CN104264475B - A kind of preparation method of Waterproof Breathable silk fabric - Google Patents
A kind of preparation method of Waterproof Breathable silk fabric Download PDFInfo
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- CN104264475B CN104264475B CN201410528987.4A CN201410528987A CN104264475B CN 104264475 B CN104264475 B CN 104264475B CN 201410528987 A CN201410528987 A CN 201410528987A CN 104264475 B CN104264475 B CN 104264475B
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- 239000004744 fabric Substances 0.000 title claims abstract description 90
- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- 238000004544 sputter deposition Methods 0.000 claims abstract description 29
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims abstract description 27
- 238000000034 method Methods 0.000 claims abstract description 20
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 20
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims abstract description 18
- 239000007788 liquid Substances 0.000 claims abstract description 17
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims abstract description 14
- IIZPXYDJLKNOIY-JXPKJXOSSA-N 1-palmitoyl-2-arachidonoyl-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCC\C=C/C\C=C/C\C=C/C\C=C/CCCCC IIZPXYDJLKNOIY-JXPKJXOSSA-N 0.000 claims abstract description 9
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229910021529 ammonia Inorganic materials 0.000 claims abstract description 9
- 239000000787 lecithin Substances 0.000 claims abstract description 9
- 229940067606 lecithin Drugs 0.000 claims abstract description 9
- 235000010445 lecithin Nutrition 0.000 claims abstract description 9
- 238000001755 magnetron sputter deposition Methods 0.000 claims abstract description 9
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 claims abstract description 9
- 125000005375 organosiloxane group Chemical group 0.000 claims abstract description 8
- 229920001343 polytetrafluoroethylene Polymers 0.000 claims abstract description 8
- 239000004810 polytetrafluoroethylene Substances 0.000 claims abstract description 8
- 229910052786 argon Inorganic materials 0.000 claims abstract description 7
- 238000010849 ion bombardment Methods 0.000 claims abstract description 7
- 150000002500 ions Chemical class 0.000 claims abstract description 7
- 238000002386 leaching Methods 0.000 claims abstract description 7
- 229950000845 politef Drugs 0.000 claims abstract description 7
- 238000012545 processing Methods 0.000 claims abstract description 7
- KPUWHANPEXNPJT-UHFFFAOYSA-N disiloxane Chemical class [SiH3]O[SiH3] KPUWHANPEXNPJT-UHFFFAOYSA-N 0.000 claims 1
- 230000003115 biocidal effect Effects 0.000 abstract description 4
- 241000255789 Bombyx mori Species 0.000 description 13
- 238000012360 testing method Methods 0.000 description 9
- 239000011248 coating agent Substances 0.000 description 5
- 238000000576 coating method Methods 0.000 description 5
- 239000000203 mixture Substances 0.000 description 4
- 238000003756 stirring Methods 0.000 description 4
- 238000004078 waterproofing Methods 0.000 description 4
- 239000000835 fiber Substances 0.000 description 3
- 238000011160 research Methods 0.000 description 3
- 230000000844 anti-bacterial effect Effects 0.000 description 2
- 238000003912 environmental pollution Methods 0.000 description 2
- 238000007306 functionalization reaction Methods 0.000 description 2
- 230000002401 inhibitory effect Effects 0.000 description 2
- 239000003960 organic solvent Substances 0.000 description 2
- 241000894006 Bacteria Species 0.000 description 1
- 241000255794 Bombyx mandarina Species 0.000 description 1
- 235000016735 Manihot esculenta subsp esculenta Nutrition 0.000 description 1
- 241000658379 Manihot esculenta subsp. esculenta Species 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 241000283898 Ovis Species 0.000 description 1
- 241000124033 Salix Species 0.000 description 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 210000000170 cell membrane Anatomy 0.000 description 1
- 210000002421 cell wall Anatomy 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 230000006870 function Effects 0.000 description 1
- 208000015181 infectious disease Diseases 0.000 description 1
- 230000002458 infectious effect Effects 0.000 description 1
- 230000003834 intracellular effect Effects 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- 230000000670 limiting effect Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 230000007096 poisonous effect Effects 0.000 description 1
- -1 poly tetrafluoroethylene Polymers 0.000 description 1
- 229940058401 polytetrafluoroethylene Drugs 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 230000028327 secretion Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
Abstract
The invention discloses the preparation method of a kind of Waterproof Breathable silk fabric, comprise the following steps: be stand-by after silk fabric is carried out degumming process；By titanium oxide, organosiloxane, lecithin, propylene glycol, ammonia adds in homogenizer, and high-speed stirred obtains dressing liquid；Being dipped by silk fabric after degumming in above-mentioned dressing liquid, two leaching two bundles, pick-up is 70%；Taking out silk fabric, use cold water wash clean, 70 100 DEG C are dried 10 30min, and 120 150 DEG C bake 5 10min；Silk fabric after processing is placed on the vacuum chamber sample stage of magnetron sputtering apparatus, before sputtering, target is sputtered 5 10min, then with argon ion bombardment PTFE target, the little molecule or the ion that are mainly composed of politef penetrate from target, deposit to silk fabric surface, thus form Waterproof Breathable silk fabric.The Waterproof Breathable silk fabric of the present invention remains the feel of former silk fabric, style and color, and poisture-penetrability is good, also has certain antibiotic property.
