CN104284910B - 利用加热和氧源减少变色的含氟聚合物树脂处理 - Google Patents
利用加热和氧源减少变色的含氟聚合物树脂处理 Download PDFInfo
- Publication number
- CN104284910B CN104284910B CN201380023540.5A CN201380023540A CN104284910B CN 104284910 B CN104284910 B CN 104284910B CN 201380023540 A CN201380023540 A CN 201380023540A CN 104284910 B CN104284910 B CN 104284910B
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- CN
- China
- Prior art keywords
- fluoropolymer
- fluoropolymer resin
- reactor
- ptfe
- tfe
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F114/00—Homopolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen
- C08F114/18—Monomers containing fluorine
- C08F114/26—Tetrafluoroethene
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F214/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen
- C08F214/18—Monomers containing fluorine
- C08F214/26—Tetrafluoroethene
- C08F214/262—Tetrafluoroethene with fluorinated vinyl ethers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F8/00—Chemical modification by after-treatment
- C08F8/06—Oxidation
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F2800/00—Copolymer characterised by the proportions of the comonomers expressed
- C08F2800/20—Copolymer characterised by the proportions of the comonomers expressed as weight or mass percentages
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F6/00—Post-polymerisation treatments
- C08F6/006—Removal of residual monomers by chemical reaction, e.g. scavenging
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F6/00—Post-polymerisation treatments
- C08F6/14—Treatment of polymer emulsions
- C08F6/22—Coagulation
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F6/00—Post-polymerisation treatments
- C08F6/26—Treatment of polymers prepared in bulk also solid polymers or polymer melts
- C08F6/28—Purification
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Polymerisation Methods In General (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201261644664P | 2012-05-09 | 2012-05-09 | |
| US61/644664 | 2012-05-09 | ||
| PCT/US2013/039372 WO2013169573A1 (en) | 2012-05-09 | 2013-05-03 | Fluoropolymer resin treatment employing heating and oxygen source to reduce discoloration |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104284910A CN104284910A (zh) | 2015-01-14 |
| CN104284910B true CN104284910B (zh) | 2017-12-15 |
Family
ID=48428703
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201380023540.5A Active CN104284910B (zh) | 2012-05-09 | 2013-05-03 | 利用加热和氧源减少变色的含氟聚合物树脂处理 |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US9175115B2 (https=) |
| EP (1) | EP2847236B1 (https=) |
| JP (1) | JP6280917B2 (https=) |
| CN (1) | CN104284910B (https=) |
| WO (1) | WO2013169573A1 (https=) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US9646268B1 (en) * | 2011-06-16 | 2017-05-09 | Brunswick Corporation | Systems and methods of supporting a product life cycle management (PLM) implementation |
| US9175110B2 (en) * | 2012-05-09 | 2015-11-03 | The Chemours Company Fc, Llc | Fluoropolymer resin treatment employing melt extrusion and exposure to oxygen source to reduce discoloration |
| JP6135753B2 (ja) * | 2013-03-27 | 2017-05-31 | 旭硝子株式会社 | 末端基変換方法および末端安定化方法 |
| JP6801429B2 (ja) * | 2016-12-19 | 2020-12-16 | 東ソー株式会社 | 超高分子量ポリエチレンパウダー及びその製造方法 |
| WO2019031617A1 (ja) | 2017-08-10 | 2019-02-14 | ダイキン工業株式会社 | 精製ポリテトラフルオロエチレン水性分散液の製造方法、改質ポリテトラフルオロエチレン粉末の製造方法、ポリテトラフルオロエチレン成形体の製造方法、及び、組成物 |
| SG11202000862YA (en) | 2017-08-10 | 2020-02-27 | Daikin Ind Ltd | Method for producing purified polytetrafluoroethylene aqueous dispersion liquid, method for producing modified polytetrafluoroethylene powder, method for producing polytetrafluoroethylene molded body, and composition |
