CN102533082A - Aqueous environment-friendly anti-aging floor coating and preparation method thereof - Google Patents
Aqueous environment-friendly anti-aging floor coating and preparation method thereof Download PDFInfo
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- CN102533082A CN102533082A CN2011104579946A CN201110457994A CN102533082A CN 102533082 A CN102533082 A CN 102533082A CN 2011104579946 A CN2011104579946 A CN 2011104579946A CN 201110457994 A CN201110457994 A CN 201110457994A CN 102533082 A CN102533082 A CN 102533082A
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Abstract
The invention provides an aqueous environment-friendly anti-aging floor coating and a preparation method of the floor coating. The floor coating comprises components A and B in weight ratio of 4:1, wherein the component A comprises water, modified polyalcohol emulsion, wetting agent, dispersing agent, thickening agent, defoaming agent, flatting agent, filler and anti-settling agent and the component B comprises aqueous curing agent and drier. The preparation method of the invention comprises the steps of putting water, the thickening agent, the wetting agent, the dispersing agent, the defoaming agent and the filler in a dispersing vat to disperse at a high speed, adding the emulsion, a color paste, the anti-settling agent, an ultraviolet absorbent and the flatting agent, uniformly mixing and packaging to obtain the component A; and putting the aqueous curing agent and the drier in the dispersing vat to disperse for 10-20min, uniformly mixing and packaging to obtain the component B. The floor coating of the invention has the advantages of environmental friendliness, soft gloss, wear and shock resistance, simpleness and convenience for construction, ultraviolet and aging resistance, long service life and suitability of being used indoors and outdoors.
Description
Technical field
The present invention relates to a kind of terrace paint, ageing-resistant terrace paint of a kind of specifically aqueous, environmental protective and preparation method thereof.
Technical background
Terrace is a kind of building materials that get into China in recent years, is mainly used in to lay ground.Terrace be applicable to some for health conditions requiring than higher place with require anti-impact to press the anticorrosive underground parking of looking like attrition resistantly, factory's storehouse (cross fork truck) etc.
Be used for floor coating at present and mostly be oily material and bi-component aqueous epoxy coating, the oiliness terrace paint contains the benzene series diluting solvent mostly, has toxicity, can cause very big pollution to environment, also can threaten the healthy of the mankind, does not meet environmental requirement; But the raising of Along with people's environmental consciousness, coating all develop in the hydrotropismsization direction, and existing bi-component aqueous epoxy coating surface scratch resistance is poor, and ageing-resistant performance is bad, and work-ing life is short.
Summary of the invention
The invention provides ageing-resistant terrace paint of a kind of aqueous, environmental protective and method thereof; All starting material all reach the environmental requirement of national interior decoration standard among the present invention; Adopt mica powder of wet process to improve its ageing-resistant performance at surface side filler; The adding of UV light absorber can make it when outdoor environment is used, improve the anti-ultraviolet property of filming, and surface luster is soft, wear resistance is good, the ageing-resistant long service life of Ginkgo Biloba Leaf Extract.
