CN104367536A - Facial mask containing cordyceps militaris ingredients and preparation method thereof - Google Patents
Facial mask containing cordyceps militaris ingredients and preparation method thereof Download PDFInfo
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Abstract
The invention provides a facial mask containing cordyceps militaris ingredients. The facial mask is prepared from components A, B, C, D and E according to the parts by weight, wherein the component A is prepared from pure water, hydrolyzed oat proteins, xylitol, tranexamic acid and dipotassium glycyrrhizinate; the component B is prepared from glycerin and transparent xanthan gum; the component C is prepared from butanediol, nipagin esters and a scutellaria baicalensis root extract; the component D is prepared from adenosine disodium triphosphate, a cordyceps extract, hydrolyzed royal jellies, fermented aloes, a purslane extract, a persimmon leaf extract, an orange peel extract, a phellinus linteus extract, a white willow bark extract, a vanilla extract, a Lengxiang rose extract, a mung bean extract, a green tea extract, a rice bran extract, a jasmine extract, a peach seed extract and a cinnamomum camphora leaf extract; the component E is deionized water. The invention also provides a preparation method of the facial mask containing cordyceps militaris ingredients. The facial mask prepared by adopting the method has the characteristics of safety, no toxicity and wrinkle resistance and is lower in production cost.
Description
Technical field
The present invention relates to cosmetic field, particularly relate to a kind of facial film containing Cordyceps militaris (L.) Link. composition and preparation method thereof.
Background technology
Cordyceps militaris (L.) Link. formal name used at school Cordyceps militaris (L.) Link. (
cordyceps militaris), it and Cordyceps of Qinghai Province belong to Eumycota Ascomycotina Cordyceps, therefore, are called belonging to together " brother " of Cordyceps by expert.The perfect stage of Cordyceps militaris (L.) Link. life cycle comprises mycelial growth and sporophore growth.The insect larvaes such as Lepidoptera, coleoptera, Diptera or pupa infect the spore of Paecilomyces varioti, and when environmental condition is suitable for, spore just sprouts formation mycelium, and mycelium draws the nutrition in worm (pupa) body as the material of its growth promoter and the energy.After mycelia decomposes the various tissue in worm (pupa) body and organ, hyphostoma development transfers reproductive growth to by nourishing and growing, mycelium twist together gradually be differentiated to form sclerotium and pass that the external top becoming crocus or Chinese red is slightly expanded, in bar-shaped Stroma (sporophore), the many heads from polypide of Stroma, chest, caudad etc. stretch out.
Wild Cordyceps militaris (L.) Link. is similar to traditional Cordyceps, very rare at occurring in nature.Most research is thought, Cordyceps militaris (L.) Link. is close with natural cordyceps on active ingredient, and its medicinal and edibility can match in excellence or beauty with natural Cordyceps.The Cordyceps militaris (L.) Link. cellulose content of factorial praluction is higher than natural cordyceps, and the content of its protein, aminoacid, vitamin and trace element has has all met or exceeded the level of natural cordyceps.Plant in Cordyceps reported more than 350, Cordyceps militaris (L.) Link. is the rare Cordyceps that can form a large amount of cordycepin.Because with Cordyceps sibship recently, effective ingredient is quite even higher, and can artificial culture, Cordyceps militaris (L.) Link. becomes the Ideal Substitute of natural cordyceps.Riched Cordyceps Militaris is containing various bioactivators, as Cordyceps polysaccharide, cordycepin, cordycepic acid, SOD enzyme, adenosine, polypeptide/aminoacid, mannitol etc., with the cosmetics that Cordyceps militaris (L.) Link. extract is made for raw material, then there is antioxidation, defying age and the effect such as nutrition, check melanin synthesis is provided, extra-nutrition can be produced to human skin, improve coarse, effect such as enhancing elasticity, moisturizing whitening etc.
To increase due to the age and the various factors such as seasonal variations, ultraviolet radiation, smoking, operating pressure are large, sitting before computer, television set, contact radioactive substance causes the skin problem of people, as skin corium subside, moisture-retaining capacity declines, xerosis cutis is aging.Therefore, cosmetics have become the requisite articles for daily use of one of people.Do not stimulate skin due to easy to use, safe, can frequently use, facial film has more and more been active status in Cosmetic Market.Facial film be clean, nurse, the cosmetics of nutrition skin of face; The principle of facial film utilizes the blink covering face, the air that temporary transient isolation is extraneous and pollution, improve skin temperature, skin expansion pore, promote sweat gland secretion and metabolism, the oxygen content of skin is made to increase, be conducive to the oil substances that skin gets rid of the metabolic product of epidermis cell and accumulation, moisture in facial film infiltrates the horny layer of epidermis, makes skin become soft, light is flexible naturally.
At present, existing facial film is much miscellaneous, but wherein great majority are all with the addition of some chemical compositions inside, consumer is after life-time service similar products, may there is anaphylaxis in skin, cause corse sweat pore, produce dependency, even bring out Other diseases.Therefore, need exploitation badly a kind of containing large number of biological active component, existing good result of use, the healthy Novel facial mask of consumer can not be damaged again.
