CN104337725B - Skin whitening and moisturizing mask containing nymphaea hybrid extractives and preparing method thereof - Google Patents
Skin whitening and moisturizing mask containing nymphaea hybrid extractives and preparing method thereof Download PDFInfo
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Abstract
The invention provides a skin whitening and moisturizing mask. The skin whitening and moisturizing mask comprises, by mass, 3%-10% of propylene glycol, 3%-10% of glycerinum, 3%-8% of butanediol, 2%-8% of vitamin C ethylether, 1%-4% of witch hazel extractives, 3%-8% of nymphaea hybrid extractives, 1%-5% of natural beta glucan, 0.1%-0,5% of dipotassium glycyrrhizinate, 0.1%-0.5% of carbomer 940, 0.1%-0.5% of triethanolamine, 0.1%-0.5% of collagen peptide powder and the balanced deionized water. The skin whitening and moisturizing mask is characterized in that the nymphaea hybrid extractives are composed of nymphaea hybrid total polysaccharides and nymphaea hybrid general flavone. The skin whitening and moisturizing mask has pure natural phytoextraction ingredients, is free of toxic and side effects, free of medicine dependence, excellent in skin touch and obvious in effect, and has the effects of skin whitening, moisturizing, deep moisturizing, skin moistening and beautifying.
Description
Technical field：
The invention belongs to household chemicals technical field, and in particular to a kind of whitening moisturizing face masque.
Background technology：
In personal nursing class daily chemical products, facial mask is the preferable facial-care product that a kind of depth is liked by consumer, people
The nursing of skin of face is especially paid attention to, pursue the maintenance of facial appearance.Mask product on the market has much at present, there is U.S.
Fine flour film, moisture saver mask, MASQUE APAISANT HYDRATANT etc., but the effect of many facial masks is not caused by natural component, some chemical substances
The side effects such as skin of face allergy can be caused, more there is severe patient to further relate to heavy metals exceeding standard.And consumer is for pure natural plant
Thing composition, especially pure natural plant ingredients can collect whitening again has great demand with moisture-keeping functions with the facial mask of the whole body.
The content of the invention：
The present invention is intended to provide it is a kind of with skin whitening, moisturizing, deep water supplement, moisturizing face-nursing function containing Plant functional into
The facial mask for dividing.
Specifically, whitening moisturizing face masque of the invention is made up of following raw materials according to mass percent：Propane diols 3 ~
10%, glycerine 3 ~ 10%, butanediol 3 ~ 8%, VCE 2 ~ 8%, hazel extract 1 ~ 4%, perfume lotus flower is extracted
Thing 3 ~ 8%, natural beta glucan 1 ~ 5%, dipotassium glycyrrhizinate 0.1 ~ 0.5%, card ripple 940 0.1 ~ 0.5%, triethanolamine 0.1 ~
0.5%, collagen Gly-His-Lys 0.1 ~ 0.5%, balance of deionized water.The perfume Flos Nelumbinis extract is by perfume lotus flower total starches
Constituted with perfume lotus flower general flavone.
Wherein, the quality proportioning of the perfume Flos Nelumbinis extract each component is preferably perfume lotus flower total starches：Perfume lotus flower
General flavone is 3：1；More preferably：Perfume lotus flower total starches account for the 3% of facial mask raw material, and perfume lotus flower general flavone accounts for facial mask raw material
1%。
Additionally, the whitening moisturizing face masque is preferably made up of by mass percentage following raw materials：Propane diols 6%, glycerine
5%, butanediol 3%, VCE 3%, hazel extract 4%, perfume Flos Nelumbinis extract 4%, natural beta glucan
3%, dipotassium glycyrrhizinate 0.2%, card ripple 940 0.2%, triethanolamine 0.2%, collagen Gly-His-Lys 0.2%, balance of deionization
Water.The perfume Flos Nelumbinis extract is made up of perfume lotus flower total starches and perfume lotus flower general flavone.