The ageing-resistant terrace paint of a kind of aqueous, environmental protective comprises A, B component, it is characterized in that the composition of each component and weight percent are following:
The A component
The B component
Waterborne curing agent 90%-99%
Siccative 1%-10%
Said A, B component proportioning are 4: 1
Wherein: emulsion be in uncle's acrylic emulsion (like reaching of treasured PD-9A), pure-acrylic emulsion (like the rich RS-986D of Ahmedabad), the hydroxyl functional water-borne acrylic resin (like Bayer 2457) any one; Pure-acrylic emulsion is the pure acrylic acid ester copolymer, belongs to the anionic emulsion, and particle diameter is small, is applicable to multiple formulation for coating material, has good pollution resistance, alkali resistance, wear resistance, photostabilization and weathering resistance, and good adhesive is arranged; Water-borne acrylic resin is compared with traditional solvent based coating, and it is low, safe in utilization that water-borne coatings has price, saves the resource and the energy, reduces advantages such as environmental pollution and public hazards;
Wetting agent is ROHM sodium water solution or the aqueous copolymers solution that contains high pigment affinity groups (TEGO Dispers752w);
Dispersion agent is modified soybean Yelkin TTS (like the LIPOTIN A modified soybean Yelkin TTS of EVONIK company) or ROHM amine salt;
Thickening material is non-ionic polyurethane polymkeric substance (like TEGO ViscoPlus3030) or modified urea solution (like German Bi Ke BYK420);
Skimmer is polyether siloxane copolymer emulsion (like the Foamex805 of TEGO company) or aqueous emulsion of dimethyl polysiloxane fluid (like the Foamex 835 of TEGO company production);
Flow agent is modified polyorganosiloxane (like moral modest (Deuchem) the Shanghai chemistry Levaslip W-455 of ltd) or Yodo Sol GH 28 solution (like the BYK-394 of German Bi Ke);
Anti-settling agent is aerosil (like the R972 of goldschmidt chemical corporation) or organobentonite;
UV light absorber is UVNUL MS-40 or salicylic acid phenyl ester;
Waterborne curing agent is Bayer HDI (six methylene diisocyanates) or isophorone diisocyanate;
Said water is deionized water.
Said filler is a mica powder of wet process, or the mixture of mica powder of wet process and process white or silicon powder; Said mill base is no resin waterborne general color paste, like the H3G 100-CN of Clariant company, the M8810 of Suzhou Sunmun Technology Co., Ltd..
Said siccative is stannous octoate or zinc octoate.
The preparation method of the ageing-resistant terrace paint of a kind of aqueous, environmental protective is characterized in that:
A component: disperse cylinder to add whole thickening materials in the formula ratio while stirring the whole water inputs in the above A component formula amount earlier with 300-500 rev/min; Add wetting agent, dispersion agent, skimmer, filler then; With after 1000-1500 rev/min of high speed dispersion 20-30 minute, drop into emulsion, mill base in regular turn, anti-settling agent, UV light absorber, flow agent again; Stir packing;
B component: disperse cylinder to pack after 10-20 minute whole waterborne curing agents in the above B component formula amount and siccative input with 800-1000 rev/min speed dispersion;
Before the construction, weigh at 4: 1, pour the A that weighs up, B group material into the spice bucket, stir 5-10 minute until evenly just can with whisking appliance according to A, B component weight ratio.
Each item performance index of the present invention have have all met or exceeded the oiliness system and the bi-component waterborne system terrace lacquer of existing market, and the pencil hardness of the ageing-resistant terrace paint of aqueous, environmental protective has reached 3H; Sticking power≤1; Shock-resistant kg.cm (1 grade) II level; Wear resistance/(750g/500r)≤0.029; Ultimate compression strength>=70; Bending strength>=7.0; Anti-skid (k29-5673 standard)>=7.6.
Beneficial effect of the present invention:
1. the present invention adopts the modified polyalcohol emulsion with good pollution resistance, alkali resistance, wear resistance, photostabilization and weathering resistance, uses that whole coating surface gloss is soft, wear resistance good, ageing-resistant long service life;
2. the present invention increases UV light absorber, and extraordinary anti-ultraviolet property is arranged;
Filler be mica powder of wet process or mica powder of wet process and process white, silicon powder any one or a few, mica powder of wet process has the aging-resistant function, can improve the ageing-resistant performance of filming, and the life-span of filming is improved greatly;
4. the present invention is a kind of aqueous double-component modified polyurethane material, promptly can be used for indoorly also can being used for outdoor floor material;
5. the present invention is when temperature 25 is spent, and 3 hours surface dryings were done solid work in 12 hours, and its rate of drying is fast.