Description
Technical field:
The present invention relates to silk fabric technical field of modification, be specifically related to a kind of Waterproof Breathable silkworm
The preparation method of silk fabrics.
Background technology:
Silkworm silk is matured silkworm secretion silk liquid concretionary continuous fiber when cocooing, " the most natural
Silk ".It is as Pilus Caprae seu Ovis, is one of animal fiber of utilizing the earliest of the mankind, according to food
Difference, divides again Bombyxmori Linnaeus, Antherea pernyi Guerin-Meneville, cassava silkworm, wild silkworm, willow silkworm and giant silkworm etc..Silk fabric by
Graceful, comfortable and easy to wear, soft in its outward appearance and be widely loved by the people, but it is raw to be as people
The raising that running water is flat, silk fabric functionalization is required more and more higher by people, and therewith, silkworm silk is knitted
The functionalization finishing technique of thing also grows up, and such as antibiotic finish, acid-proof arrange, uvioresistant
Line arrangement, Waterproof Breathable arrangement etc..
So-called Waterproof Breathable silk fabric, refers to that water does not the most immerse silk fabric,
And the perspiration that human body distributes can be transmitted to the external world by silk fabric as water vapor
A kind of functional fabric.With Waterproof Breathable silk fabric make clothing can meet cold, sleet,
Dress in the vile weathers such as strong wind needs, and also can perspire moisture-inhibiting under bigger labor intensity,
Comfortable and easy to wear, moreover it is possible in chemical, poisonous and infectious environment, to play isolation, filter and moisture-inhibiting is made
With.Therefore, the economic and military developed country such as the U.S., West Europe, Japan all knits Waterproof Breathable
Thing is classified as high-tech product geared to the 21st century, puts into a large amount of material resources, financial resources carry out research and open
Send out, and use the aspects such as the protective garment under mal-condition, gym suit and easy dress successively.Domestic
Also many scientific research institutions are had to research and develop this series products.
The preparation method of Waterproof Breathable silk fabric mainly has following three kinds the most both at home and abroad: (1)
Tight structure silk fabric；(2) wet-process coating silk fabric；(3) laminated film composite silk
Fabric.The commercialization of three of the above method, but still have weak point.Such as, silkworm silk is utilized
Silk fabric water pressure resistance prepared by the tight structure of fabric own is the lowest, and prepared by coating waterproof
Wet silk fabric drapability and flexibility are relatively poor, and moisture permeability is relatively low, and attachment fastness is the most relatively
Difference, Waterproof Breathable silk fabric prepared by laminated film method, due to two-dimensional film drawing process relatively
Complexity, relatively costly.
Summary of the invention:
The present invention provides the preparation method of a kind of Waterproof Breathable silk fabric.This preparation method thus can
Retain the feel of former silk fabric, style and color, and poisture-penetrability is good, also have certain
Antibiotic property.This dry coating, tack is good, difficult drop-off.Sputter coating process does not uses
Organic solvent, non-environmental-pollution problem.
