CN104357932A - Cotton fiber with good light resistance and preparation method of cotton fiber - Google Patents
Cotton fiber with good light resistance and preparation method of cotton fiber Download PDFInfo
- Publication number
- CN104357932A CN104357932A CN201410542394.3A CN201410542394A CN104357932A CN 104357932 A CN104357932 A CN 104357932A CN 201410542394 A CN201410542394 A CN 201410542394A CN 104357932 A CN104357932 A CN 104357932A
- Authority
- CN
- China
- Prior art keywords
- parts
- cotton fiber
- minute
- add
- fiber
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention discloses cotton fiber with good light resistance. The cotton fiber is characterized by being prepared by raw materials in parts by weight as follows: 20-25 parts of cotton fiber, 13-17 parts of waste cotton fiber, 4-7 parts of acetate fiber, 11-14 parts of ramie fiber, 2-3 parts of hydroxypropyl guar, 1-3 parts of sodium tetraborate decahydrate, 2-4 parts of light calcined magnesia, 6-8 parts of pine tar, 14-16 parts of isopropyl alcohol, 25-28 parts of 4,4-diaminodiphenyl ether, 2.1-3.5 parts of graphene, 2-3 parts of rust-brown crotalaria, 3-4 parts of plumbagella, 1-3 parts of radix isatidis, 100-110 parts of 1-butyl-3-ethylimidazolium dibutyl phosphate, 110-120 parts of 1-butyl-3-methylimidazole acetate, 3-5 parts of an auxiliary and an appropriate amount of water. According to the cotton fiber, acetate fiber is introduced, so that the cotton fiber has good light resistance; waste cotton fiber and other effective ingredients are further added, and accordingly, the defect of poor dyeing property is overcome; and the toughness and the thermal insulation property of the cotton fiber are improved, meanwhile, the utilization rate of waste cotton is increased, and the cost is reduced.
Description
Technical field
The present invention relates to textile material technical field, be specifically related to good cotton fiber of a kind of light resistance and preparation method thereof.
Background technology
Cotton fiber is fiber coating on the seed of Malvaceae cotton, and also known as cotton, being called for short cotton, is the main raw material of China's textile industry.The moisture absorption of cotton fiber goods and good permeability, wear-resisting washable, soft and warming, wear warmth retention property winter good, dress in summer is ventilative nice and cool, is widely used in the field such as garment material, drapery.
But cotton fiber makes it apply to be restricted because it exists many defects in the prior art.Such as cotton fiber goods are subject to microbial action, are easily corroded by bacterium, mould, and antibacterial and mouldproof effect is not remarkable; The anti-uv-ray of cotton fiber own is poor, makes it make summer clothes and skin chromogenesis precipitation can be caused even to cause cutaneum carcinoma; Cotton fiber flame retardant effect is poor, and the disaster hidden-trouble caused thus is in rising trend.For overcoming the deficiencies in the prior art, be necessary natural cotton fiber in addition modification, thus be obtainedly applicable to the cotton fiber with functions such as cost low, function diversification, fire-retardant, intensity high, sterilization uvioresistant, radiation proofs of modern for the different demands of cotton fiber goods.
Summary of the invention
Object of the present invention is just to provide good cotton fiber of a kind of light resistance and preparation method thereof, to overcome the deficiencies in the prior art.
The object of the present invention is achieved like this:
The cotton fiber that a kind of light resistance is good, it is characterized in that, be made up of the raw material of following weight portion: cotton fiber 20-25, waste cotton fiber 13-17, acetate fibre 4-7, ramee 11-14, hydroxypropyl guar gum 2-3, sodium tetraborate decahydrate 1-3, light calcined magnesia 2-4, pine tar 6-8, isopropyl alcohol 14-16,4,4-diaminodiphenyl ether 25-28, Graphene 2.1-3.5, rust-coloured crotalaria herb with root 2-3, littleflower plumbagella herb 3-4, Radix Isatidis 1-3,1-butyl-3-ethyl imidazol(e) dibutylphosphoric acid ester 100-110,1-butyl-3-N-Methylimidazoleacetic salt 110-120, auxiliary agent 3-5, suitable quantity of water.
