CN104306281A - Oil-control emulsion and preparation method thereof - Google Patents

Oil-control emulsion and preparation method thereof Download PDF

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Publication number
CN104306281A
CN104306281A CN201410497390.8A CN201410497390A CN104306281A CN 104306281 A CN104306281 A CN 104306281A CN 201410497390 A CN201410497390 A CN 201410497390A CN 104306281 A CN104306281 A CN 104306281A
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parts
potassium sorbate
soluble polymer
potassium
flos
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CN201410497390.8A
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Chinese (zh)
Inventor
吴克
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Jiangsu Qilikang Skin Pharmaceutical Co Ltd
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Jiangsu Qilikang Skin Pharmaceutical Co Ltd
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Priority to CN201410497390.8A priority Critical patent/CN104306281A/en
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Abstract

The invention discloses an oil-control emulsion and a preparation method thereof. The oil-control emulsion comprises, by weight, 40-80 parts of witch hazel, 20-75 parts of calendula, 20-40 parts of trollflower, 20-40 parts of potassium lauroylamphodiethylsorbate, 10-25 parts of potassium sorbate, 5-15 parts of liquor, 20-40 parts of sodium aliphatate, 20-65 parts of clove oil, 20-30 parts of amnion liquid, 10-30 parts of thiamine, 30-50 parts of potassium palmitate, 20-70 parts of cetanol, 40-80 parts of glycerol and 50-90 parts of a water-soluble polymer. The preparation method comprises the following steps of putting witch hazel, calendula and trollflower into liquor to obtain an immersion liquid, crushing witch hazel, calendula and trollflower, adding potassium lauroylamphodiethylsorbate, potassium sorbate, sodium aliphatate, cetanol, glycerol and the water-soluble polymer into the crushed materials, carrying out heating stirring to obtain a uniform mixture, adding the immersion liquid into the mixture, carrying out high-rate mixing, adding the rest of the components into the mixture, and carrying out mixing to obtain a uniform mixture. Witch hazel, calendula and trollflower can obviously improve water content of the skin and has lasting moisture retention and oil control effects.

