CN105687093B - A kind of natural anti-aging red pomegranate skin care item and preparation method thereof - Google Patents

A kind of natural anti-aging red pomegranate skin care item and preparation method thereof Download PDF

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CN105687093B
CN105687093B CN201610189191.XA CN201610189191A CN105687093B CN 105687093 B CN105687093 B CN 105687093B CN 201610189191 A CN201610189191 A CN 201610189191A CN 105687093 B CN105687093 B CN 105687093B
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red pomegranate
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pomegranate
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崔曦方
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GANSU XIANGCAOFANG NATIVE PRODUCTS CO Ltd
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Abstract

The present invention discloses a kind of natural anti-aging red pomegranate skin care item and preparation method thereof, belongs to cosmetic technical field.The skin care item are formulated by following raw material:Red pomegranate pulp extract, red pomegranate severe edema due to hypofunction of the spleen extract, red pomegranate seed oil, red pomegranate flower essential oil, chlorella growth factor, red jujube polysaccharide, silk essence, angelica extract, phellodendron extract, licorice, Bulbus Lilii extract, rose, tea tree hydrosol, silk gum, water soluble pearl powder, cocoyl alanine triethanolamine salt, Cocoamidopropyl betaine, lauric monoglyceride and glacier water surplus.The present invention using red pomegranate flower, seed, skin, pulp extract as primary raw material, it is aided with the natural components such as Radix Glycyrrhizae, silk essence, chlorella extract, maintenance skin can be improved, effectively dispel the dry aging cutin of skin surface, it is excessive to control skin oil and fat secretion, has the function of skin maintenance and cosmetic benefits, enhances the elasticity and vigor of skin, deep layer cleaning is moistened, and has senile-resistant efficacy.

Description

A kind of natural anti-aging red pomegranate skin care item and preparation method thereof
Technical field
The invention belongs to cosmetic technical fields, and in particular to a kind of natural anti-aging red pomegranate skin care item and its preparation side Method.
Background technique
Red pomegranate is a kind for pomegranate, after maturation pericarp be pink due to gain the name.Red pomegranate have Yimeng red pomegranate, Beautiful purchase red pomegranate.It gains the name due to the former is because of the main product of red pomegranate, the latter is due to the processing technology of red pomegranate and raw material are applied It gains the name.Red pomegranate nature and flavor are sweet, sour and astringent, warm, and the substances such as vitamin C, Punica granatum L. polyphenol and anthocyanidin rich in, have very in fruit Toxin expelling well, anti-oxidation efficacy also contain the mineral matter elements such as linolenic acid, vitamin B6, E and folic acid and calcium, magnesium, zinc, energy Supplement skin institute's dehydration point rapidly, enables skin quality more become clear soft and moist.Therefore, many domestic and international well-known beauty and skin care brand all lands It is continuous to be proposed the skin care item containing pomegranate beauty element.
Summary of the invention
An object of the present invention is to provide a kind of natural anti-aging red pomegranate skin care item, and another object is to provide the day The preparation method of right anti-aging red pomegranate skin care item.
To achieve the goals above, the technical solution adopted by the present invention is as follows:
A kind of natural anti-aging red pomegranate skin care item, are formulated by the raw material of following weight ratio:Red pomegranate pulp extracts Object 10~15%, red pomegranate severe edema due to hypofunction of the spleen extract 1~7%, red pomegranate seed oil 1~4%, red pomegranate flower essential oil 3~6%, chlorella are raw The long factor 5~8%, red jujube polysaccharide 1~2%, silk essence 3~4%, angelica extract 3~6%, phellodendron extract 3~4%, Radix Glycyrrhizae It is extract 4~5%, Bulbus Lilii extract 2~3%, rose 1~2%, tea tree hydrosol 0.5~1%, silk gum 2~3%, water-soluble Property pearl powder 1~3%, cocoyl alanine triethanolamine salt 3~5%, Cocoamidopropyl betaine 1~3%, lauric acid Monoglyceride 1~2% and glacier water surplus.
