CN104351206B - A kind of wettable powder of Tebuconazole and garlicin - Google Patents
A kind of wettable powder of Tebuconazole and garlicin Download PDFInfo
- Publication number
- CN104351206B CN104351206B CN201410630610.XA CN201410630610A CN104351206B CN 104351206 B CN104351206 B CN 104351206B CN 201410630610 A CN201410630610 A CN 201410630610A CN 104351206 B CN104351206 B CN 104351206B
- Authority
- CN
- China
- Prior art keywords
- tebuconazole
- garlicin
- wettable powder
- present
- powder
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- PXMNMQRDXWABCY-UHFFFAOYSA-N 1-(4-chlorophenyl)-4,4-dimethyl-3-(1H-1,2,4-triazol-1-ylmethyl)pentan-3-ol Chemical compound C1=NC=NN1CC(O)(C(C)(C)C)CCC1=CC=C(Cl)C=C1 PXMNMQRDXWABCY-UHFFFAOYSA-N 0.000 title claims abstract description 27
- 239000005839 Tebuconazole Substances 0.000 title claims abstract description 27
- 239000004563 wettable powder Substances 0.000 title claims abstract description 26
- 241000221785 Erysiphales Species 0.000 claims abstract description 11
- 235000010799 Cucumis sativus var sativus Nutrition 0.000 claims abstract description 10
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 9
- 239000000843 powder Substances 0.000 claims abstract description 9
- 239000004615 ingredient Substances 0.000 claims abstract description 4
- 239000002994 raw material Substances 0.000 claims description 7
- 238000005507 spraying Methods 0.000 claims description 4
- 244000299906 Cucumis sativus var. sativus Species 0.000 claims 1
- 229920003171 Poly (ethylene oxide) Polymers 0.000 claims 1
- -1 polyoxyethylene Polymers 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 15
- 230000002265 prevention Effects 0.000 abstract description 10
- 240000008067 Cucumis sativus Species 0.000 abstract description 9
- 230000002045 lasting effect Effects 0.000 abstract description 4
- 230000000844 anti-bacterial effect Effects 0.000 abstract description 2
- 239000012752 auxiliary agent Substances 0.000 abstract description 2
- 201000010099 disease Diseases 0.000 description 8
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 8
- 239000003814 drug Substances 0.000 description 7
- 238000000034 method Methods 0.000 description 7
- 230000003902 lesion Effects 0.000 description 5
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 4
- 239000000575 pesticide Substances 0.000 description 4
- 240000002234 Allium sativum Species 0.000 description 3
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 3
- 235000004611 garlic Nutrition 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 241000234282 Allium Species 0.000 description 2
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 2
- 239000003899 bactericide agent Substances 0.000 description 2
- 238000011835 investigation Methods 0.000 description 2
- 231100000572 poisoning Toxicity 0.000 description 2
- 230000000607 poisoning effect Effects 0.000 description 2
- 238000001228 spectrum Methods 0.000 description 2
- 150000003852 triazoles Chemical class 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- JDLKFOPOAOFWQN-VIFPVBQESA-N Allicin Natural products C=CCS[S@](=O)CC=C JDLKFOPOAOFWQN-VIFPVBQESA-N 0.000 description 1
- 240000002791 Brassica napus Species 0.000 description 1
- 235000006008 Brassica napus var napus Nutrition 0.000 description 1
- 241000219112 Cucumis Species 0.000 description 1
- 235000015510 Cucumis melo subsp melo Nutrition 0.000 description 1
- 241000234280 Liliaceae Species 0.000 description 1
- 241000221662 Sclerotinia Species 0.000 description 1
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 description 1
- 229930182558 Sterol Natural products 0.000 description 1
- FJJCIZWZNKZHII-UHFFFAOYSA-N [4,6-bis(cyanoamino)-1,3,5-triazin-2-yl]cyanamide Chemical compound N#CNC1=NC(NC#N)=NC(NC#N)=N1 FJJCIZWZNKZHII-UHFFFAOYSA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- JDLKFOPOAOFWQN-UHFFFAOYSA-N allicin Chemical compound C=CCSS(=O)CC=C JDLKFOPOAOFWQN-UHFFFAOYSA-N 0.000 description 1
- 235000010081 allicin Nutrition 0.000 description 1
