CN104292868A - X-ray radiation resistant wood fiber and preparation method thereof - Google Patents
X-ray radiation resistant wood fiber and preparation method thereof Download PDFInfo
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- CN104292868A CN104292868A CN201410454663.0A CN201410454663A CN104292868A CN 104292868 A CN104292868 A CN 104292868A CN 201410454663 A CN201410454663 A CN 201410454663A CN 104292868 A CN104292868 A CN 104292868A
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Abstract
The invention discloses an X-ray radiation resistant wood fiber which is characterized by being prepared from the following raw materials in parts by weight: 40-45 parts of a wood fiber, 1.1-2.1 parts of a nano silver fiber, 16-18 parts of a wheat straw fiber, 8-10 parts of an aluminum silicate fiber, 1-2 parts of cassava starch, 0.3-0.6 part of zinc borate, 4.3-6.5 parts of barium sulfate, 0.4-0.6 part of polyethylene glycol, 2.1-3.2 parts of folium artemisiae argyi oil, 2.1-4.2 parts of epoxy flaxseed oil, 2-5 parts of ethylene bisoleamide, 0.3-0.6 part of vanillin, 0.2-0.4 part of petroleum sodium sulfonate, 13-16 parts of ramie root, 1-3 parts of radix scutellariae, 2-4 parts of radix puerariae, 3-5 parts of an auxiliary agent, and a proper amount of water. The X-ray shielding agent barium sulfate is modified and then added to the raw materials, and thus the X-ray radiation resistant wood fiber has good X-ray radiation resistant durability, excellent mechanical properties and good textile processability, and can be widely used in industries for production of clothing and nonwovens for workers contacting X rays for a long term.
Description
Technical field
The present invention relates to a kind of xylon modification field, be specifically related to xylon of a kind of X-ray radiation protection and preparation method thereof.
Background technology
Pure natural wood fiber product selects 2 to 3 years life natural free of contamination Australia fast growing trees, pulverizes high temperature steaming and become wood pulp extraction fiber to make.Reject sugar in timber and fat part through special technique and production technique, and sophistication eradicates the electrostatic reaction of material, without any composition chemically in whole process, the same with cotton be all 100% green product.There is natural antibiotic health care, remove peculiar smell, from self-cleaning clearly function, soft-touch, does not harden hardening, be one real, the healthy products of pure green.Therefore the extremely popular favor of pure natural xylon, is widely used in the fields such as towel, underwear, T-shirt, kitchen towel, socks, shirt, Western-style clothes, baby's textiles, bedclothes, curtain, fabric, bedding and padding.
In prior art, xylon is inflammable exists many weak points: because xylon has the water absorbability more superior than cotton fibre and ventilation property, therefore apt to rot time for being processed into fiberboard, easy conductive, inflammable etc., and xylon is compared to comparatively hard for quality time knitting cotton fibre, sense of touch is poor; Secondly, because time prepared by xylon, starting material are limited, and existing life multiple demands cannot be met, so xylon is restricted in its use range of a very long time, the solution the deficiencies in the prior art that the functional strong innovation wood fibers such as a kind of novel energy-saving environment-friendly, low cost, function diversification, fire-retardant, intensity is high, sterilization uvioresistant, radioprotective can be all greatly possible.
Summary of the invention
Object of the present invention is just to provide xylon of a kind of X-ray radiation protection and preparation method thereof, to overcome the deficiencies in the prior art.
The object of the present invention is achieved like this:
A kind of xylon of X-ray radiation protection, it is characterized in that, be made up of the raw material of following weight part: xylon 40-45, nano silver fibre 1.1-2.1, wheat straw fiber 16-18, aluminum silicate fiber 8-10, tapioca (flour) 1-2, zinc borate 0.3-0.6, barium sulfate 4.3-6.5, polyoxyethylene glycol 0.4-0.6, Oleum Folium Artemisiae Argyi 2.1-3.2, epoxy linseed oil 2.1-4.2, ethylene two amine hydroxybenzene 2-5, Vanillin 0.3-0.6, petroleum sodium sulfonate 0.2-0.4, Ramie Root 13-16, root of large-flowered skullcap 1-3, root of kudzu vine 2-4, auxiliary agent 3-5, suitable quantity of water.
