CN104413406A - Processing craft for extracting composite bone collagen from yak bone - Google Patents
Processing craft for extracting composite bone collagen from yak bone Download PDFInfo
- Publication number
- CN104413406A CN104413406A CN201310406154.6A CN201310406154A CN104413406A CN 104413406 A CN104413406 A CN 104413406A CN 201310406154 A CN201310406154 A CN 201310406154A CN 104413406 A CN104413406 A CN 104413406A
- Authority
- CN
- China
- Prior art keywords
- bone
- yak
- collagen
- composite bone
- composite
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 210000000988 bone and bone Anatomy 0.000 title claims abstract description 51
- 102000008186 Collagen Human genes 0.000 title claims abstract description 17
- 108010035532 Collagen Proteins 0.000 title claims abstract description 17
- 229920001436 collagen Polymers 0.000 title claims abstract description 17
- 239000002131 composite material Substances 0.000 title claims abstract description 17
- 239000002994 raw material Substances 0.000 claims description 7
- 239000000843 powder Substances 0.000 claims description 3
- 239000000463 material Substances 0.000 abstract description 11
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract description 6
- 239000002253 acid Substances 0.000 abstract description 6
- 239000002537 cosmetic Substances 0.000 abstract description 4
- 238000000227 grinding Methods 0.000 abstract description 3
- 238000001035 drying Methods 0.000 abstract description 2
- 239000008187 granular material Substances 0.000 abstract 2
- 238000001914 filtration Methods 0.000 abstract 1
- 238000002386 leaching Methods 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 230000001376 precipitating effect Effects 0.000 abstract 1
- 238000010025 steaming Methods 0.000 abstract 1
- 239000011505 plaster Substances 0.000 description 5
- 238000003756 stirring Methods 0.000 description 5
- 238000009835 boiling Methods 0.000 description 4
- 239000012535 impurity Substances 0.000 description 4
- 150000003839 salts Chemical class 0.000 description 4
- 239000002893 slag Substances 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 239000000284 extract Substances 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 235000016709 nutrition Nutrition 0.000 description 3
- 238000001556 precipitation Methods 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 235000014347 soups Nutrition 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 102000011759 adducin Human genes 0.000 description 2
- 108010076723 adducin Proteins 0.000 description 2
- 239000010775 animal oil Substances 0.000 description 2
- 230000035764 nutrition Effects 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 239000013049 sediment Substances 0.000 description 2
- 239000006228 supernatant Substances 0.000 description 2
- 238000010792 warming Methods 0.000 description 2
- 208000010392 Bone Fractures Diseases 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- 229920002567 Chondroitin Polymers 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- DLGJWSVWTWEWBJ-HGGSSLSASA-N chondroitin Chemical compound CC(O)=N[C@@H]1[C@H](O)O[C@H](CO)[C@H](O)[C@@H]1OC1[C@H](O)[C@H](O)C=C(C(O)=O)O1 DLGJWSVWTWEWBJ-HGGSSLSASA-N 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 230000029087 digestion Effects 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 238000013467 fragmentation Methods 0.000 description 1
- 238000006062 fragmentation reaction Methods 0.000 description 1
- 235000001497 healthy food Nutrition 0.000 description 1
- 238000002372 labelling Methods 0.000 description 1
- 244000144972 livestock Species 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000010907 mechanical stirring Methods 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23J—PROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
- A23J1/00—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites
- A23J1/10—Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites from hair, feathers, horn, skins, leather, bones, or the like
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/981—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of mammals or bird
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Abstract
The invention provides a processing craft for extracting composite bone collagen from yak bone. Composite bone collagen in yak bone is extracted by the following procedures: selecting the yak bone material, crushing, steaming, separating, grinding, carrying out acid leaching, removing acid, filtering, carrying out alcohol precipitating, dewatering and drying, so that high-concentration composite bone collage granules can be prepared. The composite bone collage granules can be used for preparing various nourishments, health care products and cosmetics.
Description
Technical field
The invention belongs to livestock products manufacture field, relate to and extract nutriment from Yak Bone, from Yak Bone, especially extract the processing technology of Composite Bone collagen.