Or be preferably made up of by mass percentage following raw materials：Propane diols 6%, glycerine 5%, butanediol 3%, vitamin
C ethylethers 3%, hazel extract 4%, perfume Flos Nelumbinis extract 4%（Perfume lotus flower total starches account for the 3% of facial mask raw material, perfume
Water lotus flower general flavone accounts for the 1% of facial mask raw material）, natural beta glucan 3%, dipotassium glycyrrhizinate 0.2%, card ripple 940 0.2%, three second
Hydramine 0.2%, collagen Gly-His-Lys 0.2%, balance of deionized water.
Perfume lotus flower total starches are natural plant polyose glue in the ovary of perfume lotus flower flower, are demonstrate,proved through experiment
It is bright effectively to alleviate skin of face and dry peeling, furfur, pruitus etc. with very strong replenishing water and preserving moisture effect, actively protect
Shield skin of face, completely cuts off skin agings for causing such as extraneous stimulation, inflammation and environmental pollution etc., is that skin can keep more holding
Long water profit state, reaches effect of moisturizing and deep water supplement.
And perfume lotus flower general flavone then from perfume lotus flower pistil and part ovary in, tests prove that, it has
The suppression tyrosinase activity more stronger than traditional whitening compound ursin, is a kind of very effective tyrosinase inhibitor.Junket
Propylhomoserin enzyme is the rate-limiting enzyme of B16 cell, not only determines the speed of B16 cell, or melanocyte differen-tiation is ripe
Characteristic mark.In human body, tyrosinase is then primarily present in the melanocyte of skin epidermal cells, tyrosinase
Activity is related to melanin genesis amount, controls its vigor to can control melanogenesis amount.Therefore, tyrosinase inhibitor is by as tool
The additive for having whitening function is added in cosmetics.In the Inhibition test to tyrosinase, the addition of perfume lotus flower general flavone
Dosage suppresses tyrosinase effect in 0 ~ 0.2mg/ml with obvious, and effect is better than the positive control bear of comparable sodium
Fruit glycosides.
Additionally, the natural beta glucan in this formula is a kind of natural β-Portugal of new type water-solubility for having actinomyces to produce gathering
Sugar, has activation to the macrophage in human body skin, can promote collagen and elastin laminin increase in skin, so that
Improve skin appearance；Then contain various tannins in hazel extract, can adjust sebum secretion, restrain skin pore,
Confrontation is allergic；VCE is ascorbic derivative, has more excellent stability than vitamin C and resists
Oxidation effectiveness, is applied to then have excellent whitening function in daily chemical products；Therefore these the natural components compatibilities in being formulated make
With rear, complementary effect is can reach,
Whitening moisturizing face masque in the present invention uses above-mentioned pure natural components as functional components, without any side effects,
Without drug dependence, skin sense is splendid, effect is significant, with skin whitening, moisturizing, deep water supplement, the effect of moisturizing beauty treatment.
Brief description of the drawings
Fig. 1 is the perfume lotus flower total starches moisturizing result of the test of the embodiment of the present invention 13, and line below represents hyaluronic acid
Sodium, line above represents perfume lotus flower total starches.
Fig. 2 suppresses tyrosinase activity result of the test, line below for the perfume lotus flower general flavone of the embodiment of the present invention 14
Ursin is represented, line above represents perfume lotus flower general flavone.
Specific embodiment：
Embodiment 1：The preparation method of perfume lotus flower total starches
Take dried perfume lotus flower ovary to crush, cross 40 mesh sieves, weigh 200g, plus 25 times of water of amount in 100 DEG C of water-baths
Middle 4~5h of hot dipping, gauze initial filter, centrifugation.The dregs of a decoction are extracted 2 times again with method, merge three supernatants, and 70 DEG C of rotated evaporimeter subtracts
Pressure is concentrated into the 1/5 of original volume, to adding 95% ethanol to be precipitated in concentrate, when the concentration of alcohol for adding reaches 60%（Body
Product content）When, there are a large amount of flocculent deposits to occur, stand 24h, centrifugation.Precipitation absolute ethyl alcohol, acetone, ether are washed successively
Wash, be vacuum dried, obtain perfume lotus flower total starches.
