CN104480745A - Fabric dyeing process based on persimmon extract and application of related dyed fabric - Google Patents
Fabric dyeing process based on persimmon extract and application of related dyed fabric Download PDFInfo
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- CN104480745A CN104480745A CN201410779626.7A CN201410779626A CN104480745A CN 104480745 A CN104480745 A CN 104480745A CN 201410779626 A CN201410779626 A CN 201410779626A CN 104480745 A CN104480745 A CN 104480745A
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Abstract
The invention belongs to the field of fabric dyeing, and in particular relates to a fabric dyeing process adopting a persimmon extract as a dye and an application of a related dyed fabric. According to the process, persimmons are subjected to special process treatment to obtain a dyeing solution, and the dyeing treatment of a fabric by using the dyeing solution can be performed without a mordant and can achieve a good dyeing effect. Adverse effects of heavy metal ions in the mordant on human bodies and environments are avoided; and compared with 'alkali extraction', 'alcohol extraction' and the like in the prior art, the fabric dyeing process disclosed by the invention is simple in treatment process of the persimmons and low in cost, and after dyeing, the dyeing fastness of various fabrics can achieve good use characteristics.
Description
Technical field
The invention belongs to dye field on fabric, particularly a kind of persimmon extract that adopts is as the upper dyeing technique of dyestuff to fabric and the application of relevant DYED FABRICS.
Background technology
Reinforcement along with people's environmental consciousness and the pay attention to day by day to human health, part synthetic dyestuffs more and more receive publicity to the negative effect that health and ecological environment produce.Early there are some researches show: have more than 100 kind of common dyes to produce carcinogen.The developed countries such as Germany in 1994 have promulgated the regulation of these dyestuffs of forbidding.Moreover, along with the consumption of earth petroleum resources, the raw material problem of synthetic dyestuffs also comes out gradually, and therefore, scientific research personnel starts to be devoted to develop " natural environmental-protective dyestuff " and " environment-protecting clean dyeing and finishing technology ".
The application of natural plant dye has long history, the period of Ming and Qing, and the preparation of China's natural dye and staining technique have all had significant progress.But the affinity of most of natural plant dye to fiber is low, just must can anchors on fiber by mordant, complete the dyeing to fabric.In mordant dyeing technique, conventional mordant is mostly heavy metal ion, as: copper, iron, chromium or aluminium etc., this all can produce certain harm to human body and environment.Be restricted along with part kind in synthetic dyestuffs is subject to heavy metal ion content in forbidding and textiles, the technology of developmental research " natural plant dye is without under the environment of mordant; realize upper dye to fabric ", has become the vital task of development textiles Eco-friendly machining at present.
Persimmon is the fruit that people prefer to eat, sweet greasy good to eat, nutritious.Persimmon nutritive value is very high, and contained vitamin and sugar are than general fruit height 1-2 doubly left and right.If a people eats 1 persimmon for one day, the vitamin C absorbed just can meet the half of one day requirement substantially.So it is very useful for eating a little persimmon to health.The traditional Chinese medical science thinks that it is sweet of low station puckery, returns lung taste large intestine channel.There is moistening lung for removing phlegm, clearing heat and promoting fluid, antidysentery with astringent, invigorating spleen and reinforcing stomach, the multiple efficacies such as ease constipation, cooling blood and hemostasis of promoting the production of body fluid.Containing the abundant trace element such as carrotene, riboflavin, vitamin.But adopt persimmon extract also fewer as the Research Literature of dye for fabrics.
Summary of the invention
Technical problem to be solved by this invention is: when being dyeed as dyestuff to fabric by persimmon extract in prior art, needs could realize by mordant.
For solving this technical problem, the technical solution used in the present invention is: by persimmon is carried out special PROCESS FOR TREATMENT, obtain dye liquor, when adopting this dye liquor to carry out dyeing process to fabric, can carry out under without the prerequisite of mordant, and play good upper dye effect.
Concrete technology route in the present invention is:
(1) process of persimmon: select and also do not have ripe blue or green persimmon, blue or green persimmon is cleaned, dries, is crushed to 0.8-1.5cm
3particle after, the blue or green persimmon particle obtained is soaked spontaneous fermentation in deionized water, water temperature control be 32-35 DEG C, fermentation time is 2-4 days (48-96h), water consumption for just to flood blue or green persimmon particle,
After having fermented, filter, the filtrate obtained is the solution of blue or green persimmon extract, and the filtrate obtained is carried out freeze drying, obtains blue or green persimmon extract powder, and sealing is kept in Dark Place;
(2) dyeing: the blue or green persimmon extract powder obtained in step (1) is added deionization dilution with water, obtain uniform dilution, and to control the mass concentration of blue or green persimmon extract in dilution be 0.5-1.2%, and the pH value of dilution is regulated to be 3-5; Be immersed in the dilution of gained by the linen of cleaning, dye to fabric, controlling dyeing condition is that bath raio is 1:20-30, and dyeing temperature is 60-70 DEG C, and dyeing time is 40-60 minutes; Wash after dyeing and dry, obtaining DYED FABRICS.
