CN104398872A - 一种化痰的中药软胶囊及其制备方法和应用 - Google Patents

一种化痰的中药软胶囊及其制备方法和应用 Download PDF

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CN104398872A
CN104398872A CN201410608087.0A CN201410608087A CN104398872A CN 104398872 A CN104398872 A CN 104398872A CN 201410608087 A CN201410608087 A CN 201410608087A CN 104398872 A CN104398872 A CN 104398872A
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李正梅
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Abstract

本发明提供了一种具有化痰作用的中药软胶囊，由剪刀股10份、铁马鞭12份、酒瓶花14份、荷莲豆草10份、胜红蓟8份等药物提取制备得到，提取方法包括水提醇沉，喷雾干燥，本发明具有良好的化痰作用。

Description

一种化痰的中药软胶囊及其制备方法和应用
技术领域
本发明涉及中药技术领域，具体涉及一种化痰的中药软胶囊及制备方法和应用。
背景技术
痰为津液所化。津液是人体正常生理性体液，痰是有形的一种病理产物。多因外感风寒湿热之盛，内伤七情饮食之郁，以致气逆液浊而成多量稀粘之汁。痰与饮常常互称，在临床上又有鉴别：粘而稠者为痰，清而稀者为饮。痰色黄者属于热证，色白者属于寒证。舌苔腻者多属湿痰，舌红口干者多为燥痰。因此研究开发化痰药显得非常有意义。
发明内容
发明目的：为了解决上述问题，本发明的目的在于提供一种化痰的中药软胶囊及制备方法和应用。
技术方案：本发明的目的是通过如下的方案实现的：
一种化痰的中药软胶囊，它由如下重量份数的原料药制备得到：剪刀股10份、铁马鞭12份、酒瓶花14份、荷莲豆草10份、胜红蓟8份、金钗股10份、罗望子15份、金龙胆草8份、草玉梅10份、红药子12份、乌泡刺10份、绒毛鸭脚木10份、金丝草12份、三点金草10份、大叶骨牌草15份。
所述的中药化痰的软胶囊，制备方法包括如下步骤：取以上原料药加水煎煮2次，每次加水量为药材重量的10倍量，每次煎煮2小时，合并煎液，浓缩至65℃时相对密度为1.10，加乙醇使含醇量的体积百分比达65％，搅拌，静置，过滤，滤液减压浓缩至65℃时相对密度为1.20并回收乙醇，得浓缩液，喷雾干燥，喷雾干燥条件为：进风温度为100，出风温度为80℃，物料温度为70℃，雾化压力为0.2兆帕，喷雾速度为10ml/s，粉碎成干浸膏粉，过100目筛，加入植物油适量，混合，用胶体磨研磨，冷至室温，压制，干燥，去油，晾干，即得。
所述化痰的中药软胶囊在制备化痰药物中的应用。
本发明中剪刀股为菊科苦荬菜属植物剪刀股Ixeris debilis A.Gray，以全草入药。夏秋采收，鲜用或晒干。清热凉血，利尿消肿。用于肺热咳嗽，喉痛，口腔溃疡，急性结膜炎，阑尾炎，水肿，小便不利；外用治乳腺炎，疮疖肿毒，皮肤瘙痒。
铁马鞭为豆科胡枝子属植物铁马鞭Lespedeza pilosa(Thunb.)Sieb.et Zucc.，以全株入药。夏秋采,晒干。清热散结，活血止痛，行水消肿。用于颈淋巴结结核，冷脓肿，虚热不退，水肿，腰腿筋骨痛；外用治乳腺炎。
酒瓶花为杜鹃花科杜鹃花属植物亮毛杜鹃Rhododendron microphyton Franch.，以根入药。夏秋采集,洗净,切片晒干或鲜用。能清热解表，利尿。用于感冒，急、慢性肾炎，肾盂肾炎，小儿惊风。
荷莲豆草为石竹科荷莲豆草属植物荷莲豆草Drymaria diandra Blume的全草。夏秋采，洗净鲜用或晒干。清热解毒，利尿通便，活血消肿，退翳。用于急性肝炎，胃痛，疟疾，翼状胬肉，腹水，便秘；外用治骨折，疮痈，蛇咬伤。
胜红蓟为菊科胜红蓟属植物藿香蓟Ageratum conyzoides L.，以全草或叶及嫩茎入药。夏秋采收，洗净，鲜用或晒干。祛风清热，止痛，止血，排石。用于上呼吸道感染，扁桃体炎，咽喉炎，急性胃肠炎，胃痛，腹痛，崩漏，肾结石，膀胱结石；外用治湿疹，鹅口疮，痈疮肿毒，蜂窝织炎，下肢溃疡，中耳炎，外伤出血。本发明以全草入药。
金钗股为兰科钗子兰属植物柱叶钗子兰Luisia teretifolia Gaudich.,以全草入药。清热解毒，截疟，催吐。用于扁桃体炎，咽喉炎，恶性疟疾，中耳炎，骨折。
罗望子为豆科罗望子属植物罗望子Tamarindus indica L.,以果实入药。春季采,除去种子,晒干。清热解暑，消食化积。用于中暑，食欲不振，小儿疳积，妊娠呕吐，便秘。