The purpose of the present invention is achieved through the following technical solutions:
The preparation method of a kind of Waterproof Breathable silk fabric, comprises the following steps:
(1) after silk fabric being carried out degumming process stand-by；
(2) by titanium oxide, organosiloxane, lecithin, propylene glycol, ammonia adds at a high speed
In blender, high-speed stirred, obtain dressing liquid；
(3) silk fabric after degumming is dipped in above-mentioned dressing liquid, two leaching two bundles, roll
Remaining rate is 70%；
(4) taking out silk fabric, use cold water wash clean, 70-100 DEG C is dried 10-30min,
120-150 DEG C bakes 5-10min；
(5) silk fabric after processing is placed on the vacuum chamber sample stage of magnetron sputtering apparatus,
Before sputtering, target is sputtered 5-10min, then with argon ion bombardment PTFE target, main component
Little molecule or ion for politef penetrate from target, deposit to silk fabric surface, from
And form Waterproof Breathable silk fabric.
Preferred as technique scheme, the dressing liquid in step (2), in parts by weight,
Including titanium oxide 50 parts, organosiloxane 10 parts, 5 parts of lecithin, propylene glycol 30 parts,
Ammonia 2 parts.
Preferred as technique scheme, the bath raio in step (3) is 1:20-60.
Preferred as technique scheme, in step (5), sputtering time is 60min, target
Away from for 5cm.
Preferred as technique scheme, sputtering equipment used in step (5) is Gao Zhen
Empty magnetron sputtering apparatus Perkin-Elmer 4400.
Preferred as technique scheme, the output of sputtering equipment is 300W.
The beneficial effects of the present invention is: poly tetrafluoroethylene is only deposited on fiber, source textile
Pore structure retained, therefore Waterproof Breathable function can be had concurrently,.This dry coating is for changing
Learning bonding, fastness is good, the transparent the most several microns of thickness of film.And nano oxidized in silk fabric
Titanium can react with bacteria cell wall, cell membrane or intracellular members, thus it is thin to destroy antibacterial
Born of the same parents' metabolism, stops it to breed, and reaches antibacterial purpose.The present invention utilizes sessile drop method to measure contact
The hydrophobicity of silk fabric is checked at angle, and after sputtering, water droplet drops in the contact on silk fabric surface
Angle is 112 °, utilizes Japan's KESF2TL П type precision thermal property tester test, before sputtering
The heat leakage amount of silk fabric be 1.460W/m2K, the heat of the silk fabric after sputtering dissipates
Vector is 1.33W/m2k.This preparation method thus can retain the feel of former silk fabric, style and
Color, and poisture-penetrability is good, also has certain antibiotic property.This dry coating, tack
Good, difficult drop-off.Sputter coating process does not use organic solvent, non-environmental-pollution problem.
Detailed description of the invention:
In order to deepen the understanding of the present invention, below in conjunction with embodiment, the present invention is made the most in detail
Stating, this embodiment is only used for explaining the present invention, is not intended that limiting the scope of the present invention.
Embodiment 1
(1) after silk fabric being carried out degumming process, use cold water wash clean, dry stand-by；
(2) by titanium oxide 50 parts, organosiloxane 5 parts, 2 parts of lecithin, propylene glycol
10 parts, in 2 parts of addition homogenizers of ammonia, stir 5h when 20000 revs/min,
Obtain dressing liquid；
(3) silk fabric after degumming is dipped in above-mentioned dressing liquid, two leaching two bundles, roll
Remaining rate is 70%, and bath raio is 1:20；
(4) taking out silk fabric, use cold water wash clean, 70 DEG C are dried 30min, and 120 DEG C bake
10min；
(5) silk fabric after processing is placed on the vacuum chamber sample stage of magnetron sputtering apparatus,
Sputtering power is 300W, and sputtering time is 30min, with argon ion bombardment PTFE target, main
Little molecule or the ion of wanting composition to be politef penetrate from target, deposit to silk fabric table
Face, thus form Waterproof Breathable silk fabric.