Embodiment 2：The preparation method of perfume lotus flower general flavone
Take dried perfume lotus flower band pistil ovary to crush, cross 40 mesh sieves, weigh 200g, petroleum ether degreasing twice, often
Secondary 2 h, filtering.Extracted twice with 75% alcohol heat reflux after filter residue drying, every time 3 h.Merge after extract solution suction filtration, decompression
It is 1 to be concentrated to solid-liquid ratio：2, separated with HPD-400 macroreticular resins, eluant, eluent is respectively 30%, 60% ethanol.By 60% ethanol stream part
Perfume lotus flower general flavone is vacuum dried to obtain after eluent is concentrated under reduced pressure.
Embodiment 3：The preparation method of natural beta glucan
Natural exocellular polysaccharide of the beta glucan as produced by agrobacterium ZX09 is prepared, and its preparation method is referring to patent
（The patent No.：201010146371.2；Inventor：Zhang Jianfa, repaiies intelligent, the Zhu Bin of love；Patent name：Agrobacterium ZX09, uses soil
Water-soluble natural beta glucan of bacillus ZX09 productions and preparation method thereof and the application on blood sugar is reduced）In the middle of specification
Embodiment 3.
Embodiment 4：The preparation method of hazel extract
Take Hamamelidaceae Plants sweetgum（Liquidambar formosana）Fruit and browse, crushed after being dried, mistake
40 mesh sieves；100g is weighed, adds 500mL petroleum ethers, heating water bath backflow 2h to decolourize, filter while hot, after filter residue and drying, add
1000mL deionized waters, with Microwave-assisted firing refluxing extraction 3h, filter while hot, and supernatant is hazel extract.
Embodiment 5：The preparation method of the whitening moisturizing face masque containing perfume Flos Nelumbinis extract
A kind of whitening moisturizing face masque containing perfume Flos Nelumbinis extract, including following mass ratio component：Propane diols 6%, it is sweet
Oil 5%, butanediol 3%, VCE 3%, hazel extract 4%, perfume Flos Nelumbinis extract 4%（Perfume lotus flower total starches
The 3% of facial mask raw material is accounted for, perfume lotus flower general flavone accounts for the 1% of facial mask raw material）, natural beta glucan 3%, dipotassium glycyrrhizinate 0.2%, card
Ripple 940 0.2%, triethanolamine 0.2%, collagen Gly-His-Lys 0.2%, balance of deionized water.
Facial mask liquid will be formed after the composition of said components uniformly mixing, non-woven fabrics or silk mask paper are put into facial mask liquid
Immersion is packed after 15 minutes.
Embodiment 6：The preparation method of the whitening moisturizing face masque containing perfume Flos Nelumbinis extract
A kind of whitening moisturizing face masque containing perfume Flos Nelumbinis extract, including following mass ratio component：Propane diols 3%, it is sweet
Oil 3%, butanediol 3%, VCE 2%, hazel extract 1%, perfume Flos Nelumbinis extract 3%（Perfume lotus flower is total
Polysaccharide accounts for the 2.25% of facial mask raw material, and perfume lotus flower general flavone accounts for the 0.75% of facial mask raw material）, natural beta glucan 1%, glycyrrhizic acid
Dipotassium 0.1%, card ripple 940 0.1%, triethanolamine 0.1%, collagen Gly-His-Lys 0.1%, balance of deionized water.
Facial mask liquid will be formed after the composition of said components uniformly mixing, non-woven fabrics or silk mask paper are put into facial mask liquid
Immersion is packed after 15 minutes.
Embodiment 7：The preparation method of the whitening moisturizing face masque containing perfume Flos Nelumbinis extract
A kind of whitening moisturizing face masque containing perfume Flos Nelumbinis extract, including following mass ratio component：Propane diols 10%, it is sweet
Oil 10%, butanediol 8%, VCE 8%, hazel extract 4%, perfume Flos Nelumbinis extract 8%（Perfume lotus flower
Total starches account for the 6% of facial mask raw material, and perfume lotus flower general flavone accounts for the 2% of facial mask raw material）, natural beta glucan 5%, dipotassium glycyrrhizinate
0.5%, card ripple 940 0.5%, triethanolamine 0.5%, collagen Gly-His-Lys 0.5%, balance of deionized water.
Facial mask liquid will be formed after the composition of said components uniformly mixing, non-woven fabrics or silk mask paper are put into facial mask liquid
Immersion is packed after 15 minutes.