- 235000001014 amino acid Nutrition 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 235000013339 cereals Nutrition 0.000 description 1
- 238000000205 computational method Methods 0.000 description 1
- 230000017858 demethylation Effects 0.000 description 1
- 238000010520 demethylation reaction Methods 0.000 description 1
- 230000006806 disease prevention Effects 0.000 description 1
- 230000000857 drug effect Effects 0.000 description 1
- 238000009313 farming Methods 0.000 description 1
- 235000012055 fruits and vegetables Nutrition 0.000 description 1
- 230000000855 fungicidal effect Effects 0.000 description 1
- 230000002070 germicidal effect Effects 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 239000003112 inhibitor Substances 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 150000002898 organic sulfur compounds Chemical class 0.000 description 1
- 244000052769 pathogen Species 0.000 description 1
- 230000001717 pathogenic effect Effects 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 230000003449 preventive effect Effects 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000005070 sampling Methods 0.000 description 1
- 150000003432 sterols Chemical class 0.000 description 1
- 235000003702 sterols Nutrition 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
Landscapes
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The present invention relates to the wettable powder of a kind of Tebuconazole and garlicin, in described wettable powder, effective ingredient is Tebuconazole and garlicin；Auxiliary agent is that alkylphenol-polyethenoxy is phonetic, spaonin powder, kieselguhr.Powdery mildew of cucumber is had extraordinary prevention effect by wettable powder of the present invention, the present invention utilizes the bactericidal activity of Tebuconazole and garlicin to have good synergism, effectively enhance the effect of the prevention to powdery mildew of cucumber and treatment, morbidity early stage dispenser instant effect, and the lasting period is long, on non-Target crops without impact.
Description
Technical field
The present invention relates to the wettable powder of a kind of Tebuconazole and garlicin, be specifically related to the wettable powder of Tebuconazole and garlicin for preventing and treating powdery mildew of cucumber, belong to technical field of pesticide.
Background technology
Tebuconazole belongs to triazole bactericidal agent, is sterol demethylation inhibitor.Tebuconazole is a kind of efficient, wide spectrum, interior absorption triazole bactericidal agent, has protection, treats, roots out three zones, and fungicidal spectrum is wide, the lasting period is long.These product are used for preventing and treating sclerotinia rot of colza, and not only preventive effect is good, and have resistant to lodging, the features such as production-increasing function is obvious.It is the seed treatment for Important Economic crop or the efficient germicide of face sprinkling, can effectively prevent and treat the multiple rust of cereal crop, powdery mildew, net blotch, root rot, head blight etc..
Garlicin (Allicin) is a kind of organosulfur compound extracted from the bulb (Bulbus Allii head) of Liliaceae allium Bulbus Allii (AlliumSativum), exists in Bulbus Allii Cepae and other alliums.Formal name used at school GIUCOSinoate.Pale yellow oily liquid body.Boiling point 80-85 DEG C (0.2kPa), relative density 1.112(20/4 DEG C), index of refraction 1.561.It is dissolved in ethanol, chloroform or ether.Dissolubility 2.5% (quality) (10 DEG C) in water, its pH value of water solution is 6.5, has grease precipitate to be formed during standing.Can dissolve each other with ethanol, ether and benzene.Thermokalite is unstable, acid is stable.By in the bulb being present in liliaceous plant Bulbus Allii, the garlic aminoacid existed converting generation under big allinase effect.Exist in the bulb of Herba Alii fistulosi.Having strong big garlic odour, taste is peppery.
