CN104403531A - 一种防电磁干扰型耐火绝缘漆及其制备方法 - Google Patents

一种防电磁干扰型耐火绝缘漆及其制备方法 Download PDF

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CN104403531A
CN104403531A CN201410671600.0A CN201410671600A CN104403531A CN 104403531 A CN104403531 A CN 104403531A CN 201410671600 A CN201410671600 A CN 201410671600A CN 104403531 A CN104403531 A CN 104403531A
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张庆
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Abstract

本发明公开了一种防电磁干扰型耐火绝缘漆,其特征在于,由下列重量份的原料制成:醇酸树脂28-34、碳酸镐2-3、氟碳树脂22-26、矿物油5-7、蜂蜡1-3、聚苯乙烯6-8、磷钛粉2-4、200﹟溶剂油10-12、二甲苯6-9、立德粉4-6、苯并三氮唑2-3、耐盐雾助剂ZT-7192-4、过氧化二异丙苯1-2、抗氧剂10101-3、苯二甲酸二丁酯2-3、磷片状石墨粉3-4、电熔镁砂4-6、N-甲基吡咯烷酮3-5、助剂4-7;本发明提供的油漆具有很高的强度和韧性,耐冲击性能好,还具有耐磨和抗氧化的性能;在潮湿的环境下仍然保持良好的耐火绝缘性能,添加的助剂具有良好的抗电磁干扰性能,可用于电力设备的防护和保护,降低危险系数,提高安全性。