| CN111675814B (zh) * | 2020-04-27 | 2022-06-07 | 山东东岳高分子材料有限公司 | 一种高流动氟树脂浆料及其制备方法 |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3700627A (en) * | 1970-05-25 | 1972-10-24 | Pennwalt Corp | Decolorized polytetrafluoroethylene |
| EP1043353A1 (en) * | 1997-12-25 | 2000-10-11 | Daikin Industries, Ltd. | Method for modifying fluoropolymer |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE462019A (https=) * | 1943-10-25 | |||
| US2784170A (en) | 1953-04-23 | 1957-03-05 | Union Carbide & Carbon Corp | Heat-stabilized polychlorotrifluoro-ethylene utilizing metal nitrites |
| FR1140964A (fr) | 1956-01-04 | 1957-08-22 | Pechiney | Perfectionnement aux polymères d'oléfines fluorées et chlorofluorées |
| FR1143777A (fr) | 1956-02-22 | 1957-10-04 | Electro Chimie Soc D | Procédé d'amélioration des polymères fluorés |
| NL121076C (https=) | 1959-05-05 | |||
| US3282875A (en) | 1964-07-22 | 1966-11-01 | Du Pont | Fluorocarbon vinyl ether polymers |
| US3391099A (en) | 1966-04-25 | 1968-07-02 | Du Pont | Polymerization process |
| JPS4538906B1 (https=) | 1967-12-27 | 1970-12-08 | Daikin Ind Ltd | |
| FR1600355A (https=) | 1968-01-18 | 1970-07-20 | ||
| FR2042250A5 (https=) | 1969-04-01 | 1971-02-05 | Du Pont | |
| US4036802A (en) | 1975-09-24 | 1977-07-19 | E. I. Du Pont De Nemours And Company | Tetrafluoroethylene copolymer fine powder resin |
| US4358545A (en) | 1980-06-11 | 1982-11-09 | The Dow Chemical Company | Sulfonic acid electrolytic cell having flourinated polymer membrane with hydration product less than 22,000 |
| US4552631A (en) | 1983-03-10 | 1985-11-12 | E. I. Du Pont De Nemours And Company | Reinforced membrane, electrochemical cell and electrolysis process |
| US4626587A (en) | 1984-01-16 | 1986-12-02 | E. I. Du Pont De Nemours And Company | Extrusion finishing of perfluorinated copolymers |
| US4743658A (en) | 1985-10-21 | 1988-05-10 | E. I. Du Pont De Nemours And Company | Stable tetrafluoroethylene copolymers |
| US4675380A (en) | 1985-10-25 | 1987-06-23 | E. I. Du Pont De Nemours And Company | Melt-processible tetrafluoroethylene/perfluoroolefin copolymer granules and processes for preparing them |
| US4940525A (en) | 1987-05-08 | 1990-07-10 | The Dow Chemical Company | Low equivalent weight sulfonic fluoropolymers |
| GB9017156D0 (en) | 1990-08-03 | 1990-09-19 | Ici Plc | Stabilisation of fluoropolymers |
| US5277943A (en) * | 1992-06-30 | 1994-01-11 | Pall Corporation | Thermal bleaching process for non-contaminating fluorocarbon fiber media |
| TW272214B (https=) | 1993-03-26 | 1996-03-11 | Hercules Inc | |
| US5391709A (en) | 1993-11-17 | 1995-02-21 | E. I. Du Pont De Nemours And Company | Purification process of PTFE using fiber bed and heated air |
| US5637748A (en) | 1995-03-01 | 1997-06-10 | E. I. Du Pont De Nemours And Company | Process for synthesizing fluorinated nitrile compounds |
| US5703185A (en) | 1995-08-17 | 1997-12-30 | E. I. Du Pont De Nemours And Company | Fluoropolymer extrusion process |
| US5859086A (en) * | 1996-08-07 | 1999-01-12 | Competitive Technologies Of Pa, Inc. | Light directed modification fluoropolymers |
| JP3852136B2 (ja) | 1996-09-09 | 2006-11-29 | ダイキン工業株式会社 | 含フッ素重合体の安定化方法 |
| US6664337B2 (en) | 1996-09-09 | 2003-12-16 | Daikin Industries, Ltd. | Method for stabilizing fluorine-containing polymer |
| US5866711A (en) | 1996-09-13 | 1999-02-02 | E. I. Du Pont De Nemours And Company | Fluorocyanate and fluorocarbamate monomers and polymers thereof |
| US5969067A (en) | 1996-09-13 | 1999-10-19 | E.I. Dupont De Nemours And Company | Phosphorus-containing fluoromonomers and polymers thereof |
