CN104356805A - Anti-static thermal insulation water-based paint and preparation method thereof - Google Patents
Anti-static thermal insulation water-based paint and preparation method thereof Download PDFInfo
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- CN104356805A CN104356805A CN201410590613.5A CN201410590613A CN104356805A CN 104356805 A CN104356805 A CN 104356805A CN 201410590613 A CN201410590613 A CN 201410590613A CN 104356805 A CN104356805 A CN 104356805A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/14—Paints containing biocides, e.g. fungicides, insecticides or pesticides
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/24—Electrically-conducting paints
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
- C09D7/62—Additives non-macromolecular inorganic modified by treatment with other compounds
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
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Abstract
The invention discloses an anti-static thermal insulation water-based paint which is characterized by being prepared from the following raw materials in parts by weight: 30-40 parts of acrylic resin emulsion, 2-3 parts of tourmaline powder, 25-35 parts of water-based aluminum paste, 1-2 parts of calcium bentonite, 2-3 parts of glass wool, 1-2 parts of polycarboxylate ammonium salt dispersing agents, 1-2 parts of octyl tin mercaptide, 3-5 parts of ethyl alcohol, 2-3 parts of triethanolamine, 2-3 parts of nano antimony tin oxide, 1-3 parts of 5-chlorine-2-methyl-4-isothiazolin-3-ketone, 1-5 parts of polypropylene staple fibers, 2-3 parts of nano-copper powder, 0.3-0.5 part of tetraethylene glycol monolaurate, 0.5-1.0 part of calcined kaolin, 1-2 parts of dioctyl phthalate, 7-9 parts of thermal insulation sizing agents and 14-20 parts of deionized water. The water-based paint is low in VOC value, does not contain the organic solvents such as heavy metal and benzene, has a plurality of functions of thermal insulation, sterilization, mould prevention, algae prevention, anti-static function and aging resistance, has high weather fastness and adhesive force, and is wide in application range, green, environment-friendly and excellent in performance.
Description
Technical field
The present invention relates to a kind of coating and preparation method thereof, particularly a kind of anti-static heat-insulating water-borne coatings and preparation method thereof.
Background technology
Coating is applied to body surface can be formed and have protection, the class I liquid I of solid-state film of decoration or property (as insulation, anticorrosion, mark etc.) or the general name of solid material.The application of coating starts from prehistoric, and even to this day, paint field is also in development.Look around, coating is ubiquitous, its functional and ornamental leap various fields.Every coating using water as solvent or make dispersion medium, all can be described as water-borne coatings.Water-borne coatings comprises water soluble paint, water-reducible coatings, water-dispersible paint three kinds, compared with traditional solvent based coating, water-borne coatings has that price is low, use safety, saving resource and the energy, reduce the advantage such as environmental pollution and public hazards, because becoming the Main way of current development coatings industry.
What thermal insulating coating referred to grow up in recent years a kind ofly have heat insulation, sun-proof, energy-saving and environmental protection, construction is simple and easy, the duration is short, the functional coating of instant effect.Thermal insulating coating mainly contains three kinds from the classification of characteristic principle, isolated conduction type thermal insulating coating, reflection type thermal insulation coating and Radiation Heat-insulated Paint.Wherein isolation-type thermal insulating coating can prevent outdoor heat from entering indoor with heat exchange pattern.Most widely used is compound silicate insulating paint, thermofin poor effect is smeared for skin inside holding and indoor canopy, the coating of compound silicate insulating paint very easily absorbs water, and water-intake rate is high, moisture evaporation slow, just loses heat-blocking action once water suction.Radiation Heat-insulated Paint be by thermal radiation by the heat radiation in buildings to aerial, buildings temperature is reduced.Reflection type thermal insulation coating, directly reflexes to aerial by sun power, instead of first absorption, rear transmitting, should be more effective to the cooling of buildings.The present invention is directed to this situation, adopt and there is the material of effect of heat insulation and material of construction by a series of reaction bonded, there is excellent effect of heat insulation, and solve the quartz sand mine tailing piling and abandon to the harm of environment.
Summary of the invention
The object of this invention is to provide a kind of anti-static heat-insulating water-borne coatings and preparation method thereof.