Described auxiliary agent is made up of following raw materials in part by weight: tealeaves fiber 10-13, nano zine oxide 2-4, silicon powder 1-3, dual polyethylene polydimethylsiloxane 0.03-0.05, glyceryl monostearate 1.2-3.1, polyoxyethylene glycol 3-6, methylisothiazolinone 2.1-3.6, Oleum Pelargonii Graveolentis 3.2-4.7, Flos Pelargonii Hortori 0.2-0.4, linolic acid 1.3-2.4, Dyhard RU 100 0.1-0.2, ethyl acrylate 4-7, fire retardant CP 0.04-0.07, its preparation method be first by nano zine oxide ultrasonic disperse in polyoxyethylene glycol, add tealeaves blending in of fibers and stir 5-8 hour, take out drying and grinding 10-15 minute, obtained modification tealeaves fiber, then by Oleum Pelargonii Graveolentis, Flos Pelargonii Hortori adds water stirring, and add silicon powder and stir 30-40 minute, spraying dry obtains modified silicon micro mist, finally by ethyl acrylate, linolic acid, Dyhard RU 100, methylisothiazolinone stirring and evenly mixing, adds above-mentioned obtained modification tealeaves fiber and modified silicon micro mist, glyceryl monostearate, dual polyethylene polydimethylsiloxane, fire retardant CP supersound process 30-40 minute and get final product.
The preparation method of the xylon of described a kind of X-ray radiation protection, is characterized in that comprising the following steps:
(1) add water after getting Ramie Root, the root of large-flowered skullcap, the root of kudzu vine pulverizing boiling pulping, adds nano silver fibre agitation grinding 20-30 minute, send in defibrator and be processed into modified composite fiber;
(2) polyoxyethylene glycol is added to the water stirring, add barium sulfate, tapioca (flour), petroleum sodium sulfonate heated and stirred grinding 30-40 minute, spraying dry obtains modified barium sulphate;
(3) by Oleum Folium Artemisiae Argyi, epoxy linseed oil stirring and evenly mixing, ethylene two amine hydroxybenzene, Vanillin, modified barium sulphate supersound process 20-40 minute is added;
(4) xylon, wheat straw fiber, aluminum silicate fiber, modified composite fiber are put into pulverizing mill and worn into 80-100 order powder, putting into high mixer after drying mixes to 80-90 DEG C, add step (3) reaction product and remaining component is mixed to 100-120 DEG C, leave standstill supersound process 10-15 minute after 15-20 hour, wash, filter, dry to constant weight and get final product.
The present invention has following beneficial effect: the present invention will add in raw material after X-ray screener barium sulfate modified column, add again the obtained xylon such as nano silver fibre, wheat straw fiber, aluminum silicate fiber, Ramie Root, the root of large-flowered skullcap to have X-ray radiation protection persistence good and have good mechanical property simultaneously, textile processibility is good, clothes and the Non-Woven Fabric Industry of the staff making Long Term Contact X-ray can be widely used in, and rational technology, simple, be applicable to suitability for industrialized production.
Embodiment
The xylon of described a kind of X-ray radiation protection, it is characterized in that, be made up of the raw material of following weight part: xylon 43, nano silver fibre 1.8, wheat straw fiber 17, aluminum silicate fiber 8, tapioca (flour) 1, zinc borate 0.3, barium sulfate 4.7, polyoxyethylene glycol 0.4, Oleum Folium Artemisiae Argyi 2.8, epoxy linseed oil 3.1, ethylene two amine hydroxybenzene 2, Vanillin 0.5, petroleum sodium sulfonate 0.2, Ramie Root 15, the root of large-flowered skullcap 1, the root of kudzu vine 2, auxiliary agent 5, suitable quantity of water.
Described auxiliary agent is made up of following raw materials in part by weight: tealeaves fiber 12, nano zine oxide 2, silicon powder 1, dual polyethylene polydimethylsiloxane 0.05, glyceryl monostearate 1.9, polyoxyethylene glycol 4, methylisothiazolinone 2.8, Oleum Pelargonii Graveolentis 4.5, Flos Pelargonii Hortori 0.3, linolic acid 1.9, Dyhard RU 100 0.1, ethyl acrylate 4, fire retardant CP 0.07, its preparation method be first by nano zine oxide ultrasonic disperse in polyoxyethylene glycol, add tealeaves blending in of fibers and stir 5-8 hour, take out drying and grinding 10-15 minute, obtained modification tealeaves fiber, then by Oleum Pelargonii Graveolentis, Flos Pelargonii Hortori adds water stirring, and add silicon powder and stir 30-40 minute, spraying dry obtains modified silicon micro mist, finally by ethyl acrylate, linolic acid, Dyhard RU 100, methylisothiazolinone stirring and evenly mixing, adds above-mentioned obtained modification tealeaves fiber and modified silicon micro mist, glyceryl monostearate, dual polyethylene polydimethylsiloxane, fire retardant CP supersound process 30-40 minute and get final product.
