CN104630934A - Flame resistant fabric material and preparation method thereof - Google Patents
Flame resistant fabric material and preparation method thereof Download PDFInfo
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- CN104630934A CN104630934A CN201510100311.XA CN201510100311A CN104630934A CN 104630934 A CN104630934 A CN 104630934A CN 201510100311 A CN201510100311 A CN 201510100311A CN 104630934 A CN104630934 A CN 104630934A
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Abstract
The invention discloses a flame resistant fabric material and a preparation method thereof. The flame resistant fabric material is prepared from the following components in parts by weight: 78-93 parts of PBT (polybutylece terephthalate), 45-68 parts of polyacrylamide, 12-25 parts of trimethylolpropane, 8-14 parts of cyanoethyl cellulose, 5-18 parts of zinc oxide, 2-5 parts of melamine, 1-3 parts of diphenyl methane diisocyanate and 150-175 parts of acetone. The invention further provides a preparation method of the flame resistant fabric material, and the preparation method comprises the following steps: heating the materials until the materials flow backward, enabling the materials to flow backward further, carrying out reaction for 20-50 minutes, stirring for reaction at the temperature of 90-105 DEG C for 2-3 hours, melting at the temperature of 185-205 DEG C, spinning, drawing, and drying to obtain the flame resistant fabric material.
Description
Technical field
The invention belongs to textile material field, particularly a kind of retardant fabric material and preparation method thereof.
Background technology
A kind of flame-retardant textile of bicomponent fiber of skin-core structure is disclosed in Chinese patent CN1732295A, adopt the polymer with fire resistance as skin portion, thermoplastic polymer as core composition, but due to the feel of this fabric harder, poor heat stability, is thus limited in very many-sided application.
A kind of production method of cellulose-containing textile material is disclosed in Chinese patent CN1331767A, owing to needing to use a large amount of crosslinking agents in that patent, although the fiber that can make of crosslinking agent has good mechanical strength, but crosslinking agent to the contaminative of environment and environmental stability poor, the mechanical property that material keeps lasting can not be made.
Along with improving constantly of people's awareness of safety, there has also been corresponding requirements to the fire resistance of fabric, particularly fabric is for prevention, the effect delaying or stop fire.Because general fire retardant mostly is halogen system and phosphorus system, major part all has larger toxicity, and need to use formaldehyde or toluene in preparation process, make organic substance residues, produce certain dangerous to health, meanwhile, fabric feeling is after treatment hard, strength damage is large, wearing comfort is low, has a strong impact on quality and the result of use of flame-retardant textile.
Summary of the invention
For above-mentioned demand, the object of this invention is to provide a kind of retardant fabric material and preparation method thereof.The retardant fabric material that the present invention obtains can be used for the fields such as interior decoration, bedding and clothes.
Object of the present invention can be achieved through the following technical solutions:
A kind of retardant fabric material, be made up of the component comprising following weight portion:
Described component also comprises cotton fibriia 0-30 weight portion.
Described component also comprises coconut oil Pn 0-5 weight portion.
A preparation method for retardant fabric material, the method comprises the following steps:
(1) melamine 2-5 weight portion, methyl diphenylene diisocyanate 1-3 weight portion and acetone 80-105 weight portion is taken, mix, add PBT78-93 weight portion, cyanethyl cellulose 8-14 weight portion, polyacrylamide 45-68 weight portion, trimethylolpropane 12-25 weight portion, zinc oxide 5-18 weight portion, cotton fibriia 0-30 weight portion and coconut oil Pn 0-5 weight portion successively;
(2) heating above-mentioned material to producing backflow, continuing to keep back flow reaction 20-50 minute, stirring reaction 2-3 hour at 90-105 DEG C, melting at 185-205 DEG C, spinning, by tractive process, dry, obtained retardant fabric material.
The speed of described tractive is 1500-1650m/min.
Compared with prior art, beneficial effect of the present invention:
(1) retardant fabric material of the present invention is with PBT and polyacrylamide for main raw material, and obtained fibrous material has good processability, and mechanical strength is high.