Summary of the invention
For the problems referred to above, the invention provides a kind of facial film containing Cordyceps militaris (L.) Link. composition and preparation method thereof, there is safety non-toxic, crease-resistant feature, and production cost is lower.
For realizing above-mentioned purpose of the present invention, the invention provides a kind of facial film containing Cordyceps militaris (L.) Link. composition, is formulated by weight by A, B, C, D and E five kinds of component raw material.
Component A: pure water 34-47 part, hydrolysis avenin 1.7-2.3 part, xylitol 1.7-2.3 part, Trenaxmine 0.8-1.2 part, glycyrrhizic acid dipotassium 0.08-0.12 part.
B component: glycerol 1.7-2.3 part, transparent HANSHENGJIAO 0.05-0.07 part.
Component C: butanediol 2.2-3 part, Nipagin ester (PHENONIP) 0.1-0.25 part, scutellariae,radix extract 0.6-0.8 part.
D component: adenosine triphosphate disodium salt 0.04-0.06 part, Cordyceps extract 0.85-1.2 part, hydrolysis Lac regis apis 0.4-0.6 part, Aloe fermented product 0.5-1.0 part, Herba portulacae extract 0.1-0.3 part, Folium Kaki extract 0.1-0.3 part, orange peel extract 0.01-0.1 part, phellinus linteus extract 0.01-0.1 part, Salix Babylonica L.P.E 0.01-0.03 part, vanilla extract 0.01-0.03 part, Lengxiang rose flower extract 0.01-0.03 part, Semen phaseoli radiati extract 0.01-0.03 part, green tea extract 0.01-0.03 part, rice bran extract 0.01-0.02 part, Flos Jasmini Sambac extract 0.01-0.02 part, Semen Persicae extract 0.01-0.02 part, Lignum cinnamomi camphorae leaf extract 0.01-0.02 part.
Component E: deionized water (pH=7) 42-58 part.
In described D component, the preparation method of Cordyceps extract is: get Powdered or original state Cordyceps militaris (L.) Link.sporophore 40-100g, add alkali ion water 100-300ml, mixed liquor is obtained after concussion (100-300rpm) 10-50min, described mixed liquor is through collected after centrifugation centrifuged supernatant, gained primary deposition thing adds 100-300ml alkali ion water again and carries out second extraction, extracts three times altogether successively; Merge three centrifuged supernatant and the concentrated solution of concentrated 20-30ml, the dehydrated alcohol adding concentrated solution 2-4 times amount makes it under 4 DEG C of conditions, precipitate 8-12h, incline and supernatant and obtain precipitate, this precipitate absolute ethanol washing, freeze-day with constant temperature at a certain temperature between 10 DEG C-20 DEG C, obtain polysaccharide crude, be Cordyceps extract.
Described alkali ion water is by carrying out electrolysis generation by pure water.
Described alkali ion water index is pH:9.80-13.80, current potential: >=-120mV.
In described D component, the preparation method of Aloe fermented product is.
(1) surface cleaning: Fresh leaf of aloe clear water wash clean, described clear water can not use the tap water containing bleach, because bleach can cause aloe liquid variable color, go bad.
(2) ultraviolet radiation sterilization: after the Fresh leaf of aloe of wash clean dries, be transported into preparation of samples room, described preparation of samples room is sterilizing room (indoor have sterilizer), carries out uv light irradiation sterilization 5-30min.
(3) remove leaf skin: in sterilizing room, remove Fresh leaf of aloe leaf skin, cut open crust with the blade of sterilization, and aloe gel juice is taken out; Gel juice and Ye Pi are respectively charged into Plastic Drum.
(4) high speed pulverization and precipitation: leaf skin tissue mashing, become dilute slurry with high speed disintegrator (rotating speed 10000-30000, time 0.2-5 minute); Then precipitation process is carried out; Namely supernatant becomes Folium Aloe natural juice.
(5) preparation of Aloe fermented product: described Aloe fermented product comprises Aloe gel fermented product and Folium Aloe fermented product.
1., be culture medium with aloe gel juice, take Hansenula anomala as inoculation strain, the inoculum concentration 1%-10%(percent by volume of bacterium liquid).Fermentation temperature 26 DEG C-31 DEG C, fermentation time is 20-30 days, and gained fermented product is Aloe gel fermented product.
2., with Folium Aloe natural juice for culture medium, take Hansenula anomala as inoculation strain, the inoculum concentration 1%-10%(percent by volume of bacterium liquid).Fermentation temperature 26 DEG C-31 DEG C, fermentation time is 20-30 days, and gained fermented product is Folium Aloe fermented product.
