CN104411812A - 洗涤剂颗粒的制造方法、洗涤剂颗粒和包含所述颗粒的洗涤剂组合物 - Google Patents
洗涤剂颗粒的制造方法、洗涤剂颗粒和包含所述颗粒的洗涤剂组合物 Download PDFInfo
- Publication number
- CN104411812A CN104411812A CN201380036325.9A CN201380036325A CN104411812A CN 104411812 A CN104411812 A CN 104411812A CN 201380036325 A CN201380036325 A CN 201380036325A CN 104411812 A CN104411812 A CN 104411812A
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- Prior art keywords
- weight
- detergent
- acid
- detergent composition
- sodium carbonate
- Prior art date
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- 239000003599 detergent Substances 0.000 title claims abstract description 95
- 239000000203 mixture Substances 0.000 title claims abstract description 62
- 238000000034 method Methods 0.000 title claims abstract description 60
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 18
- 230000008569 process Effects 0.000 title abstract description 9
- 239000008187 granular material Substances 0.000 title abstract 7
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims abstract description 62
- 239000003945 anionic surfactant Substances 0.000 claims abstract description 45
- 239000002253 acid Substances 0.000 claims abstract description 41
- 229910000029 sodium carbonate Inorganic materials 0.000 claims abstract description 30
- 239000002002 slurry Substances 0.000 claims abstract description 28
- -1 alkali metal salt Chemical class 0.000 claims abstract description 27
- 229910052783 alkali metal Inorganic materials 0.000 claims abstract description 19
- 239000002243 precursor Substances 0.000 claims abstract description 19
- 229920005646 polycarboxylate Polymers 0.000 claims abstract description 15
- 239000003513 alkali Substances 0.000 claims abstract description 9
- 239000002245 particle Substances 0.000 claims description 62
- 239000000126 substance Substances 0.000 claims description 18
- 239000000344 soap Substances 0.000 claims description 13
- 238000005507 spraying Methods 0.000 claims description 11
- 150000001875 compounds Chemical class 0.000 claims description 9
- 150000002632 lipids Chemical class 0.000 claims description 8
- 150000004760 silicates Chemical class 0.000 claims description 8
- VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 claims description 7
- NIXOWILDQLNWCW-UHFFFAOYSA-N Acrylic acid Chemical compound OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 6
- OFOBLEOULBTSOW-UHFFFAOYSA-N Propanedioic acid Natural products OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 claims description 6
- 239000000975 dye Substances 0.000 claims description 6
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- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 claims description 6
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- 150000001734 carboxylic acid salts Chemical class 0.000 claims description 3
- 239000002304 perfume Substances 0.000 claims description 3
- 235000019353 potassium silicate Nutrition 0.000 claims description 3
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims description 3
- 239000007844 bleaching agent Substances 0.000 claims description 2
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- 229920001495 poly(sodium acrylate) polymer Polymers 0.000 claims description 2
- 239000001509 sodium citrate Substances 0.000 claims description 2
- NNMHYFLPFNGQFZ-UHFFFAOYSA-M sodium polyacrylate Chemical group [Na+].[O-]C(=O)C=C NNMHYFLPFNGQFZ-UHFFFAOYSA-M 0.000 claims description 2
- MWNQXXOSWHCCOZ-UHFFFAOYSA-L sodium;oxido carbonate Chemical compound [Na+].[O-]OC([O-])=O MWNQXXOSWHCCOZ-UHFFFAOYSA-L 0.000 claims description 2
- HRXKRNGNAMMEHJ-UHFFFAOYSA-K trisodium citrate Chemical compound [Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O HRXKRNGNAMMEHJ-UHFFFAOYSA-K 0.000 claims description 2
- 150000008051 alkyl sulfates Chemical class 0.000 claims 2
- BGRWYDHXPHLNKA-UHFFFAOYSA-N Tetraacetylethylenediamine Chemical compound CC(=O)N(C(C)=O)CCN(C(C)=O)C(C)=O BGRWYDHXPHLNKA-UHFFFAOYSA-N 0.000 claims 1
- NIXOWILDQLNWCW-UHFFFAOYSA-M acrylate group Chemical group C(C=C)(=O)[O-] NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 claims 1
- 229940038773 trisodium citrate Drugs 0.000 claims 1
- 238000002156 mixing Methods 0.000 abstract description 20
- 238000001694 spray drying Methods 0.000 abstract description 11
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 abstract description 7
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- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/08—Silicates
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
- C11D11/02—Preparation in the form of powder by spray drying
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
- C11D11/04—Special methods for preparing compositions containing mixtures of detergents by chemical means, e.g. by sulfonating in the presence of other compounding ingredients followed by neutralising
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/10—Carbonates ; Bicarbonates
