CN107049879B - A kind of cream containing okra extracting solution - Google Patents
A kind of cream containing okra extracting solution Download PDFInfo
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- CN107049879B CN107049879B CN201710442845.XA CN201710442845A CN107049879B CN 107049879 B CN107049879 B CN 107049879B CN 201710442845 A CN201710442845 A CN 201710442845A CN 107049879 B CN107049879 B CN 107049879B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/342—Alcohols having more than seven atoms in an unbroken chain
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/925—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of animal origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
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Abstract
The invention discloses a kind of creams containing okra extracting solution, and count by weight percentage, raw material composition and content are as follows: okra extracting solution 0.1~5%;Oily phase 25.0~30.0%;Water phase 68.4~74.65%;Preservative 0.1~0.2%;Essence 0.1~0.2%;Inorganic salts 0.1~1.0%.The present invention is the characteristics of mainly containing the effective components such as okra polysaccharide, flavones Polyphenols using okra extracting solution, with the science collocation such as glycerin monostearate, hexadeca-octadecyl alcohol, isobutyl palmitate, octyl/decyl glyceryl ester, refined wool fat, be made after reasonable formula with anti-inflammatory, whitening, moisturizing, anti-aging cream product.
Description
Technical field
The invention belongs to cosmetic fields, are related to a kind of creams, specifically a kind of frost containing okra extracting solution
Cream.
Background technique
Moisturizing is the key that skin nursing, and it is all skins that moisture-retention function of skin decline, which will lead to a variety of skin problem moisturizings,
The basis of skin nursing is just ensuring skin no matter any age, gender, any kind of skin require moisturizing daily
It is wet to be to maintain the skin permanent youth, it is not susceptible to suffer from dermopathic important link.
People increasingly pursue now it is pure natural, therefore seek from nature the functions such as natural skin whitening, moisturizing raw material at
For people's pursuit new to cosmetics.
Okra is as health-care vegetable of earning foreign exchange, and proteins,vitamins,minerals are more in okra fruit, inorganic salts, vitamin
B1, Vc content are above Kidney bean.It is reported that 100g okra edible part dry matter containing cellulose 9.42g, calcium 0.67g, phosphorus
0.56g, iron 0.8mg, Vc 29.95mg and potassium, zinc, manganese etc..Huang Agen etc. determines nutritional ingredient and correlation in okra
The content of active constituent contains protein 22.98%, total reducing sugar 19.92%, polysaccharide in dry light yellow gumbo fruit as the result is shown
2.00%, fat 9.40% and flavones 2.56%;In old fruit contain protein 15.78% and total reducing sugar 9.48%, polysaccharide 1.1%,
Fat 14.36%, flavones 1.48%.Okra also has quite high medical value.The drug effect of okra is early in " herbal guiding principle
Mesh " in have been described, setose abelmoschus root, stem, flower, seed etc. can be used as medicine, have certain antitumaous effect, root inducing diuresis for removing edema,
Cough with lung heat is controlled, seed good efficacy to suffering from a deficiency of the kidney controls indigestion etc..Domestic and foreign scholars have done largely its chemical component and pharmacological action
Analysis and research, main component have amino acid and protein, microelement, polysaccharide, flavone compound, and Lv Meiyun etc. has found,
Edible okra is rich in trace elements zn, Mn, for it there is raising immunity to provide reason with the medical value for reducing injury of lungs
By foundation;Wang Junyao, the effect experiment result of Li Jianhua etc. show that okra has antifatigue effect.In addition, okra
Antitumaous effect is also gradually revealed.Liu et al. the study found that the sensibility of insulin can be improved in the extract of okra.Okada
Y's etc. studies have shown that okra seed can be obviously improved the activity of tnf antibody.Sabitha V etc. is reported
To the physiological activity of anti-diabetic and lipidemia, these, which are studied, confirms okra anti-swollen for okra kind skin and seed powder
The activity of tumor, hypoglycemic etc. is prominent, has good medical value.
Summary of the invention
For above-mentioned technical problem in the prior art, the present invention provides a kind of creams containing okra extracting solution,
This creams containing okra extracting solution will solve cream anti-inflammatory in the prior art, whitening, moisturizing, anti-aging
The technical issues of effect cannot be provided simultaneously with.
The present invention provides a kind of creams containing okra extracting solution, count by weight percentage, raw material composition and
Content is as follows:
The oil is mutually Brij72, Brij721, glycerin monostearate, hexadeca-octadecyl alcohol, dimethicone, palm
The mixture that the different monooctyl ester of acid, octyl/decyl glyceryl ester, white oil, lanolin and BHT are formed;
The water phase is the mixture that propylene glycol, glycerol, xanthan gum and ionized water form;
The preservative is imidazolidinyl urea, hydantoins, isothiazolinone, any one in methylparaben;
The inorganic salts are sodium chloride, any one or two or more institutes in potassium chloride, magnesium sulfate or magnesium chloride
The mixture of composition.