The industrial crops cultivated areas such as the difficulty of prevention and cure of current phytopathogen is increasing, on the one hand, along with the change of pattern of farming, melon fruits and vegetables progressively expand, and disease occurrence degree, occur quantity all to increase, and in preventing and treating, difficulty strengthens；On the other hand, the resistance of pathogen rises year by year under lasting medicament selection pressure, and the prevention effect of single dose is more and more weak, and control of plant disease faces significant challenge.
Summary of the invention
For the problems referred to above, the invention provides the wettable powder of a kind of Tebuconazole and garlicin, the present invention is effective, holding effect is long, to non-Target crops safety.
Technical scheme is as follows:
The wettable powder of a kind of Tebuconazole and garlicin, in described wettable powder, effective ingredient is Tebuconazole and garlicin；Auxiliary agent is that alkylphenol-polyethenoxy is phonetic, spaonin powder, kieselguhr.
Further, each raw material components percentage in wettable powder of the present invention:
Tebuconazole 1%-50%, garlicin 0.1%-1%, the phonetic 5%-10% of alkylphenol-polyethenoxy, spaonin powder 3%-8%, kieselguhr add to 100%.
Further, each raw material components percentage in wettable powder of the present invention:
Tebuconazole 10%-40%, garlicin 0.1%-0.5%, the phonetic 6%-9% of alkylphenol-polyethenoxy, spaonin powder 4%-8%, kieselguhr add to 100%.
Further, each raw material components percentage in wettable powder of the present invention:
Tebuconazole 30%, garlicin 0.3%, alkylphenol-polyethenoxy are phonetic 7.2%, spaonin powder 5%, kieselguhr add to 100%.
Wettable powder of the present invention is used for preventing and treating powdery mildew of cucumber；Insecticide-applying way is spraying；Dispenser period is their early stage；Annual spraying times is 1 or 2 time；Effective ingredient dosage of the present invention is 8 grams/ha-15 grams/ha, it is preferred that dosage is 9.3 grams/ha.
Powdery mildew of cucumber is had extraordinary prevention effect by wettable powder of the present invention, the present invention utilizes the bactericidal activity of Tebuconazole and garlicin to have good synergism, effectively enhance the effect of the prevention to powdery mildew of cucumber and treatment, morbidity early stage dispenser instant effect, and the lasting period is long, on non-Target crops without impact.
Detailed description of the invention
Below in conjunction with specific embodiment further describe the present invention, advantages of the present invention and feature will be with describe and apparent.But embodiment is only exemplary, the scope of the present invention is not constituted any restriction.It will be understood by those skilled in the art that and the details of technical solution of the present invention and form can be modified or replace lower without departing from the spirit and scope of the present invention, but these amendments and replacement each fall within protection scope of the present invention.
Embodiment 1
30% Tebuconazole and 0.3% garlicin wettable powder
Each raw material components percentage:
Tebuconazole 30%, garlicin 0.3%, alkylphenol-polyethenoxy are phonetic 7.2%, spaonin powder 5%, kieselguhr add to 100%.
By above-mentioned each composition application conventional pesticide process technology, the wettable powder goods being suitable for agriculturally using made.In the present embodiment, the co-toxicity coefficient of Tebuconazole and garlicin is 199.84.
Embodiment 2
40% Tebuconazole and 0.1% garlicin wettable powder
Each raw material components percentage:
Tebuconazole 40%, garlicin 0.1%, alkylphenol-polyethenoxy are phonetic 8%, spaonin powder 3.5%, kieselguhr add to 100%.
By above-mentioned each composition application conventional pesticide process technology, the wettable powder goods being suitable for agriculturally using made.In the present embodiment, the co-toxicity coefficient of Tebuconazole and garlicin is 174.65.
Embodiment 3
10% Tebuconazole and 1% garlicin wettable powder
Each raw material components percentage:
Tebuconazole 10%, garlicin 1%, alkylphenol-polyethenoxy are phonetic 5%, spaonin powder 7.5%, kieselguhr add to 100%.