Ultimate compression strength of the present invention, shock resistance are good; Surface luster is soft; Anti-ultraviolet property is outstanding, ageing-resistant long service life; It is simple and convenient to construct, and all starting material compliance with environmental protection requirements all.
Embodiment
Below in conjunction with embodiment the present invention is further specified.
Embodiment one: the ageing-resistant terrace paint of said aqueous, environmental protective, comprise A, B component, and the composition and the weight percent of each component are following:
The A component
The B component
Bayer HDI 90%
Stannous octoate 10%
A kind of method for preparing the ageing-resistant terrace paint of above aqueous, environmental protective is characterized in that:
A component: earlier disperse cylinder to add 1% nonionic polyurethane polymkeric substance (TEGO 3030) simultaneously with 300-500 rev/min of stirring 10% deionized water input in the above A set of dispense; Add 2% ROHM sodium water solution, 1.6% modified soybean Yelkin TTS (the LIPOTIN A of EVONIK company), 1.4% polyether siloxane copolymer emulsion (Foamex of TEGO company 805), 5% mica powder of wet process (Shijiazhuang star Hai Gaoke non-metallic material ltd), 5% SILICA FUME (Huzhou Jing Yuan quartz ware factory) then; Again with after 1000-1500 rev/min of high speed dispersion 20-30 minute; Drop into uncle's acrylic emulsion (treasured reaches chemical industry PD-9A) of 60.4%, 9% mill base (the H3G 100-CN of Clariant company), 2% fumed silica (R972 of goldschmidt chemical corporation), 0.5% UVNUL MS-40,2.1% modified polyorganosiloxane (the modest Deuchem of the moral Shanghai chemistry Levaslip W-455 of ltd) successively; Stir packing;
B component: disperse cylinder to pack after 10-20 minute 90% Bayer HDI and 10% stannous octoate input in the above B component compositing formula amount with 800-1000 rev/min speed dispersion;
Before the construction, weigh at 4: 1, pour the A that weighs up, B group material into the spice bucket, stir 5-10 minute until evenly just can with whisking appliance according to A, B component weight ratio.
Embodiment two: the ageing-resistant terrace paint of said aqueous, environmental protective, comprise A, B component, and the composition and the weight percent of each component are following:
The A component
The B component
Isophorone diisocyanate 95%
Stannous octoate 5%
A kind of method for preparing the ageing-resistant terrace paint of above aqueous, environmental protective is characterized in that:
A component: earlier disperse cylinder to add 0.2% modified urea solution (BYK420) simultaneously with 300-500 rev/min of stirring 15% deionized water input in the above A set of dispense; Add 0.5% ROHM sodium water solution, 0.5% modified soybean Yelkin TTS (LIPOTINA of EVONIK company), 0.3% aqueous emulsion of dimethyl polysiloxane fluid (Foamex of TEGO company 835), 25% mica powder of wet process (Shijiazhuang star Hai Gaoke non-metallic material Ltd), 5% process white (Jinan Venus permanent white sand source mill) then; Again with after 1000-1500 rev/min of high speed dispersion 20-30 minute; Drop into 42.3% pure-acrylic emulsion, 10% mill base (the H3G 100-CN of Clariant company), 0.6% organobentonite (Xinyang Boulder mining industry), 0.1% UVNUL MS-40,2.1% modified polyorganosiloxane (the modest Deuchem of the moral Shanghai chemistry Levaslip W-455 of ltd); Stir packing;
B component: disperse cylinder to pack after 10-20 minute 95% isophorone diisocyanate and 5% stannous octoate input in the above B component compositing formula amount with 800-1000 rev/min speed dispersion;
Before the construction, weigh at 4: 1, pour the A that weighs up, B group material into the spice bucket, stir 5-10 minute until evenly just can with whisking appliance according to A, B component weight ratio.
