CN104450086A - 一种精密仪器用防霉润滑脂及其制备方法 - Google Patents
一种精密仪器用防霉润滑脂及其制备方法 Download PDFInfo
- Publication number
- CN104450086A CN104450086A CN201410674248.6A CN201410674248A CN104450086A CN 104450086 A CN104450086 A CN 104450086A CN 201410674248 A CN201410674248 A CN 201410674248A CN 104450086 A CN104450086 A CN 104450086A
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- CN
- China
- Prior art keywords
- parts
- lubricating grease
- fatty alcohol
- mildew
- precision instrument
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000004519 grease Substances 0.000 title claims abstract description 40
- 230000001050 lubricating effect Effects 0.000 title claims abstract description 35
- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- 238000000465 moulding Methods 0.000 title abstract 6
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims abstract description 36
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 36
- 239000000203 mixture Substances 0.000 claims abstract description 32
- 150000003242 quaternary ammonium salts Chemical class 0.000 claims abstract description 25
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims abstract description 20
- 239000005995 Aluminium silicate Substances 0.000 claims abstract description 18
- 229960000583 acetic acid Drugs 0.000 claims abstract description 18
- 235000012211 aluminium silicate Nutrition 0.000 claims abstract description 18
- 229910052921 ammonium sulfate Inorganic materials 0.000 claims abstract description 18
- 235000011130 ammonium sulphate Nutrition 0.000 claims abstract description 18
- 239000012362 glacial acetic acid Substances 0.000 claims abstract description 18
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims abstract description 18
- 229940085675 polyethylene glycol 800 Drugs 0.000 claims abstract description 18
- 229940051841 polyoxyethylene ether Drugs 0.000 claims abstract description 18
- 229920000056 polyoxyethylene ether Polymers 0.000 claims abstract description 18
- WSFQLUVWDKCYSW-UHFFFAOYSA-M sodium;2-hydroxy-3-morpholin-4-ylpropane-1-sulfonate Chemical compound [Na+].[O-]S(=O)(=O)CC(O)CN1CCOCC1 WSFQLUVWDKCYSW-UHFFFAOYSA-M 0.000 claims abstract description 18
- 239000003112 inhibitor Substances 0.000 claims description 23
- 230000003647 oxidation Effects 0.000 claims description 23
- 238000007254 oxidation reaction Methods 0.000 claims description 23
- JHUFGBSGINLPOW-UHFFFAOYSA-N 3-chloro-4-(trifluoromethoxy)benzoyl cyanide Chemical compound FC(F)(F)OC1=CC=C(C(=O)C#N)C=C1Cl JHUFGBSGINLPOW-UHFFFAOYSA-N 0.000 claims description 16
- 229920002593 Polyethylene Glycol 800 Polymers 0.000 claims description 16
- XEFQLINVKFYRCS-UHFFFAOYSA-N Triclosan Chemical compound OC1=CC(Cl)=CC=C1OC1=CC=C(Cl)C=C1Cl XEFQLINVKFYRCS-UHFFFAOYSA-N 0.000 claims description 16
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 claims description 16
- 229960003500 triclosan Drugs 0.000 claims description 16
- 238000000034 method Methods 0.000 claims description 14
- 238000010438 heat treatment Methods 0.000 claims description 12
- 239000012467 final product Substances 0.000 claims description 7
- NLZUEZXRPGMBCV-UHFFFAOYSA-N Butylhydroxytoluene Chemical compound CC1=CC(C(C)(C)C)=C(O)C(C(C)(C)C)=C1 NLZUEZXRPGMBCV-UHFFFAOYSA-N 0.000 claims description 5
- JBIROUFYLSSYDX-UHFFFAOYSA-M benzododecinium chloride Chemical compound [Cl-].CCCCCCCCCCCC[N+](C)(C)CC1=CC=CC=C1 JBIROUFYLSSYDX-UHFFFAOYSA-M 0.000 claims description 4
- WJUMWVJBOZKPPU-UHFFFAOYSA-N 2,3-bis(6-methylheptyl)-N-phenylaniline Chemical compound C(CCCCC(C)C)C=1C(=C(C=CC1)NC1=CC=CC=C1)CCCCCC(C)C WJUMWVJBOZKPPU-UHFFFAOYSA-N 0.000 claims description 3
