CN104585760A - Process for processing sea cucumber decoction - Google Patents
Process for processing sea cucumber decoction Download PDFInfo
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- CN104585760A CN104585760A CN201510019771.XA CN201510019771A CN104585760A CN 104585760 A CN104585760 A CN 104585760A CN 201510019771 A CN201510019771 A CN 201510019771A CN 104585760 A CN104585760 A CN 104585760A
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- Prior art keywords
- sea cucumber
- water cooking
- cooking liquid
- concentrated
- liquid
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- 241000251511 Holothuroidea Species 0.000 title claims abstract description 79
- 238000000034 method Methods 0.000 title claims abstract description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 41
- 229910001385 heavy metal Inorganic materials 0.000 claims abstract description 16
- 239000007788 liquid Substances 0.000 claims description 51
- 238000010411 cooking Methods 0.000 claims description 33
- 238000005516 engineering process Methods 0.000 claims description 9
- 238000001914 filtration Methods 0.000 claims description 8
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 claims description 7
- 238000005342 ion exchange Methods 0.000 claims description 7
- 239000003456 ion exchange resin Substances 0.000 claims description 7
- 229920003303 ion-exchange polymer Polymers 0.000 claims description 7
- 239000000546 pharmaceutical excipient Substances 0.000 claims description 6
- 239000003463 adsorbent Substances 0.000 claims description 5
- 239000011521 glass Substances 0.000 claims description 5
- 238000003754 machining Methods 0.000 claims description 5
- 239000002245 particle Substances 0.000 claims description 5
- 239000007787 solid Substances 0.000 claims description 5
- 239000006228 supernatant Substances 0.000 claims description 5
- 239000003826 tablet Substances 0.000 claims description 4
- 229910052751 metal Inorganic materials 0.000 claims description 3
- 239000002184 metal Substances 0.000 claims description 3
- 238000010521 absorption reaction Methods 0.000 claims description 2
- 239000006210 lotion Substances 0.000 claims description 2
- 150000001413 amino acids Chemical class 0.000 abstract description 3
- 150000004676 glycans Chemical class 0.000 abstract description 3
- 229920001282 polysaccharide Polymers 0.000 abstract description 3
- 239000005017 polysaccharide Substances 0.000 abstract description 3
- 239000002351 wastewater Substances 0.000 abstract description 3
- 230000009286 beneficial effect Effects 0.000 abstract description 2
- 235000013305 food Nutrition 0.000 abstract description 2
- 238000002360 preparation method Methods 0.000 abstract description 2
- 229930182490 saponin Natural products 0.000 abstract description 2
- -1 saponin compounds Chemical class 0.000 abstract description 2
- 239000011573 trace mineral Substances 0.000 abstract description 2
- 235000013619 trace mineral Nutrition 0.000 abstract description 2
- 239000000126 substance Substances 0.000 abstract 2
- 239000004480 active ingredient Substances 0.000 abstract 1
- 239000008187 granular material Substances 0.000 abstract 1
- 239000012535 impurity Substances 0.000 abstract 1
- 235000015097 nutrients Nutrition 0.000 abstract 1
- 239000001397 quillaja saponaria molina bark Substances 0.000 abstract 1
- 239000002994 raw material Substances 0.000 abstract 1
- 230000000717 retained effect Effects 0.000 abstract 1
- 239000002699 waste material Substances 0.000 abstract 1
- 150000002500 ions Chemical class 0.000 description 8
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 6
- 239000011651 chromium Substances 0.000 description 3
- 239000003480 eluent Substances 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 235000016709 nutrition Nutrition 0.000 description 3
- 239000004375 Dextrin Substances 0.000 description 2
- 229920001353 Dextrin Polymers 0.000 description 2
- GUBGYTABKSRVRQ-QKKXKWKRSA-N Lactose Natural products OC[C@H]1O[C@@H](O[C@H]2[C@H](O)[C@@H](O)C(O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@H]1O GUBGYTABKSRVRQ-QKKXKWKRSA-N 0.000 description 2