Embodiment three
The ageing-resistant terrace paint of said aqueous, environmental protective comprises A, B component, and the composition and the weight percent of each component are following:
The A component
The B component
Isophorone diisocyanate 97%
Zinc octoate 3%
A kind of method for preparing the ageing-resistant terrace paint of above aqueous, environmental protective is characterized in that:
A component: earlier disperse cylinder to add 0.6% nonionic polyurethane polymkeric substance (TEGO 3030) simultaneously with 300-500 rev/min of stirring 12% deionized water input in the above A set of dispense; Add 1.1% the aqueous copolymers solution that contains high pigment affinity groups (TEGO 752W), 0.8% ammonium polyacrylate salt, 0.8% polyether siloxane copolymer emulsion (Foamex805 of TEGO company), 20% mica powder of wet process (Shijiazhuang star Hai Gaoke non-metallic material Ltd) then; Again with after 1000-1500 rev/min of high speed dispersion 20-30 minute; Drop into 50.5% hydroxyl functional water-borne acrylic resin (Bayer 2457), 12.2% mill base (the generation name SM8810 of company), 1.2% fumed silica (R972 of goldschmidt chemical corporation), 0.3% salicylic acid phenyl ester, 0.5% Yodo Sol GH 28 solution (German Bi Ke BYK-394); Stir packing;
B component: disperse cylinder to disperse packing after 10-20 minute 97% isophorone diisocyanate in the above B component compositing formula amount and 3% zinc octoate input with 800-1000 rev/min speed;
Before the construction, weigh at 4: 1, pour the A that weighs up, B group material into the spice bucket, stir 5-10 minute until evenly with whisking appliance according to A, B component weight ratio, then directly on the ground of handling well with the cylinder roller coating or use the scraper blade coating.
The oiliness system that has has all met or exceeded existing market according to the ageing-resistant terrace paint each item of aqueous, environmental protective performance index of above embodiment preparation is coated with lacquer with bi-component waterborne system terrace, and the pencil hardness of the ageing-resistant terrace paint of aqueous, environmental protective has reached 3H; Sticking power≤1; Shock-resistant kg.cm (1 grade) II level; Wear resistance/(750g/500r)≤0.029; Ultimate compression strength>=70; Bending strength>=7.0; Anti-skid (k29-5673 standard)>=7.6.
Claims (5)
1. the ageing-resistant terrace paint of aqueous, environmental protective comprises A, B component, it is characterized in that the composition of each component and weight percent are following:
The A component
The B component
Waterborne curing agent 90%-99%
Siccative 1%-10%
Said A, B component proportioning are 4: 1
Wherein: emulsion be in uncle's acrylic emulsion, pure-acrylic emulsion, the hydroxyl functional water-borne acrylic resin any one;
Wetting agent is ROHM sodium water solution or the aqueous copolymers solution that contains high pigment affinity groups;
Dispersion agent is modified soybean Yelkin TTS or ROHM amine salt;
Thickening material is nonionic polyurethane polymkeric substance or German Bi Ke BYK420 modified urea solution;
Skimmer is polyether siloxane copolymer emulsion or aqueous emulsion of dimethyl polysiloxane fluid;
Flow agent is modified polyorganosiloxane or Yodo Sol GH 28 solution;
Anti-settling agent is fumed silica or organobentonite;
UV light absorber is UVNUL MS-40 or salicylic acid phenyl ester;
Waterborne curing agent is Bayer HDI or isophorone diisocyanate.
2. the ageing-resistant terrace paint of a kind of aqueous, environmental protective according to claim 1 is characterized in that: said water is deionized water.
3. the ageing-resistant terrace paint of a kind of aqueous, environmental protective according to claim 1 is characterized in that: said filler is a mica powder of wet process, or the mixture of mica powder of wet process and process white or silicon powder; Said mill base is no resin waterborne general color paste.
4. the ageing-resistant terrace paint of a kind of aqueous, environmental protective according to claim 1 is characterized in that: said siccative is stannous octoate or zinc octoate.
