CN104430890A - Pueraria flower juice and milk beverage and preparation method thereof - Google Patents
Pueraria flower juice and milk beverage and preparation method thereof Download PDFInfo
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Abstract
The invention discloses pueraria flower juice and milk beverage and a preparation method thereof. A formula is specifically as follows: the adding amount of pueraria flower juice is 5%, the adding amount of sucrose is 8%, the adding amount of pure milk is 30%, the adding amount of a composite stabilizer is 0.1% and the balance is mineral water. Compared with a traditional de-alcoholic product, for the beverage prepared by adopting the method provided by the invention, besides adopting plant components, the healthcare function of milk is combined, so that the prepared beverage satisfies the health conception of moderns.
Description
Technical field
The invention belongs to technical field of beverage, relate to a kind of FI puerariae juice milk drink and preparation method thereof.
Background technology
Wine is the common treasures of the people of other countries, and the history of wine is of long standing and well established, and according to historian's textual criticism, our people drinks and brewages drinks, existing several thousand history.China is Wine production and consumption big country, and conservative estimation has the crowd of alcohol drinking patterns and dependent crowd about 1.5 hundred million.Along with the consumption of the alcohol of raising gradually (ethanol) beverage of people's living standard is also in increase, crapulent incidence of being thereupon grown up also corresponding rising.As everyone knows, acute alcoholism, alcohol dependence are one of society problems.Long-term alcohol can cause the damage of whole body multisystem, and alcohol directly or indirectly can cause chronic gastritis, peptic ulcer and alcoholic-toxic cirrhosis.Unconfined excessive consumption of alcohol, easily causes hepatic lesion, and alcoholic hepatitis or cirrhosis, finally develop into hepatocellular carcinoma, and severe patient can be dead because of ethanol extra-inhibitory central nervous system.Therefore, indulge in excessive drinking to health be harmful to.For a long time, people just adopt various method to remove and alleviate brought discomfort of drinking.In the consumption of food and drink, full-natural nutritive, health care, easily novel disintoxicating product will more and more be subject to everybody favor.Therefore the disintoxicating product of development of new is also imperative.
About the research of disintoxicating product, in Japan, the nineties just starts the beverage developing aspect of relieving the effect of alcohol, and some alcohol-decomposing beverages also come into vogue thenceforth step by step.But these beverages of Japan are mostly containing some artificial synthetic ingredients, the drink extracted with this function plant of root of kudzu vine pure natural will be the product of a Chaoyang.In China, a lot of institution of higher learning and R&D institution is just had to be devoted to the research of disintoxicating product at present, such as Jin Gelu is a kind of new alcohol-decomposing beverage of food science and technology institute of Agricultural University Of Hunan development in 2004, since putting on market, the test of multiple marketing point in the whole nation, it is respond well that the consumer of 80% thinks that this product relieves the effect of alcohol.This product is formulated primarily of the root of kudzu vine, Tea Polyphenols, glucose, butanedioic acid, fumaric acid, Glu and ascorbic acid etc.
At present at the more common product relieved the effect of alcohol of China, as Antialcoholic tea, health protection tea, fruit tea of sobering up, relieving alcoholism and protecting liver drink, alcohol-decomposing beverage etc., these products are main mainly with the traditional Chinese medicine ingredients of relieving the effect of alcohol greatly, then add other the composition that protects the liver, but do not have health-care efficacy.
Summary of the invention
The object of the invention is to overcome above-mentioned technological deficiency, provide a kind of FI puerariae juice milk drink and preparation method thereof, select effect relatively preferably Chinese medicine FI puerariae of relieving the effect of alcohol, the health care in conjunction with dairy products is theoretical, develops novel drink, to cater to the health care theory of modern.FI puerariae is widely distributed in China, and plant resources enriches, and has very high using value.This study portion content, in conjunction with the nutrition of milk, has sober-up function and the functional food with certain nutritive value to developing, for its more wide exploitation in medical treatment, functional food etc. provide theoretical foundation.For the extraction of FI puerariae flavone compound, in line with the principle reducing cost, economize energy, this invention takes mineral water lixiviate assisted microwave synthesis method to extract flavone compound in FI puerariae, object is to reduce operating procedure, reduces extraction cost, is convenient to directly and cow's milk mixture manufacturing FI puerariae juice milk drink.