Description

A kind of control fat liquor and preparation method thereof
Technical field
The invention belongs to skin care field, particularly relate to a kind of control fat liquor and preparation method thereof.
Background technology
Control oil refers to the fat content of adjustment skin secretion.No matter be neutral skin, or oiliness, mixed skin, generally all can be fuel-displaced, and easily fuel-displaced place is exactly T district.General control oil method washes one's face with control oil product and duty exactly.Have the people of the oiliness skin of 80% all to there is the phenomenon of hydropenia, this vigorous oil quantity well can be hidden the situation of skin hydropenia.If you are eternal control oil when skin protection, and not supplementing moisture content to skin, the startup that the balance sysmte in health will be spontaneous, skin can constantly secrete more oils and fats, supplement a large amount of oils and fats run off with this, skin also can be allowed to become more and more oil.Further, also need in fat secretion process to consume a large amount of moisture content, what high temperature caused sweats in a large number, all may increase the weight of the water shortage status of skin.
Chinese patent application 200780034885 discloses a kind of emulsion, this product can be the form of sunscreen product or cosmetics, and the method for producing described product is provided, and comprise the formula of this emulsion type products and active component, in addition, the application as sunscreen product of described emulsion types product and at least one sunscreen composition is comprised.The emulsion sun-proof result of this patent application is good, but wherein with the addition of oil components, can produce greasy feeling while strengthening moisturizing and sun-proof result.
Chinese patent application 201410112391 discloses natural plant sun emulsion, it is natural plants Folium Pini, Aloe, Radix Scutellariae, the liquid that spirulina and Rhizoma Phragmitis rutin mixed extract and daily use chemicals heating raw materials are made, there is multiple energy accelerated cell growth, promote tissue repair, regeneration, wound healing, excellent nutrition Glycerin, moisturizing, antiallergic, Sun-proof, anti-ultraviolet burning to skin, solar control dermatitis, face mite and bacteriological infection, effectively sun-proof, promote skin metabolism, reduce wrinkle of skin, strengthen skin elasticity and gloss, skin protection, the several physiological active substances of beauty treatment.Effectively play the natural anti-Exposure to Sunlight of natural plants, the cosmetology effect of anti-ultraviolet.This patent application is mixed by multiple emulsion, but wherein too much containing active component, comparatively glutinous greasy after using, and controls oily DeGrain.
Summary of the invention
The present invention is directed to the deficiencies in the prior art, provide a kind of control fat liquor and preparation method thereof, the oil-control ability of control fat liquor is strong, and control oil is lasting.
The present invention is by the following technical solutions:
A kind of control fat liquor, comprises the raw material of following parts by weight: Radix Hamamelidis Mollis 40 ~ 80 parts, Flos Inulae 20 ~ 75 parts, Flos Trollii 20 ~ 40 parts, lauroyl both sexes base diethyl potassium sorbate 20 ~ 40 parts, potassium sorbate 10 ~ 25 parts, Chinese liquor 5 ~ 15 parts, sodium soap 20 ~ 40 parts, Oleum Caryophylli 20 ~ 65 parts, amniotic fluid 20 ~ 30 parts, thiamine 10 ~ 30 parts, potassium palmitate 30 ~ 50 parts, spermol 20 ~ 70 parts, glycerol 40 ~ 80 parts, water-soluble polymer 50 ~ 90 parts.
As preferably, comprise the raw material of following parts by weight: Radix Hamamelidis Mollis 60 parts, Flos Inulae 55 parts, Flos Trollii 30 parts, lauroyl both sexes base diethyl potassium sorbate 30 parts, potassium sorbate 15 parts, Chinese liquor 10 parts, sodium soap 30 parts, Oleum Caryophylli 45 parts, amniotic fluid 25, thiamine 20 parts, potassium palmitate 40 parts, spermol 45 parts, glycerol 60 parts, water-soluble polymer 70 parts.
As preferably, water-soluble polymer is the one in methylcellulose, ethyl cellulose or sodium carboxymethyl cellulose.
As preferably, the alcoholic strength of Chinese liquor is 10 ~ 20%.
The preparation method of above-mentioned control fat liquor, comprises the following steps:
(1) Radix Hamamelidis Mollis, Flos Inulae, Flos Trollii are put into Chinese liquor and soaked 5 ~ 10h, soak is for subsequent use;