- 229910052804 chromium Inorganic materials 0.000 description 2
- 235000019425 dextrin Nutrition 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000002372 labelling Methods 0.000 description 2
- 239000008101 lactose Substances 0.000 description 2
- 229910052753 mercury Inorganic materials 0.000 description 2
- 229920001467 poly(styrenesulfonates) Polymers 0.000 description 2
- 239000011701 zinc Substances 0.000 description 2
- SQDAZGGFXASXDW-UHFFFAOYSA-N 5-bromo-2-(trifluoromethoxy)pyridine Chemical compound FC(F)(F)OC1=CC=C(Br)C=N1 SQDAZGGFXASXDW-UHFFFAOYSA-N 0.000 description 1
- 229920001287 Chondroitin sulfate Polymers 0.000 description 1
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 1
- 101100127285 Drosophila melanogaster unc-104 gene Proteins 0.000 description 1
- 208000005189 Embolism Diseases 0.000 description 1
- 229920002683 Glycosaminoglycan Polymers 0.000 description 1
- 229930188089 Holothurin Natural products 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 230000000259 anti-tumor effect Effects 0.000 description 1
- 230000010100 anticoagulation Effects 0.000 description 1
- 229910052785 arsenic Inorganic materials 0.000 description 1
- 230000000975 bioactive effect Effects 0.000 description 1
- 230000033228 biological regulation Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 238000009395 breeding Methods 0.000 description 1
- 230000001488 breeding effect Effects 0.000 description 1
- 229940059329 chondroitin sulfate Drugs 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000006071 cream Substances 0.000 description 1
- 230000001079 digestive effect Effects 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 230000020764 fibrinolysis Effects 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 229930182470 glycoside Natural products 0.000 description 1
- 150000002338 glycosides Chemical class 0.000 description 1
- MAWWITJOQDJRJF-ADBICINLSA-M holothurin Chemical compound [Na+].O[C@@H]1[C@@H](OC)[C@H](O)[C@@H](C)O[C@H]1O[C@@H]1[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O)[C@H](O[C@H]3[C@@H](OC[C@H]([C@@H]3O)OS([O-])(=O)=O)O[C@@H]3C([C@H]4[C@](C=5[C@H]([C@@]6(CC[C@]7(O)[C@](C)([C@H]8OC(C)(C)CC8)OC(=O)[C@@]76[C@@H](O)C=5)C)CC4)(C)CC3)(C)C)O[C@@H]2C)O)O[C@H](C)[C@H]1O MAWWITJOQDJRJF-ADBICINLSA-M 0.000 description 1
- 235000012907 honey Nutrition 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 238000001095 inductively coupled plasma mass spectrometry Methods 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 229910052745 lead Inorganic materials 0.000 description 1
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 235000008935 nutritious Nutrition 0.000 description 1
- 230000002980 postoperative effect Effects 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 235000017709 saponins Nutrition 0.000 description 1
- 238000007493 shaping process Methods 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
Abstract
The invention discloses a process for processing sea cucumber decoction. Waste sea cucumber water is used as a raw material, after removing heavy metals and impurities, granule and dry extract preparations are prepared by concentrating to remove insoluble substance. Waste water after sea cucumber decoction processing contains a lot of nutrient substances, such as polysaccharide, saponin compounds, amino acids and a variety of trace elements beneficial to human body, the heavy metals in the waste water are removed, thus the sea cucumber water can meet the food safety standards, so that the sea cucumber water is recycled, the deep processing degree and the added value of sea cucumber are increased, the active ingredients of the sea cucumber are almost completely retained, and the process is suitable for the deep processing of sea cucumber.
Description
Technical field
The present invention relates to sea cucumber water cooking liquid processing technology, belong to sea cucumber deep process technology field.
