaolin
Iron-holder is less than 1.6wt%；The attaclay iron-holder is less than 1.2wt%.
3. the preparation method according to claim 1 for twisting tire ceramic antique bricks, it is characterised in that：Step 2) the mud bar is straight
Footpath is 20~30mm, and length is 200~300mm；Step 3) the colored a diameter of 20~30mm of mud bar, length be 200~
300mm。
4. the preparation method according to claim 1 for twisting tire ceramic antique bricks, it is characterised in that：Step 2) and step 3) institute
Digestion time is stated for 48~72h.
5. the preparation method according to claim 1 for twisting tire ceramic antique bricks, it is characterised in that：Step 3) colorant is
One kind in manganese red, cobalt blue and chrome green, colorant quality is the 2~4% of respective blanks quality, and colorant average grain diameter is 1~10 μm.
6. the preparation method according to claim 1 for twisting tire ceramic antique bricks, it is characterised in that：Step 4) the colour mixture mud
A diameter of 40~the 60mm of bar, length is 200~300mm.
7. the preparation method according to claim 1 for twisting tire ceramic antique bricks, it is characterised in that：Step 5) the green compact table
Face is square, and the square length of side is 300~400mm.
8. the preparation method according to claim 1 for twisting tire ceramic antique bricks, it is characterised in that step 5) the plastic compression method
Molding technological condition is：Application pressure is 7~8MPa, and the dwell time is 5s.
9. the preparation method according to claim 1 for twisting tire ceramic antique bricks, it is characterised in that：Step 6) dried strip
Part is dry 24h at 100 DEG C；The firing condition is 1150~1250 DEG C of 20~24h of firing.
10. one kind twists tire ceramic antique bricks, it is characterised in that prepared according to any methods describeds of claim 1-9, it is accorded with
Close the requirement of BIa class Imitation Rock Porcelain Tiles in standard GB/T/T 4100-2006.
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| CN201510150405.8A CN104773997B (en) | 2015-03-31 | 2015-03-31 | A kind of preparation method for twisting tire ceramic antique bricks |
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| CN201510150405.8A CN104773997B (en) | 2015-03-31 | 2015-03-31 | A kind of preparation method for twisting tire ceramic antique bricks |
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| CN104773997B true CN104773997B (en) | 2017-07-11 |
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Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105174971B (en) * | 2015-09-07 | 2018-03-06 | 山东硅元新型材料股份有限公司 | Twist the preparation method of tire ceramics |
| CN106007659A (en) * | 2016-05-17 | 2016-10-12 | 岑溪市新建球陶瓷有限公司 | Preparation method of archaized brick |
| CN106007667A (en) * | 2016-05-17 | 2016-10-12 | 岑溪市新建球陶瓷有限公司 | Archaized brick |
| CN106242499A (en) * | 2016-07-05 | 2016-12-21 | 吴勇龙 | A kind of production technology twisting tire porcelain |
| CN114248332A (en) * | 2020-09-24 | 2022-03-29 | 郭自敏 | Method for manufacturing antique brick carving by using twister technique |
| CN112390529A (en) * | 2020-12-02 | 2021-02-23 | 重庆唯美陶瓷有限公司 | Porcelain matte archaized brick and manufacturing method thereof |
| CN112851301A (en) * | 2021-01-18 | 2021-05-28 | 湖南省醴陵市兆荣瓷业有限公司 | Manufacturing method and formula of archaized tile |
| CN113087493A (en) * | 2021-04-02 | 2021-07-09 | 陕西科技大学 | Whole-body antique porcelain tile with imitated twisted tire natural ornamentation and preparation method thereof |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1297510C (en) * | 2004-06-18 | 2007-01-31 | 孟庆洪 | Blank with grinding placenta stone, products of grinding placenta stone and method for producing same |
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