Described auxiliary agent is made up of following raw materials in part by weight: diethylenetriamine 1-2, epoxychloropropane 3-6, glyoxal 7-9, ethylene glycol 12-14, polyhexamethylene guanide 0.4-0.7, Foral 1.2-2.5, natrium citricum 2.1-2.6, alkyl phosphate 5-7, fatty alcohol-polyoxyethylene ether 6-8, nano silicon 2-3, its preparation method is by swelling for nano silicon room temperature in distilled water 23 hours, form suspension, then diethylenetriamine, epoxychloropropane, glyoxal, ethylene glycol, alkyl phosphate, fatty alcohol-polyoxyethylene ether mix and blend is also warming up to 140-160 DEG C of stirring 1-2 hour, join in above-mentioned suspension and stir 30-40 minute, add other residual componentss again strong agitation 2-3 hour and get final product.
The preparation method of the cotton fiber that described a kind of light resistance is good, is characterized in that comprising the following steps:
(1) by rust-coloured crotalaria herb with root, littleflower plumbagella herb, Radix Isatidis boiling 4-6 hour, filter, the waste cotton fiber put in filtrate after cotton fiber, acetate fibre, ramee and sterilization bleaching soaks 7-10 hour, add hydroxypropyl guar gum again and stir 30-40 minute, after filtering drying, grind to form 80-100 order powder;
(2) retort is put in above-mentioned Chinese medicine filter residue oven dry and carbonize 30-40 minute, add Graphene, light calcined magnesia pulverizes and spray into pine tar, add isopropyl alcohol again, 4,4-diaminodiphenyl ethers put into reactor together and be warming up to 160-180 DEG C, keep temperature to stir 1-2 hour;
(3) step (1) product is placed in step (2) and soaks 15-20 minute, roll compacting 10-15 minute, steam treatment 5-10 minute, clean and dry;
(4) finally take 1-butyl-3-ethyl imidazol(e) dibutylphosphoric acid ester, 1-butyl-3-N-Methylimidazoleacetic salt drops in reactor and stirs and evenly mixs, add step (3) product and stir 20-40 minute, be heated to 100-115 DEG C, add other residual components stirring reaction 40-60 minute again, obtained spinning solution, finally carries out spinning, winding, boundling, stretching by obtained spinning solution and get final product.
The present invention has following beneficial effect: cotton fiber provided by the invention, by introducing acetate fibre, make cotton fiber light resistance good, also add waste cotton fiber and other active ingredient, improve the defect of dyeability difference, and improve toughness and the thermal property of cotton fiber, the utilization rate simultaneously promoting waste cotton reduces cost.
Detailed description of the invention
The cotton fiber that described a kind of light resistance is good, it is characterized in that, be made up of the raw material of following weight portion: cotton fiber 23, waste cotton fiber 14, acetate fibre 5, ramee 12, hydroxypropyl guar gum 2, sodium tetraborate decahydrate 1, light calcined magnesia 2, pine tar 6, isopropyl alcohol 15,4,4-diaminodiphenyl ether 26, Graphene 2.8, rust-coloured crotalaria herb with root 2, littleflower plumbagella herb 4, Radix Isatidis 1,1-butyl-3-ethyl imidazol(e) dibutylphosphoric acid ester 100,1-butyl-3-N-Methylimidazoleacetic salt 110, auxiliary agent 3, suitable quantity of water.
Described auxiliary agent is made up of following raw materials in part by weight: diethylenetriamine 1, epoxychloropropane 5, glyoxal 8, ethylene glycol 13, polyhexamethylene guanide 0.5, Foral 1.6, natrium citricum 2.5, alkyl phosphate 6, fatty alcohol-polyoxyethylene ether 8, nano silicon 3, its preparation method is by swelling for nano silicon room temperature in distilled water 23 hours, form suspension, then diethylenetriamine, epoxychloropropane, glyoxal, ethylene glycol, alkyl phosphate, fatty alcohol-polyoxyethylene ether mix and blend is also warming up to 140-160 DEG C of stirring 1-2 hour, join in above-mentioned suspension and stir 30-40 minute, add other residual componentss again strong agitation 2-3 hour and get final product.
Preparation method comprises the following steps:
(1) by rust-coloured crotalaria herb with root, littleflower plumbagella herb, Radix Isatidis boiling 4-6 hour, filter, the waste cotton fiber put in filtrate after cotton fiber, acetate fibre, ramee and sterilization bleaching soaks 7-10 hour, add hydroxypropyl guar gum again and stir 30-40 minute, after filtering drying, grind to form 80-100 order powder;
(2) retort is put in above-mentioned Chinese medicine filter residue oven dry and carbonize 30-40 minute, add Graphene, light calcined magnesia pulverizes and spray into pine tar, add isopropyl alcohol again, 4,4-diaminodiphenyl ethers put into reactor together and be warming up to 160-180 DEG C, keep temperature to stir 1-2 hour;
(3) step (1) product is placed in step (2) and soaks 15-20 minute, roll compacting 10-15 minute, steam treatment 5-10 minute, clean and dry;
(4) finally take 1-butyl-3-ethyl imidazol(e) dibutylphosphoric acid ester, 1-butyl-3-N-Methylimidazoleacetic salt drops in reactor and stirs and evenly mixs, add step (3) product and stir 20-40 minute, be heated to 100-115 DEG C, add other residual components stirring reaction 40-60 minute again, obtained spinning solution, finally carries out spinning, winding, boundling, stretching by obtained spinning solution and get final product.