Embodiment 8：The preparation method of the whitening moisturizing face masque containing perfume Flos Nelumbinis extract
A kind of whitening moisturizing face masque containing perfume Flos Nelumbinis extract, including following mass ratio component：Propane diols 3%, it is sweet
Oil 3%, butanediol 3%, VCE 2%, hazel extract 1%, perfume Flos Nelumbinis extract 4%（Perfume lotus flower is total
Polysaccharide accounts for the 3% of facial mask raw material, and perfume lotus flower general flavone accounts for the 1% of facial mask raw material）, natural beta glucan 1%, dipotassium glycyrrhizinate
0.1%, card ripple 940 0.1%, triethanolamine 0.1%, collagen Gly-His-Lys 0.1%, balance of deionized water.
Facial mask liquid will be formed after the composition of said components uniformly mixing, non-woven fabrics or silk mask paper are put into facial mask liquid
Immersion is packed after 15 minutes.
Embodiment 9：The preparation method of the whitening moisturizing face masque containing perfume Flos Nelumbinis extract
A kind of whitening moisturizing face masque containing perfume Flos Nelumbinis extract, including following mass ratio component：Propane diols 10%, it is sweet
Oil 10%, butanediol 8%, VCE 8%, hazel extract 4%, perfume Flos Nelumbinis extract 4%（Perfume lotus flower is total
Polysaccharide accounts for the 3% of facial mask raw material, and perfume lotus flower general flavone accounts for the 1% of facial mask raw material）, natural beta glucan 5%, dipotassium glycyrrhizinate
0.5%, card ripple 940 0.5%, triethanolamine 0.5%, collagen Gly-His-Lys 0.5%, balance of deionized water.
Facial mask liquid will be formed after the composition of said components uniformly mixing, non-woven fabrics or silk mask paper are put into facial mask liquid
Immersion is packed after 15 minutes.
Embodiment 10：The preparation method of the whitening moisturizing face masque containing perfume Flos Nelumbinis extract
A kind of whitening moisturizing face masque containing perfume Flos Nelumbinis extract, including following mass ratio component：Propane diols 6%, it is sweet
Oil 5%, butanediol 3%, VCE 3%, hazel extract 4%, perfume Flos Nelumbinis extract 4%（Perfume lotus flower total starches
The 2% of facial mask raw material is accounted for, perfume lotus flower general flavone accounts for the 2% of facial mask raw material）, natural beta glucan 3%, dipotassium glycyrrhizinate 0.2%, card
Ripple 940 0.2%, triethanolamine 0.2%, collagen Gly-His-Lys 0.2%, balance of deionized water.
Facial mask liquid will be formed after the composition of said components uniformly mixing, non-woven fabrics or silk mask paper are put into facial mask liquid
Immersion is packed after 15 minutes.
Embodiment 11：The preparation method of the whitening moisturizing face masque containing perfume Flos Nelumbinis extract
A kind of whitening moisturizing face masque containing perfume Flos Nelumbinis extract, including following mass ratio component：Propane diols 3%, it is sweet
Oil 3%, butanediol 3%, VCE 2%, hazel extract 1%, perfume Flos Nelumbinis extract 3%（Perfume lotus flower is total
Polysaccharide accounts for the 2% of facial mask raw material, and perfume lotus flower general flavone accounts for the 1% of facial mask raw material）, natural beta glucan 1%, dipotassium glycyrrhizinate
0.1%, card ripple 940 0.1%, triethanolamine 0.1%, collagen Gly-His-Lys 0.1%, balance of deionized water.
Facial mask liquid will be formed after the composition of said components uniformly mixing, non-woven fabrics or silk mask paper are put into facial mask liquid
Immersion is packed after 15 minutes.
Embodiment 12：The preparation method of the whitening moisturizing face masque containing perfume Flos Nelumbinis extract
A kind of whitening moisturizing face masque containing perfume Flos Nelumbinis extract, including following mass ratio component：Propane diols 10%, it is sweet
Oil 10%, butanediol 8%, VCE 8%, hazel extract 4%, perfume Flos Nelumbinis extract 8%（Perfume lotus flower
Total starches account for the 4% of facial mask raw material, and perfume lotus flower general flavone accounts for the 4% of facial mask raw material）, natural beta glucan 5%, dipotassium glycyrrhizinate
0.5%, card ripple 940 0.5%, triethanolamine 0.5%, collagen Gly-His-Lys 0.5%, balance of deionized water.