Its concrete technical scheme is:
A kind of FI puerariae juice milk drink, its formula is specially: the addition of FI puerariae juice is 5%, the addition of sucrose is 8%, the addition of plain chocolate is 30%, compound stabilizer 0.1%, and surplus is mineral water.
A preparation method for FI puerariae juice milk drink of the present invention, comprises the following steps:
100g FI puerariae is put into large beaker, soaks with the mineral water of FI puerariae dose 15 times, 60 DEG C of water-bath preheating 1h, micro-wave oven intermittent radiation 15min, microwave power 700W; Divide three times, each 5min, stops 5min; Six layers of filtered through gauze, the centrifugal 10min of filtered fluid 5000rpm, centrifugate adopt rotary evaporation in vacuo be concentrated into about with the leaching liquor of the homogenous quantities such as FI puerariae, sealing, for subsequent use 0 ~ 4 DEG C of refrigeration;
Compound stabilizer 0.1%, sucrose are used boiling water stirring and dissolving after being dry mixed conjunction again, adds in plain chocolate, then add FI puerariae juice, mix, 65 DEG C of homogeneous, 85 DEG C of pasteurize 15s, are finished product after cooling.
Described compound stabilizer 0.1% specifically comprises CMC0.04%, carragheen 0.03%, xanthans 0.03%.
Compared with prior art, beneficial effect of the present invention is:
1, the FI puerariae flavonoid content of flooding assisted microwave synthesis method extraction is higher, is directly used for producing drink convenient.
2, compared with traditional disintoxicating product, except appliable plant composition, combine again the health care of cow's milk, obtained drink meets the health care theory of modern.
Accompanying drawing explanation
Fig. 1 is the preparation flow schematic diagram of FI puerariae juice;
Fig. 2 be FI puerariae juice milk drink manufacture schematic flow sheet;
Fig. 3 is flavones calibration curve;
Detailed description of the invention
Below in conjunction with specific embodiment, technical scheme of the present invention is described in more detail.
(1) screening of FI puerariae extracting flavonoids method
1, water-boiling method
Take dry FI puerariae medicine materical crude slice 20g, mineral water 300ml is preheating 1h in 60 DEG C of water-baths, then boils 3h, stops 0.5h, then boils 0.5h.6 layers of filtered through gauze.Filtered fluid is concentrated into 100ml, and the centrifugal 10min of 5000rpm, gets supernatant.Write down remaining volume.
2, water extract method
Take FI puerariae 20g, mineral water 300ml, 60 DEG C of water-bath preheating 1h.Six layers of filtered through gauze, filtered fluid is concentrated into 100ml, and the centrifugal 10min of 5000rpm, gets supernatant.Write down remaining volume.
3, flooding-microwave assisting method
Take dry FI puerariae medicine materical crude slice 20g, mineral water 300ml, 60 DEG C of water-bath preheating 1h.Micro-wave oven intermittent radiation 15min, microwave power 700W; Divide three times, each 5min, stops 5min.6 layers of filtered through gauze.Be concentrated into 100ml, the centrifugal 10min of 5000rpm.Get supernatant.Write down remaining volume.
4, alkali liquor extraction method
Take 20g FI puerariae, with 5%NaOH or saturated Ca (OH)
2300ml is preheating 1h in 60 DEG C of water-baths, and six layers of filtered through gauze, are concentrated into 100ml, and the centrifugal 10min of 5000rpm, gets supernatant.Write down remaining volume.