5. prepare the preparation method of the ageing-resistant terrace paint of the described aqueous, environmental protective of claim 1, it is characterized in that:
A component: disperse cylinder with 300-500 rev/min of stirring the whole water inputs in the A component formula amount in the claim 1 earlier; Add in the formula ratio all thickening materials while stirring, add wetting agent, dispersion agent, skimmer, filler then, again with after 1000-1500 rev/min of high speed dispersion 20-30 minute; Drop into emulsion, mill base in regular turn; Anti-settling agent, UV light absorber, flow agent stir, packing;
B component: disperse cylinder to pack after 10-20 minute whole waterborne curing agents in the B component formula amount in the claim 1 and siccative input with 800-1000 rev/min speed dispersion;
Before the construction, weigh at 4: 1, pour the A that weighs up, B group material into the spice bucket, stir 5-10 minute until evenly just can with whisking appliance according to A, B component weight ratio.
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Cited By (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102807813A (en) * | 2012-08-16 | 2012-12-05 | 广州立邦涂料有限公司 | Waterborne polyurethane floor paint |
| CN103320002A (en) * | 2013-06-28 | 2013-09-25 | 江苏海田技术有限公司 | Acrylic resin coating and preparation method thereof |
| CN105462445A (en) * | 2015-12-15 | 2016-04-06 | 沪宝新材料科技（上海）股份有限公司 | Water-borne floor paint capable of degrading formaldehyde |
| CN105860810A (en) * | 2016-06-22 | 2016-08-17 | 漳州鑫展旺化工有限公司 | High-performance environment-friendly sliding resistant coating |
| CN105885590A (en) * | 2016-06-20 | 2016-08-24 | 吴国强 | Novel acrylic heavy-load-tolerant floor paint |
| CN105907143A (en) * | 2016-06-20 | 2016-08-31 | 吴国强 | Novel acrylic acid anticorrosion floor paint |
| CN105969011A (en) * | 2016-06-20 | 2016-09-28 | 吴国强 | Novel wear-resistant acrylic floor paint |
| CN106433347A (en) * | 2016-09-21 | 2017-02-22 | 苏州瑞斯格电子科技有限公司 | High-wear-resistance nano crylic acid terrace paint |
| CN106433433A (en) * | 2016-09-21 | 2017-02-22 | 苏州瑞斯格电子科技有限公司 | Environmental-friendly colored nano polyurethane floor paint |
| CN107057526A (en) * | 2017-05-16 | 2017-08-18 | 枣阳市同邦达科技有限公司 | It is a kind of to be used for the material modified of cathode electrodip painting mill base, mill base and preparation method |
| CN107142020A (en) * | 2017-05-18 | 2017-09-08 | 福建华夏蓝新材料科技有限公司 | A kind of environment-friendly imitation stone texture artistic floors coating and preparation method thereof |
| CN107434381A (en) * | 2016-05-27 | 2017-12-05 | 立邦涂料（中国）有限公司 | A kind of extraordinary floor coatings aqueous polyurethane mortar composite coating and its preparation method and application |
| CN108047925A (en) * | 2017-12-13 | 2018-05-18 | 山东诺威体育产业有限公司 | Polyurethane gravity flow self-leveling floor material and preparation method thereof |
| CN109554109A (en) * | 2018-07-10 | 2019-04-02 | 成都虹润制漆有限公司 | A kind of aqueous thick-slurry type bi-component hybrid inorganic-organic self-leveling floor coating and preparation method thereof |
| CN109609010A (en) * | 2018-12-12 | 2019-04-12 | 厦门安必信新材料科技有限公司 | A kind of super abrasive aqueous polyurethane floor coatings and preparation method thereof |
| CN111647244A (en) * | 2020-04-13 | 2020-09-11 | 南京弘志教育装备科技有限公司 | Water-based acrylic acid runway surface material and preparation and application thereof |