Making method comprises the following steps:
(1) add water after getting Ramie Root, the root of large-flowered skullcap, the root of kudzu vine pulverizing boiling pulping, adds nano silver fibre agitation grinding 20-30 minute, send in defibrator and be processed into modified composite fiber;
(2) polyoxyethylene glycol is added to the water stirring, add barium sulfate, tapioca (flour), petroleum sodium sulfonate heated and stirred grinding 30-40 minute, spraying dry obtains modified barium sulphate;
(3) by Oleum Folium Artemisiae Argyi, epoxy linseed oil stirring and evenly mixing, ethylene two amine hydroxybenzene, Vanillin, modified barium sulphate supersound process 20-40 minute is added;
(4) xylon, wheat straw fiber, aluminum silicate fiber, modified composite fiber are put into pulverizing mill and worn into 80-100 order powder, putting into high mixer after drying mixes to 80-90 DEG C, add step (3) reaction product and remaining component is mixed to 100-120 DEG C, leave standstill supersound process 10-15 minute after 15-20 hour, wash, filter, dry to constant weight and get final product.
The technical parameter index of the xylon using the present invention to produce is as follows:
(1) soft, fluffy smooth flexible, intensity is high;
(2) oxygen index (OI): 28.9%, flame retardant effect is excellent;
(3) bacteriostasis rate of finished product to intestinal bacteria, streptococcus aureus, Candida albicans is all greater than 99.6%.
Claims (2)
1. the xylon of an X-ray radiation protection, it is characterized in that, be made up of the raw material of following weight part: xylon 40-45, nano silver fibre 1.1-2.1, wheat straw fiber 16-18, aluminum silicate fiber 8-10, tapioca (flour) 1-2, zinc borate 0.3-0.6, barium sulfate 4.3-6.5, polyoxyethylene glycol 0.4-0.6, Oleum Folium Artemisiae Argyi 2.1-3.2, epoxy linseed oil 2.1-4.2, ethylene two amine hydroxybenzene 2-5, Vanillin 0.3-0.6, petroleum sodium sulfonate 0.2-0.4, Ramie Root 13-16, root of large-flowered skullcap 1-3, root of kudzu vine 2-4, auxiliary agent 3-5, suitable quantity of water, described auxiliary agent is made up of following raw materials in part by weight: tealeaves fiber 10-13, nano zine oxide 2-4, silicon powder 1-3, dual polyethylene polydimethylsiloxane 0.03-0.05, glyceryl monostearate 1.2-3.1, polyoxyethylene glycol 3-6, methylisothiazolinone 2.1-3.6, Oleum Pelargonii Graveolentis 3.2-4.7, Flos Pelargonii Hortori 0.2-0.4, linolic acid 1.3-2.4, Dyhard RU 100 0.1-0.2, ethyl acrylate 4-7, fire retardant CP 0.04-0.07, its preparation method be first by nano zine oxide ultrasonic disperse in polyoxyethylene glycol, add tealeaves blending in of fibers and stir 5-8 hour, take out drying and grinding 10-15 minute, obtained modification tealeaves fiber, then by Oleum Pelargonii Graveolentis, Flos Pelargonii Hortori adds water stirring, and add silicon powder and stir 30-40 minute, spraying dry obtains modified silicon micro mist, finally by ethyl acrylate, linolic acid, Dyhard RU 100, methylisothiazolinone stirring and evenly mixing, adds above-mentioned obtained modification tealeaves fiber and modified silicon micro mist, glyceryl monostearate, dual polyethylene polydimethylsiloxane, fire retardant CP supersound process 30-40 minute and get final product.