Description

一种防电磁干扰型耐火绝缘漆及其制备方法
技术领域
本发明涉及一种油漆及其制备方法,特别是一种防电磁干扰型耐火绝缘漆及其制备方法。
背景技术
    社会生活中随着电器、电子和电力设备的覆盖化,虽然给人们生活中带来诸多便捷之处,但随之而来的确是电磁波辐射对人体和环境的危害。抑制电磁辐射最为简便和有效的方法是利用电磁屏蔽材料实现电磁屏蔽。电磁屏蔽材料通过与空气之间的阻抗差实现对电磁波的反射和通过自身的电磁感应实现对电磁波的涡流衰减。由于金属材料良好的导电性,传统的高效电磁屏蔽材料为金属板材,主要是钢板。然而,由于钢板自身重量重、制作安装复杂,成本高昂、移动困难等缺点大大限制了屏蔽材料的适用领域,导致目前电磁屏蔽的现状是,除在某些十分必要场合下,不得不采用这类传统材料实现电磁屏蔽之外,在许多其它应用领域,包括电子设备安全、信息保护和环境治理等方面,电磁屏蔽技术并没有得到应有的应用,影响了电子设备的正常安全使用以及人们的健康生活。因此,研究开发高效、易于使用、性价比高的新型电磁屏蔽材料已成为治理空间污染,改善生活环境的关键要素。面对日益增长的社会需求,新型高效电磁屏蔽材料具有十分显著的社会和经济效益。
发明内容
本发明的目的是提供一种防电磁干扰型耐火绝缘漆及其制备方法。
为了实现本发明的目的,本发明通过以下方案实施:
一种防电磁干扰型耐火绝缘漆,由下列重量份的原料制成:醇酸树脂28-34、碳酸镐2-3、氟碳树脂22-26、矿物油5-7、蜂蜡1-3、聚苯乙烯6-8、磷钛粉2-4、200﹟溶剂油10-12、二甲苯6-9、立德粉4-6、苯并三氮唑2-3、耐盐雾助剂ZT-7192-4、过氧化二异丙苯1-2、抗氧剂10101-3、苯二甲酸二丁酯2-3、磷片状石墨粉3-4、电熔镁砂4-6、N-甲基吡咯烷酮3-5、助剂4-7;
所述助剂是由下列重量份的原料制成:铝酸酯偶联剂DL-4111-2、聚异丁烯4-6、三乙醇胺油酸皂1-2、双十二碳醇酯1-3、过氧化环己酮1-2、乙酰丙酮锌2-3、桉树油3-5、防老剂MB1-2、甲基丙烯酸5-8、甲基丙烯酸乙酯12-15、1,2-苯并异噻唑啉-3-酮2-3、氧化钼3-5、氧化铋2-4、银包铜粉4-6、炭黑3-5、导电云母5-7、乙醇2-4、十二烷基磺酸钠1-2;制备方法是(1)将氧化钼、氧化铋、银包铜粉、炭黑、导电云母加到球磨机中球磨2-3小时,再加到煅烧炉中600-800°C煅烧20-30分钟,取出粉碎加到铝酸酯偶联剂DL-411和乙醇的混合溶液中,超声分散10-20分钟,烘干后和十二烷基磺酸钠混合备用;(2)将甲基丙烯酸、甲基丙烯酸乙酯、乙酰丙酮锌、桉树油加到反应釜中,升高温度至70-80°C,加入过氧化环己酮,搅拌反应1-2小时;(3)将步骤(1)的产物加到步骤(2)中,继续反应20-30分钟,再加入聚酰胺蜡及其他剩余物质,充分搅拌混合均匀即可。
本发明所述一种防电磁干扰型耐火绝缘漆,由以下具体步骤制成:
(1)将碳酸镐、磷钛粉、立德粉、磷片状石墨粉、电熔镁砂加到200﹟溶剂油、二甲苯和N-甲基吡咯烷酮的混合溶液中,超声分散20-30分钟,加热至50-80°C时加入苯二甲酸二丁酯、抗氧剂1010、助剂继续搅拌反应30-40分钟;
(2)将步骤(1)的产物继续升高温度至80-90°C,加入醇酸树脂、氟碳树脂、聚苯乙烯、过氧化二异丙苯,1200-1400转/分下高速混合搅拌反应1-2小时;
(3)将剩余物质加到步骤(2)的产物中,混合均匀后加到研磨机中研磨分散均匀,过滤得到细度为20-40μm的物料,包装即可。
本发明的优点是:本发明提供的油漆具有很高的强度和韧性,耐冲击性能好,还具有耐磨和抗氧化的性能;在潮湿的环境下仍然保持良好的耐火绝缘性能,添加的助剂具有良好的抗电磁干扰性能,可用于电力设备的防护和保护,降低危险系数,提高安全性。
具体实施方案  
下面通过具体实例对本发明进行详细说明。
 一种防电磁干扰型耐火绝缘漆,由下列重量份(公斤)的原料制成:醇酸树脂29、碳酸镐2、氟碳树脂25、矿物油5、蜂蜡1、聚苯乙烯7、磷钛粉2、200﹟溶剂油10、二甲苯8、立德粉5、苯并三氮唑2、耐盐雾助剂ZT-7192、过氧化二异丙苯1、抗氧剂10102、苯二甲酸二丁酯2、磷片状石墨粉3、电熔镁砂5、N-甲基吡咯烷酮5、助剂6;
所述助剂是由下列重量份(公斤)的原料制成:铝酸酯偶联剂DL-411 2、聚异丁烯5、三乙醇胺油酸皂1、双十二碳醇酯2、过氧化环己酮1、乙酰丙酮锌2、桉树油4、防老剂MB1、甲基丙烯酸7、甲基丙烯酸乙酯13、1,2-苯并异噻唑啉-3-酮2、氧化钼4、氧化铋3、银包铜粉5、炭黑4、导电云母7、乙醇3、十二烷基磺酸钠1;制备方法是(1)将氧化钼、氧化铋、银包铜粉、炭黑、导电云母加到球磨机中球磨2-3小时,再加到煅烧炉中600-800°C煅烧20-30分钟,取出粉碎加到铝酸酯偶联剂DL-411和乙醇的混合溶液中,超声分散10-20分钟,烘干后和十二烷基磺酸钠混合备用;(2)将甲基丙烯酸、甲基丙烯酸乙酯、乙酰丙酮锌、桉树油加到反应釜中,升高温度至70-80°C,加入过氧化环己酮,搅拌反应1-2小时;(3)将步骤(1)的产物加到步骤(2)中,继续反应20-30分钟,再加入聚酰胺蜡及其他剩余物质,充分搅拌混合均匀即可。
本发明所述一种防电磁干扰型耐火绝缘漆,由以下具体步骤制成:
(1)将碳酸镐、磷钛粉、立德粉、磷片状石墨粉、电熔镁砂加到200﹟溶剂油、二甲苯和N-甲基吡咯烷酮的混合溶液中,超声分散20-30分钟,加热至50-80°C时加入苯二甲酸二丁酯、抗氧剂1010、助剂继续搅拌反应30-40分钟;
(2)将步骤(1)的产物继续升高温度至80-90°C,加入醇酸树脂、氟碳树脂、聚苯乙烯、过氧化二异丙苯,1200-1400转/分下高速混合搅拌反应1-2小时;
(3)将剩余物质加到步骤(2)的产物中,混合均匀后加到研磨机中研磨分散均匀,过滤得到细度为20-40μm的物料,包装即可。
本发明的油漆漆膜平整,无硬块,硬度:3H,附着力:1级,耐热性实验(300°C,120h):漆膜完整,不脱落,耐碱性实验(72h):不起泡,不起皱,不脱落,耐酸性实验(72h):不起泡,不起皱,不脱落,耐人工老化性实验:1200h不起泡、不剥落、无裂纹,电磁屏蔽率实验:40dB。