This Waterproof Breathable silk fabric carries out water proofing property and poisture-penetrability test, and test result shows
Showing: after sputtering, it is 120 ° that water droplet drops in the contact angle on silk fabric surface, the silkworm after sputtering
The heat leakage amount of silk fabrics is 1.43W/m2k。
Embodiment 2
(1) after silk fabric being carried out degumming process, use cold water wash clean, dry stand-by；
(2) by titanium oxide 80 parts, organosiloxane 10 parts, 10 parts of lecithin, propylene glycol
30 parts, in 3 parts of addition homogenizers of ammonia, stir 2h when 30000 revs/min,
Obtain dressing liquid；
(3) silk fabric after degumming is dipped in above-mentioned dressing liquid, two leaching two bundles, roll
Remaining rate is 70%, and bath raio is 1:60；
(4) taking out silk fabric, use cold water wash clean, 100 DEG C are dried 10min, 150 DEG C of roastings
Dry 5min；
(5) silk fabric after processing is placed on the vacuum chamber sample stage of magnetron sputtering apparatus,
Sputtering power is 400W, and sputtering time is 20min, with argon ion bombardment PTFE target, main
Little molecule or the ion of wanting composition to be politef penetrate from target, deposit to silk fabric table
Face, thus form Waterproof Breathable silk fabric.
This Waterproof Breathable silk fabric carries out water proofing property and poisture-penetrability test, and test result shows
Showing: after sputtering, it is 119 ° that water droplet drops in the contact angle on silk fabric surface, the silkworm after sputtering
The heat leakage amount of silk fabrics is 1.35W/m2k。
Embodiment 3
(1) after silk fabric being carried out degumming process, use cold water wash clean, dry stand-by；
(2) by titanium oxide 60 parts, organosiloxane 7 parts, 5 parts of lecithin, propylene glycol
20 parts, in 2 parts of addition homogenizers of ammonia, stir 3h when 25000 revs/min,
Obtain dressing liquid；
(3) silk fabric after degumming is dipped in above-mentioned dressing liquid, two leaching two bundles, roll
Remaining rate is 70%, and bath raio is 1:35；
(4) taking out silk fabric, use cold water wash clean, 80 DEG C are dried 15min, and 130 DEG C bake
7min；
(5) silk fabric after processing is placed on the vacuum chamber sample stage of magnetron sputtering apparatus,
Sputtering power is 300W, and sputtering time is 60min, with argon ion bombardment PTFE target, main
Little molecule or the ion of wanting composition to be politef penetrate from target, deposit to silk fabric table
Face, thus form Waterproof Breathable silk fabric.
This Waterproof Breathable silk fabric carries out water proofing property and poisture-penetrability test, and test result shows
Showing: after sputtering, it is 112 ° that water droplet drops in the contact angle on silk fabric surface, the silkworm after sputtering
The heat leakage amount of silk fabrics is 1.33W/m2k。
Embodiment 4
(1) after silk fabric being carried out degumming process, use cold water wash clean, dry stand-by；
(2) by titanium oxide 70 parts, organosiloxane 8 parts, 8 parts of lecithin, propylene glycol
20 parts, in 3 parts of addition homogenizers of ammonia, stir 4h when 28000 revs/min,
Obtain dressing liquid；
(3) silk fabric after degumming is dipped in above-mentioned dressing liquid, two leaching two bundles, roll
Remaining rate is 70%, and bath raio is 1:45；
(4) taking out silk fabric, use cold water wash clean, 90 DEG C are dried 25min, and 140 DEG C bake
9min；
(5) silk fabric after processing is placed on the vacuum chamber sample stage of magnetron sputtering apparatus,
Sputtering power is 500W, and sputtering time is 30min, with argon ion bombardment PTFE target, main
Little molecule or the ion of wanting composition to be politef penetrate from target, deposit to silk fabric table
Face, thus form Waterproof Breathable silk fabric.
This Waterproof Breathable silk fabric carries out water proofing property and poisture-penetrability test, and test result shows
Showing: after sputtering, it is 130 ° that water droplet drops in the contact angle on silk fabric surface, the silkworm after sputtering
The heat leakage amount of silk fabrics is 1.45W/m2k。
Claims (5)
1. the preparation method of a Waterproof Breathable silk fabric, it is characterised in that include following step
Rapid:
(1) after silk fabric being carried out degumming process stand-by；
(2) by titanium oxide, organosiloxane, lecithin, propylene glycol, ammonia adds at a high speed
In blender, high-speed stirred, obtain dressing liquid；
(3) padding in above-mentioned dressing liquid by the silk fabric after degumming, two leachings two are rolled, and roll
Remaining rate is 70%；
(4) taking out silk fabric, use cold water wash clean, 70-100 DEG C is dried 10-30min,
120-150 DEG C bakes 5-10min；
(5) silk fabric after processing is placed on the vacuum chamber sample stage of magnetron sputtering apparatus,
Before sputtering, target is sputtered 5-10min, then with argon ion bombardment PTFE target, main component
Little molecule or ion for politef penetrate from target, deposit to silk fabric surface, from
And form Waterproof Breathable silk fabric.