The technical parameter index of the cotton fiber using the present invention to produce is as follows:
(1) pliability is fluffy smooth flexible, and intensity is high, flame retardant effect is excellent;
(2) bacteriostasis rate of finished product to Escherichia coli, staphylococcus aureus, Candida albicans is all greater than 97%;
(3) after 30 washings, antibiotic rate still reaches 92%.
Claims (2)
1. the cotton fiber that a light resistance is good, it is characterized in that, be made up of the raw material of following weight portion: cotton fiber 20-25, waste cotton fiber 13-17, acetate fibre 4-7, ramee 11-14, hydroxypropyl guar gum 2-3, sodium tetraborate decahydrate 1-3, light calcined magnesia 2-4, pine tar 6-8, isopropyl alcohol 14-16,4,4-diaminodiphenyl ether 25-28, Graphene 2.1-3.5, rust-coloured crotalaria herb with root 2-3, littleflower plumbagella herb 3-4, Radix Isatidis 1-3,1-butyl-3-ethyl imidazol(e) dibutylphosphoric acid ester 100-110,1-butyl-3-N-Methylimidazoleacetic salt 110-120, auxiliary agent 3-5, suitable quantity of water, described auxiliary agent is made up of following raw materials in part by weight: diethylenetriamine 1-2, epoxychloropropane 3-6, glyoxal 7-9, ethylene glycol 12-14, polyhexamethylene guanide 0.4-0.7, Foral 1.2-2.5, natrium citricum 2.1-2.6, alkyl phosphate 5-7, fatty alcohol-polyoxyethylene ether 6-8, nano silicon 2-3, its preparation method is by swelling for nano silicon room temperature in distilled water 23 hours, form suspension, then diethylenetriamine, epoxychloropropane, glyoxal, ethylene glycol, alkyl phosphate, fatty alcohol-polyoxyethylene ether mix and blend is also warming up to 140-160 DEG C of stirring 1-2 hour, join in above-mentioned suspension and stir 30-40 minute, add other residual componentss again strong agitation 2-3 hour and get final product.
2. the preparation method of the cotton fiber that a kind of light resistance according to claim 1 is good, is characterized in that comprising the following steps:
(1) by rust-coloured crotalaria herb with root, littleflower plumbagella herb, Radix Isatidis boiling 4-6 hour, filter, the waste cotton fiber put in filtrate after cotton fiber, acetate fibre, ramee and sterilization bleaching soaks 7-10 hour, add hydroxypropyl guar gum again and stir 30-40 minute, after filtering drying, grind to form 80-100 order powder;
(2) retort is put in above-mentioned Chinese medicine filter residue oven dry and carbonize 30-40 minute, add Graphene, light calcined magnesia pulverizes and spray into pine tar, add isopropyl alcohol again, 4,4-diaminodiphenyl ethers put into reactor together and be warming up to 160-180 DEG C, keep temperature to stir 1-2 hour;
(3) step (1) product is placed in step (2) and soaks 15-20 minute, roll compacting 10-15 minute, steam treatment 5-10 minute, clean and dry;
(4) finally take 1-butyl-3-ethyl imidazol(e) dibutylphosphoric acid ester, 1-butyl-3-N-Methylimidazoleacetic salt drops in reactor and stirs and evenly mixs, add step (3) product and stir 20-40 minute, be heated to 100-115 DEG C, add other residual components stirring reaction 40-60 minute again, obtained spinning solution, finally carries out spinning, winding, boundling, stretching by obtained spinning solution and get final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410542394.3A CN104357932A (en) | 2014-10-15 | 2014-10-15 | Cotton fiber with good light resistance and preparation method of cotton fiber |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410542394.3A CN104357932A (en) | 2014-10-15 | 2014-10-15 | Cotton fiber with good light resistance and preparation method of cotton fiber |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104357932A true CN104357932A (en) | 2015-02-18 |
Family
ID=52525232
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410542394.3A Pending CN104357932A (en) | 2014-10-15 | 2014-10-15 | Cotton fiber with good light resistance and preparation method of cotton fiber |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104357932A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106087091A (en) * | 2016-07-21 | 2016-11-09 | 山传雷 | A kind of menthone modified cellulose fibre and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101225552A (en) * | 2008-02-04 | 2008-07-23 | 东华大学 | Method for dissolving and processing wood/cotton bamboo hemp fibre by employing ionic liquid |