Claims (2)

1.一种防电磁干扰型耐火绝缘漆,其特征在于,由下列重量份的原料制成:醇酸树脂28-34、碳酸镐2-3、氟碳树脂22-26、矿物油5-7、蜂蜡1-3、聚苯乙烯6-8、磷钛粉2-4、200﹟溶剂油10-12、二甲苯6-9、立德粉4-6、苯并三氮唑2-3、耐盐雾助剂ZT-7192-4、过氧化二异丙苯1-2、抗氧剂10101-3、苯二甲酸二丁酯2-3、磷片状石墨粉3-4、电熔镁砂4-6、N-甲基吡咯烷酮3-5、助剂4-7;
所述助剂是由下列重量份的原料制成:铝酸酯偶联剂DL-4111-2、聚异丁烯4-6、三乙醇胺油酸皂1-2、双十二碳醇酯1-3、过氧化环己酮1-2、乙酰丙酮锌2-3、桉树油3-5、防老剂MB1-2、甲基丙烯酸5-8、甲基丙烯酸乙酯12-15、1,2-苯并异噻唑啉-3-酮2-3、氧化钼3-5、氧化铋2-4、银包铜粉4-6、炭黑3-5、导电云母5-7、乙醇2-4、十二烷基磺酸钠1-2;制备方法是(1)将氧化钼、氧化铋、银包铜粉、炭黑、导电云母加到球磨机中球磨2-3小时,再加到煅烧炉中600-800°C煅烧20-30分钟,取出粉碎加到铝酸酯偶联剂DL-411和乙醇的混合溶液中,超声分散10-20分钟,烘干后和十二烷基磺酸钠混合备用;(2)将甲基丙烯酸、甲基丙烯酸乙酯、乙酰丙酮锌、桉树油加到反应釜中,升高温度至70-80°C,加入过氧化环己酮,搅拌反应1-2小时;(3)将步骤(1)的产物加到步骤(2)中,继续反应20-30分钟,再加入聚酰胺蜡及其他剩余物质,充分搅拌混合均匀即可。
2.根据权利要求1所述一种防电磁干扰型耐火绝缘漆,其特征在于,由以下具体步骤制成:
(1)将碳酸镐、磷钛粉、立德粉、磷片状石墨粉、电熔镁砂加到200﹟溶剂油、二甲苯和N-甲基吡咯烷酮的混合溶液中,超声分散20-30分钟,加热至50-80°C时加入苯二甲酸二丁酯、抗氧剂1010、助剂继续搅拌反应30-40分钟;
(2)将步骤(1)的产物继续升高温度至80-90°C,加入醇酸树脂、氟碳树脂、聚苯乙烯、过氧化二异丙苯,1200-1400转/分下高速混合搅拌反应1-2小时;
(3)将剩余物质加到步骤(2)的产物中,混合均匀后加到研磨机中研磨分散均匀,过滤得到细度为20-40μm的物料,包装即可。
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