Preferably, the natural anti-aging red pomegranate skin care item, are formulated by the raw material of following weight ratio:Red stone Pomegranate pulp extract 12.5%, red pomegranate bark extract 4%, red pomegranate seed oil 2.5%, red pomegranate flower essential oil 4.5%, chlorella Growth factor 6.5%, red jujube polysaccharide 1.5%, silk essence 3.5%, angelica extract 4.5%, phellodendron extract 3.5%, Radix Glycyrrhizae mention Take object 4.5%, Bulbus Lilii extract 2.5%, rose 1.5%, tea tree hydrosol 1%, silk gum 2.5%, water soluble pearl powder 2%, cocoyl alanine triethanolamine salt 4%, Cocoamidopropyl betaine 2%, lauric monoglyceride 1.5% and ice River water 35.5%.
The present invention also provides the preparation methods of the natural anti-aging red pomegranate skin care item, include the following steps:
(1) scarlet pomegranate is taken to clean, red pomegranate pulp is first directly squeezed the juice and obtains red pomegranate Normal juice by demucilage, seed, skin, Clarification filtration collects clear liquid, is freeze-dried after concentration, obtains red pomegranate pulp extract;Then red pomegranate seed is dried, it is aqueous Rate control squeezing in 8~10%, investment squeezer, temperature are controlled at 50~80 DEG C, are obtained primary red pomegranate seed oil, are taken out residual Slag is crushed to 80 mesh, and seed slag end puts into Ultrasonic Wave-Assisted Extraction in petroleum ether, by solid-liquid ratio (w/v) 1:10, in Extracting temperature 35 ~50 DEG C, 1~2h is extracted under conditions of ultrasonic power 60W, vacuum distillation obtains secondary red pomegranate seed oil, merges primary red stone The active carbon of its quality 2~5% is added in obtained mixing seed oil for pomegranate seed oil and secondary red pomegranate seed oil, stir 10~ 20min, filtering obtain red pomegranate seed oil;Red pomegranate skin is dried, 60~80 mesh are crushed to, 15~20 times of its quality amounts are added Water, Ultrasonic Wave-Assisted Extraction under conditions of 45~85 DEG C, ultrasonic power 80W, 2~3h of extraction time are then centrifuged for, mistake Filter is concentrated under reduced pressure, and freeze-drying obtains red pomegranate bark extract;
(2)) red pomegranate fresh flower and water investment distillation still are distilled, the mass ratio of red pomegranate fresh flower and water is 1:5~6, It is passed through steam into distillation still to directly heat red pomegranate fresh flower and water, distills 5~5.5h, the vacuum degree in distillation still is -0.8 ~-0.1MPa, vapo(u)rizing temperature are 90~95 DEG C, oil water separator are imported after the distillate that distillation still comes out is cooling, at 28-38 DEG C Under the conditions of carry out water-oil separating, discard water layer, obtained oil reservoir is red pomegranate flower essential oil;
(3) red pomegranate pulp extract, red pomegranate bark extract, chlorella growth factor, red is sequentially added in glacial water Jujube polysaccharide, angelica extract, phellodendron extract, licorice, Bulbus Lilii extract, rose, tea tree hydrosol, and stir, 35~55 DEG C are then heated to, continuously adding silk gum, silk essence, water soluble pearl powder makes to dissolve, and obtains component A;
(4) red pomegranate seed oil and red pomegranate flower essential oil are mixed, are heated to 45~65 DEG C, it is sweet that lauric acid list is added thereto Grease, cocoyl alanine triethanolamine salt, Cocoamidopropyl betaine, stirring evenly makes miscible, obtains component B;
(5) under the conditions of 40 DEG C of temperature, component A and component B is mixed, supplies glacial water, emulsification uniformly, is down to room temperature, examines Filling, packaging after survey is qualified.