| CN103014892A (en) * | 2012-12-26 | 2013-04-03 | 东华大学 | Preparation method of cellulose acetate fiber |
| CN103046151A (en) * | 2012-12-18 | 2013-04-17 | 青岛大学 | Graphene blend regenerated cellulose fiber and preparation method thereof |
| CN103696142A (en) * | 2013-12-10 | 2014-04-02 | 马鞍山湖滨无纺布科技有限公司 | Mould-proof mothproof non-woven fabric and preparation method thereof |
-
2014
- 2014-10-15 CN CN201410542394.3A patent/CN104357932A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101225552A (en) * | 2008-02-04 | 2008-07-23 | 东华大学 | Method for dissolving and processing wood/cotton bamboo hemp fibre by employing ionic liquid |
| CN103046151A (en) * | 2012-12-18 | 2013-04-17 | 青岛大学 | Graphene blend regenerated cellulose fiber and preparation method thereof |
| CN103014892A (en) * | 2012-12-26 | 2013-04-03 | 东华大学 | Preparation method of cellulose acetate fiber |
| CN103696142A (en) * | 2013-12-10 | 2014-04-02 | 马鞍山湖滨无纺布科技有限公司 | Mould-proof mothproof non-woven fabric and preparation method thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106087091A (en) * | 2016-07-21 | 2016-11-09 | 山传雷 | A kind of menthone modified cellulose fibre and preparation method thereof |
| CN106087091B (en) * | 2016-07-21 | 2018-05-01 | 青岛邦特生态纺织科技有限公司 | A kind of menthones modified cellulose fibre and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104278359A (en) | Cotton fibers with antibacterial and insect-resisting effects and production method of cotton fibers | |
| CN104775205B (en) | A kind of multifunctional blended yarn and its application | |
| CN104195665B (en) | Eider down composite fibre that a kind of waste and old down fiber/acrylic staple fibre is compound and preparation method thereof | |
| CN104264276A (en) | Mildew-proof down feather composite fiber and preparation method thereof | |
| CN104213247A (en) | Water-washable silk composite fiber and preparation method thereof | |
| CN104762692A (en) | Moisture-absorbing thermal-insulation down composite fiber and manufacturing method thereof | |
| CN105820588A (en) | Composite silk textile material and preparation method thereof | |
| CN104947223A (en) | Low-damage green ecological bacteriostatic down fiber and making method thereof | |
| CN104292868A (en) | X-ray radiation resistant wood fiber and preparation method thereof | |
| CN104831407A (en) | Compound warm down feather composite fiber and producing method thereof | |
| CN104357933A (en) | Ultraviolet-proof cotton fiber and preparation method thereof | |
| CN104357948A (en) | Cotton fiber modified by dead sea black mud and preparation method of cotton fiber | |
| CN104278356A (en) | Chinese herbal medicine antibacterial cotton fibers and production method thereof | |
| CN104562259A (en) | Mothproof fire resistant fiber | |
| CN104294399A (en) | Down feather composite fibers with jasmine fragrance and preparation method thereof | |
| CN104357946A (en) | Radiation-proof flame-retardant cotton fiber and preparation method thereof | |
| CN104357932A (en) | Cotton fiber with good light resistance and preparation method of cotton fiber | |
| CN104831411A (en) | Multifunctional mothproof down feather composite fiber and producing method thereof | |
| CN104947222A (en) | Light and fluffy ecological bacteriostatic down fiber and making method thereof | |
| CN104357949A (en) | Antibacterial warm-keeping cotton fiber with seaweed carbon fibers added and preparation method of cotton fiber | |
| CN104790063A (en) | Odor-removing down feather composite fiber and preparation method thereof | |
| CN104313877A (en) | Coupling agent modifying method for bamboo fibers | |
| CN104947233A (en) | Antistatic ecological bacteriostatic down fiber and making method thereof | |
| CN104947232A (en) | Washable anti-radiation ecological bacteriostatic down fiber and making method thereof | |
| CN104294400A (en) | Cotton fibers with antibacterial anti-mite effects and manufacturing method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20150218 |
|
| RJ01 | Rejection of invention patent application after publication |