Present invention also offers the DYED FABRICS of a kind of above-mentioned employing persimmon extract as dyestuff, as the application of anti-UV fabric, compared to without hyperchromatic fabric, there is obvious UVResistant effect;
Present invention also offers the DYED FABRICS of a kind of above-mentioned employing persimmon extract as dyestuff, as the application of antibiotic fabric, fabric is also in antibiotic finish in the process of dyeing;
Present invention also offers and a kind ofly preventing and treating the application in soil-borne disease based on persimmon extract as the DYED FABRICS of dyestuff, during embody rule, to there is the plant of tree bar structure as controlling object, DYED FABRICS based on persimmon extract is wrapped in the overground part tree bar part of plant, wraps up 1-2 layers of fabric.
Beneficial effect of the present invention is: same using the extract of persimmon as dyestuff, the present invention, compared with existing extraction process, under only needing that persimmon is placed in certain environment, makes it slowly ferment; Compared with the means such as " alkali extraction " of the prior art, " alcohol extracting ", simple, with low cost to the treatment process of persimmon in the present invention.
The persimmon extract dye liquor obtained after process of the present invention, can dye to fabric, reach same Color under the prerequisite departing from mordant, avoids the harmful effect to human body and environment of heavy metal ion in mordant; And after upper dye, the upper dye fastness of fabric can reach good serviceability, and imparts the effect of the certain UVResistant effect of fabric, antibacterial effect, anti-soil-borne disease.
Detailed description of the invention
Embodiment 1
(1) process of persimmon: select and also do not have ripe blue or green persimmon, blue or green persimmon is cleaned, dries, is crushed to 0.8-1.2cm
3particle after, the blue or green persimmon particle obtained is soaked spontaneous fermentation in deionized water, water temperature control be 35 DEG C, fermentation time is 4 days (96h), water consumption for just to flood blue or green persimmon particle,
After having fermented, filter, the filtrate obtained is the solution of blue or green persimmon extract, and the filtrate obtained is carried out freeze drying, obtains blue or green persimmon extract powder, and sealing is kept in Dark Place;
(2) dyeing: the blue or green persimmon extract powder obtained in step (1) is added deionization dilution with water, obtain uniform dilution, and to control the mass concentration of blue or green persimmon extract in dilution be 1%, and the pH value of dilution is regulated to be 4; Be immersed in the dilution of gained by the linen sheet of cleaning, dye to linen sheet, controlling dyeing condition is that bath raio is 1:26, and dyeing temperature is 70 DEG C, and dyeing time is 50 minutes; Washing after dyeing is also dried at 70 DEG C, obtains the linen that dyes.After dyeing, fabric is silver gray, and concrete serviceability is as shown in table 1.
Embodiment 2
(1) process of persimmon: select and also do not have ripe blue or green persimmon, blue or green persimmon is cleaned, dries, is crushed to 1.0-1.5cm
3particle after, the blue or green persimmon particle obtained is soaked spontaneous fermentation in deionized water, water temperature control be 32 DEG C, fermentation time is 4 days (96h), water consumption for just to flood blue or green persimmon particle,
After having fermented, filter, the filtrate obtained is the solution of blue or green persimmon extract, and the filtrate obtained is carried out freeze drying, obtains blue or green persimmon extract powder, and sealing is kept in Dark Place;
(2) dyeing: the blue or green persimmon extract powder obtained in step (1) is added deionization dilution with water, obtain uniform dilution, and to control the mass concentration of blue or green persimmon extract in dilution be 1%, and the pH value of dilution is regulated to be 5; Be immersed in the dilution of gained by the linen sheet of cleaning, dye to linen sheet, controlling dyeing condition is that bath raio is 1:25, and dyeing temperature is 65 DEG C, and dyeing time is 60 minutes; Washing after dyeing is also dried at 70 DEG C, obtains DYED FABRICS.After dyeing, fabric is silver gray, and concrete serviceability is as shown in table 1.