Advantageous effects of the invention:The present invention is mentioned using red pomegranate as primary raw material using its flower, seed, skin, pulp It takes object to be aided with the natural components such as Radix Glycyrrhizae, silk essence, chlorella extract, maintenance skin can be improved, effectively dispel the dry aging of skin surface Cutin, control skin oil and fat secretion is excessive, has the function of skin maintenance and cosmetic benefits, enhances the elasticity and vigor of skin, and deep layer cleaning is moistened, There is senile-resistant efficacy.
Specific embodiment
Elaboration further is made to the present invention below with reference to embodiment, is not constituted to any range limitation of the invention.
Embodiment 1
A kind of natural anti-aging red pomegranate skin care item, are formulated by the raw material of following weight ratio:Red pomegranate pulp extracts Object 10%, red pomegranate severe edema due to hypofunction of the spleen extract 1%, red pomegranate seed oil 1%, red pomegranate flower essential oil 3%, chlorella growth factor 5%, jujube Polysaccharide 1%, silk essence 3%, angelica extract 3%, phellodendron extract 3%, licorice 4%, Bulbus Lilii extract 2%, rose Hydrosol 1%, tea tree hydrosol 0.5%, silk gum 2%, water soluble pearl powder 1%, cocoyl alanine triethanolamine salt 3%, coconut palm Oleamide propyl betaine 1%, lauric monoglyceride 1% and glacier water surplus.
The preparation method of the natural anti-aging red pomegranate skin care item, includes the following steps:
(1) scarlet pomegranate is taken to clean, red pomegranate pulp is first directly squeezed the juice and obtains red pomegranate Normal juice by demucilage, seed, skin, Clarification filtration collects clear liquid, is freeze-dried after concentration, obtains red pomegranate pulp extract;Then red pomegranate seed is dried, it is aqueous Rate control squeezing in 8%, investment squeezer, temperature are controlled at 50 DEG C, are obtained primary red pomegranate seed oil, are taken out residue, crush To 80 mesh, seed slag end puts into Ultrasonic Wave-Assisted Extraction in petroleum ether, by solid-liquid ratio (w/v) 1:10, in 35 DEG C of Extracting temperature, ultrasound 1h is extracted under conditions of power 60W, is evaporated under reduced pressure, secondary red pomegranate seed oil is obtained, and merges primary red pomegranate seed oil and secondary is red The active carbon of its quality 2% is added in obtained mixing seed oil, stirs 10min, filtering obtains red pomegranate seed oil for granada seed oil; Red pomegranate skin is dried, 60 mesh are crushed to, be added 15 times of its quality amount water, Ultrasonic Wave-Assisted Extraction under conditions of 45 DEG C, Ultrasonic power 80W, extraction time 2h, is then centrifuged for, and filters, and is concentrated under reduced pressure, and freeze-drying obtains red pomegranate bark extract;
(2)) red pomegranate fresh flower and water investment distillation still are distilled, the mass ratio of red pomegranate fresh flower and water is 1:5, to It is passed through steam in distillation still to directly heat red pomegranate fresh flower and water, distills 5h, the vacuum degree in distillation still is -0.8MPa, is steamed Evaporating temperature is 90 DEG C, imports oil water separator after the distillate that distillation still comes out is cooling, grease point is carried out under the conditions of 28-38 DEG C From discarding water layer, obtained oil reservoir is red pomegranate flower essential oil;
(3) red pomegranate pulp extract, red pomegranate bark extract, chlorella growth factor, red is sequentially added in glacial water Jujube polysaccharide, angelica extract, phellodendron extract, licorice, Bulbus Lilii extract, rose, tea tree hydrosol, and stir, 35 DEG C are then heated to, continuously adding silk gum, silk essence, water soluble pearl powder makes to dissolve, and obtains component A;
(4) red pomegranate seed oil and red pomegranate flower essential oil are mixed, are heated to 45 DEG C, be added thereto lauric monoglyceride, Cocoyl alanine triethanolamine salt, Cocoamidopropyl betaine, stirring evenly makes miscible, obtains component B;
(5) under the conditions of 40 DEG C of temperature, component A and component B is mixed, supplies glacial water, emulsification uniformly, is down to room temperature, examines Filling, packaging after survey is qualified.