Described Herba portulacae extract, Folium Kaki extract, orange peel extract, scutellariae,radix extract, phellinus linteus extract, Salix Babylonica L.P.E, vanilla extract, Lengxiang rose flower extract, Semen phaseoli radiati extract, green tea extract, rice bran extract, Flos Jasmini Sambac extract, Semen Persicae extract, the preparation method of Lignum cinnamomi camphorae leaf extract is: get pulverous Herba Portulacae respectively, Folium Kaki, orange peel, scutellariae,radix, Phellinus igniarius (L. ex Fr.) Quel., salicis, Rhizoma et radix valerianae, Lengxiang rose flower, Semen phaseoli radiati, green tea, Testa oryzae, Flos Jasmini Sambac, Semen Persicae, Lignum cinnamomi camphorae leaf, mixed liquor is obtained after adding alkali ion water concussion respectively, described mixed liquor is through collected after centrifugation centrifuged supernatant, gained primary deposition thing adds alkali ion water respectively again and carries out second extraction, extract three times altogether successively, merge three centrifuged supernatant and concentrate to obtain concentrated solution, namely obtaining Herba portulacae extract, Folium Kaki extract, orange peel extract, scutellariae,radix extract, phellinus linteus extract, Salix Babylonica L.P.E, vanilla extract, Lengxiang rose flower extract, Semen phaseoli radiati extract, green tea extract, rice bran extract, Flos Jasmini Sambac extract, Semen Persicae extract, Lignum cinnamomi camphorae leaf extract respectively.
The present invention also provides a kind of preparation method of the facial film containing Cordyceps militaris (L.) Link. composition, comprises the following steps.
Step one, component E deionized water is added blending tank and stir (revolution 30-100rpm) and be warmed up to 80 DEG C in proportion.
Step 2, add component A raw material stirring and dissolve, and keep after 20min in 80 DEG C, stir and be cooled to 40-45 DEG C.
Step 3, to add after the 40 DEG C of preheatings of B component raw material, add component C raw material stirring dissolve and cool to 30-35 DEG C simultaneously, after adding D component raw material stirring and dissolving again, with 50-100 order filter-cloth filtering, gained filtrate ageing 12h-48h, obtains facial mask liquid, this facial mask liquid is adsorbed on wet cotton paper, subpackage is also packed, and is finished product.
Compared with prior art beneficial effect of the present invention.
The invention provides a kind of facial film containing Cordyceps militaris (L.) Link. composition and preparation method thereof; the described facial film containing Cordyceps militaris (L.) Link. composition contains Aloe fermented product, hydrolysis avenin, Cordyceps extracting solution, hydrolysis Lac regis apis, Herba portulacae extract, Folium Kaki extract, orange peel extract, scutellariae,radix extract, phellinus linteus extract, Salix Babylonica L.P.E, vanilla extract, Lengxiang rose flower extract, Semen phaseoli radiati extract, green tea extract, rice bran extract, Flos Jasmini Sambac extract, Semen Persicae extract, Lignum cinnamomi camphorae leaf extract, totally ten eight kinds of active component.Wherein Aloe fermented product has elimination scytitis and antibacterial action, and can significantly improve the anti-wrinkle effect of facial film, is especially applicable to middle and aged women and uses.Herba Portulacae contains abundant SL3 fatty acid and vitamin A sample material.SL3 fatty acid forms the necessary material of cell membrane; Vitamin A sample substance maintains epithelial tissue as the normal function of skin, cornea.Orange peel extract contains terpenoid substance, plays antibacterial and natural perfume material.Containing a large amount of tannic acid in Folium Kaki, can effectively kill various antibacterial and fungus, there is effect that is clean and skin care.Lac regis apis rich in proteins, the material such as aminoacid, vitamin, lipoid, certain herbaceous plants with big flowers acetic acid, trace element, folic acid, acetylcholine, nucleic acid, has the effects such as regulation of skin metabolism and antioxidation.Hydrolysis avenin is rich in hydrolyzed protein, plays instant convergence and level and smooth effect; Scutellariae,radix extract is rich in flavone compound, has the effects such as antibacterial and contraction.Flos Jasmini Sambac extract has antioxidation and bacteria resistance function.To sum up, the present invention has the feature of safety non-toxic containing the facial film of Cordyceps militaris (L.) Link. composition, and raw material is easy to get, and preparation method is simple, and production cost is lower.
Detailed description of the invention
The present invention is further described below in conjunction with specific embodiment.
The invention provides a kind of facial film containing Cordyceps militaris (L.) Link. composition, is formulated by weight by A, B, C, D and E five kinds of component raw material.
Component A: pure water 40.39 parts, hydrolysis avenin 2 parts, xylitol 2 parts, Trenaxmine 1 part, glycyrrhizic acid dipotassium 0.1 part.
B component: glycerol 2 parts, transparent HANSHENGJIAO 0.06 part.
Component C: butanediol 3 parts, Nipagin ester 0.2 part, scutellariae,radix extract 0.7 part.