(2) retardant fabric material of the present invention is owing to adding melamine and methyl diphenylene diisocyanate makes fibrous material have good fire resistance, add trimethylolpropane and cyanethyl cellulose makes material have good submissive performance simultaneously, effectively can reduce the friction between fiber, reduce the generation of balling-up and electrostatic phenomenon, and certain ageing resistace can be had.
(3) retardant fabric material of the present invention, its preparation method is simple, is easy to suitability for industrialized production.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is further illustrated.
Embodiment 1
(1) take melamine 2kg, methyl diphenylene diisocyanate 1kg and acetone 80kg, mix, add PBT78kg, cyanethyl cellulose 8kg, polyacrylamide 45kg, trimethylolpropane 12kg and zinc oxide 5kg successively;
(2) heat above-mentioned material to producing backflow, continue to keep back flow reaction 20 minutes, stirring reaction 2 hours at 105 DEG C, melting at 185 DEG C, spinning, carries out tractive process with the speed of 1500m/min, dry, obtained retardant fabric material.
The performance test results of obtained retardant fabric material is as shown in table 1.
Embodiment 2
(1) take melamine 2kg, methyl diphenylene diisocyanate 1kg and acetone 80kg, mix, add PBT93kg, cyanethyl cellulose 8kg, polyacrylamide 68kg, trimethylolpropane 12kg and zinc oxide 5kg successively;
(2) heat above-mentioned material to producing backflow, continue to keep back flow reaction 20 minutes, stirring reaction 2 hours at 105 DEG C, melting at 185 DEG C, spinning, carries out tractive process with the speed of 1500m/min, dry, obtained retardant fabric material.
The performance test results of obtained retardant fabric material is as shown in table 1.
Embodiment 3
(1) melamine 5kg, methyl diphenylene diisocyanate 3kg and acetone 105kg is taken, mix, add PBT93kg, cyanethyl cellulose 14kg, polyacrylamide 68kg, trimethylolpropane 25kg, zinc oxide 18kg, cotton fibriia 30kg and coconut oil Pn 5kg successively;
(2) heat above-mentioned material to producing backflow, continue to keep back flow reaction 50 minutes, stirring reaction 2 hours at 95 DEG C, melting at 205 DEG C, spinning, carries out tractive process with the speed of 1550m/min, dry, obtained retardant fabric material.
The performance test results of obtained retardant fabric material is as shown in table 1.
Embodiment 4
(1) melamine 2kg, methyl diphenylene diisocyanate 1kg and acetone 105kg is taken, mix, add PBT93kg, cyanethyl cellulose 14kg, polyacrylamide 68kg, trimethylolpropane 25kg, zinc oxide 18kg, cotton fibriia 30kg and coconut oil Pn 5kg successively;
(2) heat above-mentioned material to producing backflow, continue to keep back flow reaction 50 minutes, stirring reaction 2 hours at 95 DEG C, melting at 205 DEG C, spinning, carries out tractive process with the speed of 1550m/min, dry, obtained retardant fabric material.
The performance test results of obtained retardant fabric material is as shown in table 1.
Embodiment 5
(1) melamine 3kg, methyl diphenylene diisocyanate 3kg and acetone 95kg is taken, mix, add PBT83kg, cyanethyl cellulose 12kg, polyacrylamide 58kg, trimethylolpropane 20kg, zinc oxide 12kg, cotton fibriia 10kg and coconut oil Pn 3kg successively;
(2) heat above-mentioned material to producing backflow, continue to keep back flow reaction 30 minutes, stirring reaction 3 hours at 90 DEG C, melting at 195 DEG C, spinning, carries out tractive process with the speed of 1650m/min, dry, obtained retardant fabric material.
The performance test results of obtained retardant fabric material is as shown in table 1.
Embodiment 6
(1) melamine 4kg, methyl diphenylene diisocyanate 2kg and acetone 95kg is taken, mix, add PBT83kg, cyanethyl cellulose 10kg, polyacrylamide 58kg, trimethylolpropane 20kg, zinc oxide 13kg, cotton fibriia 15kg and coconut oil Pn 5kg successively;
(2) heat above-mentioned material to producing backflow, continue to keep back flow reaction 30 minutes, stirring reaction 3 hours at 90 DEG C, melting at 195 DEG C, spinning, carries out tractive process with the speed of 1650m/min, dry, obtained retardant fabric material.