Embodiment 2
A kind of natural anti-aging red pomegranate skin care item, are formulated by the raw material of following weight ratio:Red pomegranate pulp extracts Object 15%, red pomegranate severe edema due to hypofunction of the spleen extract 7%, red pomegranate seed oil 4%, red pomegranate flower essential oil 6%, chlorella growth factor 8%, jujube Polysaccharide 2%, silk essence 4%, angelica extract 6%, phellodendron extract 4%, licorice 5%, Bulbus Lilii extract 3%, rose Hydrosol 2%, tea tree hydrosol 1%, silk gum 3%, water soluble pearl powder 3%, cocoyl alanine triethanolamine salt 5%, cocounut oil Amido propyl betaine 3%, lauric monoglyceride 2% and glacier water surplus.
The preparation method of the natural anti-aging red pomegranate skin care item, includes the following steps:
(1) scarlet pomegranate is taken to clean, red pomegranate pulp is first directly squeezed the juice and obtains red pomegranate Normal juice by demucilage, seed, skin, Clarification filtration collects clear liquid, is freeze-dried after concentration, obtains red pomegranate pulp extract;Then red pomegranate seed is dried, it is aqueous Rate control squeezing in 10%, investment squeezer, temperature are controlled at 80 DEG C, are obtained primary red pomegranate seed oil, are taken out residue, crush To 80 mesh, seed slag end puts into Ultrasonic Wave-Assisted Extraction in petroleum ether, by solid-liquid ratio (w/v) 1:10, in 50 DEG C of Extracting temperature, ultrasound 2h is extracted under conditions of power 60W, is evaporated under reduced pressure, secondary red pomegranate seed oil is obtained, and merges primary red pomegranate seed oil and secondary is red The active carbon of its quality 5% is added in obtained mixing seed oil, stirs 20min, filtering obtains red pomegranate seed oil for granada seed oil; Red pomegranate skin is dried, 80 mesh are crushed to, the water of 20 times of its quality amounts, ultrasonic wave assisted Leaching under conditions of 45~85 DEG C is added It mentions, ultrasonic power 80W, extraction time 3h is then centrifuged for, and is filtered, and is concentrated under reduced pressure, and freeze-drying obtains red pomegranate bark extract;
(2)) red pomegranate fresh flower and water investment distillation still are distilled, the mass ratio of red pomegranate fresh flower and water is 1:6, to It is passed through steam in distillation still to directly heat red pomegranate fresh flower and water, distills 5.5h, the vacuum degree in distillation still is -0.1MPa, Vapo(u)rizing temperature is 95 DEG C, imports oil water separator after the distillate that distillation still comes out is cooling, grease is carried out under the conditions of 28-38 DEG C Separation, discards water layer, obtained oil reservoir is red pomegranate flower essential oil;
(3) red pomegranate pulp extract, red pomegranate bark extract, chlorella growth factor, red is sequentially added in glacial water Jujube polysaccharide, angelica extract, phellodendron extract, licorice, Bulbus Lilii extract, rose, tea tree hydrosol, and stir, 55 DEG C are then heated to, continuously adding silk gum, silk essence, water soluble pearl powder makes to dissolve, and obtains component A;
(4) red pomegranate seed oil and red pomegranate flower essential oil are mixed, are heated to 65 DEG C, be added thereto lauric monoglyceride, Cocoyl alanine triethanolamine salt, Cocoamidopropyl betaine, stirring evenly makes miscible, obtains component B;
(5) under the conditions of 40 DEG C of temperature, component A and component B is mixed, supplies glacial water, emulsification uniformly, is down to room temperature, examines Filling, packaging after survey is qualified.