| US6689833B1 (en) | 1997-04-09 | 2004-02-10 | E. I. Du Pont De Nemours And Company | Fluoropolymer stabilization |
| JPH11100543A (ja) | 1997-09-29 | 1999-04-13 | Daikin Ind Ltd | 塗料組成物 |
| JP4792612B2 (ja) | 1998-11-04 | 2011-10-12 | ダイキン工業株式会社 | 含フッ素重合体の安定化方法 |
| EP1054023A1 (fr) | 1999-05-21 | 2000-11-22 | Atofina | Procédé de modification chimique de polymères fluorés électrodes de batterie lithium-ion et revètement de substrats métallique comportant ces polymères ainsi modifiés |
| JP2003082020A (ja) | 2001-09-11 | 2003-03-19 | Daikin Ind Ltd | 含フッ素重合体の製造方法 |
| FR2842203A1 (fr) | 2002-07-12 | 2004-01-16 | Atofina | Procede de fabrication du polymere du fluorure de vinylidene |
| US6875902B2 (en) | 2002-11-06 | 2005-04-05 | National Institute Of Advanced Industrial Science And Technology | Method decomposing fluorine-containing organic material |
| US6838545B2 (en) * | 2002-11-08 | 2005-01-04 | E. I. Du Pont De Nemours And Company | Reaction of fluoropolymer melts |
| US20070129500A1 (en) | 2003-09-10 | 2007-06-07 | Eiji Honda | Stabilized fluoropolymer and method for producing same |
| JPWO2005033150A1 (ja) | 2003-10-01 | 2007-11-15 | ダイキン工業株式会社 | 含フッ素重合体組成物製造方法及び含フッ素重合体組成物 |
| US7790041B2 (en) | 2004-08-11 | 2010-09-07 | E.I. Du Pont De Nemours And Company | Removing fluorosurfactant from aqueous fluoropolymer dispersions |
| US7671111B2 (en) | 2005-02-10 | 2010-03-02 | E.I. Du Pont De Nemours And Company | Monitoring column breakthrough in a process for removing fluorosurfactant from aqueous fluoropolymer dispersions |
| ITMI20050705A1 (it) | 2005-04-20 | 2006-10-21 | Solvay Solexis Spa | Processo per la preparazione di dispersori di fluoropolimeri |
| CN101243108B (zh) | 2005-08-08 | 2012-08-22 | 阿科玛股份有限公司 | 使用非氟化的表面活性剂聚合含氟聚合物 |
| WO2007061914A1 (en) | 2005-11-18 | 2007-05-31 | E.I. Du Pont De Nemours And Company | Core/shell polymer |
| EP1845116A1 (en) | 2006-04-11 | 2007-10-17 | Solvay Solexis S.p.A. | Fluoropolymer dispersion purification |
| JP2010229163A (ja) | 2007-07-24 | 2010-10-14 | Daikin Ind Ltd | 精製含フッ素ポリマーの製造方法 |
| WO2009020187A1 (ja) | 2007-08-07 | 2009-02-12 | Daikin Industries, Ltd. | 低分子量ポリテトラフルオロエチレン水性分散液、低分子量ポリテトラフルオロエチレン粉末及び低分子量ポリテトラフルオロエチレンの製造方法 |
| CN102066307A (zh) | 2008-06-24 | 2011-05-18 | 旭硝子株式会社 | 含氟化合物的精制方法 |
| US20130303717A1 (en) | 2012-05-09 | 2013-11-14 | E I Du Pont De Nemours And Company | Fluoropolymer Dispersion Treatment Employing Oxidizing Agent to Reduce Fluoropolymer Resin Discoloration |
-
2013
- 2013-05-02 US US13/875,337 patent/US9175115B2/en active Active
- 2013-05-03 JP JP2015511544A patent/JP6280917B2/ja active Active
- 2013-05-03 EP EP13722250.1A patent/EP2847236B1/en active Active
- 2013-05-03 WO PCT/US2013/039372 patent/WO2013169573A1/en not_active Ceased
- 2013-05-03 CN CN201380023540.5A patent/CN104284910B/zh active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3700627A (en) * | 1970-05-25 | 1972-10-24 | Pennwalt Corp | Decolorized polytetrafluoroethylene |
| EP1043353A1 (en) * | 1997-12-25 | 2000-10-11 | Daikin Industries, Ltd. | Method for modifying fluoropolymer |
Also Published As
| Publication number | Publication date |
|---|---|
| EP2847236A1 (en) | 2015-03-18 |
| CN104284910A (zh) | 2015-01-14 |
| JP2015516025A (ja) | 2015-06-04 |
| JP6280917B2 (ja) | 2018-02-14 |
| US20130303715A1 (en) | 2013-11-14 |
| US9175115B2 (en) | 2015-11-03 |
| WO2013169573A1 (en) | 2013-11-14 |
| EP2847236B1 (en) | 2022-01-19 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20171227 Address after: Delaware, USA Patentee after: Como Efsee Co.,Ltd. Address before: Wilmington, Delaware, USA Patentee before: E. I. du Pont de Nemours and Co. |