Background technology
As everyone knows, Animal Bone collagen contains abundant collagen, chondroitin, calcium activated, amino acid and other various nutrient elements, can be widely used in healthy food industry and cosmetic industry.Yak is due to the growing environment of uniqueness, and the weather of highland and severe cold anoxic, the features such as strong ultraviolet radiation and growth cycle length, make the nutritional labeling of Yak Bone and kind very abundant.By extraction processing technology provided by the invention, the useful component in Yak Bone is extracted, become the powder of high enrichment, can be used for making various nutriment, health products and cosmetics.
Summary of the invention
The invention provides a kind of processing technology extracting Composite Bone collagen from Yak Bone, the useful component in Yak Bone is extracted, become the Composite Bone collagen powder of high enrichment.
The technical solution adopted for the present invention to solve the technical problems is: a kind of processing technology extracting Composite Bone collagen from Yak Bone, comprises the steps:
1. select materials: select healthy fresh yak bones as raw material, except the surface impurity of attachment removal;
2. broken: the rear crusher in crushing of Yak Bone cleaning;
3. boiling: by broken for Yak Bone block, drop in cooker, add the water of 1 ~ 2 times, and stir, pass into steam and make soup be warming up to 110 ~ 130 DEG C, under pressure is 0.1 ~ 0.2MP, hot digestion 2.5 ~ 3.5 hours;
4. be separated: the raw material after boiling is thrown solid-liquid separating machine and is separated, isolate animal oil and bone soup and bone slag;
5. defibrination: isolated bone slag is carried out defibrination through bone mud mill;
5. acidleach: defibrination uses acid soak 7 ~ 8 days at 10 ~ 25 DEG C of temperature, constantly stirs, makes the insoluble inorganic salts in broken bone mud change into solubility salt;
6. move back acid: add in alkaline water and acid solution, regulate solution pH value to be neutral, to promote the dissolving of nutrition;
7. filter: except decorticating, skeletal grain and other impurity;
8. concentrated: transpiring moisture, reduce volume, become rare plaster material;
9. alcohol precipitation: stir and add 95 % alcohol, by the utility Precipitation in rare plaster material;
10. dewater: repeatedly add content 95 % alcohol to the sediment collected, the moisture content in material is oozed out the object reaching dehydration;
11. dry: drying box 60 DEG C ~ 65 DEG C exhausting are dried, and obtain Yak Bone Composite Bone collagen particle, grinding packs.
The invention has the beneficial effects as follows, taking raw material is Yak Bone, and Yak Bone ossein rich content, extracts the ossein in Yak Bone, can be used for making various nutriment, health products and cosmetics.
Specific embodiment
Below in conjunction with embodiment, the present invention is further described.
1. select healthy fresh Yak Bone 100kg as raw material, except the surface impurity of attachment removal, clean rear crusher in crushing;
2. dropped in cooker by the bone block after fragmentation, the water gaging such as to add, water will flood bone block, passed into steam and was warming up to 120 DEG C, and pressure is 0.15MP, under mechanical stirring, and boiling 3 hours;
3. the raw material after boiling is put into solid-liquid separating machine to be separated, isolate bone slag, animal oil and bone soup;
4. isolated bone slag is about 55kg, is used bone mud to grind and carries out defibrination;
5. soak 7 days at 15 DEG C of temperature with 3.5% hydrochloric acid 80L, constantly stir, make the insoluble inorganic salts in aggregate change into solubility salt;
6. progressively add NaHC0
3in solution and acid solution, addition regulates solution pH value for till neutrality, to promote the dissolving of nutrition to reach;
7. carry out centrifugally operated in batches with 3000 revs/min, centrifuge, with except decorticating, skeletal grain and other impurity, stay supernatant;
8. supernatant is heated to 60 DEG C ~ 65 DEG C, and with transpiring moisture, make liquid concentration become rare plaster material, about 8kg, volume is about original 10 ~ 15%;
9. stir and add 95 % alcohol in rare plaster material, by the utility Precipitation in rare plaster material, the amount added is 2 times amount, static 1 hour of capping, then upper strata Diluted Alcohol is extracted out, leave sediment, 3 ~ 4 times repeatedly, until material progressively becomes solid discrete particles by rare paste;
10. the drip pan of splendid attire material being placed on temperature controls in 65 DEG C of baking ovens, exhausting is dry, make moisture control dry end below 10%, must about 7kg Composite Bone collagen, packed by dried material grinding, gained Composite Bone collagen accounts for fresh raw material and weighs 7 ~ 10 & about % again.
