CN104387774B - 一种环保阻燃复合六方氮化硼软片的制备方法 - Google Patents
一种环保阻燃复合六方氮化硼软片的制备方法 Download PDFInfo
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- CN104387774B CN104387774B CN201410775115.8A CN201410775115A CN104387774B CN 104387774 B CN104387774 B CN 104387774B CN 201410775115 A CN201410775115 A CN 201410775115A CN 104387774 B CN104387774 B CN 104387774B
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- Prior art keywords
- boron nitride
- hexagonal boron
- powder
- nitride film
- preparation
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- PZNSFCLAULLKQX-UHFFFAOYSA-N Boron nitride Chemical compound N#B PZNSFCLAULLKQX-UHFFFAOYSA-N 0.000 title claims abstract description 101
- 229910052582 BN Inorganic materials 0.000 title claims abstract description 73
- 239000003063 flame retardant Substances 0.000 title claims abstract description 19
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 title claims abstract description 18
- 238000002360 preparation method Methods 0.000 title claims abstract description 17
- 230000007613 environmental effect Effects 0.000 title claims abstract description 16
- 239000000843 powder Substances 0.000 claims abstract description 55
- 238000000034 method Methods 0.000 claims abstract description 15
- 238000002156 mixing Methods 0.000 claims abstract description 15
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 claims abstract description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 claims abstract description 13
- 229910000077 silane Inorganic materials 0.000 claims abstract description 12
- 239000000047 product Substances 0.000 claims abstract description 11
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000011265 semifinished product Substances 0.000 claims abstract description 10
- 239000000741 silica gel Substances 0.000 claims abstract description 10
- 229910002027 silica gel Inorganic materials 0.000 claims abstract description 10
- 150000002978 peroxides Chemical class 0.000 claims abstract description 9
- 229940008099 dimethicone Drugs 0.000 claims abstract description 5
- 239000004205 dimethyl polysiloxane Substances 0.000 claims abstract description 5
- 235000013870 dimethyl polysiloxane Nutrition 0.000 claims abstract description 5
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 claims abstract description 5
- 238000004513 sizing Methods 0.000 claims abstract description 5
- 239000012808 vapor phase Substances 0.000 claims abstract description 5
- 239000002245 particle Substances 0.000 claims description 17
- JNGZXGGOCLZBFB-IVCQMTBJSA-N compound E Chemical compound N([C@@H](C)C(=O)N[C@@H]1C(N(C)C2=CC=CC=C2C(C=2C=CC=CC=2)=N1)=O)C(=O)CC1=CC(F)=CC(F)=C1 JNGZXGGOCLZBFB-IVCQMTBJSA-N 0.000 claims description 10
- 239000000463 material Substances 0.000 claims description 8
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 claims description 6
- 229910021502 aluminium hydroxide Inorganic materials 0.000 claims description 6
- 150000001875 compounds Chemical class 0.000 claims description 6
- VTHJTEIRLNZDEV-UHFFFAOYSA-L magnesium dihydroxide Chemical compound [OH-].[OH-].[Mg+2] VTHJTEIRLNZDEV-UHFFFAOYSA-L 0.000 claims description 6
- 239000000347 magnesium hydroxide Substances 0.000 claims description 6
- 229910001862 magnesium hydroxide Inorganic materials 0.000 claims description 6
- 238000010074 rubber mixing Methods 0.000 claims description 4
- WYTZZXDRDKSJID-UHFFFAOYSA-N (3-aminopropyl)triethoxysilane Chemical compound CCO[Si](OCC)(OCC)CCCN WYTZZXDRDKSJID-UHFFFAOYSA-N 0.000 claims description 3
- 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 claims description 3
- DMWVYCCGCQPJEA-UHFFFAOYSA-N 2,5-bis(tert-butylperoxy)-2,5-dimethylhexane Chemical compound CC(C)(C)OOC(C)(C)CCC(C)(C)OOC(C)(C)C DMWVYCCGCQPJEA-UHFFFAOYSA-N 0.000 claims 1
- 239000000203 mixture Substances 0.000 abstract description 3