By above-mentioned each composition application conventional pesticide process technology, the wettable powder goods being suitable for agriculturally using made.In the present embodiment, the co-toxicity coefficient of Tebuconazole and garlicin is 155.87.
Test example 1 present invention prevention effect to powdery mildew of cucumber
1, test method
Test site, in Liaocheng of Shandong Province, is Fructus Cucumidis sativi for studying thing, and test sets every mu of comparison totally 10 process, often processes and repeats 4 times, and random district group arranges, and plot area is 40 square metres.
2, control time and number of times
Before dispenser, after the 1st medicine after 7 days and the 2nd dispenser 7 days, 14 days, every community adopted diagonal 5 sampling, every some investigation 20 strains, investigates occurring degree by leaf classification, and calculating disease refers to and prevention effect.
Grade scale is as follows:
0 grade: anosis；
1 grade: lesion area accounts for less than the 5% of one-piece blade area；
3 grades: lesion area accounts for the 6%-15% of one-piece blade area；
5 grades: lesion area accounts for the 16%-25% of one-piece blade area；
7 grades: lesion area accounts for the 26%-50% of one-piece blade area；
9 grades: lesion area accounts for more than the 50% of one-piece blade area.
3, drug effect computational methods
Sick leaf rate (%)=sick number of sheets/investigate the total number of sheets × 100；
Disease index=∑ (the sick number of sheets × relative level numerical value at different levels)/(investigating the total number of sheets × 9) × 100
Prevention effect (%)=[before 1-(blank district medicine disease index after disease index × treatment region medicine)/(after blank district medicine disease index before disease index × treatment region medicine)] × 100.
4, poisoning investigation method
After dispenser, continuous 14d estimates medicament to whether crop has poisoning.
5, result of the test and analysis
The effect that each process prevents and treats powdery mildew of cucumber is as shown in table 1:
The table 1 wettable powder of the present invention prevention effect to powdery mildew of cucumber
Test result indicate that, Fructus Cucumidis sativi is divided disease prevention effect notable by wettable powder of the present invention in vain, and on non-Target crops without impact.
Claims (1)
1. the wettable powder of a Tebuconazole and garlicin, it is characterised in that each raw material components percentage in described wettable powder:
Tebuconazole 30%, garlicin 0.3%, alkylphenol polyoxyethylene 7.2%, spaonin powder 5%, kieselguhr add to 100%；
Described wettable powder is used for preventing and treating powdery mildew of cucumber；Insecticide-applying way is spraying；Dispenser period is their early stage；Annual spraying times is 2 times；Effective ingredient dosage is 9.3 grams/ha.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410630610.XA CN104351206B (en) | 2014-11-11 | 2014-11-11 | A kind of wettable powder of Tebuconazole and garlicin |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410630610.XA CN104351206B (en) | 2014-11-11 | 2014-11-11 | A kind of wettable powder of Tebuconazole and garlicin |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104351206A CN104351206A (en) | 2015-02-18 |
| CN104351206B true CN104351206B (en) | 2016-07-20 |
Family
ID=52518600
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410630610.XA Active CN104351206B (en) | 2014-11-11 | 2014-11-11 | A kind of wettable powder of Tebuconazole and garlicin |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104351206B (en) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105284948A (en) * | 2015-12-05 | 2016-02-03 | 济南舜昊生物科技有限公司 | Wettable powder containing thiram |
| US11452294B2 (en) * | 2017-12-06 | 2022-09-27 | North Carolina State University | Use of tebuconazole for annual bluegrass (Poa annua) control in turfgrasses |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1288662A (en) * | 2000-06-22 | 2001-03-28 | 张长兴 | Farm chemical for preventing and controlling black spot of fruit tree |