Further, a kind of cream containing okra extracting solution, count by weight percentage, raw material composition
And content is as follows:
The oil is mutually Brij72, Brij721, glycerin monostearate, hexadeca-octadecyl alcohol, dimethicone, palm
The mixture that the different monooctyl ester of acid, octyl/decyl glyceryl ester, white oil, lanolin and BHT are formed;
The water phase is the mixture that propylene glycol, glycerol, xanthan gum and ionized water form;
The preservative is imidazolidinyl urea;
The inorganic salts are sodium chloride.
Further, a kind of cream containing okra extracting solution, count by weight percentage, raw material composition
And content is as follows:
The oil is mutually Brij72, Brij721, glycerin monostearate, hexadeca-octadecyl alcohol, dimethicone, palm
The mixture that the different monooctyl ester of acid, octyl/decyl glyceryl ester, white oil, lanolin and BHT are formed;
The water phase is the mixture that propylene glycol, glycerol, xanthan gum and ionized water form;
The preservative is hydantoins;
The inorganic salts are magnesium sulfate.
Further, a kind of cream containing okra extracting solution, count by weight percentage, raw material composition
And content is as follows:
The oil is mutually Brij72, Brij721, glycerin monostearate, hexadeca-octadecyl alcohol, dimethicone, palm
The mixture that the different monooctyl ester of acid, octyl/decyl glyceryl ester, white oil, lanolin and BHT are formed;
The water phase is the mixture that propylene glycol, glycerol, xanthan gum and ionized water form;
The preservative is that isothiazolinone is one of;
The inorganic salts are potassium chloride.
The present invention also provides a kind of above-mentioned cream containing okra extracting solution, the systems of the okra extracting solution
Preparation Method includes the following steps:
1) okra dry powder is taken to be dissolved in the water that addition in extraction vessel is its 10~15 times of quality, at 60~70 DEG C of temperature
Under, ultrasonic 30min~60min, extracting solution decompression filters, and filtrate decompression concentration removes 95% water, obtains the first filtrate;
2) filter cake is added in extraction vessel, the ethyl alcohol or mass percent concentration for adding its 5~10 times of quality are
95% ethyl alcohol, ultrasound 30min~60min at 40~50 DEG C of temperature, extracting solution decompression filter, and filtrate decompression steams ethyl alcohol,
The second filtrate is obtained, the first filtrate and the second filtrate are merged, mixed liquor is obtained by filtration okra through 400~500 mesh silica gel and extracts
Liquid.
Okra extracting solution is mainly contained effective components, the present invention such as okra polysaccharide, flavones Polyphenols and is mentioned using okra
Take liquid and glycerin monostearate, hexadeca-octadecyl alcohol, isobutyl palmitate, octyl/decyl glyceryl ester, refined wool fat etc.
Science collocation, be made after reasonable formula with anti-inflammatory, whitening, moisturizing, anti-aging cream product.
The present invention is compared with prior art, and technological progress is significant.The present invention utilizes okra anti-inflammatory, whitening, guarantor
Wet, anti-aging function provides a kind of cream containing okra extracting solution in conjunction with cosmetics, come meet people to not
Congenerous cosmetics demand enriches cosmetics type.
Detailed description of the invention
Fig. 1 subject 1 is different, and test orientation moisturizing value changes with time.
Fig. 2 subject 2 is different, and test orientation moisturizing value changes with time.
Fig. 3 subject 3 is different, and test orientation moisturizing value changes with time.
Specific embodiment
Understand to make the objectives, technical solutions, and advantages of the present invention clearer, with reference to embodiments, to the present invention
It is further elaborated.It should be appreciated that specific embodiment described herein is used merely to explain the present invention, it is not used to
Limit the present invention.
Below in conjunction with specific embodiment, in the present invention technology and application scheme understand and be fully described by.
The preparation of 1 okra extracting solution of embodiment
Okra dry powder 100g is taken to be dissolved in the water that 1000g is added in extraction vessel, at 65 DEG C, ultrasonic 60min, mixed liquor
Decompression filters, and filtrate decompression concentration removes 95% or so water, and residual filtrate 60g is spare, and filter cake continuously adds in extraction vessel
200g ethyl alcohol or 95% ethyl alcohol, the ultrasound 60min at 45 DEG C is added, extracting solution decompression filters, and filtrate decompression steams ethyl alcohol, remaining
50g propylene glycol is added in object to be sufficiently stirred to obtain liquor B, merges liquid A, B, mixed liquor is obtained by filtration through 400~500 mesh silica gel
Okra extracting solution 110g.