Facial mask liquid will be formed after the composition of said components uniformly mixing, non-woven fabrics or silk mask paper are put into facial mask liquid
Immersion is packed after 15 minutes.
Embodiment 13：The moisturizing experiment of perfume lotus flower total starches
1 material and instrument
Perfume lotus flower total starches, are prepared by embodiment 1；Sodium Hyaluronate, Furuida Biochemical Co., Ltd., Shandong changes
Cosmetic level.
Drier, Nanjing Xu Dong drying equipments factory；Measuring cup, Suzhou City Asia-Pacific glass for chemical equipment-building Instrument Ltd.；
Glass plate and filter paper（7.5 cm*7.5 cm）, the self-control of this laboratory；The limited public affairs of electronic balance LEVER, Kai Feng groups
Department.
2 test methods
Moisturizing is tested：At 20 DEG C, by finite concentration under 79% humidity（0.5%）Polysaccharide solution and reference substance hyaluronic acid
Xinhua filter paper of the sodium solution uniform application at a certain size（7.5 cm*7.5 cm）It is upper then to be claimed using analytical precision balances
Weight.Weighed once every 20 min.In order to control humidity, experiment is controlled from the saturated solution that ammonium chloride is placed in drier
Humidity processed.
Moisturizing rate=1-（Mn refers to the moisture for losing, and M0 refers to example weight）.
3rd, result of the test
As shown in Figure of description Fig. 1.
Result of the test as shown in Figure 1, as seen from the figure, the performance of keeping humidity of perfume lotus flower total starches and hyaluronic acid acid sodium
It is similar, and slightly it is better than Sodium Hyaluronate, show that perfume lotus flower total starches have good performance of keeping humidity, hyaluronic acid acid can be replaced
Sodium is used in cosmetics.
Embodiment 14：Perfume lotus flower general flavone suppresses tyrosinase experiments
1st, material, reagent and instrument
Perfume lotus flower general flavone：Prepared by embodiment 2；Fresh potato, it is commercially available.
TYR（L-Tyrosine, Sigma company）；Ursin（Beijing Baily Lai Si biochemistry corporation,Ltd.s）；
95% ethanol, dimethyl sulfoxide (DMSO)（DMSO）, phosphoric acid, disodium hydrogen phosphate, sodium dihydrogen phosphate, concentrated hydrochloric acid, be it is commercially available analysis it is pure.
Tissue mashing machine（Model JJ-2, high honour instrument manufacturing Co., Ltd of Jintan City of Jiangsu Province）；UV, visible light light splitting light
Degree meter（Model T6 New Worlds, Beijing Pu Xi all purpose instruments Co., Ltd）；Centrifuge（Model 80-1, Shanghai Surgical Operation Equipment Factory）；
Digital display thermostat water bath（Model HH-4, Jintan City south of the River instrument plant）；
2nd, method
2.1 preparation of reagents
Sodium phosphate buffer（1/15M, pH=6.8）：Accurately weigh 1.0001 g sodium dihydrogen phosphates, 1.1860 g phosphoric acid hydrogen
Disodium, after adding a small amount of deionized water dissolving, is settled to 500mL, and 4 DEG C of Refrigerator stores are standby.