D component: adenosine triphosphate disodium salt 0.05 part, Cordyceps extract 1 part, hydrolysis Lac regis apis 0.5 part, Aloe fermented product 0.6 part, Herba portulacae extract 0.15 part, Folium Kaki extract 0.15 part, orange peel extract 0.02 part, phellinus linteus extract 0.02 part, Salix Babylonica L.P.E 0.02 part, vanilla extract 0.01 part, Lengxiang rose flower extract 0.01 part, Semen phaseoli radiati extract 0.01 part, green tea extract 0.01 part, rice bran extract 0.01 part, Flos Jasmini Sambac extract 0.01 part, 0.01 part, Semen Persicae extract, Lignum cinnamomi camphorae leaf extract 0.01 part.
Component E: deionized water (pH=7) 50 parts.
In described D component, the preparation method of Cordyceps extract is: get Powdered or original state Cordyceps militaris (L.) Link.sporophore 50g, add alkali ion water 100ml, concussion (200rpm) 30min, mixed liquor is through collected after centrifugation centrifuged supernatant, gained primary deposition thing adds 100ml alkali ion water again and carries out second extraction, extracts three times altogether successively; Merge three extracting solution and the concentrated solution of concentrated 30ml, the dehydrated alcohol adding concentrated solution 3 times amount makes it under 4 DEG C of conditions, precipitate 10h, inclines to supernatant and obtain precipitate, this precipitate absolute ethanol washing, dry under constant temperature 10 DEG C of conditions, obtain polysaccharide crude, be Cordyceps extract.
Described alkali ion water is by carrying out electrolysis generation by pure water; Described pure water is after electrolysis, and enrichment hydroxide ion in water near negative electrode, in alkalescence, obtains alkali ion water.
The alkali ion water index that described alkali ion water outlet produces is pH:9.80-13.80, current potential: >=-120mv.
With distilled water extraction Cordyceps militaris (L.) Link.sporophore effective ingredient, extraction efficiency is 17%, and the extraction efficiency of alkali ion water is 23%.As can be seen here, described alkali ion water extraction Cordyceps militaris (L.) Link.sporophore effective ingredient has not only increased substantially extraction efficiency, also avoid the pollution because using chemical solvent to bring.
In described D component, the preparation method of Aloe fermented product is.
(1) surface cleaning: first Fresh leaf of aloe clear water wash clean, described clear water can not use the tap water containing bleach, because bleach can cause aloe liquid variable color, go bad.
(2) ultraviolet irradiation sterilization: after the Fresh leaf of aloe of wash clean dries, be transported into preparation of samples room, described preparation of samples room is sterilizing room (indoor have sterilizer), carries out uv light irradiation sterilization 6min.
(3) remove leaf skin: in sterilizing room, remove Folium Aloe skin, cut open crust with the blade of sterilization, and aloe gel juice is taken out; Gel juice and Ye Pi are respectively charged into Plastic Drum.
(4) high speed pulverization and precipitation: leaf skin tissue mashing, become dilute slurry with high speed disintegrator (rotating speed 20000, time 3 minutes); Then precipitation process is carried out; Namely supernatant becomes Folium Aloe natural juice.
(5) preparation of Aloe fermented product: described Aloe fermented product comprises Aloe gel fermented product and Folium Aloe fermented product.
1. be, with aloe gel juice culture medium, with Hansenula anomala (lot number: AS2.297, Bei Nuo bio tech ltd, Shanghai) for inoculation strain, inoculum concentration 4%(percent by volume).Fermentation temperature 28 DEG C, fermentation time is 25 days, and gained fermented product is Aloe gel fermented product.
2., with Folium Aloe natural juice for culture medium, with Hansenula anomala (lot number: AS2.297, Bei Nuo bio tech ltd, Shanghai) for inoculation strain, inoculum concentration 4%(percent by volume).Fermentation temperature 28 DEG C, fermentation time is 25 days, and gained fermented product is Folium Aloe fermented product.
Prior art commonly uses Aloe original juice, and the present invention adopts Aloe fermented product, and this Aloe fermented product has following benefit compared with the Aloe original juice not through fermenting: composition is more various and molecule is less, thus is more easily absorbed by the skin.
Described Herba portulacae extract, Folium Kaki extract, orange peel extract, scutellariae,radix extract, phellinus linteus extract, Salix Babylonica L.P.E, vanilla extract, Lengxiang rose flower extract, Semen phaseoli radiati extract, green tea extract, rice bran extract, Flos Jasmini Sambac extract, Semen Persicae extract, the preparation method of Lignum cinnamomi camphorae leaf extract is: get pulverous Herba Portulacae respectively, Folium Kaki, orange peel, scutellariae,radix, Phellinus igniarius (L. ex Fr.) Quel., salicis, Rhizoma et radix valerianae, Lengxiang rose flower, Semen phaseoli radiati, green tea, Testa oryzae, Flos Jasmini Sambac, Semen Persicae, Lignum cinnamomi camphorae leaf, mixed liquor is obtained after adding alkali ion water concussion respectively, described mixed liquor is through collected after centrifugation centrifuged supernatant, gained primary deposition thing adds alkali ion water respectively again and carries out second extraction, extract three times altogether successively, merge three centrifuged supernatant and concentrate to obtain concentrated solution, namely obtaining Herba portulacae extract, Folium Kaki extract, orange peel extract, scutellariae,radix extract, phellinus linteus extract, Salix Babylonica L.P.E, vanilla extract, Lengxiang rose flower extract, Semen phaseoli radiati extract, green tea extract, rice bran extract, Flos Jasmini Sambac extract, Semen Persicae extract, Lignum cinnamomi camphorae leaf extract respectively.