The antioxygenic property of 2 okra extracting solution of embodiment is tested
(1) configuration of DPPH solution: precision weighs the DPPH of 8mg (being accurate to 0.0001g), is dissolved in surely with dehydrated alcohol
In 100mL volumetric flask, the DPPH solution that concentration is 2*10-4mol/L is obtained.It is placed in refrigerator and saves with spare.
(2) 5g/L, 10g/L, 15g/L are accurately configured, 20g/L, 25g/L, the okra extracting solution of 30g/L mass concentration,
(3) 2mLDPPH is added into tool plug test tube, distilled water 2mL is protected from light and places 30min at room temperature, surveys at 517nm
Its fixed absorbance (A0), the sample solution for separately taking test tube that different quality concentration is added replace the same aforesaid operations of distilled water, and measurement is inhaled
Luminosity (A1), with sample solution and the isometric mixed determining absorbance (A2) of distilled water, using VC as positive reference substance, Vc concentration is matched
It is made as 0.00025,0.0005,0.0025,0.005,0.025,0.05,0.075,0.10g/L, using distilled water as blank pair
According to.
The clearance rate (%) of DPPH are as follows: [1- (A1-A2)/A0] * 100
The Scavenging activity of 1 DPPH free radical of table is tested
As can be seen from the above table okra extracting solution have stronger free radical scavenging ability, okra extracting solution it is dense
The Scavenging activity for spending higher DPPH free radical is stronger, but as the Scavenging activity amplification of the increase DPPH free radical of concentration becomes
In stabilization.
3 cream of embodiment prepares specific example and performance test
(1) cream prepares specific example
The formula of table 21
The formula of table 32
Continued 5-10
The formula of table 43
Continued 5-11
The formula of table 54
Experimental procedure:
(1) each component in A phase is accurately weighed in 120mL beaker A;
(2) deionized water is accurately weighed in 120mL beaker B, one by one disperses remaining component in B phase in water phase;
(3) load weighted A phase beaker is placed in heating plate and is heated, temperature controls within the scope of 75-80 DEG C;
(4) load weighted water phase is also placed in heating plate and is heated within the scope of 75-80 DEG C, heated while stirring;
(5) reach 80 DEG C (two-phase temperature difference is the smaller the better) to two-phase temperature, A phase is slowly added to B under agitation
In phase beaker, homogeneous 2min (just emulsification);
(6) continue to be stirred with blender, speed is slowed down, when temperature is down to 50 DEG C, C phase is added, is adjusted with PH test paper
PH;
(7) continue stirring 30 minutes or so, until system is uniform, stops stirring and it is waited to be down to room temperature, complete cream production.
(note: the cosmetics of production are the cream systems of 100g)
(2) cream stability is tested
The organoleptic indicator of 6 cream of table, physical and chemical index (being standard with QB/T 1857~2013)
According to 1857~2013 standard of QB/T of table 6-1, the detection of physical and chemical index is carried out to obtained cream, to protect
The cream product that card joined okra extracting solution meets professional standard.
Detection method is as follows:
(1) heat resistance is tested.It takes the cream of 30g to be put in beaker, is placed in the drying box that constant temperature is 40 DEG C for 24 hours
Afterwards, sample is taken out, is restored to room temperature, observing cream, whether there is or not layerings, precipitation phenomenon.
(2) cold tolerance is tested.The cream of 30g is taken to be put in beaker, being placed on temperature is that constant temperature is for 24 hours in -5 DEG C of refrigerator
Afterwards, sample is taken out, warms naturally to room temperature, whether there is or not layerings, precipitation phenomenon for observation cream.
(3) centrifugal test.Cream 5g is weighed, is packed into in graduated centrifuge tube, sets 2000r/ for centrifuge
Min takes out, and whether there is or not laminations for observation cream.
Experimental result and analysis:
Four obtained creams of experiment pass through heat-resisting cold-resistant experiment, bright with having no before experiment after spontaneous recovery to room temperature
Significant difference is different, finds no layering and precipitation phenomenon.This shows formula effectively, and joined the cream product symbol of okra extracting solution
Professional standard is closed, it is also errorless in experimental implementation.
(3) the skin moisture-keeping performance test of cream
Laboratory apparatus and material:
Corneometer825 moisture of skin tester is purchased from German CK company;Dehydrated alcohol;Alcohol cotton;Beaker;
Experimental procedure:
(1) healthy volunteer is selected.Subject is without any dermatopathy, and subject is without any dermatopathy, recipient site
Skin is without exception, does not also smear the external preparations such as any external drug and cosmetics.
(2) subject needs unified mild detergent to clean inner forearm face before testing, (the temperature in constant environment
Degree is 20-22 DEG C, relative humidity 40%-60%, is sat quietly 30 minutes;Dduring test, subject cannot arbitrarily run and walk about
Or leave the environmental field of test, it should which holding is emotionally stable, and mood is gentle, never exciting.