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/37—Polymers
- C11D3/3746—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- C11D3/3757—(Co)polymerised carboxylic acids, -anhydrides, -esters in solid and liquid compositions
- C11D3/3761—(Co)polymerised carboxylic acids, -anhydrides, -esters in solid and liquid compositions in solid compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/37—Polymers
- C11D3/3746—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- C11D3/3784—(Co)polymerised monomers containing phosphorus
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- Chemical & Material Sciences (AREA)
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- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
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- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Detergent Compositions (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP12175590 | 2012-07-09 | ||
| EP12175590.4 | 2012-07-09 | ||
| PCT/EP2013/062387 WO2014009101A1 (en) | 2012-07-09 | 2013-06-14 | Process for the production of a detergent granule, detergent granule and detergent composition comprising said granule |
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| Publication Number | Publication Date |
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| CN104411812A true CN104411812A (zh) | 2015-03-11 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201380036325.9A Pending CN104411812A (zh) | 2012-07-09 | 2013-06-14 | 洗涤剂颗粒的制造方法、洗涤剂颗粒和包含所述颗粒的洗涤剂组合物 |
Country Status (11)
| Country | Link |
|---|---|
| EP (1) | EP2870229B1 (es) |
| CN (1) | CN104411812A (es) |
| AR (1) | AR091694A1 (es) |
| BR (1) | BR112014030610B1 (es) |
| CL (1) | CL2015000018A1 (es) |
| ES (1) | ES2753025T3 (es) |
| IN (1) | IN2015MN00006A (es) |
| MX (1) | MX354484B (es) |
| PH (1) | PH12014502727B1 (es) |
| WO (1) | WO2014009101A1 (es) |
| ZA (1) | ZA201409406B (es) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113444584A (zh) * | 2021-06-25 | 2021-09-28 | 山东新华莎罗雅生物技术有限公司 | 固体酶清洗剂及其制备方法 |
| CN113444588A (zh) * | 2021-06-25 | 2021-09-28 | 山东新华莎罗雅生物技术有限公司 | 医疗器械固体清洗剂及其生产工艺 |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN117500901A (zh) | 2021-05-19 | 2024-02-02 | 联合利华知识产权控股有限公司 | 制备喷雾干燥的洗涤剂颗粒的方法 |
| WO2024088878A1 (en) * | 2022-10-24 | 2024-05-02 | Unilever Ip Holdings B.V. | Spray-dried laundry particle |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1066881A (zh) * | 1991-04-12 | 1992-12-09 | 普罗格特-甘布尔公司 | 形成高活性表面活性剂颗粒的表面活性剂膏的化学结构 |
| EP1914297A1 (en) * | 2006-10-16 | 2008-04-23 | The Procter & Gamble Company | A spray-drying process for preparing a low density, low builder, highly water-soluble spray-dried detergent powder |
| CN101688158A (zh) * | 2008-05-22 | 2010-03-31 | 荷兰联合利华有限公司 | 通过干中和制造洗涤剂颗粒 |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA1297376C (en) * | 1985-11-01 | 1992-03-17 | David Philip Jones | Detergent compositions, components therefor, and processes for theirpreparation |
-
2013
- 2013-06-14 CN CN201380036325.9A patent/CN104411812A/zh active Pending
- 2013-06-14 MX MX2015000427A patent/MX354484B/es active IP Right Grant
- 2013-06-14 WO PCT/EP2013/062387 patent/WO2014009101A1/en active Application Filing
- 2013-06-14 BR BR112014030610-9A patent/BR112014030610B1/pt active IP Right Grant
- 2013-06-14 EP EP13730199.0A patent/EP2870229B1/en active Active
- 2013-06-14 ES ES13730199T patent/ES2753025T3/es active Active
- 2013-07-08 AR ARP130102415 patent/AR091694A1/es active IP Right Grant
-
2014
- 2014-12-05 PH PH12014502727A patent/PH12014502727B1/en unknown
- 2014-12-19 ZA ZA2014/09406A patent/ZA201409406B/en unknown
-
2015
- 2015-01-02 IN IN6MUN2015 patent/IN2015MN00006A/en unknown
- 2015-01-06 CL CL2015000018A patent/CL2015000018A1/es unknown
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1066881A (zh) * | 1991-04-12 | 1992-12-09 | 普罗格特-甘布尔公司 | 形成高活性表面活性剂颗粒的表面活性剂膏的化学结构 |
| EP1914297A1 (en) * | 2006-10-16 | 2008-04-23 | The Procter & Gamble Company | A spray-drying process for preparing a low density, low builder, highly water-soluble spray-dried detergent powder |
| CN101688158A (zh) * | 2008-05-22 | 2010-03-31 | 荷兰联合利华有限公司 | 通过干中和制造洗涤剂颗粒 |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113444584A (zh) * | 2021-06-25 | 2021-09-28 | 山东新华莎罗雅生物技术有限公司 | 固体酶清洗剂及其制备方法 |
| CN113444588A (zh) * | 2021-06-25 | 2021-09-28 | 山东新华莎罗雅生物技术有限公司 | 医疗器械固体清洗剂及其生产工艺 |
Also Published As
| Publication number | Publication date |
|---|---|
| PH12014502727A1 (en) | 2015-02-02 |
| MX2015000427A (es) | 2015-03-12 |
| MX354484B (es) | 2018-03-07 |
| AR091694A1 (es) | 2015-02-25 |
| BR112014030610B1 (pt) | 2021-04-20 |
| WO2014009101A1 (en) | 2014-01-16 |
| CL2015000018A1 (es) | 2015-02-27 |
| IN2015MN00006A (es) | 2015-10-16 |
| EP2870229A1 (en) | 2015-05-13 |
| EP2870229B1 (en) | 2019-08-07 |
| PH12014502727B1 (en) | 2015-02-02 |
| ZA201409406B (en) | 2016-08-31 |
| BR112014030610A2 (pt) | 2017-06-27 |
| ES2753025T3 (es) | 2020-04-07 |
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