The present invention also provides a kind of preparation method of the facial film containing Cordyceps militaris (L.) Link. composition, comprises the following steps.
Step one, component E deionized water is added blending tank and stir (revolution 50rpm) and be warmed up to 80 DEG C in proportion.
Step 2, add component A raw material stirring and dissolve, and keep after 20min in 80 DEG C, stir and be cooled to 40 DEG C.
Step 3, to add after the 40 DEG C of preheatings of B component raw material, add component C raw material stirring dissolve and cool to 30 DEG C simultaneously, after adding D component raw material stirring and dissolving again, with 50-100 order filter-cloth filtering, gained filtrate ageing 24h, obtains facial mask liquid, this facial mask liquid is adsorbed on wet cotton paper, subpackage is also packed, and is finished product.
The efficacy assessments of the present embodiment formula composition and preparation method thereof gained mask product.
1, practical effect evaluation: participating in facial film effect evaluation and test interviewee number is 28 people, the present embodiment of applying ointment or plaster, containing the facial film 3 times weekly of Cordyceps militaris (L.) Link. composition, is for 10 times a course for the treatment of.Use the present embodiment containing after facial film one course for the treatment of of Cordyceps militaris (L.) Link. composition, objective evaluation is made to this facial film moisturizing, moisturizing, elite trap, elite volatility, facial film abnormal smells from the patient, often kind of effect judgment criteria is divided into third gear, wherein moisturizing: first grade is that moistening effect is very good, second gear is that moistening effect is general, and third gear is that moistening effect is bad; Moisturizing: first grade for moisturizing effect clearly, second gear is that moisturizing effect is general, and third gear is that moisturizing effect is bad; Elite trap: first grade is easy to absorb for elite, and second gear is that elite assimilation effect is general, and third gear is that elite assimilation effect is bad; Elite volatility: first grade is still have a large amount of elite after using, second gear is elite amount part minimizing after use, and third gear obviously reduces for using rear elite amount; Abnormal smells from the patient: first grade is natural comfortable, second gear is that chemical reagent is obvious, and third gear is not for having peculiar taste.Concrete evaluation result is in table 1.
Table 1: the present invention evaluates containing the facial film result of use of Cordyceps militaris (L.) Link. composition.
| First grade | Second gear | Third gear | |
| Moisturizing | 17 | 11 | 0 |
| Moisturizing | 16 | 12 | 0 |
| Elite trap | 26 | 2 | 0 |
| Elite volatility | 0 | 1 | 27 |
| Abnormal smells from the patient | 4 | 0 | 24 |
As shown in Table 1, the present invention has the effect of good moisturizing, moisturizing, nutrition, convergence containing the facial film of Cordyceps militaris (L.) Link. composition.
2, moisture-keeping efficacy evaluation: moisture-keeping efficacy evaluation adopts external weight method, according to the difference of cosmetic composition moisture absorption, performance of keeping humidity, different wetting agent molecules is different to the active force of hydrone, absorbs moisture different with keeping the ability of moisture.Hygroscopic effect power is large, strong to water molecules power, and absorb and keep the amount of moisture also larger, closure is good, also lacking of moisture loss.Utilize adhesive tape to imitate the biomaterial such as horny layer, epidermis, cosmetics smeared by adhesive tape, the application feature of simulation pragmatize cosmetic.Under the condition of constant temperature and humidity after certain hour (4 hours), weigh sample and place the of poor quality of front and back, obtain the loss of sample size, the effect of moisturizing ingredient moisturizing can be calculated.
With the present embodiment facial mask liquid for sample is directly measured, determine that the moisturizing rate of this facial film is about 52.5% by experiment.
3, senile-resistant efficacy evaluation: senile-resistant efficacy evaluation adopts in-vitro evaluation method, and working sample is to the Scavenging activity of free radical.Comprise three indexs, be respectively: remove the mensuration of DPPH ability, remove the mensuration of superoxide anion ability and the mensuration of scavenging hydroxyl ability.
In the mensuration removing DPPH ability, the present embodiment is 23.16%-48.29% containing the clearance rate of the facial film of Cordyceps militaris (L.) Link. composition; In the mensuration removing superoxide anion ability, the present embodiment is 22.46%-47.5% containing the facial film of Cordyceps militaris (L.) Link. composition to the suppression ratio of superoxide anion; In the mensuration of scavenging hydroxyl ability, the present embodiment is 16.32%-26.01% containing the facial film of Cordyceps militaris (L.) Link. composition to the clearance rate of hydroxy radical.