Claims (2)
1. from Yak Bone, extracting a processing technology for Composite Bone collagen, it is characterized in that by Yak Bone as raw material, from wherein extracting Composite Bone collagen.
2. a kind of processing technology extracting Composite Bone collagen from Yak Bone according to claim 1, its Composite Bone collagen extracted is powder.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310406154.6A CN104413406A (en) | 2013-09-09 | 2013-09-09 | Processing craft for extracting composite bone collagen from yak bone |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310406154.6A CN104413406A (en) | 2013-09-09 | 2013-09-09 | Processing craft for extracting composite bone collagen from yak bone |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104413406A true CN104413406A (en) | 2015-03-18 |
Family
ID=52964337
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310406154.6A Pending CN104413406A (en) | 2013-09-09 | 2013-09-09 | Processing craft for extracting composite bone collagen from yak bone |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104413406A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105753972A (en) * | 2016-04-27 | 2016-07-13 | 中国农业科学院农产品加工研究所 | Method for co-production of yak ossein peptide chelated calcium and bone polypeptide |
| CN106619177A (en) * | 2016-11-25 | 2017-05-10 | 兰州大学 | Whitening and moisturizing cosmetic of white yak bone collagen protein peptide and preparation method of whitening and moisturizing cosmetic |
| CN106727255A (en) * | 2017-03-03 | 2017-05-31 | 王书敏 | A kind of shampoo comprising natural surfactant and preparation method thereof |
| CN112022790A (en) * | 2020-09-08 | 2020-12-04 | 湖南神农国油生态农业发展有限公司 | Eye cream capable of effectively slowing fine line regeneration and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1334302A (en) * | 2001-04-08 | 2002-02-06 | 内蒙古草原兴发股份有限公司 | Process for preparing bone collagen |
| CN1385489A (en) * | 2002-05-22 | 2002-12-18 | 赵成军 | Working technology for extracting ossein from animal cartilage |
| CN1507802A (en) * | 2002-12-17 | 2004-06-30 | 中国科学院西北高原生物研究所 | Yak bone crystal extraction and separation process |
| CN102229971A (en) * | 2011-05-10 | 2011-11-02 | 苏州瑞蓝博中药技术开发有限公司 | Method for preparing collagen peptides by using fresh yak bones |
-
2013
- 2013-09-09 CN CN201310406154.6A patent/CN104413406A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1334302A (en) * | 2001-04-08 | 2002-02-06 | 内蒙古草原兴发股份有限公司 | Process for preparing bone collagen |
| CN1385489A (en) * | 2002-05-22 | 2002-12-18 | 赵成军 | Working technology for extracting ossein from animal cartilage |
| CN1507802A (en) * | 2002-12-17 | 2004-06-30 | 中国科学院西北高原生物研究所 | Yak bone crystal extraction and separation process |
| CN102229971A (en) * | 2011-05-10 | 2011-11-02 | 苏州瑞蓝博中药技术开发有限公司 | Method for preparing collagen peptides by using fresh yak bones |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105753972A (en) * | 2016-04-27 | 2016-07-13 | 中国农业科学院农产品加工研究所 | Method for co-production of yak ossein peptide chelated calcium and bone polypeptide |
| CN106619177A (en) * | 2016-11-25 | 2017-05-10 | 兰州大学 | Whitening and moisturizing cosmetic of white yak bone collagen protein peptide and preparation method of whitening and moisturizing cosmetic |
| CN106727255A (en) * | 2017-03-03 | 2017-05-31 | 王书敏 | A kind of shampoo comprising natural surfactant and preparation method thereof |
| CN106727255B (en) * | 2017-03-03 | 2020-09-15 | 王书敏 | Shampoo containing natural surfactant and preparation method thereof |
| CN112022790A (en) * | 2020-09-08 | 2020-12-04 | 湖南神农国油生态农业发展有限公司 | Eye cream capable of effectively slowing fine line regeneration and preparation method thereof |
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| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20150318 |
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| WD01 | Invention patent application deemed withdrawn after publication |