Background technology
In the sea cucumber processing process that current tradition is conventional, by sea cucumber poach, then send out and make various food, sea cucumber water cooking liquid is drained as waste water substantially, in boiling process, some soluble nutritious components of sea cucumber also enter in water cooking liquid, such as sea cucumber polysaccharide, saponins compound, amino acid and multiple to human body healthy trace elements with household, while nutriment enters water cooking liquid, the heavy metal on sea cucumber surface enters in water cooking liquid, even if breeding environment is subject to light contamination, due to sea cucumber poor growth, so will the more heavy metal of enrichment, such as every, plumbous, mercury, chromium, zinc etc., heavy metal in sea cucumber water cooking liquid will exceed standard, direct discharge can cause environmental pollution, wherein nutritional labeling also runs off thereupon.
Summary of the invention
Technical problem solved by the invention is to provide a kind of sea cucumber water cooking liquid processing technology effectively utilizing sea cucumber water cooking liquid.
The technical solution used in the present invention is sea cucumber water cooking liquid processing technology, comprises the following steps:
A, the sea cucumber water cooking liquid got in Holothurian machining process, remove the heavy metal ion in sea cucumber water cooking liquid by ion-exchange or absorption method;
B, filter sea cucumber water cooking liquid with flame filter press;
C, concentrated by sea cucumber water cooking liquid with multi-effect evaporator, being concentrated into solid content is 10g-60g/100ml;
D, employing flame filter press or centrifuge carry out filtration and obtain sea cucumber concentrated liquid;
E, in sea cucumber concentrated liquid, add adsorbent, filter, get supernatant.
F, in sea cucumber concentrated liquid, add excipient, make particle, tablet or lotion.
In step a, heavy-metal ion removal adopts ion-exchange, gets glass column or metal column that internal diameter is 5-50cm, every 1ml sea cucumber water cooking liquid 5-12g ion exchange resin.
The invention has the beneficial effects as follows by sea cucumber utilization rate from live sea cucumber less than 18%, dried sea-cucumber brings up to more than 98% less than 5%; Be close to and remain sea cucumber active component completely, sea cucumber polysaccharide is thoroughly separated and is absorbed by the body; Product have antitumor, improve immunity, anticoagulation, promotion fibrinolysis, suppress the effects such as embolism formation; Be convenient to digest and assimilate, be applicable to various crowd and take, particularly suitable heavy patient, postoperative patient, the patient of digestive function difference; Take can reach for 5-10 days and take the bimestrial effect of dried sea-cucumber.
Accompanying drawing explanation
Fig. 1 is the flow chart of employing technique of the present invention.
Detailed description of the invention
Embodiment one:
Sea cucumber water cooking liquid processing technology, comprises the following steps:
A, the sea cucumber water cooking liquid got in Holothurian machining process, remove the heavy metal ion in sea cucumber water cooking liquid by ion-exchange, adopts Purolite S-950, Imac TMR, D301, Dowex 50x8 plasma exchanger resin material.Get the glass column that internal diameter is 10cm, dry method upper prop, for D301, every 1ml sea cucumber water cooking liquid 5g ion exchange resin is the aqueous hydrochloric acid solution wash-out of 6.5 with pH value.
B, filtered by the eluent flame filter press in step a, plate-frame filtering fineness is 100 orders.
C, concentrated further by step b gained solution multi-effect evaporator, being concentrated into solid content is 30g-60g/100ml;
D, employing flame filter press or centrifuge carry out filtration and obtain sea cucumber concentrated liquid;
E, in sea cucumber concentrated liquid, add adsorbent, filter, get supernatant.
F, by further for sea cucumber concentrated liquid simmer down to medicinal extract, then add excipient, such as dextrin, the weight proportion of dextrin and excipient is 1:0.5, then shaping, dry, makes particle or tablet.
The nutritional labeling needed for body such as active mucopolysaccharide, Sea Cucumber Glycosides, protein, amino acid extracted is comprised in fresh sea cucumber in this technique gained particle or tablet; and the multiple bioactive ingredients such as chondroitin sulfate, holothurin and mucoitin sulfate, be convenient to digest and assimilate.