4, pH value measures: take film sample 1g(and be accurate to 0.1g), adding distil water 10g, is heated to 40 DEG C, and is constantly stirred to evenly, measures after being cooled to room temperature with pH meter.
Mensuration the present embodiment is 5.4-7.0 containing the pH value of the facial film of Cordyceps militaris (L.) Link. composition.
5, measuring drying time: the tackness that can reflect facial film drying time, is one of important indicator weighing facial film quality.Facial film is too short for drying time, and effective ingredient is not easily absorbed by the skin, and easily produces strong pulling force to skin and caused discomfort; Drying time is long, uses inconvenience, and skin dehydration is more, and the assimilation effect of effective ingredient is not good enough yet.Particularly, take 0.2g film sample, uniform application, on clean microscope slide (25.4mm × 76.2mm), makes film sample tile whole slide surface; Then, at being placed in room temperature 20 ± 5 DEG C, recording drying time, be as the criterion with tack-free.
Mensuration the present embodiment is 15-35min containing the drying time of the facial film of Cordyceps militaris (L.) Link. composition.
6, Stability Determination.
(1) heat resistant test: be placed in 40 DEG C and deposit 24h, observe whether have layering, oil slick phenomenon, whether color and luster changes.After tested, the present embodiment finds the front no significant difference of itself and test containing the facial film visual observations of Cordyceps militaris (L.) Link. composition, and layering, oil slick phenomenon do not occur, and color and luster, also without significant change, shows that mask product thermostability is better.
(2) low temperature resistant test: be placed in-5 DEG C and deposit 24h, observe whether have layering, oil slick phenomenon, whether color and luster changes.After tested, the present embodiment finds the front no significant difference of itself and test containing the facial film visual observations of Cordyceps militaris (L.) Link. composition, and layering, oil slick phenomenon do not occur, and color and luster, also without significant change, shows that mask product tolerance to cold is better.
(3) thermal cycling test: be placed in 40 DEG C and deposit 24h, deposit 24h, then deposit 24h in-5 DEG C in room temperature, circulates 3 times successively, and observe whether have layering, oil slick and oil impregnate phenomenon, whether color and luster changes.After tested, the present embodiment finds the front no significant difference of itself and test containing the facial film visual observations of Cordyceps militaris (L.) Link. composition, and layering, oil slick phenomenon do not occur, and color and luster, also without significant change, shows that mask product is cold-resistant better hot.
(4) whether dewatering ability: centrifugal 20min under being placed in 300 r/min, observe and have moisture to separate out.After tested, containing the facial film visual observations of Cordyceps militaris (L.) Link. composition, the present embodiment finds that its anhydrous assay goes out, lamination does not occur, shows that mask product dewatering ability is better.
Claims (5)
1., containing a facial film for Cordyceps militaris (L.) Link. composition, be formulated by A, B, C, D and E five kinds of component raw material:
Component A: pure water 34-47 part, hydrolysis avenin 1.7-2.3 part, xylitol 1.7-2.3 part, Trenaxmine 0.8-1.2 part, glycyrrhizic acid dipotassium 0.08-0.12 part;
B component: glycerol 1.7-2.3 part, transparent HANSHENGJIAO 0.05-0.07 part;
Component C: butanediol 2.2-3 part, Nipagin ester 0.1-0.25 part, scutellariae,radix extract 0.6-0.8 part;
D component: adenosine triphosphate disodium salt 0.04-0.06 part, Cordyceps extract 0.85-1.2 part, hydrolysis Lac regis apis 0.4-0.6 part, Aloe fermented product 0.5-1.0 part, Herba portulacae extract 0.1-0.3 part, Folium Kaki extract 0.1-0.3 part, orange peel extract 0.01-0.1 part, phellinus linteus extract 0.01-0.1 part, Salix Babylonica L.P.E 0.01-0.03 part, vanilla extract 0.01-0.03 part, Lengxiang rose flower extract 0.01-0.03 part, Semen phaseoli radiati extract 0.01-0.03 part, green tea extract 0.01-0.03 part, rice bran extract 0.01-0.02 part, Flos Jasmini Sambac extract 0.01-0.02 part, Semen Persicae extract 0.01-0.02 part, Lignum cinnamomi camphorae leaf extract 0.01-0.02 part,