(3) 2*4cm is scratched with ruler2, the sample of phase homogenous quantities is weighed within this range, is averagely applied within the scope of this,
Different time is selected, the moisture of skin of each test point is measured respectively, is as a result indicated with humidity measurements;
As shown in Figure 1, 2, 3, it can be seen that by the correlation results of this three groups of experiments after okra extracting solution is added,
The blank group that the numeric ratio of moisturizing is not added wants high, and concentration is positively correlated;In addition, be added okra extracting solution after, with when
Between increase, the reduction amount of moisturizing numerical value than not plus the blank group of okra extracting solution it is some higher, and okra mentions
Take the concentration of liquid higher, moisturizing numerical value is higher.
Claims (4)
1. a kind of cream containing okra extracting solution, it is characterised in that count by weight percentage, raw material composition and content
It is as follows:
The preparation method of the okra extracting solution includes the following steps:
1) it takes okra dry powder to be dissolved in the water that addition in extraction vessel is its 10~15 times of quality to surpass at 60~70 DEG C of temperature
Sound 30min~60min, extracting solution decompression filter, and filtrate decompression concentration removes 95% water, obtain the first filtrate;
2) filter cake is added in extraction vessel, the ethyl alcohol or mass percent concentration for adding its 5~10 times of quality are 95%
Ethyl alcohol, ultrasound 30min~60min at 40~50 DEG C of temperature, extracting solution decompression filter, and filtrate decompression steams ethyl alcohol, obtain the
Two filtrates, merge the first filtrate and okra extracting solution is obtained by filtration through 400~500 mesh silica gel in the second filtrate, mixed liquor;
The described oil is mutually that Brij72, Brij721, glycerin monostearate, hexadeca-octadecyl alcohol, dimethicone, palmitinic acid are different
The mixture that monooctyl ester, octyl/decyl glyceryl ester, white oil, lanolin and BHT are formed;
The water phase is the mixture that propylene glycol, glycerol, xanthan gum and ionized water form;
The preservative is imidazolidinyl urea, hydantoins, isothiazolinone, any one in methylparaben;
The inorganic salts are by any one in sodium chloride, potassium chloride, magnesium sulfate or magnesium chloride or two or more form
Mixture.
2. a kind of cream containing okra extracting solution as described in claim 1, it is characterised in that count by weight percentage,
Its raw material composition and content are as follows:
The described oil is mutually that Brij72, Brij721, glycerin monostearate, hexadeca-octadecyl alcohol, dimethicone, palmitinic acid are different
The mixture that monooctyl ester, octyl/decyl glyceryl ester, white oil, lanolin and BHT are formed;
The water phase is the mixture that propylene glycol, glycerol, xanthan gum and ionized water form;
The preservative is imidazolidinyl urea;
The inorganic salts are sodium chloride.
3. a kind of cream containing okra extracting solution as described in claim 1, it is characterised in that count by weight percentage,
Its raw material composition and content are as follows:
The described oil is mutually that Brij72, Brij721, glycerin monostearate, hexadeca-octadecyl alcohol, dimethicone, palmitinic acid are different
The mixture that monooctyl ester, octyl/decyl glyceryl ester, white oil, lanolin and BHT are formed;
The water phase is the mixture that propylene glycol, glycerol, xanthan gum and ionized water form;
The preservative is hydantoins;
The inorganic salts are magnesium sulfate.
4. a kind of cream containing okra extracting solution as described in claim 1, it is characterised in that count by weight percentage,
Its raw material composition and content are as follows:
The described oil is mutually that Brij72, Brij721, glycerin monostearate, hexadeca-octadecyl alcohol, dimethicone, palmitinic acid are different
The mixture that monooctyl ester, octyl/decyl glyceryl ester, white oil, lanolin and BHT are formed;
The water phase is the mixture that propylene glycol, glycerol, xanthan gum and ionized water form;
The preservative is that isothiazolinone is one of;
The inorganic salts are potassium chloride.
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KR102539398B1 (en) | 2021-03-31 | 2023-06-02 | 숙명여자대학교산학협력단 | Composition for Inhibiting Inflammation containing Sous Vide-treated Okra |
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CN109718259B (en) * | 2017-10-30 | 2021-08-06 | 马晓萍 | Okra mite removing agent, okra mite removing patch and preparation method thereof |
CN110538110A (en) * | 2019-09-20 | 2019-12-06 | 杭州美库生物医药有限公司 | Method for extracting okra colloid by spray drying method and application of okra colloid in cosmetics |
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KR102539398B1 (en) | 2021-03-31 | 2023-06-02 | 숙명여자대학교산학협력단 | Composition for Inhibiting Inflammation containing Sous Vide-treated Okra |
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