The performance test results of obtained retardant fabric material is as shown in table 1.
The method specified according to textile combustion performance test normal beam technique in standard GB/T/T 5455-1997 measures.Concrete outcome is as shown in table 1.
Table 1
The invention is not restricted to embodiment here, those skilled in the art, according to announcement of the present invention, do not depart from improvement that scope makes and amendment all should within protection scope of the present invention.
Claims (5)
1. a retardant fabric material, is characterized in that, is made up of the component comprising following weight portion:
2. retardant fabric material according to claim 1, is characterized in that, described component also comprises cotton fibriia 0-30 weight portion.
3. retardant fabric material according to claim 1, is characterized in that, described component also comprises coconut oil Pn 0-5 weight portion.
4. a preparation method for retardant fabric material, is characterized in that, the method comprises the following steps:
(1) melamine 2-5 weight portion, methyl diphenylene diisocyanate 1-3 weight portion and acetone 80-105 weight portion is taken, mix, add PBT78-93 weight portion, cyanethyl cellulose 8-14 weight portion, polyacrylamide 45-68 weight portion, trimethylolpropane 12-25 weight portion, zinc oxide 5-18 weight portion, cotton fibriia 0-30 weight portion and coconut oil Pn 0-5 weight portion successively;
(2) heating above-mentioned material to producing backflow, continuing to keep back flow reaction 20-50 minute, stirring reaction 2-3 hour at 90-105 DEG C, melting at 185-205 DEG C, spinning, by tractive process, dry, obtained retardant fabric material.
5. the preparation method of retardant fabric material according to claim 4, is characterized in that, the speed of described tractive is 1500-1650m/min.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510100311.XA CN104630934B (en) | 2015-03-06 | 2015-03-06 | A kind of retardant fabric material and preparation method thereof |
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| CN201510100311.XA CN104630934B (en) | 2015-03-06 | 2015-03-06 | A kind of retardant fabric material and preparation method thereof |
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| CN104630934A true CN104630934A (en) | 2015-05-20 |
| CN104630934B CN104630934B (en) | 2016-12-07 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110938892A (en) * | 2019-12-13 | 2020-03-31 | 江苏集萃先进高分子材料研究所有限公司 | Halogen-free flame-retardant super-smoke-suppression fiber and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| KR101045387B1 (en) * | 2009-01-22 | 2011-06-30 | 웅진케미칼 주식회사 | Polyester fiber having uv blockingproperty and flame retardant, and manufacturing method thereof |
| CN101538764A (en) * | 2009-04-23 | 2009-09-23 | 上海神九纺织科技有限公司 | Blended yarn weaved fabric based on novel flame retardant viscose, preparation method and application thereof |
| CN101857985A (en) * | 2010-03-12 | 2010-10-13 | 郑庆云 | Magnesium hydroxide and aluminum hydroxide PBT/PET composite fiber and preparation method thereof |
| CN103319737B (en) * | 2013-06-21 | 2015-12-09 | 武汉大学 | A kind of preparation method of cellulose/zinc oxide nanoparticle composite material |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110938892A (en) * | 2019-12-13 | 2020-03-31 | 江苏集萃先进高分子材料研究所有限公司 | Halogen-free flame-retardant super-smoke-suppression fiber and preparation method thereof |
| CN110938892B (en) * | 2019-12-13 | 2021-06-04 | 江苏集萃先进高分子材料研究所有限公司 | Halogen-free flame-retardant super-smoke-suppression fiber and preparation method thereof |
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Effective date of registration: 20211228 Address after: 473000 north section of Hengshan Road, Guanzhuang work District, Nanyang City, Henan Province Patentee after: NANYANG YANAN INDUSTRY CO.,LTD. Address before: 215200 Hengfan Bridge Road, Songling Town, Wujiang District, Suzhou City, Jiangsu Province Patentee before: SUZHOU AILIFANG CLOTHING Co.,Ltd. |
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