In order to realize object of the present invention, the present invention is by following scheme implementation:
A kind of anti-static heat-insulating water-borne coatings, be made up of the raw material of following weight part: Emulsion acrylic resin 30-40, tourmaline powder 2-3, water aluminum-silver slurry 25-35, calcium-base bentonite 1-2, glass wool 2-3, poly carboxylic acid ammonium salt dispersion agent 1-2, octyl mercaptan tin 1-2, ethanol 3-5, trolamine 2-3, nano antimony tin oxide 2-3, CMIT 1-3, polypropene staple 1-5, copper nanoparticle 2-3, TEG mono-laurate defoamer 0.3-0.5, calcined kaolin 0.5-1.0, o-phthalic acid dibutyl ester 1-2, heat-insulating slurry 7-9, deionized water 14-20,
Described heat-insulating slurry is made up of the raw material of following weight part: nano ceramic fibers 5-7, aluminous cement 20-25, quartz sand mine tailing 20-25, wilkinite 3-5, pearlstone 6-8, polyvinyl alcohol 2-3, aluminum phosphate 4-5, rock wool fibers 5-7, silicon powder 2-4, polyoxyethylenated alcohol sodium sulfate 1-2, lauryl methacrylate(LMA) 12-15, Silane coupling agent KH550 1-2, ethanol 20-30, distilled water 30-40, preparation method is that lauryl methacrylate(LMA) is added in ethanol and fully dissolves by (1), add quartz sand mine tailing again, wilkinite, pearlstone and silicon powder carry out pre-dispersed in 0.3-0.6 hour to stir under 400-600 rev/min, add Silane coupling agent KH550 again to stir and to be added in sand mill that to carry out grinding to form slurry for subsequent use after 15-25 minute, (2) by nano ceramic fibers, rock wool fibers, polyoxyethylenated alcohol sodium sulfate and distilled water mix and blend, high speed shear pulp body, (3) step (1) product is mixed with step (2) product, add all the other remaining components, stir 2-3 hour with the speed of 300-500 rev/min and get final product.
A kind of anti-static heat-insulating water-borne coatings of the present invention, be made up of following concrete steps:
(1) under the rotating speed of 1000-2000 rev/min, disperse 20-30 minute to obtain the material of fineness at 20-30um deionized water, calcium-base bentonite, tourmaline powder, glass wool, nano antimony tin oxide, copper nanoparticle, calcined kaolin, then add poly carboxylic acid ammonium salt dispersion agent and heat-insulating slurry continuation stirring 20-30 minute;
(2) Emulsion acrylic resin, water aluminum-silver slurry, o-phthalic acid dibutyl ester are added to mixing and stirring in Scattered Kettle and are heated to 60-80 ° of C, then the slurry added in step (1) and trolamine are to continue under the rotating speed of 300-500 rev/min to stir 30-50 minute;
(3) in the reaction system of step (2), add all the other surplus materialss, be added to grinding distribution in sand mill after stirring even, filter and package.
Advantage of the present invention is: water-borne coatings VOC value of the present invention is low, not containing the organic solvent such as heavy metal and benzene, there is heat insulation, sterilization, the anti-algae of mildew-resistant, the multiple effect such as antistatic, ageing-resistant, and there is high weathering resistance and sticking power, coating use range of the present invention is wide, is a kind of environmental protection and excellent performance water-borne coatings.
specific embodiments
Below by specific examples, the present invention is described in detail.