TYR solution (7.5 mmol/L)：The g of TYR 0.2721 accurately is weighed, few drops concentrated hydrochloric acid is first added,
Plus the mL of deionized water about 50, after low-grade fever is completely dissolved, adjust pH to 7.0, plus deionized water to be settled to 200 with sodium hydroxide solution
mL。
By test solution：The g of perfume lotus flower general flavone 0.1000 accurately is weighed, 20 mL dimethyl sulfoxide (DMSO)s are dissolved in respectively, obtain 5
The prepare liquid of mg/mL, then two-fold dilution to 2.5 mg/mL, 1.25 mg/mL, 0.625 mg/mL, 0.3125 mg/mL,
0.15625 mg/mL。
Positive control（+CK）：0.1000 g ursin powder accurately is weighed, is dissolved in the deionized water of 20 mL, obtained
The positive control mother liquor of 5.00 mg/mL, then two-fold dilution to 2.5 mg/mL, 1.2500 mg/mL, 0.6250 mg/mL,
0.3125 mg/mL、0.1562mg/mL。
The preparation of 2.2 tyrosine enzyme liquids
Potato is cleaned, in 4 DEG C of precooling 4h or so.Peeling, is cut into about 1 × 1 × 1cm3 fourth shapes, is freezed in -20 DEG C
Night.Weigh, by 1: 1 (W:V ratio) adds 4 DEG C of sodium phosphate buffers of precooling, and homogenate, 3 layers are made of tissue mashing machine
Filtered through gauze, filtrate is centrifuged 10 min in 4000 r/min, and supernatant is the tyrosinase crude enzyme liquid of gained, 4 DEG C of preservations, 2 h
Inside it is finished.
Suppression of 2.3 samples to tyrosinase activity
The mL test systems of table 15 are designed
Note：During with spectrophotometer measurement light absorption value, " receiving test solution ", " standard control ", " positive control " are respectively with " negative
Control 1 ", " negative control 2 ", " negative control 3 " zeroing.
In this system, by test solution, including positive control ursin final concentration（mg/mL）Gradient is 0.03125,
0.0625,0.125,0.25,0.5.
During experiment, to sequentially added in test tube phosphate buffer, various concentrations gradient by test solution（It is right including the positive
According to）, enzyme liquid, in 30 DEG C of min of water-bath 10.Substrate TYR is subsequently adding, timing is immediately begun to.When determining 20 min of reaction
Light absorption value under 475 nm wavelength.With corresponding negative control as reference during measure, calculated with following equation and receive test solution（Including sun
Property control）To the inhibiting rate of tyrosinase, and according to the near of concentration-enzyme inhibition rate curve estimation half-inhibition concentration (IC50)
Like value.
Wherein, " A " is the light absorption value of standard control, and " B " is by test solution（Or positive control）Light absorption value
Each experiment do 3 it is parallel.Inhibiting rate is high to show that its inhibition strength to tyrosinase activity is high.
3rd, result of the test
As shown in Figure of description Fig. 2.
Result of the test as shown in Fig. 2 as seen from Figure 2, in the range of experimental concentration, with the rising of concentration, sample
And positive control is in rising trend to the inhibiting rate of tyrosinase, shows as dose-dependent inhibition.In experimental concentration model
In enclosing, perfume lotus flower general flavone to the inhibiting rate of tyrosinase apparently higher than ursin inhibiting rate.Therefore, perfume lotus flower is always yellow
Ketone can be as a kind of new plant source whitening agent, in allocating various creams into.
Embodiment 15：The experiment on probation of perfume lotus flower whitening moisturizing face masque
Given the test agent：Self-control perfume lotus flower whitening moisturizing face masque, is prepared by embodiment 5
Tested crowd：The people of volunteer 20, is women, 18 ~ 55 one full year of life, healthy
Subject presses facial mask application method, after spreading on face 20min, face is cleaned with warm water, washes away residual facial mask liquid.
All subjects find no it is red itch and IR, readme feels smooth comfortable, without greasy feeling, is particularly suitable for making in summer
With.And according to routine use method, twice daily, observe 15 d, investigation result such as table 2.
The perfume lotus flower whitening moisturizing face masque of table 2 tries out investigation result
As can be seen from Table 2, there is perfume lotus flower whitening moisturizing face masque more excellent skin whitening, moisturizing to act on, its combination property
It is excellent.