Embodiment 3
A kind of natural anti-aging red pomegranate skin care item, are formulated by the raw material of following weight ratio:Red pomegranate pulp extracts Object 12.5%, red pomegranate bark extract 4%, red pomegranate seed oil 2.5%, red pomegranate flower essential oil 4.5%, chlorella growth factor 6.5%, red jujube polysaccharide 1.5%, silk essence 3.5%, angelica extract 4.5%, phellodendron extract 3.5%, licorice 4.5%, Bulbus Lilii extract 2.5%, rose 1.5%, tea tree hydrosol 1%, silk gum 2.5%, water soluble pearl powder 2%, coconut palm Oleoyl alanine triethanolamine salt 4%, Cocoamidopropyl betaine 2%, lauric monoglyceride 1.5% and glacial water 35.5%.
The preparation method of the natural anti-aging red pomegranate skin care item, includes the following steps:
(1) scarlet pomegranate is taken to clean, red pomegranate pulp is first directly squeezed the juice and obtains red pomegranate Normal juice by demucilage, seed, skin, Clarification filtration collects clear liquid, is freeze-dried after concentration, obtains red pomegranate pulp extract;Then red pomegranate seed is dried, it is aqueous Rate control squeezing in 9%, investment squeezer, temperature are controlled at 65 DEG C, are obtained primary red pomegranate seed oil, are taken out residue, crush To 80 mesh, seed slag end puts into Ultrasonic Wave-Assisted Extraction in petroleum ether, by solid-liquid ratio (w/v) 1:10, in 45 DEG C of Extracting temperature, ultrasound 1.5h is extracted under conditions of power 60W, is evaporated under reduced pressure, secondary red pomegranate seed oil is obtained, and it is oily and secondary to merge primary red pomegranate seed Red pomegranate seed is oily, and the active carbon of its quality 3.5% is added in obtained mixing seed oil, stirs 15min, filtering obtains red pomegranate Seed oil;Red pomegranate skin is dried, 80 mesh are crushed to, the water of 18 times of its quality amounts is added, ultrasonic wave assists under conditions of 65 DEG C Extraction, ultrasonic power 80W, extraction time 2.5h are then centrifuged for, and are filtered, and are concentrated under reduced pressure, and freeze-drying obtains red pomegranate skin and mentions Take object;
(2)) red pomegranate fresh flower and water investment distillation still are distilled, the mass ratio of red pomegranate fresh flower and water is 1:5.5 It is passed through steam into distillation still to directly heat red pomegranate fresh flower and water, distills 5~5.5h, the vacuum degree in distillation still is- 0.5MPa, vapo(u)rizing temperature are 93 DEG C, import oil water separator after the distillate that distillation still comes out is cooling, carry out under the conditions of 32 DEG C Water-oil separating discards water layer, and obtained oil reservoir is red pomegranate flower essential oil;
(3) red pomegranate pulp extract, red pomegranate bark extract, chlorella growth factor, red is sequentially added in glacial water Jujube polysaccharide, angelica extract, phellodendron extract, licorice, Bulbus Lilii extract, rose, tea tree hydrosol, and stir, 45 DEG C are then heated to, continuously adding silk gum, silk essence, water soluble pearl powder makes to dissolve, and obtains component A;
(4) red pomegranate seed oil and red pomegranate flower essential oil are mixed, are heated to 55 DEG C, be added thereto lauric monoglyceride, Cocoyl alanine triethanolamine salt, Cocoamidopropyl betaine, stirring evenly makes miscible, obtains component B;
(5) under the conditions of 40 DEG C of temperature, component A and component B is mixed, supplies glacial water, emulsification uniformly, is down to room temperature, examines Filling, packaging after survey is qualified.