Embodiment 3:
(1) adopt conventional " alcohol extracting " method, extract blue or green persimmon, concrete steps are: select and also do not have ripe blue or green persimmon, cleaned, dry, be crushed to 0.8-1.2cm by blue or green persimmon
3particle after, the blue or green persimmon particle obtained is joined pH value 9, concentration of volume percent is refluxing extraction in 50% ethanol water, the mass ratio of blue or green persimmon particle and ethanol water is 1: 40; Extract is warming up to 90 DEG C, insulation 1.5h; Filter and the filtrate obtained is carried out freeze drying, obtaining blue or green persimmon extract powder, and sealing is kept in Dark Place;
(2) dyeing in the present embodiment is consistent with the dyeing in embodiment 1, and after dyeing, fabric is very shallow pink colour, and concrete serviceability is as shown in table 1.
Embodiment 4:
(1) adopt conventional " alkali extraction " method, extract blue or green persimmon, concrete steps are: select and also do not have ripe blue or green persimmon, cleaned, dry, be crushed to 0.8-1.2cm by blue or green persimmon
3particle after, the blue or green persimmon particle obtained is immersed in pH be 9 the soda ash aqueous solution be solvent, solid-liquid ratio is 1:50g/ml, return stirring 40min, cooling, filter, isolate filtrate; The filtrate obtained is carried out freeze drying, obtains blue or green persimmon extract powder, and sealing is kept in Dark Place;
(2) dyeing in the present embodiment is consistent with the dyeing in embodiment 2, and after dyeing, fabric is very shallow pink colour, and does not almost see color, and concrete serviceability is as shown in table 1.
Table 1: in embodiment 1-5, the dyeing ability of dyeing linen
Colour fastness to rubbing presses GB/T3920-2008 " textile color stability test colour fastness to rubbing " test;
Fastness to soaping presses GB/T3921-2008 " textile color stability test fastness to soaping " test;
Color fastness to light presses GB/T 8426-1998 " textile color stability test color fastness to light " test;
UV resistance ability presses GB/T18830-2009 " evaluation of textiles UV resistance performance " test;
The mensuration of color depth (K/S value): by DYED FABRICS folding twice (four layers), adopt Datacolor SF60OX Computer color testing color matching instrument to measure the K/S value of DYED FABRICS at λ max place, each sample is surveyed four times and is averaged.
Embodiment 5
To the DYED FABRICS obtained in embodiment 2, carry out the detection of anti-microbial property before and after dyeing:
The DYED FABRICS obtained in embodiment 2 is cut into the circle that diameter is 2cm, the linen sheet of undyed same size is also cut into as blank sample the circle that diameter is 2cm, for subsequent use,
Then GB/T 20944.2 is pressed---2007 agar plate diffusion methods, by the Solid nutritional base for preparing at 121 DEG C of high-temperature sterilization 20min, pour in surface plate while hot and cool, Escherichia coli are coated after condensation, linen sheet after dyeing and blank sample are tightly attached on Solid nutritional base, in incubator, cultivate 18h, observing the DYED FABRICS obtained in embodiment 2 is 88% to colibacillary antibiotic rate, and linen sheet blank sample is only 13% to colibacillary bacteriostasis rate.
Embodiment 6:
Soil property is consistent, fertility is evenly medium to select 1 piece, and has the cotton field of certain cotton wilt incidence trend, and the cotton tree in this cotton field has all grown the tree bar structure having possessed certain length.
Check the total quantity of cotton tree in above-mentioned cotton field, and randomly draw the cotton tree of 1/3 quantity, the linen sheet after the blue or green persimmon extract dyeing of the employing of preparation in embodiment 1 is adopted to be cut into suitable size, as the fabric material for wrapping up cotton tree overground part tree bar part, the overground part tree bar part that the cotton of this 1/3 quantity is set is wrapped up, wrap up two-layer, count A;
In above-mentioned cotton field, randomly draw the cotton tree of other 1/3 quantity, linen sheet after the blue or green persimmon extract dyeing of employing of preparation in same employing embodiment 1 is as the fabric material for wrapping up cotton tree overground part tree bar part, the overground part tree bar part that the cotton of this 1/3 quantity is set is wrapped up, wrap up 1 layer, count B;
Cotton for 1/3 quantity remaining in this Cotton Fields is set, adopt with same specification in embodiment 1, but set as wrapping up cotton the fabric material that overground part sets bar part without the blank linen sheet of upper dye, the overground part tree bar part that the cotton of this 1/3 quantity is set is wrapped up, wrap up two-layer, count C.
Observe the incidence of the cotton wilt of this 3 class cotton of above A, B, C tree, concrete statistical conditions are as shown in table 2:
Table 2
| Investigation strain number | The cotton wilt incidence of disease | |
| A | 50 | 10％ |
| B | 50 | 12％ |
| C | 50 | 64％ |
(incidence of disease (%)=morbidity strain number/investigate total strain number × 100).