Component E: deionized water 42-58 part;
In described D component, the preparation method of Cordyceps extract is: get Powdered or original state Cordyceps militaris (L.) Link.sporophore 40-100g, add alkali ion water 100-300ml, mixed liquor is obtained after concussion (100-300rpm) 10-50min, described mixed liquor is through collected after centrifugation centrifuged supernatant, gained primary deposition thing adds 100-300ml alkali ion water again and carries out second extraction, extracts three times altogether successively; Merge three centrifuged supernatant and the concentrated solution of concentrated 20-30ml, the dehydrated alcohol adding concentrated solution 2-4 times amount makes it under 4 DEG C of conditions, precipitate 8-12h, incline and supernatant and obtain precipitate, this precipitate absolute ethanol washing, freeze-day with constant temperature at a certain temperature between 10 DEG C-20 DEG C, obtain polysaccharide crude, be Cordyceps extract;
In described D component, the preparation method of Aloe fermented product is:
(1) surface cleaning: Fresh leaf of aloe clear water wash clean;
(2) ultraviolet radiation sterilization: after the Fresh leaf of aloe of wash clean dries, be transported into preparation of samples room, described preparation of samples room is sterilizing room (indoor have sterilizer), carries out uv light irradiation sterilization 5-30min;
(3) remove leaf skin: in sterilizing room, remove Fresh leaf of aloe leaf skin, cut open crust with the blade of sterilization, and aloe gel juice is taken out; Gel juice and Ye Pi are respectively charged into Plastic Drum;
(4) high speed pulverization and precipitation: leaf skin tissue mashing, become dilute slurry with high speed disintegrator (rotating speed 10000-30000, time 0.2-5 minute); Then precipitation process is carried out; Namely supernatant becomes Folium Aloe natural juice;
(5) preparation of Aloe fermented product: described Aloe fermented product comprises Aloe gel fermented product and Folium Aloe fermented product;
1., be culture medium with aloe gel juice, take Hansenula anomala as inoculation strain, the inoculum concentration 1%-10% of bacterium liquid, fermentation temperature 26 DEG C-31 DEG C, fermentation time is 20-30 days, and gained fermented product is Aloe gel fermented product;
2., with Folium Aloe natural juice for culture medium, take Hansenula anomala as inoculation strain, the inoculum concentration 1%-10% of bacterium liquid, fermentation temperature 26 DEG C-31 DEG C, fermentation time is 20-30 days, and gained fermented product is Folium Aloe fermented product;
Described Herba portulacae extract, Folium Kaki extract, orange peel extract, scutellariae,radix extract, phellinus linteus extract, Salix Babylonica L.P.E, vanilla extract, Lengxiang rose flower extract, Semen phaseoli radiati extract, green tea extract, rice bran extract, Flos Jasmini Sambac extract, Semen Persicae extract, the preparation method of Lignum cinnamomi camphorae leaf extract is: get pulverous Herba Portulacae respectively, Folium Kaki, orange peel, scutellariae,radix, Phellinus igniarius (L. ex Fr.) Quel., salicis, Rhizoma et radix valerianae, Lengxiang rose flower, Semen phaseoli radiati, green tea, Testa oryzae, Flos Jasmini Sambac, Semen Persicae, Lignum cinnamomi camphorae leaf, mixed liquor is obtained after adding alkali ion water concussion respectively, described mixed liquor is through collected after centrifugation centrifuged supernatant, gained primary deposition thing adds alkali ion water respectively again and carries out second extraction, extract three times altogether successively, merge three centrifuged supernatant and concentrate to obtain concentrated solution, namely obtaining Herba portulacae extract, Folium Kaki extract, orange peel extract, scutellariae,radix extract, phellinus linteus extract, Salix Babylonica L.P.E, vanilla extract, Lengxiang rose flower extract, Semen phaseoli radiati extract, green tea extract, rice bran extract, Flos Jasmini Sambac extract, Semen Persicae extract, Lignum cinnamomi camphorae leaf extract respectively.