A kind of anti-static heat-insulating water-borne coatings, is made up of the raw material of following weight part (kilogram): Emulsion acrylic resin 36, tourmaline powder 3, water aluminum-silver slurry 31, calcium-base bentonite 2, glass wool 2, poly carboxylic acid ammonium salt dispersion agent 1, octyl mercaptan tin 2, ethanol 4, trolamine 3, nano antimony tin oxide 2, CMIT 2, polypropene staple 3, copper nanoparticle 2, TEG mono-laurate defoamer 0.4, calcined kaolin 0.7, o-phthalic acid dibutyl ester 2, heat-insulating slurry 8, deionized water 17;
Described heat-insulating slurry is made up of the raw material of following weight part (kilogram): nano ceramic fibers 6, aluminous cement 24, quartz sand mine tailing 23, wilkinite 4, pearlstone 7, polyvinyl alcohol 3, aluminum phosphate 4, rock wool fibers 6, silicon powder 3, polyoxyethylenated alcohol sodium sulfate 1, lauryl methacrylate(LMA) 13, Silane coupling agent KH550 1.3, ethanol 26, distilled water 35, preparation method is that lauryl methacrylate(LMA) is added in ethanol and fully dissolves by (1), add quartz sand mine tailing again, wilkinite, pearlstone and silicon powder carry out pre-dispersed in 0.3-0.6 hour to stir under 400-600 rev/min, add Silane coupling agent KH550 again to stir and to be added in sand mill that to carry out grinding to form slurry for subsequent use after 15-25 minute, (2) by nano ceramic fibers, rock wool fibers, polyoxyethylenated alcohol sodium sulfate and distilled water mix and blend, high speed shear pulp body, (3) step (1) product is mixed with step (2) product, add all the other remaining components, stir 2-3 hour with the speed of 300-500 rev/min and get final product.
A kind of anti-static heat-insulating water-borne coatings of the present invention, be made up of following concrete steps:
(1) under the rotating speed of 1000-2000 rev/min, disperse 20-30 minute to obtain the material of fineness at 20-30um deionized water, calcium-base bentonite, tourmaline powder, glass wool, nano antimony tin oxide, copper nanoparticle, calcined kaolin, then add poly carboxylic acid ammonium salt dispersion agent and heat-insulating slurry continuation stirring 20-30 minute;
(2) Emulsion acrylic resin, water aluminum-silver slurry, o-phthalic acid dibutyl ester are added to mixing and stirring in Scattered Kettle and are heated to 60-80 ° of C, then the slurry added in step (1) and trolamine are to continue under the rotating speed of 300-500 rev/min to stir 30-50 minute;
(3) in the reaction system of step (2), add all the other surplus materialss, be added to grinding distribution in sand mill after stirring even, filter and package.
Coating appearance of the present invention is normal, without precipitation, without caking, water tolerance experiment (160H): without exception, alkaline resistance test (48H): without exception, abrasion resistance is tested: pass through for 10000 times, film is without breakage, artificial ageing resistance is tested: 2000 hours non-foaming, do not peel off, flawless, chalk rating≤1 grade, variable color grade≤1 grade, contamination resistance experiment (5 circulations)≤30%, heat insulation temperature difference experiment >=8 ° of C.
Claims (2)
1. an anti-static heat-insulating water-borne coatings, it is characterized in that, be made up of the raw material of following weight part: Emulsion acrylic resin 30-40, tourmaline powder 2-3, water aluminum-silver slurry 25-35, calcium-base bentonite 1-2, glass wool 2-3, poly carboxylic acid ammonium salt dispersion agent 1-2, octyl mercaptan tin 1-2, ethanol 3-5, trolamine 2-3, nano antimony tin oxide 2-3, CMIT 1-3, polypropene staple 1-5, copper nanoparticle 2-3, TEG mono-laurate defoamer 0.3-0.5, calcined kaolin 0.5-1.0, o-phthalic acid dibutyl ester 1-2, heat-insulating slurry 7-9, deionized water 14-20,
Described heat-insulating slurry is made up of the raw material of following weight part: nano ceramic fibers 5-7, aluminous cement 20-25, quartz sand mine tailing 20-25, wilkinite 3-5, pearlstone 6-8, polyvinyl alcohol 2-3, aluminum phosphate 4-5, rock wool fibers 5-7, silicon powder 2-4, polyoxyethylenated alcohol sodium sulfate 1-2, lauryl methacrylate(LMA) 12-15, Silane coupling agent KH550 1-2, ethanol 20-30, distilled water 30-40, preparation method is that lauryl methacrylate(LMA) is added in ethanol and fully dissolves by (1), add quartz sand mine tailing again, wilkinite, pearlstone and silicon powder carry out pre-dispersed in 0.3-0.6 hour to stir under 400-600 rev/min, add Silane coupling agent KH550 again to stir and to be added in sand mill that to carry out grinding to form slurry for subsequent use after 15-25 minute, (2) by nano ceramic fibers, rock wool fibers, polyoxyethylenated alcohol sodium sulfate and distilled water mix and blend, high speed shear pulp body, (3) step (1) product is mixed with step (2) product, add all the other remaining components, stir 2-3 hour with the speed of 300-500 rev/min and get final product.