Claims (2)

1. a kind of natural anti-aging red pomegranate skin care item, which is characterized in that be formulated by the raw material of following weight ratio:Red pomegranate Pulp extract 10~15%, red pomegranate severe edema due to hypofunction of the spleen extract 1~7%, red pomegranate seed oil 1~4%, red pomegranate flower essential oil 3~6%, bead Algae growth factors 5~8%, red jujube polysaccharide 1~2%, silk essence 3~4%, angelica extract 3~6%, phellodendron extract 3~4%, Radix Glycyrrhizae Extract 4~5%, Bulbus Lilii extract 2~3%, rose 1~2%, tea tree hydrosol 0.5~1%, silk gum 2~3%, water-soluble treasure Pearl powder 1~3%, cocoyl alanine triethanolamine salt 3~5%, Cocoamidopropyl betaine 1~3%, lauric monoglyceride Ester 1~2% and glacier water surplus;Its preparation step is as follows:
(1) take scarlet pomegranate to clean, red pomegranate pulp is first directly squeezed the juice and obtains red pomegranate Normal juice by demucilage, seed, skin, clarification Filtering collects clear liquid, is freeze-dried after concentration, obtains red pomegranate pulp extract;Then red pomegranate seed is dried, moisture content control System squeezing in 8~10%, investment squeezer, temperature are controlled at 50~80 DEG C, are obtained primary red pomegranate seed oil, are taken out residue, powder 80 mesh are broken to, seed slag end puts into Ultrasonic Wave-Assisted Extraction in petroleum ether, by solid-liquid ratio(w/v)1:10, in Extracting temperature 35~50 DEG C, 1~2h is extracted under conditions of ultrasonic power 60W, vacuum distillation obtains secondary red pomegranate seed oil, merges primary red pomegranate seed Oil and secondary red pomegranate seed are oily, and the active carbon of its quality 2~5% is added in obtained mixing seed oil, stirs 10~20min, mistake Filter obtains red pomegranate seed oil;Red pomegranate skin is dried, 60~80 mesh are crushed to, the water of 15~20 times of its quality amounts is added, 45 Ultrasonic Wave-Assisted Extraction under conditions of~85 DEG C, ultrasonic power 80W, 2~3h of extraction time are then centrifuged for, and filtering is depressurized dense Contracting, freeze-drying, obtains red pomegranate bark extract;
(2) red pomegranate fresh flower and water investment distillation still are distilled, the mass ratio of red pomegranate fresh flower and water is 1:5~6, Xiang Zheng It evaporating and is passed through steam in kettle red pomegranate fresh flower and water are directly heated, distill 5~5.5h, the vacuum degree in distillation still is -0.8~- 0.1MPa, vapo(u)rizing temperature are 90~95 DEG C, oil water separator are imported after the distillate that distillation still comes out is cooling, in 28-38 DEG C of item Water-oil separating is carried out under part, discards water layer, and obtained oil reservoir is red pomegranate flower essential oil;
(3) it is more that red pomegranate pulp extract, red pomegranate bark extract, chlorella growth factor, jujube are sequentially added in glacial water Sugar, angelica extract, phellodendron extract, licorice, Bulbus Lilii extract, rose, tea tree hydrosol, and stir, then 35~55 DEG C are heated to, continuously adding silk gum, silk essence, water soluble pearl powder makes to dissolve, and obtains component A;
(4) red pomegranate seed oil and red pomegranate flower essential oil are mixed, are heated to 45~65 DEG C, be added thereto lauric monoglyceride, Cocoyl alanine triethanolamine salt, Cocoamidopropyl betaine, stirring evenly makes miscible, obtains component B;
(5) under the conditions of 40 DEG C of temperature, component A and component B is mixed, supplies glacial water, emulsification uniformly, is down to room temperature, and detection is closed It is filling after lattice, packaging.
2. natural anti-aging red pomegranate skin care item as described in claim 1, which is characterized in that matched by the raw material of following weight ratio It makes:Red pomegranate pulp extract 12.5%, red pomegranate severe edema due to hypofunction of the spleen extract 4%, red pomegranate seed oil 2.5%, red pomegranate flower essential oil 4.5%, chlorella growth factor 6.5%, red jujube polysaccharide 1.5%, silk essence 3.5%, angelica extract 4.5%, phellodendron extract 3.5%, Licorice 4.5%, Bulbus Lilii extract 2.5%, rose 1.5%, tea tree hydrosol 1%, silk gum 2.5%, water soluble pearl powder 2%, cocoyl alanine triethanolamine salt 4%, Cocoamidopropyl betaine 2%, lauric monoglyceride 1.5% and glacial water 35.5%。
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