CN104521995A - Tetra-flubendiamide-contained pesticidal composition and application thereof - Google Patents
Tetra-flubendiamide-contained pesticidal composition and application thereof Download PDFInfo
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- CN104521995A CN104521995A CN201410718411.4A CN201410718411A CN104521995A CN 104521995 A CN104521995 A CN 104521995A CN 201410718411 A CN201410718411 A CN 201410718411A CN 104521995 A CN104521995 A CN 104521995A
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Abstract
The invention provides a tetra-flubendiamide-contained pesticidal composition and application thereof. The composition comprises an effective active ingredient A and an effective active ingredient B, wherein the effective active ingredient A is tetra-flubendiamide and the effective active ingredient B is any one selected from the group consisting of abamectin, emamectin benzoate and chlorfenapyr; pesticidal formulations include suspension concentrate, water emulsion, microemulsion, wettable powder, granule and water dispersible granule; the weight percentage of the two active ingredients is 0.1% to 30% : 0.1% to 50%; and the pesticidal composition also includes 5% to 20% of pesticide adjuvant, with the balance being softened water or filler. The tetra-flubendiamide-contained pesticidal composition provided by the invention is applicable to prevention and treatment of cnaphalocrocis medinalis, Chilo suppressalis and Tryporyza incertulas on rice and pests like diamondback moth, beet armyworm and cabbage caterpillar on vegetable. The composition is safe to use and friendly to environment, has excellent synergistic effects on pest control and is capable of improving control effects, reducing usage amount of pesticide and reducing usage cost of farmers.
Description
Technical field
The present invention relates to pesticide field, particularly a kind of Pesticidal combination and application thereof containing four Flubendiamides.
Background technology
Four Flubendiamides are novel pesticides that Japanese agricultural chemicals company and Bayer are developed jointly, and are mainly used in veterinary antibiotics, paddy rice and cotton control lepidoptera pest; Not only have excellent activity to adult and larva, and speed of action is fast, the lasting period is long.Because the mechanism of action is unique, therefore there is no cross resistance with conventional pesticides, to segmental appendage class beneficial insect safety, be suitable for integrated pest management and pest resistance treatment.
Four Flubendiamides are different from conventional pesticides, are ryanodine receptor activator.After using four Flubendiamides, the classical symptom of lepidopterous larvae is health atrophy gradually, similar symptom can be seen with it the insect after ryania process, and ryania is a calcium ion release channel adjuster, calcium ion release channel serves as crucial effect in contraction of muscle, and this shows to relate in insecticide four Flubendiamide mechanism the calcium ion release channel mechanism resembling the such sensitivity of ryania.Four Flubendiamides have good activity to the diamond-back moth that cinerins, benzoyl area kind, organic phosphates, carbamates have produced resistance.If four chlorantraniliproles are low toxicity, broad spectrum pesticide, all have good activity to lepidoptera pest, but the long-time single use of this kind of agricultural chemicals, are often easy to produce resistance, cause the decline of control efficiency.So must find excellent Pesticidal combination in product development, both are the synergistic effects of phase mutual, have both been conducive to the performance of drug effect, also can reduce the drug cost of peasant, are not easy to produce resistance simultaneously.
But, in prior art, lack the Pesticidal combination composite with four chlorantraniliproles, its insecticidal action is restricted.
Summary of the invention
For solving above-mentioned prior art Problems existing, the object of the present invention is to provide a kind of Pesticidal combination and the application thereof that contain four Flubendiamides, with four Flubendiamides and Avermectin or Affirm (Merck Co.) or capillary combination, form the agricultural chemicals of high-quality and efficient low toxicity.
For achieving the above object, technical scheme of the present invention is:
A kind of Pesticidal combination containing four Flubendiamides, said composition comprises effective active components A and effective active composition B, wherein effective active composition A is four Flubendiamides, effective active composition B be selected from Avermectin, emamectin-benzoate and capillary any one, the percentage by weight of its two kinds of active components is that this Pesticidal combination of 0.1 ~ 30%:50 ~ 0.1% also comprises insecticides adjuvant 5 ~ 20%, surplus demineralized water or filler.