(2) mensuration of FI puerariae flavones content
1, the drafting of flavones standard working curve
Get Puerarin standard items (Nat'l Pharmaceutical & Biological Products Control Institute) 5.0mg in 10mL small beaker, add 95% appropriate ethanol and fully dissolve.Then carefully move in 25mL volumetric flask, then with appropriate 95% ethanol washing beaker several times, and all move in volumetric flask (noting the cumulative volume of not exceed capacity bottle), add 95% ethanol and be settled to scale, fully shake up; Draw 0.2mL, 0.4mL, 0.6mL, 0.8mL, 1.0mL successively to put respectively in 5 10mL volumetric flasks, the ethanol adding 95% supply 1.0mL (as: drawing the ethanol that 0.2mL just mends 0.8mL) again adding distil water dilution be settled to scale, shake up.Simultaneously with 95% ethanol 1.0mL, with distilled water diluting to 10mL, as blank, under 250nm length ultraviolet light, measure absorbance respectively by 1cm quartz cuvette.Analyzing and processing is carried out to data, obtains the linear relation of absorbance and flavones concentration, draw flavones standard working curve.
2, the mensuration of FI puerariae flavones content
Get FI puerariae flavones and slightly carry solution, carry out suitable dilution with water or 5%NaOH.With water or 5%NaOH for blank, under wavelength 250nm, carry out OD pH-value determination pH.Bring OD value into calibration curve formula, calculate FI puerariae flavones content.
(3) technique of FI puerariae juice milk drink and formula
1, technological process and key points for operation
(1) preparation of FI puerariae juice as shown in Figure 1.
(2) key points for operation
100g FI puerariae is put into large beaker, soaks with the mineral water of FI puerariae dose 15 times, 60 DEG C of water-bath preheating 1h, micro-wave oven intermittent radiation 15min, microwave power 700W; Divide three times, each 5min, stops 5min.Six layers of filtered through gauze, the centrifugal 10min of filtered fluid 5000rpm, centrifugate adopt rotary evaporation in vacuo be concentrated into about with the leaching liquor of the homogenous quantities such as FI puerariae, sealing, for subsequent use 0 ~ 4 DEG C of refrigeration.
(3) the manufacturing as shown in Figure 2 of FI puerariae juice milk drink.
(4) key points for operation
Compound stabilizer 0.1% (CMC0.04%, carragheen 0.03%, xanthans 0.03%), sucrose are used boiling water stirring and dissolving after being dry mixed conjunction again, adds in plain chocolate, then add FI puerariae juice, mix, 65 DEG C of homogeneous, 85 DEG C of pasteurize 15s, are finished product after cooling.
2, the experiment of single factor of FI puerariae juice milk drink
Select to carry out experiment of single factor to the larger FI puerariae juice addition of FI puerariae milk beverage quality influence, sucrose addition, plain chocolate addition 3 factors, determine the suitable adding proportion of each factor.
3, the orthogonal test of FI puerariae juice milk drink
On the basis of experiment of single factor, carry out L
9(3
3), the standards of grading according to following table carry out Comprehensive Assessment.
Table 1 standards of grading table
(4) mensuration of FI puerariae flavones content
1, the drafting of Puerarin calibration curve
The absorbance recording variable concentrations Puerarin standard items by ultraviolet spectrophotometry draws the standard working curve of kudzu root flavone content, and abscissa is sample total isoflavone concentration, and ordinate is absorbance.Calculate the linear relation of sample flavones concentration and absorbance.Absorbance the results are shown in Table 2, and the standard working curve of flavones content is shown in Fig. 3.
Table 2 Puerarin titer OD value table (wavelength 250nm)
According to the OD value of measured next Puerarin titer, make Puerarin calibration curve, as Fig. 3.
2, various extracting method isoflavones extraction effect compares
After each sample dilutes 1000 times, 250nm measures OD value, and OD value result is as following table.
The OD value of each sample of table 3
Table 4 calculates concentration according to calibration curve Y=0.0595x+0.039
Contained isoflavone concentration in table 5 20g sample
All the highest by the recovery rate of the flavones analyzing known FI puerariae in the basic conditions above, FI puerariae extract flavones concentration is about 30.96mg/ml, and recovery rate is 15.48%; Next is the flavones concentration of FI puerariae water seaoning-microwave radiation exaraction is 9.39mg/ml, and recovery rate is 4.70%.Because the FI puerariae juice extracted is for the production of food, comparatively bother by the FI puerariae juice subsequent treatment that base extraction FI puerariae obtains, therefore consider selection water seaoning-microwave radiation technology process FI puerariae to obtain FI puerariae juice.