2. the facial film containing Cordyceps militaris (L.) Link. composition as claimed in claim 1, it is characterized in that, be formulated by A, B, C, D and E five kinds of component raw material:
Component A: pure water 40.39 parts, hydrolysis avenin 2 parts, xylitol 2 parts, Trenaxmine 1 part, glycyrrhizic acid dipotassium 0.1 part;
B component: glycerol 2 parts, transparent HANSHENGJIAO 0.06 part;
Component C: butanediol 3 parts, Nipagin ester 0.2 part, scutellariae,radix extract 0.7 part;
D component: adenosine triphosphate disodium salt 0.05 part, Cordyceps extract 1 part, hydrolysis Lac regis apis 0.5 part, Aloe fermented product 0.6 part, Herba portulacae extract 0.15 part, Folium Kaki extract 0.15 part, orange peel extract 0.02 part, phellinus linteus extract 0.02 part, Salix Babylonica L.P.E 0.02 part, vanilla extract 0.01 part, Lengxiang rose flower extract 0.01 part, Semen phaseoli radiati extract 0.01 part, green tea extract 0.01 part, rice bran extract 0.01 part, Flos Jasmini Sambac extract 0.01 part, 0.01 part, Semen Persicae extract, Lignum cinnamomi camphorae leaf extract 0.01 part,
Component E: deionized water 50 parts;
In described D component, the preparation method of Cordyceps extract is: get Powdered or original state Cordyceps militaris (L.) Link.sporophore 50g, add alkali ion water 100ml, concussion (200rpm) 30min, mixed liquor is through collected after centrifugation centrifuged supernatant, gained primary deposition thing adds 100ml alkali ion water again and carries out second extraction, extracts three times altogether successively; Merge three extracting solution and the concentrated solution of concentrated 30ml, the dehydrated alcohol adding concentrated solution 3 times amount makes it under 4 DEG C of conditions, precipitate 10h, inclines to supernatant and obtain precipitate, this precipitate absolute ethanol washing, dry under constant temperature 10 DEG C of conditions, obtain polysaccharide crude, be Cordyceps extract;
In described D component, the preparation method of Aloe fermented product is:
(1) surface cleaning: Fresh leaf of aloe clear water wash clean;
(2) ultraviolet irradiation sterilization: after the Fresh leaf of aloe of wash clean dries, be transported into preparation of samples room, described preparation of samples room is sterilizing room (indoor have sterilizer), carries out uv light irradiation sterilization 6min;
(3) remove leaf skin: in sterilizing room, remove Folium Aloe skin, cut open crust with the blade of sterilization, and aloe gel juice is taken out; Gel juice and Ye Pi are respectively charged into Plastic Drum;
(4) high speed pulverization and precipitation: leaf skin tissue mashing, become dilute slurry with high speed disintegrator (rotating speed 20000, time 3 minutes); Then precipitation process is carried out; Namely supernatant becomes Folium Aloe natural juice;
(5) preparation of Aloe fermented product: described Aloe fermented product comprises Aloe gel fermented product and Folium Aloe fermented product;
1., be culture medium with aloe gel juice, take Hansenula anomala as inoculation strain, inoculum concentration 4%, fermentation temperature 28 DEG C, fermentation time is 25 days, and gained fermented product is Aloe gel fermented product;
2., with Folium Aloe natural juice for culture medium, take Hansenula anomala as inoculation strain, inoculum concentration 4%, fermentation temperature 28 DEG C, fermentation time is 25 days, and gained fermented product is Folium Aloe fermented product;
Described Herba portulacae extract, Folium Kaki extract, orange peel extract, scutellariae,radix extract, phellinus linteus extract, Salix Babylonica L.P.E, vanilla extract, Lengxiang rose flower extract, Semen phaseoli radiati extract, green tea extract, rice bran extract, Flos Jasmini Sambac extract, Semen Persicae extract, the preparation method of Lignum cinnamomi camphorae leaf extract is: get pulverous Herba Portulacae respectively, Folium Kaki, orange peel, scutellariae,radix, Phellinus igniarius (L. ex Fr.) Quel., salicis, Rhizoma et radix valerianae, Lengxiang rose flower, Semen phaseoli radiati, green tea, Testa oryzae, Flos Jasmini Sambac, Semen Persicae, Lignum cinnamomi camphorae leaf, mixed liquor is obtained after adding alkali ion water concussion respectively, described mixed liquor is through collected after centrifugation centrifuged supernatant, gained primary deposition thing adds alkali ion water respectively again and carries out second extraction, extract three times altogether successively, merge three centrifuged supernatant and concentrate to obtain concentrated solution, namely obtaining Herba portulacae extract, Folium Kaki extract, orange peel extract, scutellariae,radix extract, phellinus linteus extract, Salix Babylonica L.P.E, vanilla extract, Lengxiang rose flower extract, Semen phaseoli radiati extract, green tea extract, rice bran extract, Flos Jasmini Sambac extract, Semen Persicae extract, Lignum cinnamomi camphorae leaf extract respectively.
3. the facial film containing Cordyceps militaris (L.) Link. composition as claimed in claim 1 or 2, it is characterized in that, described alkali ion water is by carrying out electrolysis generation by pure water.
4. the facial film containing Cordyceps militaris (L.) Link. composition as claimed in claim 3, it is characterized in that, described alkali ion water index is pH:9.80-13.80, current potential: >=-120mV.
5. the preparation method of the facial film containing Cordyceps militaris (L.) Link. composition as claimed in claim 4, is characterized in that:
Step one, component E deionized water is added blending tank and stir (revolution 30-100rpm) and be warmed up to 80 DEG C in proportion;
Step 2, add component A raw material stirring and dissolve, and keep after 20min in 80 DEG C, stir and be cooled to 40-45 DEG C;
Step 3, to add after the 40 DEG C of preheatings of B component raw material, add component C raw material stirring dissolve and cool to 30-35 DEG C simultaneously, after adding D component raw material stirring and dissolving again, with 50-100 order filter-cloth filtering, gained filtrate ageing 12h-48h, obtains facial mask liquid, this facial mask liquid is adsorbed on wet cotton paper, subpackage is also packed, and is finished product.
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| CN113520952A (en) * | 2021-08-13 | 2021-10-22 | 华东理工大学 | Shilixiang fragrance and preparation method of mask thereof |
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