2. a kind of anti-static heat-insulating water-borne coatings according to claim 1, is characterized in that, be made up of following concrete steps:
(1) under the rotating speed of 1000-2000 rev/min, disperse 20-30 minute to obtain the material of fineness at 20-30um deionized water, calcium-base bentonite, tourmaline powder, glass wool, nano antimony tin oxide, copper nanoparticle, calcined kaolin, then add poly carboxylic acid ammonium salt dispersion agent and heat-insulating slurry continuation stirring 20-30 minute;
(2) Emulsion acrylic resin, water aluminum-silver slurry, o-phthalic acid dibutyl ester are added to mixing and stirring in Scattered Kettle and are heated to 60-80 ° of C, then the slurry added in step (1) and trolamine are to continue under the rotating speed of 300-500 rev/min to stir 30-50 minute;
(3) in the reaction system of step (2), add all the other surplus materialss, be added to grinding distribution in sand mill after stirring even, filter and package.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201410590613.5A CN104356805A (en) | 2014-10-29 | 2014-10-29 | Anti-static thermal insulation water-based paint and preparation method thereof |
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| CN201410590613.5A CN104356805A (en) | 2014-10-29 | 2014-10-29 | Anti-static thermal insulation water-based paint and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104893486A (en) * | 2015-05-21 | 2015-09-09 | 芜湖蒲草电子商务有限公司 | Antistatic and heat-resistant coating for corrugated carton and preparation method of antistatic and heat-resistant coating |
| CN104909612A (en) * | 2015-06-09 | 2015-09-16 | 苏州云舒新材料科技有限公司 | Novel thermal-insulation heat-shielding composite material and preparation method thereof |
| CN109322214A (en) * | 2018-09-29 | 2019-02-12 | 漳州市天辰纸品包装有限公司 | A kind of dedicated corrugated paper of weatherable medicine |
| WO2022149105A1 (en) * | 2021-01-11 | 2022-07-14 | Pintureria Panoramica Limitada | Biocidal paint |
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| CN103396713A (en) * | 2013-08-11 | 2013-11-20 | 深圳市文浩建材科技有限公司 | Semi-transparent aqueous heat insulation coating and preparation method thereof |
| CN103937350A (en) * | 2014-04-16 | 2014-07-23 | 常州大学 | Graphene-rod-like aluminum-doped zinc oxide antistatic coating and preparation method thereof |
| JP2015220233A (en) * | 2014-05-13 | 2015-12-07 | ｎ−ｔｅｃｈ株式会社 | Electromagnetic wave shielding coating and electromagnetic wave shielding article |
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2014
- 2014-10-29 CN CN201410590613.5A patent/CN104356805A/en active Pending
Patent Citations (5)
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| CN1865367A (en) * | 2005-05-17 | 2006-11-22 | 上海市建筑科学研究院有限公司 | Aqueous light color nanometer static-conductive coating for inner wall and its production method |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104893486A (en) * | 2015-05-21 | 2015-09-09 | 芜湖蒲草电子商务有限公司 | Antistatic and heat-resistant coating for corrugated carton and preparation method of antistatic and heat-resistant coating |
| CN104909612A (en) * | 2015-06-09 | 2015-09-16 | 苏州云舒新材料科技有限公司 | Novel thermal-insulation heat-shielding composite material and preparation method thereof |
| CN104909612B (en) * | 2015-06-09 | 2017-03-29 | 李建尧 | A kind of heat-insulating composite material and preparation method thereof |
| CN109322214A (en) * | 2018-09-29 | 2019-02-12 | 漳州市天辰纸品包装有限公司 | A kind of dedicated corrugated paper of weatherable medicine |
| WO2022149105A1 (en) * | 2021-01-11 | 2022-07-14 | Pintureria Panoramica Limitada | Biocidal paint |
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