The preparation method of a kind of Waterproof Breathable silk fabric the most as claimed in claim 1, it is special
Levy and be: the dressing liquid in step (2), in parts by weight, including titanium oxide 50 parts, have
Organic siloxane 10 parts, 5 parts of lecithin, propylene glycol 30 parts, ammonia 2 parts.
The preparation method of a kind of Waterproof Breathable silk fabric the most as claimed in claim 1, it is special
Levy and be: the bath raio in step (3) is 1:20-60.
The preparation method of a kind of Waterproof Breathable silk fabric the most as claimed in claim 1, it is special
Levy and be: sputtering equipment used in step (5) is fine vacuum magnetron sputtering apparatus
Perkin-Elmer 4400。
5. the system of a kind of Waterproof Breathable silk fabric as according to any one of Claims 1-4
Preparation Method, it is characterised in that: the output of sputtering equipment is 300W.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410528987.4A CN104264475B (en) | 2014-10-10 | 2014-10-10 | A kind of preparation method of Waterproof Breathable silk fabric |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201410528987.4A CN104264475B (en) | 2014-10-10 | 2014-10-10 | A kind of preparation method of Waterproof Breathable silk fabric |
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| CN104264475A CN104264475A (en) | 2015-01-07 |
| CN104264475B true CN104264475B (en) | 2016-11-30 |
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| CN106967356A (en) * | 2017-03-29 | 2017-07-21 | 安徽月娇家具有限公司 | A kind of preparation method of novel environment friendly deoderizing waterproof moisture permeating fabric coating agent |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101525844A (en) * | 2009-03-31 | 2009-09-09 | 石狮市亿祥染整有限公司 | Method for producing waterproof moisture permeable fabric |
| CN102444021A (en) * | 2011-08-22 | 2012-05-09 | 翔瑞（泉州）纳米科技有限公司 | Intelligent waterproof and moisture permeable fabric |
| CN202507632U (en) * | 2012-01-04 | 2012-10-31 | 昆山华阳复合材料科技有限公司 | Composite fabric with waterproof and moisture permeable functions |
| CN103866579A (en) * | 2012-12-14 | 2014-06-18 | 东丽纤维研究所（中国）有限公司 | Ventilating waterproof moisture-permeable wet-process coating fabric, and processing method and application thereof |
-
2014
- 2014-10-10 CN CN201410528987.4A patent/CN104264475B/en not_active Expired - Fee Related
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101525844A (en) * | 2009-03-31 | 2009-09-09 | 石狮市亿祥染整有限公司 | Method for producing waterproof moisture permeable fabric |
| CN102444021A (en) * | 2011-08-22 | 2012-05-09 | 翔瑞（泉州）纳米科技有限公司 | Intelligent waterproof and moisture permeable fabric |
| CN202507632U (en) * | 2012-01-04 | 2012-10-31 | 昆山华阳复合材料科技有限公司 | Composite fabric with waterproof and moisture permeable functions |
| CN103866579A (en) * | 2012-12-14 | 2014-06-18 | 东丽纤维研究所（中国）有限公司 | Ventilating waterproof moisture-permeable wet-process coating fabric, and processing method and application thereof |
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Effective date of registration: 20190515 Address after: 226199 No. 1511 Renmin West Road, Haimen Town, Haimen City, Nantong City, Jiangsu Province (Sanhe Industrial Concentration Area) Patentee after: JIANGSU SANLIAN HOUSEHOLD TEXTILE CO., LTD. Address before: 226152 165 South Renmin Road, Hadong Town, Haimen, Nantong, Jiangsu Patentee before: Haimen he d Intellectual Property Service Co. Ltd. |
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