- OCVZNQCDPKRNDL-UHFFFAOYSA-N 2-hydroxyethyl-dimethyl-octadecylazanium;nitrate Chemical compound [O-][N+]([O-])=O.CCCCCCCCCCCCCCCCCC[N+](C)(C)CCO OCVZNQCDPKRNDL-UHFFFAOYSA-N 0.000 claims description 3
- WVJKSRJWLIVTGA-UHFFFAOYSA-M 2-hydroxyethyl-dimethyl-octadecylazanium;perchlorate Chemical compound [O-]Cl(=O)(=O)=O.CCCCCCCCCCCCCCCCCC[N+](C)(C)CCO WVJKSRJWLIVTGA-UHFFFAOYSA-M 0.000 claims description 3
- 235000010354 butylated hydroxytoluene Nutrition 0.000 claims description 3
- DDXLVDQZPFLQMZ-UHFFFAOYSA-M dodecyl(trimethyl)azanium;chloride Chemical compound [Cl-].CCCCCCCCCCCC[N+](C)(C)C DDXLVDQZPFLQMZ-UHFFFAOYSA-M 0.000 claims description 3
- NQPDZGIKBAWPEJ-UHFFFAOYSA-N pentanoic acid group Chemical group C(CCCC)(=O)O NQPDZGIKBAWPEJ-UHFFFAOYSA-N 0.000 claims description 3
- 230000003078 antioxidant effect Effects 0.000 abstract description 4
- 244000005700 microbiome Species 0.000 abstract description 2
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 abstract 2
- -1 alkyl ether ammonium sulfate Chemical class 0.000 abstract 2
- 239000003963 antioxidant agent Substances 0.000 abstract 2
- 229910052710 silicon Inorganic materials 0.000 abstract 2
- 239000010703 silicon Substances 0.000 abstract 2
- DIKJULDDNQFCJG-UHFFFAOYSA-N sodium;prop-2-ene-1-sulfonic acid Chemical compound [Na+].OS(=O)(=O)CC=C DIKJULDDNQFCJG-UHFFFAOYSA-N 0.000 abstract 2
- 239000000344 soap Substances 0.000 description 6
- 239000003795 chemical substances by application Substances 0.000 description 5
- 239000000314 lubricant Substances 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 230000005764 inhibitory process Effects 0.000 description 3
- 238000005461 lubrication Methods 0.000 description 3
- 241000233866 Fungi Species 0.000 description 2
- 239000003921 oil Substances 0.000 description 2
- 238000007789 sealing Methods 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 1
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 239000004411 aluminium Substances 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- 239000010425 asbestos Substances 0.000 description 1
- 229910052788 barium Inorganic materials 0.000 description 1
- DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 description 1
- 235000014121 butter Nutrition 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000006229 carbon black Substances 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000005553 drilling Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- 229910052744 lithium Inorganic materials 0.000 description 1
- 230000003137 locomotive effect Effects 0.000 description 1
- 239000010687 lubricating oil Substances 0.000 description 1
- 229910052748 manganese Inorganic materials 0.000 description 1
- 239000011572 manganese Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000002480 mineral oil Substances 0.000 description 1
- 235000010446 mineral oil Nutrition 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 230000035515 penetration Effects 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 229910052895 riebeckite Inorganic materials 0.000 description 1
- 230000003248 secreting effect Effects 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000012265 solid product Substances 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
Landscapes
- Lubricants (AREA)
Abstract
Description
试验方法 | 实施例1 | 实施例2 | 实施例3 | 实施例4 | 实施例5 | |
锥入度25℃,15g,5s,0.1mm | GB/T629 | 65 | 63 | 61 | 67 | 66 |
滴点,℃ | GB/T3498 | 83 | 79 | 82 | 81 | 80 |
挥发度60℃,24h,% | SH/T0048 | 0.02 | 0.05 | 0.03 | 0.04 | 0.06 |