Claims (5)
1. a kind of whitening moisturizing face masque containing perfume Flos Nelumbinis extract, is made up of by mass percentage following raw materials：Propane diols
3-10%, glycerine 3-10%, butanediol 3-8%, VCE 2-8%, hazel extract 1-4%, perfume lotus flower is carried
Take thing 3-8%, natural beta glucan 1-5%, dipotassium glycyrrhizinate 0.1-0.5%, the 0.1-0.5% of card ripple 940, triethanolamine
0.1-0.5%, collagen Gly-His-Lys 0.1-0.5%, balance of deionized water；Characterized in that, the perfume Flos Nelumbinis extract
It is made up of perfume lotus flower total starches and perfume lotus flower general flavone；
Wherein, the preparation method of perfume lotus flower total starches is：Take dried perfume lotus flower ovary to crush, cross 40 mesh sieves, weigh
200g, plus the 25 times of water of amount 4~5h of hot dipping in 100 DEG C of water-baths, gauze initial filter, centrifugation；The dregs of a decoction are extracted 2 times again with method, are merged
Three supernatants, 70 DEG C of rotated evaporimeter is concentrated under reduced pressure into the 1/5 of original volume, is sunk to 95% ethanol is added in concentrate
Form sediment, when the concentration of alcohol for adding reaches 60%, there are a large amount of flocculent deposits to occur, stand 24h, centrifugation, precipitation absolute ethyl alcohol, third
Ketone, ether are washed successively, vacuum drying, obtain perfume lotus flower total starches, wherein 60% is volume content；
The preparation method of perfume lotus flower general flavone is：Take dried perfume lotus flower band pistil ovary to crush, cross 40 mesh sieves, weigh
200g, twice, each 2h is filtered petroleum ether degreasing；Extracted twice with 75% alcohol heat reflux after filter residue drying, each 3h,
Merge after extract solution suction filtration, it is 1 to be concentrated under reduced pressure to solid-liquid ratio：2, separated with HPD-400 macroreticular resins, eluant, eluent is respectively
30%th, 60% ethanol, perfume lotus flower general flavone is vacuum dried to obtain after 60% ethanol stream part eluent is concentrated under reduced pressure；
The preparation method of hazel extract is：Take the fruit of Hamamelidaceae Plants sweetgum (Liquidambar formosana)
And browse, crushed after being dried, cross 40 mesh sieves；100g is weighed, adds 500mL petroleum ethers, heating water bath backflow 2h to decolourize, while hot
Filtering, after filter residue and drying, adds 1000mL deionized waters, with Microwave-assisted firing refluxing extraction 3h, filters while hot, and supernatant is
It is hazel extract.
2. whitening moisturizing face masque according to claim 1, it is characterised in that perfume lotus flower in the perfume Flos Nelumbinis extract
Total starches are 3 with the mass ratio of perfume lotus flower general flavone：1.
3. whitening moisturizing face masque according to claim 2, it is characterised in that perfume lotus flower in the perfume Flos Nelumbinis extract
Total starches account for the 3% of facial mask material quality, and perfume lotus flower general flavone accounts for the 1% of facial mask material quality.
4. the whitening moisturizing face masque according to any one in claim 1-3, it is characterised in that the whitening moisturizing face masque
It is made up of by mass percentage following raw materials：Propane diols 6%, glycerine 5%, butanediol 3%, VCE 3%, gold thread
Plum extract solution 4%, perfume Flos Nelumbinis extract 4%, natural beta glucan 3%, dipotassium glycyrrhizinate 0.2%, card ripple 940 0.2%,
Triethanolamine 0.2%, collagen Gly-His-Lys 0.2%, balance of deionized water.
5. the preparation method of the whitening moisturizing face masque containing perfume Flos Nelumbinis extract described in claim 1, it is characterised in that bag
Include following steps：
To by mass percentage constitute as follows first：Propane diols 3-10%, glycerine 3-10%, butanediol 3-8%, vitamin C second
Base ether 2-8%, hazel extract 1-4%, perfume lotus is formed to obtain by perfume lotus flower total starches and perfume lotus flower general flavone proportioning
Flower extract 3-8%, natural beta glucan 1-5%, dipotassium glycyrrhizinate 0.1-0.5%, the 0.1-0.5% of card ripple 940, three ethanol
Amine 0.1-0.5%, collagen Gly-His-Lys 0.1-0.5%, the composition of balance of deionized water is uniformly mixed into facial mask liquid；Then will
Packaging obtains final product whitening moisturizing face masque after non-woven fabrics or silk mask paper are put into facial mask liquid immersion 15 minutes.
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