Further, the formulation of described Pesticidal combination is suspending agent, aqueous emulsion, microemulsion, wetting powder, granule, water dispersible granules one wherein.
Further, after composite for effective active composition A and effective active composition B, add 5% dispersant, 1% wetting agent, 0.2% thickener, 0.5% preservative make agricultural chemicals suspension agent.
Further, after composite for effective active composition A and effective active composition B, add 3% dispersant, 0.5% wetting agent, filler make agricultural chemicals wettable powder.
Further, after composite for effective active composition A and effective active composition B, add 3% emulsifier and make aqueous emulsion, add 8% emulsifier and make microemulsion, add 3% emulsifier and make granule, add 10% emulsifier and make water dispersible granules.
Further, the application of described Pesticidal combination in control paddy rice rice leaf roller, striped rice borer, paddy stem borer.
Further, described Pesticidal combination is preventing and treating the application in the diamond-back moth of vegetables, beet armyworm, cabbage caterpillar.
Relative to prior art, beneficial effect of the present invention is:
After the present invention is composite, adds dispersant, wetting agent, thickener, preservative etc. and make agricultural chemicals suspension agent, its drug effect obviously than alone four Flubendiamides or Avermectin good; Also can add dispersant, wetting agent, filler etc. and make agricultural chemicals wettable powder; Also emulsifier be can add and aqueous emulsion, microemulsion, granule, water dispersible granules etc. made.Said composition use safety, environmentally friendly, to pest control, there is excellent synergistic function, can control efficiency be improved, reduce the usage amount of agricultural chemicals, reduce the use cost of peasant.
Embodiment
Below in conjunction with embodiment, the present invention program is described in further detail:
Method one: former medicine four Flubendiamide 40kg, Avermectin 10kg, dispersant 50kg, wetting agent 10kg, thickener 2kg, deionized water 888kg, through homogenizer mixing, colloid mill preliminary grinding, enters the grinding of high speed sand mill, obtains pesticide suspension concentrate.
Method two: former medicine four Flubendiamide 10kg, Avermectin 50kg, dispersant 30kg, wetting agent 2kg, inert filler 908kg, through mixer mixing, enters airslide disintegrating mill and pulverizes, obtain pesticide wettable.
Method three: former medicine four Flubendiamide 50kg, Avermectin 10kg, emulsifier 50kg, a small amount of solvent 50kg, thickener 2kg, deionized water 838kg, shears through high-speed shearing machine, obtains pesticide emulsion in water.
Method four: former medicine four Flubendiamide 10kg, Avermectin 30kg, emulsifier 100kg, a small amount of solvent 40kg, thickener 1kg, deionized water 819kg, through being uniformly mixed, obtain microemulsion.
Method five: former medicine four Flubendiamide 250kg, Avermectin 60kg, dispersant 80kg, wetting agent 20kg, inert filler 590kg, through mixer mixing, enter airslide disintegrating mill and pulverize, adding additives is mediated, and through granulator granulation, obtains pesticide water dispersible granules.
Method six: former medicine four Flubendiamide 50kg, Avermectin 10kg, dispersant 20kg, wetting agent 2kg, through mixer mixing, enters airslide disintegrating mill and pulverizes, adsorb, obtain granular pesticide with inert particulate 918kg.
Method seven: former medicine four Flubendiamide 120kg, Affirm (Merck Co.) 20kg, dispersant 60kg, wetting agent 10kg, thickener 2kg, deionized water 788kg, mix through homogenizer, colloid mill preliminary grinding, enters the grinding of high speed sand mill, obtains pesticide suspension concentrate.
Method eight: former medicine four Flubendiamide 40kg, Affirm (Merck Co.) 80kg, dispersant 20kg, wetting agent 2kg, inert filler 858kg, through mixer mixing, enters airslide disintegrating mill and pulverizes, obtain pesticide wettable.
Method nine: former medicine four Flubendiamide 10kg, Affirm (Merck Co.) 150kg, emulsifier 100kg, a small amount of solvent 60kg, thickener 2kg, deionized water 678kg, shears through high-speed shearing machine, obtains pesticide emulsion in water.