金龙胆草为菊科白酒草属植物小苦蒿Conyza blinii Lévl.，以全草入药。秋季采收，去杂质，鲜用或阴干。清热消炎，泻火解毒。用于急性黄疸型肝炎，牙痛，慢性气管炎，口腔炎，咽喉炎，扁桃体炎，肾炎，疟疾；外用治眼结膜炎，中耳炎，疮疡，湿疹，外伤出血。
草玉梅为毛茛科银莲花属植物二歧银莲花Anemone dichotoma L.，以根状茎入药。秋季挖根，晒干，解毒止痢，舒筋活血。用于痢疾，疮疖痈毒，跌打损伤。
红药子为蓼科翼蓼属植物翼蓼Pteroxygonum giraldii Damm.et Diels，以块根入药。秋季采挖，除去茎叶及须根，洗净切片晒干：清热，解毒，止血，止痛。用于肠炎，痢疾，腰腿痛，便血，崩漏；外用治烧烫伤，疮疖，狂犬咬伤。
乌泡刺为蔷薇科悬钩子属植物灰白毛莓Rubustephrodes Hance，以根、叶及种子入药。夏季采叶，秋季采根及种子，晒干，本发明以叶入药。根：祛风除湿，活血调经。用于风湿疼痛，慢性肝炎，腹泻，痢疾，跌打损伤，月经不调。叶：止血，解毒。外用治外伤出血，痈疖疮疡。种子：补气益精。用于病后体虚，神经衰弱。
绒毛鸭脚木为五加科植物穗序鹅掌柴Agalma delavayi(Franch.)Hutch.，以根入药。全年可采，切片晒干。祛风活络，补肝肾，强筋骨。用于骨折，扭挫伤，腰肌劳损，风湿关节痛，肾虚腰痛，跌打损伤恢复期。
金丝草，拉丁文名Pogonatherum crinitum(Thunb.)Kunth.金丝草属，禾本科，单子叶植物纲，被子植物门。生长在生于河边、墙隙、山坡和潮湿田圩。清热，解暑，利尿。用于感冒高热，中暑，尿路感染，肾炎水肿，黄疸型肝炎，糖尿病，小儿久热不退。本发明以全草入药。
三点金草，学名：Desmodium triflorum(L.)DC.)，豆科，蝶形花亚科，山蚂蝗族，行气止痛，温经散寒，解毒。用于中暑腹痛，疝气痛，月经不调，痛经，产后关节痛，狂犬病。本发明以全草入药。
大叶骨牌草为水龙骨科星蕨属植物江南星蕨Microsorium fortune(Moore)Ching，以全草和根状茎入药。四季可采，洗净，鲜用或晒干。清热利湿，凉血止血，消肿止痛。用于黄疸，痢疾，尿路感染，淋巴结结核，白带，风湿关节痛，咳血，吐血，便血，衄血；外用治跌打损伤，骨折，毒蛇咬伤，疔疮肿毒。本发明以全草入药。
有益效果：本发明具有良好的化痰作用。
具体实施方式
以下通过实施例形式，对本发明的上述内容再作进一步的详细说明，但不应将此理解为本发明上述主题的范围仅限于以下的实例，凡基于本发明上述内容所实现的技术均属于本发明的范围。
1.制备实施例：取剪刀股10g、铁马鞭12g、酒瓶花14g、荷莲豆草10g、胜红蓟8g、金钗股10g、罗望子15g、金龙胆草8g、草玉梅10g、红药子12g、乌泡刺10g、绒毛鸭脚木10g、金丝草12g、三点金草10g、大叶骨牌草15g，加水煎煮2次，每次加水量为药材重量的10倍量，每次煎煮2小时，合并煎液，浓缩至65℃时相对密度为1.10，加乙醇使含醇量的体积百分比达65％，搅拌，静置，过滤，滤液减压浓缩至65℃时相对密度为1.20并回收乙醇，得浓缩液，喷雾干燥，喷雾干燥条件为：进风温度为100，出风温度为80℃，物料温度为70℃，雾化压力为0.2兆帕，喷雾速度为10ml/s，粉碎成干浸膏粉，过100目筛，加入植物油适量，混合，用胶体磨研磨，冷至室温，压制，干燥，去油，晾干，即得软胶囊。
2.本发明对化痰药效试验资料
2.1材料
2.1.1动物：ICR小鼠，清洁级，雌雄各半，体重16-18g，由中国科学院上海实验动物中心提供。实验动物生产许可证：SCXK(沪)2002-0010。
2.1.2药物：按上述实施例制备成软胶囊，规格：5g生药/g、氯化铵(南京化学试剂厂，批号：20120508)。
2.2方法与结果
2.2.1对小鼠气管酚红排痰量的影响：
2.2.1.1.分组：小鼠随机分为5组：空白对照组(等容积生理盐水)，氯化铵组(1.0g/kg)、本发明高(20g/kg)、中(10g/kg)、低(5g/kg)三个剂量组。
2.2.1.2.实验方法：取小鼠50只随机分组，灌胃给药，于第5天给药后1h，腹腔注射5％酚红(0.1ml/10g体重)，30min后处死小鼠。剪下小鼠自甲状软骨至气管分支处的一段气管，放入盛有2ml生理盐水的试管中，振摇，再加入0.1ml1mol/LNaOH，用754分光光度仪(上海)在波长550nm条件下测OD值。根据酚红标准曲线查出每鼠的气管酚红排出量。
2.2.1.3实验结果：本发明高、中剂量组均能明显增加小鼠气管酚红排出量，与对照组比较差异均有显著性(P<0.05或P<0.01)(见表1)。
表1.本发明对小鼠气管酚红排痰量的影响
注：与空白对照组比较*P<0.05；**P<0.01
2.3结论实验结果表明本发明能有效增加小鼠气管粘液分泌，使酚红排出量明显增加。因此提示本发明具有化痰作用，对改善症状有一定的帮助。