Claims (6)
1. based on a fabric dyeing method for persimmon extract, it is characterized in that: described method is,
(1) process of persimmon, cleans blue or green persimmon, is crushed to 0.8-1.5cm
3particle after, the blue or green persimmon particle obtained is soaked and ferments in deionized water, water consumption for just to flood blue or green persimmon particle,
After having fermented, filter, the filtrate obtained is the solution of blue or green persimmon extract, and the filtrate obtained is carried out freeze drying, obtains blue or green persimmon extract powder, and sealing is kept in Dark Place;
(2) dyeing, the blue or green persimmon extract powder obtained in step (1) is added deionization dilution with water, obtain uniform dilution, and to control the mass concentration of blue or green persimmon extract in described dilution be 0.5-1.2%, and the pH value of described dilution is regulated to be 3-5; Be immersed in described dilution by the fabric of cleaning, dye to fabric, controlling dyeing condition is that bath raio is 1:20-30, and dyeing temperature is 60-70 DEG C, and dyeing time is 40-60 minutes; Wash after dyeing and dry, obtaining DYED FABRICS.
2., as claimed in claim 1 based on the fabric dyeing method of persimmon extract, it is characterized in that: described in step (1) ferment in deionized water be operating as, control water temperature and be 32-35 DEG C, control fermentation time is 48-96h.
3., as claimed in claim 1 based on the fabric dyeing method of persimmon extract, it is characterized in that: the fabric described in step (2) is linen.
4. the application of DYED FABRICS that obtains of colouring method as claimed in claim 1, is characterized in that: described is applied as, based on persimmon extract as the DYED FABRICS of dyestuff as the application of anti-UV fabric.
5. the application of DYED FABRICS that obtains of colouring method as claimed in claim 1, is characterized in that: described is applied as, based on persimmon extract as the DYED FABRICS of dyestuff as the application of antibiotic fabric.
6. the application of DYED FABRICS that obtains of colouring method as claimed in claim 1, is characterized in that: described is applied as, is preventing and treating the application in soil-borne disease based on persimmon extract as the DYED FABRICS of dyestuff.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105839427A (en) * | 2016-05-06 | 2016-08-10 | 长兴园顺纺织有限公司 | Environmentally friendly dyeing process of ramie fibers |
| CN110656511A (en) * | 2019-10-29 | 2020-01-07 | 樊俊国 | Persimmon dyeing method |
| CN114351462A (en) * | 2021-12-21 | 2022-04-15 | 中恒大耀纺织科技有限公司 | Preparation method of low stitch combing crack crepe fabric capable of inhibiting sweat odor |
| CN114592361A (en) * | 2020-12-04 | 2022-06-07 | 株式会社衣思时尚文化 | Natural dyeing method using fermented persimmon juice |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101302720A (en) * | 2007-05-11 | 2008-11-12 | 袁慧丽 | Method for dyeing textile using persimmon |
| CN102321982A (en) * | 2011-08-10 | 2012-01-18 | 无锡市联盛印染有限公司 | Dyeing method by using persimmon natural dye |
| KR101384694B1 (en) * | 2013-08-20 | 2014-04-14 | 동원염직 주식회사 | Complex finishing process method by loess and persimmon tannin of dyed fibers |
-
2014
- 2014-12-16 CN CN201410779626.7A patent/CN104480745B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101302720A (en) * | 2007-05-11 | 2008-11-12 | 袁慧丽 | Method for dyeing textile using persimmon |
| CN102321982A (en) * | 2011-08-10 | 2012-01-18 | 无锡市联盛印染有限公司 | Dyeing method by using persimmon natural dye |
| KR101384694B1 (en) * | 2013-08-20 | 2014-04-14 | 동원염직 주식회사 | Complex finishing process method by loess and persimmon tannin of dyed fibers |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105839427A (en) * | 2016-05-06 | 2016-08-10 | 长兴园顺纺织有限公司 | Environmentally friendly dyeing process of ramie fibers |
| CN105839427B (en) * | 2016-05-06 | 2018-08-03 | 长兴园顺纺织有限公司 | A kind of ramee environmental protection dyeing |
| CN110656511A (en) * | 2019-10-29 | 2020-01-07 | 樊俊国 | Persimmon dyeing method |
| CN114592361A (en) * | 2020-12-04 | 2022-06-07 | 株式会社衣思时尚文化 | Natural dyeing method using fermented persimmon juice |
| CN114351462A (en) * | 2021-12-21 | 2022-04-15 | 中恒大耀纺织科技有限公司 | Preparation method of low stitch combing crack crepe fabric capable of inhibiting sweat odor |
| CN114351462B (en) * | 2021-12-21 | 2023-11-17 | 中恒大耀纺织科技有限公司 | Preparation method of low-fringing cotton crepe fabric capable of inhibiting sweat odor |
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