腐蚀铜片,100℃,3h | SH/T0331 | 合格 | 合格 | 合格 | 合格 | 合格 |
防霉试验,30℃,湿度94%,30d | 自测 | 无霉菌 | 无霉菌 | 无霉菌 | 无霉菌 | 无霉菌 |
Claims (7)
Priority Applications (1)
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CN201410674248.6A CN104450086B (zh) | 2014-11-21 | 2014-11-21 | 一种精密仪器用防霉润滑脂及其制备方法 |
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CN201410674248.6A CN104450086B (zh) | 2014-11-21 | 2014-11-21 | 一种精密仪器用防霉润滑脂及其制备方法 |
Publications (2)
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CN104450086A true CN104450086A (zh) | 2015-03-25 |
CN104450086B CN104450086B (zh) | 2017-09-12 |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105421044A (zh) * | 2015-12-22 | 2016-03-23 | 常熟市泽众家用纺织品有限公司 | 床单面料 |
CN107523382A (zh) * | 2017-10-11 | 2017-12-29 | 南京仙草堂生物科技有限公司 | 一种实验室精密仪器用防晒润滑脂及其制备方法 |
CN107868690A (zh) * | 2017-12-01 | 2018-04-03 | 苏州科茂电子材料科技有限公司 | 用于精密仪器的抗磨耐热老化润滑脂及其制备方法 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2976242A (en) * | 1955-04-01 | 1961-03-21 | Exxon Research Engineering Co | Lubricating grease compositions |
CN102977986A (zh) * | 2012-12-24 | 2013-03-20 | 云南光电辅料有限公司 | 一种精密仪器用防霉润滑脂及其制备方法 |
CN103045327A (zh) * | 2012-12-22 | 2013-04-17 | 云南光电辅料有限公司 | 一种光学仪器用防水密封脂及其制备方法 |
-
2014
- 2014-11-21 CN CN201410674248.6A patent/CN104450086B/zh active Active
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2976242A (en) * | 1955-04-01 | 1961-03-21 | Exxon Research Engineering Co | Lubricating grease compositions |
CN103045327A (zh) * | 2012-12-22 | 2013-04-17 | 云南光电辅料有限公司 | 一种光学仪器用防水密封脂及其制备方法 |
CN102977986A (zh) * | 2012-12-24 | 2013-03-20 | 云南光电辅料有限公司 | 一种精密仪器用防霉润滑脂及其制备方法 |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105421044A (zh) * | 2015-12-22 | 2016-03-23 | 常熟市泽众家用纺织品有限公司 | 床单面料 |
CN107523382A (zh) * | 2017-10-11 | 2017-12-29 | 南京仙草堂生物科技有限公司 | 一种实验室精密仪器用防晒润滑脂及其制备方法 |
CN107868690A (zh) * | 2017-12-01 | 2018-04-03 | 苏州科茂电子材料科技有限公司 | 用于精密仪器的抗磨耐热老化润滑脂及其制备方法 |
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CN104450086B (zh) | 2017-09-12 |
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C06 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
CB03 | Change of inventor or designer information |
Inventor after: Sun Meiling Inventor before: Xiong Kaisheng Inventor before: Zhang Haifang Inventor before: Xie Jianting |
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CB03 | Change of inventor or designer information | ||
TA01 | Transfer of patent application right |
Effective date of registration: 20170807 Address after: 318000, three, 2-11 village gate, Baiyun Street, Jiaojiang District, Zhejiang, Taizhou Applicant after: Sun Meiling Address before: Zhongshan road Wuzhong District Mudu town of Suzhou city in Jiangsu province 215101 No. 70 Applicant before: DONGCHEN-LEADER TESTING CO., LTD. |
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TA01 | Transfer of patent application right | ||
CB03 | Change of inventor or designer information |
Inventor after: Bai Chuanhang Inventor after: Lan Bingli Inventor after: He Dehai Inventor before: Sun Meiling |
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TA01 | Transfer of patent application right |
Effective date of registration: 20170817 Address after: 518105 Guangdong city of Shenzhen province Baoan District Songgang streets Yan Chuanyan Luo Road No. 146 building four, teckwin Industrial Park Applicant after: Shenzhen Hecheng lubricating material Co., Ltd. Address before: 318000, three, 2-11 village gate, Baiyun Street, Jiaojiang District, Zhejiang, Taizhou Applicant before: Sun Meiling |
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