Claims (3)

1.一种化痰的中药软胶囊，其特征在于，它由如下重量份数的原料药制备得到：剪刀股10份、铁马鞭12份、酒瓶花14份、荷莲豆草10份、胜红蓟8份、金钗股10份、罗望子15份、金龙胆草8份、草玉梅10份、红药子12份、乌泡刺10份、绒毛鸭脚木10份、金丝草12份、三点金草10份、大叶骨牌草15份。
2.根据权利要求1所述的中药化痰的软胶囊，其特征在于，制备方法包括如下步骤：取以上原料药加水煎煮2次，每次加水量为药材重量的10倍量，每次煎煮2小时，合并煎液，浓缩至65℃时相对密度为1.10，加乙醇使含醇量的体积百分比达65％，搅拌，静置，过滤，滤液减压浓缩至65℃时相对密度为1.20并回收乙醇，得浓缩液，喷雾干燥，喷雾干燥条件为：进风温度为100，出风温度为80℃，物料温度为70℃，雾化压力为0.2兆帕，喷雾速度为10ml/s，粉碎成干浸膏粉，过100目筛，加入植物油适量，混合，用胶体磨研磨，冷至室温，压制，干燥，去油，晾干，即得。
3.根据权利要求1所述化痰的中药软胶囊在化痰药物中的应用。
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