The step of heavy-metal ion removal is for ensureing that the edible safety of sea cucumber water cooking liquid is very important.Detect through ICP-MS method, have, content of beary metal contrast is in table 1 without in the sea cucumber water oral liquid of step a, especially wherein the content of Cu, Cr, Hg, Pb, As is all lower than the regulation meeting national standard.
Sea cucumber water oral liquid after table 1 adopts heavy-metal ion removal takes liquid heavy metal with the sea cucumber mouth of a river of non-heavy-metal ion removal
Content balance table.
| Element | Raw sample ng/mL | Ng/mL after process |
| Be | 1.7450 | 1.614 |
| Na | 1461000.0000 | 854000 |
| Mg | 203600.0000 | 423.95 |
| Al | 1446.0000 | 119.6 |
| K | 154500.0000 | 0 |
| Ca | 159100.0000 | 1637 |
| V | 13.3050 | 4.0635 |
| Cr | 23.1700 | 13.245 |
| Mn | 86.2500 | 4.404 |
| Fe | 2145.0000 | 872.5 |
| Co | 4.3935 | 2.637 |
| Ni | 87.6000 | 0 |
| Cu | 231.4000 | 151.95 |
| Zn | 815.5000 | 22.28 |
| As | 134.2500 | 26.935 |
| Se | 74.0500 | 19.27 |
| Mo | 27.3700 | 59.3 |
| Ag | 5.0350 | 3.8445 |
| Cd | 12.9900 | 5.135 |
| Sb | 2.8485 | 2.2465 |
| Ba | 63.9000 | 0 |
| Tl | 2.0035 | 2.1715 |
| Pb | 4.7975 | 4.128 |
| Th | 18.8450 | 71.15 |
| U | 10.4600 | 5.555 |
| Hg | 50.8000 | 14.5050 |
Embodiment two:
A, the sea cucumber water cooking liquid got in Holothurian machining process, remove the heavy metal ion in sea cucumber water cooking liquid by ion-exchange, adopts Dowex 50x8 ion exchange resin material.Get the glass column that internal diameter is 25cm, dry method upper prop, every 1ml sea cucumber water cooking liquid 10g ion exchange resin is the aqueous hydrochloric acid solution wash-out of 6.5 with pH value.
B, filtered by the eluent flame filter press in step a, plate-frame filtering fineness is 120 orders.；
C, concentrated further by step b gained solution multi-effect evaporator, being concentrated into solid content is 45g/100ml;
D, employing flame filter press or centrifuge carry out filtration and obtain sea cucumber concentrated liquid;
E, in sea cucumber concentrated liquid, add adsorbent, filter, get supernatant.
F, by further for sea cucumber concentrated liquid simmer down to medicinal extract, then add excipient, such as lactose, the weight proportion of lactose and excipient is 1:0.6, then makes particle.
This granular preparation is easy to carry, and can wash by water and drink, and also can prepare dish cake etc. as flavouring, takes into account the nutrition of sea cucumber water with delicious.
Embodiment three:
A, the sea cucumber water cooking liquid got in Holothurian machining process, remove the heavy metal ion in sea cucumber water cooking liquid by ion-exchange, adopts Purolite S-950 ion exchange resin material.Get the glass column that internal diameter is 42cm, dry method upper prop, every 1ml sea cucumber water cooking liquid 6g ion exchange resin is 6.5 aqueous hydrochloric acid solution wash-outs with pH value.
B, filtered by the eluent flame filter press in step a, plate-frame filtering fineness is 100 orders.；
C, concentrated further by step b gained solution multi-effect evaporator, being concentrated into solid content is 32g/100ml;
D, employing flame filter press or centrifuge carry out filtration and obtain sea cucumber concentrated liquid;
E, in sea cucumber concentrated liquid, add adsorbent, filter, get supernatant.