Method ten: former medicine four Flubendiamide 20kg, Affirm (Merck Co.) 100kg, emulsifier 150kg, a small amount of solvent 50kg, thickener 2kg, deionized water 678kg, through being uniformly mixed, obtain microemulsion.
Method 11: former medicine four Flubendiamide 150kg, Affirm (Merck Co.) 30kg, dispersant 30kg, wetting agent 10kg, inert filler 780kg; through mixer mixing, enter airslide disintegrating mill and pulverize, adding additives is mediated; through granulator granulation, obtain pesticide water dispersible granules.
Method 12: former medicine four Flubendiamide 5kg, Affirm (Merck Co.) 10kg, dispersant 30kg, wetting agent 1kg, through mixer mixing, enters airslide disintegrating mill and pulverizes, adsorb, obtain granular pesticide with inert particulate 954kg.
Method 13: former medicine four Flubendiamide 200kg, capillary 250kg, dispersant 80kg, wetting agent 20kg, thickener 2kg, deionized water 448kg, through homogenizer mixing, colloid mill preliminary grinding, enters the grinding of high speed sand mill, obtains pesticide suspension concentrate.
Method 14: former medicine four Flubendiamide 150kg, capillary 300kg, dispersant 50kg, wetting agent 10kg, inert filler 490kg, through mixer mixing, enters airslide disintegrating mill and pulverizes, obtain pesticide wettable.
Method 15: former medicine four Flubendiamide 20kg, capillary 100kg, emulsifier 60kg, a small amount of solvent 50kg, thickener 2kg, deionized water 768kg, shears through high-speed shearing machine, obtains pesticide emulsion in water.
Method 16: former medicine four Flubendiamide 120kg, capillary 20kg, emulsifier 120kg, a small amount of solvent 100kg, thickener 2kg, deionized water 638kg, through being uniformly mixed, obtain microemulsion.
Method 17: former medicine four Flubendiamide 250kg, capillary 300kg, dispersant 120kg, wetting agent 20kg, inert filler 300kg; through mixer mixing, enter airslide disintegrating mill and pulverize, adding additives 10kg mediates; through granulator granulation, obtain pesticide water dispersible granules.
Method 18: former medicine four Flubendiamide 80kg, capillary 5kg, dispersant 30kg, wetting agent 10kg, through mixer mixing, enters airslide disintegrating mill and pulverizes, adsorb, obtain granular pesticide with inert particulate 875kg.
The present invention, for preventing and treating paddy rice rice leaf roller, striped rice borer, paddy stem borer, can also be applied to the insect such as diamond-back moth, beet armyworm, cabbage caterpillar of control vegetables.Said composition use safety, environmentally friendly, to pest control, there is excellent synergistic function, can control efficiency be improved, reduce the usage amount of agricultural chemicals, reduce the use cost of peasant.
Experimental example
Test of pesticide effectiveness result is as following table:
Table 1:12% A Wei. four Flubendiamides (2+10) SC prevents and treats paddy rice rice leaf roller field control effectiveness test result as following table
Table 2:45% capillary. four Flubendiamides (25+20) WDG prevents and treats paddy rice rice leaf roller field control effectiveness test result as following table
From above result of the test, Avermectin, capillary etc. have obvious synergistic effect with four Flubendiamides are composite, and under the equal dosage of active ingredient, complex preparation drug effect is significantly higher than each single dose.The same field of peasant household in this test Shi Ganlian village done.
The above, be only the specific embodiment of the present invention, but protection scope of the present invention is not limited thereto, and any change of expecting without creative work or replacement, all should be encompassed within protection scope of the present invention.Therefore, the protection domain that protection scope of the present invention should limit with claims is as the criterion.
Claims (7)
1. the Pesticidal combination containing four Flubendiamides, it is characterized in that, said composition comprises effective active components A and effective active composition B, wherein effective active composition A is four Flubendiamides, effective active composition B be selected from Avermectin, emamectin-benzoate and capillary any one, the percentage by weight of its two kinds of active components is that this Pesticidal combination of 0.1 ~ 30%:50 ~ 0.1% also comprises insecticides adjuvant 5 ~ 20%, surplus demineralized water or filler.