FI puerariae water seaoning-microwave radiation exaraction condition is: FI puerariae and water ratio are 1: 15,60 DEG C of water-bath preheating 1h, then micro-wave oven intermittent radiation 15min, microwave power 700W; Divide three times, each 5min, interval 5min in the middle of each.The method FI puerariae extracting flavonoids rate is 4.70%.
(5) process optimization of FI puerariae juice milk drink
1 experiment of single factor interpretation of result
(1) determination of FI puerariae juice addition
By plain chocolate 30%, sucrose 8%, 0.1% compound stabilizer (CMC0.04%, carragheen 0.03%, xanthans 0.03%), mixing, add the FI puerariae juice of 3%, 5%, 7%, 9%, 11% respectively, subjective appreciation is carried out to FI puerariae milk beverage, the results are shown in Table 6.
The determination of table 6 FI puerariae juice addition
As shown in Table 6, when FI puerariae juice addition is less than 5%, FI puerariae taste is not obvious; When the addition of FI puerariae juice is greater than 9%, FI puerariae taste is heavier and have obvious bitter taste; And when the addition of FI puerariae juice is that 5%, 7%, 9% mouthfeel color and luster is all relatively better.Therefore the FI puerariae juice addition of 5%, 7%, 9% carries out orthogonal test.
(2) determination of sucrose addition
By plain chocolate 30%, FI puerariae juice 7%, compound stabilizer 0.1% (CMC0.04%, carragheen 0.03%, xanthans 0.03%), mixing, add the sucrose of 4%, 6%, 8%, 10%, 12% respectively, subjective appreciation is carried out to FI puerariae milk beverage, the results are shown in Table 7.
The determination of table 7 sucrose addition
As shown in Table 7, have milk fragrance to have again FI puerariae taste when the addition of sucrose is less than 6%, but the bitter taste of FI puerariae is heavier; It is partially sweet when the addition of sucrose is greater than 10%; And the addition of FI puerariae bitter comfortable when being 6%, 8%, 10% in.Therefore select the sucrose addition of 6%, 8%, 10% to carry out orthogonal test.
(3) determination of plain chocolate addition
Get the plain chocolate of 10%, 20%, 30%, 40%, 50% respectively, then FI puerariae juice, the sucrose of 8%, the compound stabilizer (CMC0.04%, carragheen 0.03%, xanthans 0.03%) of 0.1% of 7% is added, subjective appreciation is carried out to FI puerariae milk beverage, the results are shown in Table 8.
The determination of table 8 plain chocolate addition
As shown in Table 8, when the addition of plain chocolate is less than 20%, milk taste is lighter, and FI puerariae taste is overweight; When the addition of plain chocolate is greater than 40%, milk taste is overweight, and FI puerariae taste is lighter; And the addition of plain chocolate when being 20%, 30%, 40% existing FI puerariae taste have milk fragrance, therefore select the plain chocolate addition of 20%, 30%, 40% to carry out orthogonal test.
2 orthogonal experiments analyses
On the basis of experiment of single factor, with FI puerariae juice addition, sucrose addition and plain chocolate addition for factor carries out L
9(3
3), specific design table is in table 9, and Orthogonal experiment results is in table 10.
Table 9 orthogonal test factor level
The analysis of table 10 orthogonal experiments
As shown in Table 10, the affect size of each factor on FI puerariae milk beverage is C > A > B, namely the addition of plain chocolate is the principal element affecting FI puerariae milk beverage, is secondly the addition of FI puerariae juice, is finally the addition of sucrose.Optimum formula is A
1b
2c
2, namely FI puerariae juice addition is 5%, sucrose addition is 8%, the addition of plain chocolate is 30%.