| WO2022012015A1 (en) * | 2020-07-14 | 2022-01-20 | 上海保立佳新材料有限公司 | Single-component water-proof high-hardness water-based floor paint and preparation method therefor |
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| CN102807813A (en) * | 2012-08-16 | 2012-12-05 | 广州立邦涂料有限公司 | Waterborne polyurethane floor paint |
| CN103320002A (en) * | 2013-06-28 | 2013-09-25 | 江苏海田技术有限公司 | Acrylic resin coating and preparation method thereof |
| CN105462445A (en) * | 2015-12-15 | 2016-04-06 | 沪宝新材料科技（上海）股份有限公司 | Water-borne floor paint capable of degrading formaldehyde |
| CN107434381B (en) * | 2016-05-27 | 2021-01-05 | 立邦涂料（中国）有限公司 | Special floor coating waterborne polyurethane mortar composite coating and preparation method and application thereof |
| CN107434381A (en) * | 2016-05-27 | 2017-12-05 | 立邦涂料（中国）有限公司 | A kind of extraordinary floor coatings aqueous polyurethane mortar composite coating and its preparation method and application |
| CN105885590A (en) * | 2016-06-20 | 2016-08-24 | 吴国强 | Novel acrylic heavy-load-tolerant floor paint |
| CN105907143A (en) * | 2016-06-20 | 2016-08-31 | 吴国强 | Novel acrylic acid anticorrosion floor paint |
| CN105969011A (en) * | 2016-06-20 | 2016-09-28 | 吴国强 | Novel wear-resistant acrylic floor paint |
| CN105860810A (en) * | 2016-06-22 | 2016-08-17 | 漳州鑫展旺化工有限公司 | High-performance environment-friendly sliding resistant coating |
| CN106433347A (en) * | 2016-09-21 | 2017-02-22 | 苏州瑞斯格电子科技有限公司 | High-wear-resistance nano crylic acid terrace paint |
| CN106433433A (en) * | 2016-09-21 | 2017-02-22 | 苏州瑞斯格电子科技有限公司 | Environmental-friendly colored nano polyurethane floor paint |
| CN107057526A (en) * | 2017-05-16 | 2017-08-18 | 枣阳市同邦达科技有限公司 | It is a kind of to be used for the material modified of cathode electrodip painting mill base, mill base and preparation method |
| CN107142020A (en) * | 2017-05-18 | 2017-09-08 | 福建华夏蓝新材料科技有限公司 | A kind of environment-friendly imitation stone texture artistic floors coating and preparation method thereof |
| CN108047925B (en) * | 2017-12-13 | 2021-01-01 | 山东一诺威体育产业有限公司 | Polyurethane self-leveling floor material and preparation method thereof |
| CN108047925A (en) * | 2017-12-13 | 2018-05-18 | 山东诺威体育产业有限公司 | Polyurethane gravity flow self-leveling floor material and preparation method thereof |
| CN109554109A (en) * | 2018-07-10 | 2019-04-02 | 成都虹润制漆有限公司 | A kind of aqueous thick-slurry type bi-component hybrid inorganic-organic self-leveling floor coating and preparation method thereof |
| CN109554109B (en) * | 2018-07-10 | 2020-12-15 | 成都虹润制漆有限公司 | Aqueous thick-paste type double-component organic-inorganic hybrid self-leveling floor coating and preparation method thereof |
| CN109609010A (en) * | 2018-12-12 | 2019-04-12 | 厦门安必信新材料科技有限公司 | A kind of super abrasive aqueous polyurethane floor coatings and preparation method thereof |
| CN111647244A (en) * | 2020-04-13 | 2020-09-11 | 南京弘志教育装备科技有限公司 | Water-based acrylic acid runway surface material and preparation and application thereof |
| WO2022012015A1 (en) * | 2020-07-14 | 2022-01-20 | 上海保立佳新材料有限公司 | Single-component water-proof high-hardness water-based floor paint and preparation method therefor |
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Application publication date: 20120704 |