(2) pick up Radix Hamamelidis Mollis, Flos Inulae, Flos Trollii be crushed to 300 ~ 400 orders, add lauroyl both sexes base diethyl potassium sorbate potassium sorbate, sodium soap, spermol, glycerol, water-soluble polymer, be heated to 90 ~ 100 DEG C and stir;
(3) soak for subsequent use of step (1) adds step (2), mixed at high speed, and then mix homogeneously in 10min adds Oleum Caryophylli, amniotic fluid, thiamine, potassium palmitate, mix homogeneously.
As preferably, step (1) soak time is 8 hours.
As preferably, step (3) mixing speed is 1000 ~ 2000r/min.
As preferably, step (3) mix homogeneously in 2 ~ 3min.
Principle: Radix Hamamelidis Mollis, Flos Inulae, lily feet pollen add improve emulsion moistening effect while significantly improve it and control oily effect.The active component of Radix Hamamelidis Mollis, Flos Inulae, Flos Trollii fully dissolves in Chinese liquor, controls oil pump capacity.
technique effect
Present invention adds the control fat liquor of Radix Hamamelidis Mollis, Flos Inulae, Flos Trollii powder, the moisture of skin can be made to significantly improve, and lasting and control is oily effective, experimentally known, 1h can keep water humidity substantially constant, and control oil effect during three's immixture is best.
Detailed description of the invention
Further illustrate the present invention below by specific embodiment, but be not limited to this.
embodiment 1
A kind of control fat liquor, comprises the raw material of following parts by weight: Radix Hamamelidis Mollis 40 parts, Flos Inulae 20 parts, Flos Trollii 20 parts, lauroyl both sexes base diethyl potassium sorbate 20 parts, potassium sorbate 10 parts, Chinese liquor 5 parts, sodium soap 20 parts, Oleum Caryophylli 20 parts, amniotic fluid 20 parts, thiamine 10 parts, potassium palmitate 30 parts, spermol 20 parts, glycerol 40 parts, water-soluble polymer 50 parts.
Water-soluble polymer is methylcellulose.
The alcoholic strength of Chinese liquor is 10%.
The preparation method of above-mentioned control fat liquor, comprises the following steps:
(1) Radix Hamamelidis Mollis, Flos Inulae, Flos Trollii are put into Chinese liquor and soaked 5h, soak is for subsequent use;
(2) pick up Radix Hamamelidis Mollis, Flos Inulae, Flos Trollii be crushed to 300 orders, add lauroyl both sexes base diethyl potassium sorbate potassium sorbate, sodium soap, spermol, glycerol, water-soluble polymer, be heated to 90 DEG C and stir;
(3) soak for subsequent use of step (1) adds step (2), mixed at high speed, and then mix homogeneously in 10min adds Oleum Caryophylli, amniotic fluid, thiamine, potassium palmitate, mix homogeneously.Mixing speed is 1000r/min.
embodiment 2
A kind of control fat liquor, comprises the raw material of following parts by weight: Radix Hamamelidis Mollis 80 parts, Flos Inulae 75 parts, Flos Trollii 40 parts, lauroyl both sexes base diethyl potassium sorbate 40 parts, potassium sorbate 25 parts, Chinese liquor 15 parts, sodium soap 40 parts, Oleum Caryophylli 65 parts, amniotic fluid 30 parts, thiamine 30 parts, potassium palmitate 50 parts, spermol 70 parts, glycerol 80 parts, water-soluble polymer 90 parts.
Water-soluble polymer is sodium carboxymethyl cellulose.
The alcoholic strength of Chinese liquor is 20%.
The preparation method of above-mentioned control fat liquor, comprises the following steps:
(1) Radix Hamamelidis Mollis, Flos Inulae, Flos Trollii are put into Chinese liquor and soaked 10h, soak is for subsequent use;
(2) pick up Radix Hamamelidis Mollis, Flos Inulae, Flos Trollii be crushed to 400 orders, add lauroyl both sexes base diethyl potassium sorbate potassium sorbate, sodium soap, spermol, glycerol, water-soluble polymer, be heated to 100 DEG C and stir;
(3) soak for subsequent use of step (1) adds step (2), mixed at high speed, and then mix homogeneously in 10min adds Oleum Caryophylli, amniotic fluid, thiamine, potassium palmitate, mix homogeneously.Mixing speed is 2000r/min.
embodiment 3
A kind of control fat liquor, comprises the raw material of following parts by weight: Radix Hamamelidis Mollis 60 parts, Flos Inulae 55 parts, Flos Trollii 30 parts, lauroyl both sexes base diethyl potassium sorbate 30 parts, potassium sorbate 15 parts, Chinese liquor 10 parts, sodium soap 30 parts, Oleum Caryophylli 45 parts, amniotic fluid 25, thiamine 20 parts, potassium palmitate 40 parts, spermol 45 parts, glycerol 60 parts, water-soluble polymer 70 parts.
Water-soluble polymer is ethyl cellulose.
The alcoholic strength of Chinese liquor is 15%.
The preparation method of above-mentioned control fat liquor, comprises the following steps:
(1) Radix Hamamelidis Mollis, Flos Inulae, Flos Trollii are put into Chinese liquor and soaked 8h, soak is for subsequent use;
(2) pick up Radix Hamamelidis Mollis, Flos Inulae, Flos Trollii be crushed to 350 orders, add lauroyl both sexes base diethyl potassium sorbate potassium sorbate, sodium soap, spermol, glycerol, water-soluble polymer, be heated to 95 DEG C and stir;
(3) soak for subsequent use of step (1) adds step (2), mixed at high speed, and then mix homogeneously in 10min adds Oleum Caryophylli, amniotic fluid, thiamine, potassium palmitate, mix homogeneously.Mixing speed is 1500r/min.
embodiment 4
A kind of control fat liquor, comprises the raw material of following parts by weight: Radix Hamamelidis Mollis 45 parts, Flos Inulae 25 parts, Flos Trollii 25 parts, lauroyl both sexes base diethyl potassium sorbate 25 parts, potassium sorbate 15 parts, Chinese liquor 8 parts, sodium soap 28 parts, Oleum Caryophylli 28 parts, amniotic fluid 28 parts, thiamine 18 parts, potassium palmitate 38 parts, spermol 28 parts, glycerol 48 parts, water-soluble polymer 58 parts.
Water-soluble polymer is sodium carboxymethyl cellulose.
The alcoholic strength of Chinese liquor is 20%.
The preparation method of above-mentioned control fat liquor, comprises the following steps:
(1) Radix Hamamelidis Mollis, Flos Inulae, Flos Trollii are put into Chinese liquor and soaked 10h, soak is for subsequent use;
(2) pick up Radix Hamamelidis Mollis, Flos Inulae, Flos Trollii be crushed to 400 orders, add lauroyl both sexes base diethyl potassium sorbate potassium sorbate, sodium soap, spermol, glycerol, water-soluble polymer, be heated to 100 DEG C and stir;
(3) soak for subsequent use of step (1) adds step (2), mixed at high speed, and then mix homogeneously in 10min adds Oleum Caryophylli, amniotic fluid, thiamine, potassium palmitate, mix homogeneously.Mixing speed is 2000r/min.
embodiment 5
A kind of control fat liquor, comprises the raw material of following parts by weight: Radix Hamamelidis Mollis 70 parts, Flos Inulae 70 parts, Flos Trollii 30 parts, lauroyl both sexes base diethyl potassium sorbate 30 parts, potassium sorbate 20 parts, Chinese liquor 12 parts, sodium soap 32 parts, Oleum Caryophylli 50 parts, amniotic fluid 28 parts, thiamine 18 parts, potassium palmitate 38 parts, spermol 68 parts, glycerol 75 parts, water-soluble polymer 80 parts.
Water-soluble polymer is ethyl cellulose.
The alcoholic strength of Chinese liquor is 15%.
The preparation method of above-mentioned control fat liquor, comprises the following steps:
(1) Radix Hamamelidis Mollis, Flos Inulae, Flos Trollii are put into Chinese liquor and soaked 8h, soak is for subsequent use;
(2) pick up Radix Hamamelidis Mollis, Flos Inulae, Flos Trollii be crushed to 350 orders, add lauroyl both sexes base diethyl potassium sorbate potassium sorbate, sodium soap, spermol, glycerol, water-soluble polymer, be heated to 95 DEG C and stir;
(3) soak for subsequent use of step (1) adds step (2), mixed at high speed, and then mix homogeneously in 10min adds Oleum Caryophylli, amniotic fluid, thiamine, potassium palmitate, mix homogeneously.Mixing speed is 1500r/min.
comparative example 1
Identical with embodiment 1, difference is: omit step (2).
comparative example 2
Identical with embodiment 1, difference is: step (2) only adopts Radix Hamamelidis Mollis to clay into power, and does not add Flos Inulae, Flos Trollii.
performance test
Using buccal as test zone, each product selects 10 people's tests, adopts moisture tester.10min after washed, testing moisture content, as the skin moisture content before test.Then control fat liquor is smeared, testing moisture content after 1min, testing moisture content after 1h.Below average, percentage composition.
Table 1
Test event Embodiment 1 Embodiment 2 Embodiment 3 Comparative example 1 Comparative example 2
Before test 48 45 43 45 42
Smear control fat liquor 1min 85 89 92 62 72
Smear control fat liquor 1h 83 87 90 45 55
Salubrious degree after 1h Clearly, non-greasy Clearly, non-greasy Clearly, non-greasy Greasy More greasy
Conclusion: known according to table 1, the control fat liquor successful of embodiment is better than comparative example, compared with comparative example 1, add the control fat liquor of Radix Hamamelidis Mollis, Flos Inulae, Flos Trollii powder, the moisture of skin can be made to significantly improve, and lasting and control is oily effective, and 1h can keep water humidity substantially constant, comparative example 2 illustrates, control oil effect during three's immixture is best.