- 238000011017 operating method Methods 0.000 abstract description 2
- 238000009413 insulation Methods 0.000 description 4
- 238000005259 measurement Methods 0.000 description 4
- VLKZOEOYAKHREP-UHFFFAOYSA-N hexane Substances CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 2
- 229910010272 inorganic material Inorganic materials 0.000 description 2
- 239000011147 inorganic material Substances 0.000 description 2
- 229920000642 polymer Polymers 0.000 description 2
- 150000004756 silanes Chemical class 0.000 description 2
- 238000010998 test method Methods 0.000 description 2
- 239000004593 Epoxy Substances 0.000 description 1
- 238000010622 cold drawing Methods 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 230000006835 compression Effects 0.000 description 1
- 238000007906 compression Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000012777 electrically insulating material Substances 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 239000011368 organic material Substances 0.000 description 1
- 239000002861 polymer material Substances 0.000 description 1
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 229920002545 silicone oil Polymers 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000007655 standard test method Methods 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
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- Compositions Of Macromolecular Compounds (AREA)
- Manufacture Of Macromolecular Shaped Articles (AREA)
Abstract
Description
Claims (7)
Priority Applications (1)
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CN201410775115.8A CN104387774B (zh) | 2014-12-16 | 2014-12-16 | 一种环保阻燃复合六方氮化硼软片的制备方法 |
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CN201410775115.8A CN104387774B (zh) | 2014-12-16 | 2014-12-16 | 一种环保阻燃复合六方氮化硼软片的制备方法 |
Publications (2)
Publication Number | Publication Date |
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CN104387774A CN104387774A (zh) | 2015-03-04 |
CN104387774B true CN104387774B (zh) | 2016-10-19 |
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CN201410775115.8A Active CN104387774B (zh) | 2014-12-16 | 2014-12-16 | 一种环保阻燃复合六方氮化硼软片的制备方法 |
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Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN107353433B (zh) * | 2017-07-20 | 2019-01-08 | 西北工业大学 | 纳米氢氧化镁/六方氮化硼纳米复合材料及制备方法 |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6162849A (en) * | 1999-01-11 | 2000-12-19 | Ferro Corporation | Thermally conductive thermoplastic |
CN102300949A (zh) * | 2009-01-30 | 2011-12-28 | 日东电工株式会社 | 导热性粘合剂组合物和导热性粘合片 |
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2014
- 2014-12-16 CN CN201410775115.8A patent/CN104387774B/zh active Active
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6162849A (en) * | 1999-01-11 | 2000-12-19 | Ferro Corporation | Thermally conductive thermoplastic |
CN102300949A (zh) * | 2009-01-30 | 2011-12-28 | 日东电工株式会社 | 导热性粘合剂组合物和导热性粘合片 |
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CN104387774A (zh) | 2015-03-04 |
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Address after: 523000 Guangdong Province, Dongguan city Tangxia town B Jiao Tong Silver Garden Street 1 two floor Applicant after: DONGGUAN YIPIN SILICONE ELECTRONICS MATERIALS CO., LTD. Address before: Tangxia town B Jiao Tong nine waist street 523000 Dongguan City No. 10 in Guangdong Province Applicant before: DONGGUAN YIPIN SILICONE ELECTRONICS MATERIALS CO., LTD. |
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Effective date of registration: 20190614 Address after: 523000 Longfu Garden Building 1302, Tangxia Town, Dongguan City, Guangdong Province Patentee after: Pang Hongqiao Address before: 523000 Second Floor, No. 1 Yinyuan Street, Jiaoyitang, Tangxia Town, Dongguan City, Guangdong Province Patentee before: DONGGUAN YIPIN SILICONE ELECTRONICS MATERIALS CO., LTD. |