2. the making method of the xylon of a kind of X-ray radiation protection according to claim 1, is characterized in that comprising the following steps:
(1) add water after getting Ramie Root, the root of large-flowered skullcap, the root of kudzu vine pulverizing boiling pulping, adds nano silver fibre agitation grinding 20-30 minute, send in defibrator and be processed into modified composite fiber;
(2) polyoxyethylene glycol is added to the water stirring, add barium sulfate, tapioca (flour), petroleum sodium sulfonate heated and stirred grinding 30-40 minute, spraying dry obtains modified barium sulphate;
(3) by Oleum Folium Artemisiae Argyi, epoxy linseed oil stirring and evenly mixing, ethylene two amine hydroxybenzene, Vanillin, modified barium sulphate supersound process 20-40 minute is added;
(4) xylon, wheat straw fiber, aluminum silicate fiber, modified composite fiber are put into pulverizing mill and worn into 80-100 order powder, putting into high mixer after drying mixes to 80-90 DEG C, add step (3) reaction product and remaining component is mixed to 100-120 DEG C, leave standstill supersound process 10-15 minute after 15-20 hour, wash, filter, dry to constant weight and get final product.
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| CN201410454663.0A CN104292868A (en) | 2014-09-09 | 2014-09-09 | X-ray radiation resistant wood fiber and preparation method thereof |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106633977A (en) * | 2016-11-23 | 2017-05-10 | 浙江农林大学 | Nanometer matter/biomass fibrous composite and preparation method for nanometer matter/biomass fibrous composite |
| CN106676750A (en) * | 2016-12-30 | 2017-05-17 | 浙江繁盛超纤制品有限公司 | Civil environment-friendly flame-retardant wood-fiber non-woven fabric and preparing method thereof |
| CN106738202A (en) * | 2016-12-12 | 2017-05-31 | 浙江嘉华晶体纤维有限公司 | A kind of manufacturing process of fiber profiled piece |
| CN107584838A (en) * | 2017-10-08 | 2018-01-16 | 咸阳非金属矿研究设计院有限公司 | A kind of barite medical protective garment material and preparation method thereof |
| CN109381514A (en) * | 2017-08-04 | 2019-02-26 | 中国辐射防护研究院 | A kind of Baical Skullcap root P.E and combinations thereof and purposes for radiation injury protection |
| CN112853741A (en) * | 2021-01-27 | 2021-05-28 | 东北大学 | Method for producing X-ray shielding material and X-ray shielding material |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101386185A (en) * | 2007-09-13 | 2009-03-18 | 上海国成塑料有限公司 | Treatment method of wood fiber for wood plastic composite material |
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2014
- 2014-09-09 CN CN201410454663.0A patent/CN104292868A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101386185A (en) * | 2007-09-13 | 2009-03-18 | 上海国成塑料有限公司 | Treatment method of wood fiber for wood plastic composite material |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106633977A (en) * | 2016-11-23 | 2017-05-10 | 浙江农林大学 | Nanometer matter/biomass fibrous composite and preparation method for nanometer matter/biomass fibrous composite |
| CN106738202A (en) * | 2016-12-12 | 2017-05-31 | 浙江嘉华晶体纤维有限公司 | A kind of manufacturing process of fiber profiled piece |
| CN106676750A (en) * | 2016-12-30 | 2017-05-17 | 浙江繁盛超纤制品有限公司 | Civil environment-friendly flame-retardant wood-fiber non-woven fabric and preparing method thereof |
| CN106676750B (en) * | 2016-12-30 | 2019-01-18 | 浙江繁盛超纤制品有限公司 | A kind of fire-retardant wood fiber non-woven fabric of civil environment-friendlycotton and preparation method thereof |
| CN109381514A (en) * | 2017-08-04 | 2019-02-26 | 中国辐射防护研究院 | A kind of Baical Skullcap root P.E and combinations thereof and purposes for radiation injury protection |
| CN109381514B (en) * | 2017-08-04 | 2023-01-17 | 中国辐射防护研究院 | Scutellaria baicalensis extract, composition thereof and application of scutellaria baicalensis extract in radiation injury protection |
| CN107584838A (en) * | 2017-10-08 | 2018-01-16 | 咸阳非金属矿研究设计院有限公司 | A kind of barite medical protective garment material and preparation method thereof |
| CN114506127A (en) * | 2017-10-08 | 2022-05-17 | 湖南楚天钡业有限公司 | Barite medical protective clothing material and preparation method thereof |
| CN112853741A (en) * | 2021-01-27 | 2021-05-28 | 东北大学 | Method for producing X-ray shielding material and X-ray shielding material |
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Application publication date: 20150121 |