Claims (8)

1. control a fat liquor, it is characterized in that: the raw material comprising following parts by weight: Radix Hamamelidis Mollis 40 ~ 80 parts, Flos Inulae 20 ~ 75 parts, Flos Trollii 20 ~ 40 parts, lauroyl both sexes base diethyl potassium sorbate 20 ~ 40 parts, potassium sorbate 10 ~ 25 parts, Chinese liquor 5 ~ 15 parts, sodium soap 20 ~ 40 parts, Oleum Caryophylli 20 ~ 65 parts, amniotic fluid 20 ~ 30 parts, thiamine 10 ~ 30 parts, potassium palmitate 30 ~ 50 parts, spermol 20 ~ 70 parts, glycerol 40 ~ 80 parts, water-soluble polymer 50 ~ 90 parts.
2. one control fat liquor according to claim 1, is characterized in that: the raw material comprising following parts by weight: Radix Hamamelidis Mollis 60 parts, Flos Inulae 55 parts, Flos Trollii 30 parts, lauroyl both sexes base diethyl potassium sorbate 30 parts, potassium sorbate 15 parts, Chinese liquor 10 parts, sodium soap 30 parts, Oleum Caryophylli 45 parts, amniotic fluid 25, thiamine 20 parts, potassium palmitate 40 parts, spermol 45 parts, glycerol 60 parts, water-soluble polymer 70 parts.
3. one control fat liquor according to claim 1, is characterized in that: water-soluble polymer is the one in methylcellulose, ethyl cellulose or sodium carboxymethyl cellulose.
4. one control fat liquor according to claim 1, is characterized in that: the alcoholic strength of Chinese liquor is 10 ~ 20%.
5. a kind of preparation method controlling fat liquor according to claim 1, is characterized in that: comprise the following steps:
(1) Radix Hamamelidis Mollis, Flos Inulae, Flos Trollii are put into Chinese liquor and soaked 5 ~ 10h, soak is for subsequent use;
(2) pick up Radix Hamamelidis Mollis, Flos Inulae, Flos Trollii be crushed to 300 ~ 400 orders, add lauroyl both sexes base diethyl potassium sorbate potassium sorbate, sodium soap, spermol, glycerol, water-soluble polymer, be heated to 90 ~ 100 DEG C and stir;
(3) soak for subsequent use of step (1) adds step (2), mixed at high speed, and then mix homogeneously in 10min adds Oleum Caryophylli, amniotic fluid, thiamine, potassium palmitate, mix homogeneously.
6. a kind of preparation method controlling fat liquor according to claim 5, is characterized in that: step (1) soak time is 8 hours.
7. a kind of preparation method controlling fat liquor according to claim 5, is characterized in that: step (3) mixing speed is 1000 ~ 2000r/min.
8. a kind of preparation method controlling fat liquor according to claim 5, is characterized in that: step (3) mix homogeneously in 2 ~ 3min.
CN201410497390.8A 2014-09-25 2014-09-25 Oil-control emulsion and preparation method thereof Pending CN104306281A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105232363A (en) * 2015-07-29 2016-01-13 朱耀灯 Oil-control refreshing cream and preparation method thereof

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103655329A (en) * 2013-12-10 2014-03-26 林贤文 Cleaning astringent lotion
CN103655410A (en) * 2013-11-20 2014-03-26 青岛晨讯通商贸有限公司 Makeup-removing emulsion

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103655410A (en) * 2013-11-20 2014-03-26 青岛晨讯通商贸有限公司 Makeup-removing emulsion
CN103655329A (en) * 2013-12-10 2014-03-26 林贤文 Cleaning astringent lotion

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
中华人民共和国卫生部: "《化妆品卫生规范》", 31 January 2007 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105232363A (en) * 2015-07-29 2016-01-13 朱耀灯 Oil-control refreshing cream and preparation method thereof

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Application publication date: 20150128