| CN102726415A (en) * | 2012-06-19 | 2012-10-17 | 河南省大地农化有限责任公司 | Allicin-containing prevention and treatment pesticide for crop plant diseases |
-
2014
- 2014-11-11 CN CN201410630610.XA patent/CN104351206B/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| CN104351206A (en) | 2015-02-18 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103999865B (en) | A kind of bactericidal composition and application containing cyflufenamid and dimethomorph or zoxamide | |
| CN103828812A (en) | Composition containing oligosaccharide and miazines bactericidal ingredients\ | |
| CN102293205A (en) | Osthole and ningnanmycin compound bactericide | |
| CN104351206B (en) | A kind of wettable powder of Tebuconazole and garlicin | |
| CN104351203B (en) | A kind of Tebuconazole and the microemulsion of garlicin | |
| CN104396957B (en) | For preventing and treating the microemulsion of tea tree tea geometrid | |
| CN104872204A (en) | Vegetable bactericide capable of preventing and treating phytophthora root rot of vegetables and preparation method of vegetable bactericide | |
| CN104351199B (en) | A kind of Tebuconazole and the water dispersible granules of allicin | |
| CN104542590B (en) | Active ingredient is the microemulsion of lentinan and allicin | |
| CN103814902B (en) | A kind of compositions preventing and treating Flos Chrysanthemi disease containing CGA-173506 and Difenoconazole | |
| CN104351197B (en) | A kind of Tebuconazole and the microcapsule suspension-suspendinagent agent of garlicin | |
| CN104351200B (en) | A kind of Tebuconazole and garlicin bactericidal composition | |
| CN104351204B (en) | A kind of Tebuconazole and the microcapsule suspending agent of garlicin | |
| CN103828820A (en) | Bactericidal composition containing oligosaccharide and fluoxastrobin | |
| CN104351201B (en) | A kind of chrysanthemum bactericide | |
| CN104351194B (en) | One grows cotton insecticide | |
| CN104351196B (en) | A kind of microemulsion for chrysanthemum | |
| CN104351198B (en) | A kind of microcapsule suspending agent for chrysanthemum | |
| CN104351205B (en) | A kind of water dispersible granules for chrysanthemum | |
| CN104322494B (en) | Effective ingredient is the aqueous emulsion of garlicin and jinggangmycin A | |
| CN104430377B (en) | A kind of suspension emulsion for chrysanthemum | |
| CN106577651B (en) | Composition pesticide containing metrafenone and matrine or oxymatrine | |
| CN104351202B (en) | A kind of aqueous emulsion for chrysanthemum | |
| CN103814898B (en) | Composition containing oligosaccharides and metrafenone | |
| CN108184864A (en) | A kind of complex composition and its application containing fluorine thiazole pyrrole ethyl ketone and frutus cnidii |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C41 | Transfer of patent application or patent right or utility model | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20160623 Address after: 266109, No. 111, sunny road, Chengyang District, Shandong, Qingdao Applicant after: JINAN CAVIN BIOTECHNOLOGY CO., LTD. Address before: 250001 Shandong Province, Ji'nan City District Court building 2303 No. 288 Applicant before: JINAN XINQIDIAN MEDICINE SCIENCE & TECHNOLOGY CO., LTD. |
|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CB03 | Change of inventor or designer information | ||
| CB03 | Change of inventor or designer information |
Inventor after: Lu Chunying Inventor before: Sun Bo Inventor before: Sun Qian Inventor before: Mu Kexiao Inventor before: Hao Aihua Inventor before: Wang Mengmeng |
|
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20170712 Address after: 300000 building 4, building 3-501, Ziya, Hongqiao District, Tianjin, China Patentee after: Lu Chunying Address before: 266109, No. 111, sunny road, Chengyang District, Shandong, Qingdao Patentee before: Qingdao Qingzhi Enterprise Management Consulting Co., Ltd. |
|
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20181123 Address after: 409100 First Floor of Litangba Building, Nanbin Street, Shizhu Tujia Autonomous County, Chongqing Patentee after: Shizhu Tujia Autonomous County Balong Agricultural Development Co., Ltd. Address before: 300000 Building 3-501, Ziyali 4, Hongqiao District, Tianjin Patentee before: Lu Chunying |