2. Pesticidal combination according to claim 1, is characterized in that, the formulation of described Pesticidal combination is suspending agent, aqueous emulsion, microemulsion, wetting powder, granule, water dispersible granules one wherein.
3. Pesticidal combination according to claim 2, is characterized in that, after composite for effective active composition A and effective active composition B, adds 5% dispersant, 1% wetting agent, 0.2% thickener, 0.5% preservative make agricultural chemicals suspension agent.
4. Pesticidal combination according to claim 2, is characterized in that, after composite for effective active composition A and effective active composition B, adds 3% dispersant, 0.5% wetting agent, filler make pesticide wettable.
5. Pesticidal combination according to claim 2, it is characterized in that, after composite for effective active composition A and effective active composition B, add 3% emulsifier and make aqueous emulsion, add 8% emulsifier and make microemulsion, add 3% emulsifier and make granule, add 10% emulsifier and make water dispersible granules.
6. the application of the arbitrary described Pesticidal combination of claim 1-5 in control paddy rice rice leaf roller, striped rice borer, paddy stem borer.
7. the arbitrary described Pesticidal combination of claim 1-5 is preventing and treating the application in the diamond-back moth of vegetables, beet armyworm, cabbage caterpillar.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410718411.4A CN104521995A (en) | 2014-12-02 | 2014-12-02 | Tetra-flubendiamide-contained pesticidal composition and application thereof |
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| CN201410718411.4A CN104521995A (en) | 2014-12-02 | 2014-12-02 | Tetra-flubendiamide-contained pesticidal composition and application thereof |
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| CN104521995A true CN104521995A (en) | 2015-04-22 |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105475329A (en) * | 2015-12-16 | 2016-04-13 | 济南昊泽环保科技有限公司 | Insecticidal combination containing o-phenylendiamine insecticide and indoxacarb |
| CN105475332A (en) * | 2015-12-16 | 2016-04-13 | 济南昊泽环保科技有限公司 | Insecticidal combination containing o-phenylendiamine insecticide and sulfoxaflor |
| CN105475337A (en) * | 2015-12-16 | 2016-04-13 | 济南昊泽环保科技有限公司 | Insecticidal combination containing o-phenylendiamine insecticide and imidacloprid |
| CN105475293A (en) * | 2015-12-16 | 2016-04-13 | 济南昊泽环保科技有限公司 | Insecticidal combination containing o-phenylendiamine insecticide and bromoantraniliprole |
| CN111789118A (en) * | 2020-05-27 | 2020-10-20 | 浙江中山化工集团股份有限公司 | Insecticide composition containing flubendiamide and chlorfenapyr and preparation method thereof |
-
2014
- 2014-12-02 CN CN201410718411.4A patent/CN104521995A/en active Pending
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105475329A (en) * | 2015-12-16 | 2016-04-13 | 济南昊泽环保科技有限公司 | Insecticidal combination containing o-phenylendiamine insecticide and indoxacarb |
| CN105475332A (en) * | 2015-12-16 | 2016-04-13 | 济南昊泽环保科技有限公司 | Insecticidal combination containing o-phenylendiamine insecticide and sulfoxaflor |
| CN105475337A (en) * | 2015-12-16 | 2016-04-13 | 济南昊泽环保科技有限公司 | Insecticidal combination containing o-phenylendiamine insecticide and imidacloprid |
| CN105475293A (en) * | 2015-12-16 | 2016-04-13 | 济南昊泽环保科技有限公司 | Insecticidal combination containing o-phenylendiamine insecticide and bromoantraniliprole |
| CN111789118A (en) * | 2020-05-27 | 2020-10-20 | 浙江中山化工集团股份有限公司 | Insecticide composition containing flubendiamide and chlorfenapyr and preparation method thereof |
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| PB01 | Publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
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| WD01 | Invention patent application deemed withdrawn after publication |