F, by further for sea cucumber concentrated liquid simmer down to medicinal extract, add weight ratio be the refined honey of 30%-70%, make dry cream.
The dry paste formulation of sea cucumber water is easy to carry and stores.
Claims (2)
1. sea cucumber water cooking liquid processing technology, comprises the following steps:
A, the sea cucumber water cooking liquid got in Holothurian machining process, remove the heavy metal ion in sea cucumber water cooking liquid by ion-exchange or absorption method;
B, filter sea cucumber water cooking liquid with flame filter press;
C, concentrated by sea cucumber water cooking liquid with multi-effect evaporator, being concentrated into solid content is 10g-60g/100ml;
D, employing flame filter press or centrifuge carry out filtration and obtain sea cucumber concentrated liquid;
E, in sea cucumber concentrated liquid, add adsorbent, filter, get supernatant;
F, in sea cucumber concentrated liquid, add excipient, make particle, tablet or lotion.
2. sea cucumber water cooking liquid processing technology according to claim 1, is characterized in that: in step a, heavy-metal ion removal adopts ion-exchange, gets glass column or metal column that internal diameter is 5-50cm, every 1ml sea cucumber water cooking liquid 5-12g ion exchange resin.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510019771.XA CN104585760A (en) | 2015-01-15 | 2015-01-15 | Process for processing sea cucumber decoction |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510019771.XA CN104585760A (en) | 2015-01-15 | 2015-01-15 | Process for processing sea cucumber decoction |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104585760A true CN104585760A (en) | 2015-05-06 |
Family
ID=53112094
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510019771.XA Pending CN104585760A (en) | 2015-01-15 | 2015-01-15 | Process for processing sea cucumber decoction |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104585760A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107616439A (en) * | 2017-10-17 | 2018-01-23 | 中国石油大学(华东) | A kind of technique for being enriched with Holothurian machining liquid nutritional ingredient |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1269987A (en) * | 2000-01-25 | 2000-10-18 | 威海海大海洋生物制品有限公司 | Technology for preparing concentrated kelp juice |
| CN102488251A (en) * | 2011-12-12 | 2012-06-13 | 中国海洋大学 | Sea cucumber gelatin, preparation method thereof, medicine or health product containing sea cucumber gelatin, and application of sea cucumber gelatin |
| CN101336935B (en) * | 2007-07-08 | 2013-03-13 | 谭攸恒 | Sea cucumber extract and preparation method thereof |
| CN103005528A (en) * | 2007-07-08 | 2013-04-03 | 谭攸恒 | Preparation method of sea cucumber extract |
| KR101328107B1 (en) * | 2012-09-24 | 2013-11-11 | 세종대학교산학협력단 | Food composition with water-convolvulus for excretion of heavy metals and against the oxidative damage thereof |
-
2015
- 2015-01-15 CN CN201510019771.XA patent/CN104585760A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1269987A (en) * | 2000-01-25 | 2000-10-18 | 威海海大海洋生物制品有限公司 | Technology for preparing concentrated kelp juice |
| CN101336935B (en) * | 2007-07-08 | 2013-03-13 | 谭攸恒 | Sea cucumber extract and preparation method thereof |
| CN103005528A (en) * | 2007-07-08 | 2013-04-03 | 谭攸恒 | Preparation method of sea cucumber extract |
| CN102488251A (en) * | 2011-12-12 | 2012-06-13 | 中国海洋大学 | Sea cucumber gelatin, preparation method thereof, medicine or health product containing sea cucumber gelatin, and application of sea cucumber gelatin |
| KR101328107B1 (en) * | 2012-09-24 | 2013-11-11 | 세종대학교산학협력단 | Food composition with water-convolvulus for excretion of heavy metals and against the oxidative damage thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107616439A (en) * | 2017-10-17 | 2018-01-23 | 中国石油大学(华东) | A kind of technique for being enriched with Holothurian machining liquid nutritional ingredient |
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Application publication date: 20150506 |