The quality index of 3 FI puerariae juice milk drinks
(1) organoleptic indicator of FI puerariae juice milk drink
The organoleptic indicator of table 11 FI puerariae juice milk drink
(2) physical and chemical index of FI puerariae juice milk drink
The physical and chemical index of table 12 FI puerariae juice milk drink
(3) microbiological indicator of FI puerariae juice milk drink
The microbiological indicator of table 13 FI puerariae juice milk drink
4 conclusions
The optimum formula of FI puerariae juice milk drink is: the addition of FI puerariae juice is 5%, the addition of sucrose is 8%, the addition of plain chocolate is 30%, finally complements to 100% with mineral water.Obtained Pueraria lobota flower juice beverage be light coffee color, glossy, and structural state is evenly fine and smooth, has the distinctive smell of FI puerariae juice and milk taste is strong, and during hardship is comfortable, mouthfeel is better.
Embodiment 1 FI puerariae water seaoning-microwave radiation exaraction condition
FI puerariae and water ratio are 1: 15,60 DEG C of water-bath preheating 1h, then micro-wave oven intermittent radiation 15min, microwave power 700W; Divide three times, each 5min, interval 5min in the middle of each.The method FI puerariae extracting flavonoids rate is 4.70%.
The formula of embodiment 2 FI puerariae juice milk drink
The addition of FI puerariae juice is 5%, the addition of sucrose is 8%, the addition of plain chocolate is 30%.Obtained Pueraria lobota flower juice beverage be light coffee color, glossy, and structural state is evenly fine and smooth, has the distinctive smell of FI puerariae juice and milk taste is strong, and during hardship is comfortable, mouthfeel is better.
The above; be only the present invention's preferably detailed description of the invention; protection scope of the present invention is not limited thereto; anyly be familiar with those skilled in the art in the technical scope that the present invention discloses, the simple change of the technical scheme that can obtain apparently or equivalence are replaced and are all fallen within the scope of protection of the present invention.
Claims (3)
1. a FI puerariae juice milk drink, is characterized in that, its formula is specially: the addition of FI puerariae juice is 5%, the addition of sucrose is 8%, the addition of plain chocolate is 30%, compound stabilizer 0.1%, and surplus is mineral water.
2. a preparation method for FI puerariae juice milk drink described in claim 1, is characterized in that, 100g FI puerariae is put into large beaker, soaks, 60 DEG C of water-bath preheating 1h, micro-wave oven intermittent radiation 15min, microwave power 700W with the mineral water of FI puerariae dose 15 times; Divide three times, each 5min, stops 5min; Six layers of filtered through gauze, the centrifugal 10min of filtered fluid 5000rpm, centrifugate adopt rotary evaporation in vacuo be concentrated into about with the leaching liquor of the homogenous quantities such as FI puerariae, sealing, for subsequent use 0 ~ 4 DEG C of refrigeration;
Compound stabilizer 0.1%, sucrose are used boiling water stirring and dissolving after being dry mixed conjunction again, adds in plain chocolate, then add FI puerariae juice, mix, 65 DEG C of homogeneous, 85 DEG C of pasteurize 15s, are finished product after cooling.
3. the preparation method of FI puerariae juice milk drink according to claim 2, it is characterized in that, described compound stabilizer 0.1% specifically comprises CMC0.04%, carragheen 0.03%, xanthans 0.03%.
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Cited By (3)
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| CN106857845A (en) * | 2016-12-30 | 2017-06-20 | 佛山科学技术学院 | A kind of flower of kudzuvine and milk powder relieve the effect of alcohol composite beverage and preparation method thereof |
| CN110074187A (en) * | 2019-04-18 | 2019-08-02 | 浙江李子园食品股份有限公司 | A kind of Aralia continentalis Kitag milk beverage and preparation method thereof |
| CN113521059A (en) * | 2021-09-06 | 2021-10-22 | 甘肃中医药大学 | New application of pueraria lobata small molecules in regulating alcohol dependence behavior |
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Application publication date: 20150325 |