CN107972334A - Medical textile material and preparation method and application - Google Patents

Medical textile material and preparation method and application Download PDF

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Publication number
CN107972334A
CN107972334A CN201711167103.7A CN201711167103A CN107972334A CN 107972334 A CN107972334 A CN 107972334A CN 201711167103 A CN201711167103 A CN 201711167103A CN 107972334 A CN107972334 A CN 107972334A
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China
Prior art keywords
medical
textile material
medical textile
preparation
adhesive
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Pending
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CN201711167103.7A
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Chinese (zh)
Inventor
陶友华
邹明选
余长春
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Anhui Mei Hu New Mstar Technology Ltd
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Anhui Mei Hu New Mstar Technology Ltd
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Priority to CN201711167103.7A priority Critical patent/CN107972334A/en
Publication of CN107972334A publication Critical patent/CN107972334A/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B5/00Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts
    • B32B5/02Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts characterised by structural features of a fibrous or filamentary layer
    • B32B5/022Non-woven fabric
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B27/00Layered products comprising a layer of synthetic resin
    • B32B27/06Layered products comprising a layer of synthetic resin as the main or only constituent of a layer, which is next to another layer of the same or of a different material
    • B32B27/08Layered products comprising a layer of synthetic resin as the main or only constituent of a layer, which is next to another layer of the same or of a different material of synthetic resin
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B27/00Layered products comprising a layer of synthetic resin
    • B32B27/12Layered products comprising a layer of synthetic resin next to a fibrous or filamentary layer
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B27/00Layered products comprising a layer of synthetic resin
    • B32B27/30Layered products comprising a layer of synthetic resin comprising vinyl (co)polymers; comprising acrylic (co)polymers
    • B32B27/302Layered products comprising a layer of synthetic resin comprising vinyl (co)polymers; comprising acrylic (co)polymers comprising aromatic vinyl (co)polymers, e.g. styrenic (co)polymers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B27/00Layered products comprising a layer of synthetic resin
    • B32B27/32Layered products comprising a layer of synthetic resin comprising polyolefins
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B33/00Layered products characterised by particular properties or particular surface features, e.g. particular surface coatings; Layered products designed for particular purposes not covered by another single class
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B5/00Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts
    • B32B5/22Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts characterised by the presence of two or more layers which are next to each other and are fibrous, filamentary, formed of particles or foamed
    • B32B5/24Layered products characterised by the non- homogeneity or physical structure, i.e. comprising a fibrous, filamentary, particulate or foam layer; Layered products characterised by having a layer differing constitutionally or physically in different parts characterised by the presence of two or more layers which are next to each other and are fibrous, filamentary, formed of particles or foamed one layer being a fibrous or filamentary layer
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B7/00Layered products characterised by the relation between layers; Layered products characterised by the relative orientation of features between layers, or by the relative values of a measurable parameter between layers, i.e. products comprising layers having different physical, chemical or physicochemical properties; Layered products characterised by the interconnection of layers
    • B32B7/04Interconnection of layers
    • B32B7/12Interconnection of layers using interposed adhesives or interposed materials with bonding properties
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B2250/00Layers arrangement
    • B32B2250/24All layers being polymeric
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B2262/00Composition or structural features of fibres which form a fibrous or filamentary layer or are present as additives
    • B32B2262/02Synthetic macromolecular fibres
    • B32B2262/0223Vinyl resin fibres
    • B32B2262/023Aromatic vinyl resin, e.g. styrenic (co)polymers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B2262/00Composition or structural features of fibres which form a fibrous or filamentary layer or are present as additives
    • B32B2262/02Synthetic macromolecular fibres
    • B32B2262/0253Polyolefin fibres
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B32LAYERED PRODUCTS
    • B32BLAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B2307/00Properties of the layers or laminate
    • B32B2307/70Other properties
    • B32B2307/726Permeability to liquids, absorption

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Materials For Medical Uses (AREA)

Abstract

The present invention relates to a kind of medical textile material and preparation method and application, medical textile material includes three layers, is followed successively by polypropylene non-woven layer of cloth, thermoplastic elastomer films layer and polypropylene non-woven layer of cloth from top to bottom;Wherein, the thickness of the thermoplastic elastomer films layer is 0.008~0.01mm.High moisture-inhibiting performance of the invention by using thermoplastic elastomer films, the medical textile material with three-decker being prepared is ensureing waterproof, resistant to blood, anti-alcohol and is obstructing outside the safeguard function of bacterial virus, the sweat of human body formation can also be absorbed rapidly, when the medical staff is put on medical surgical gown, Medical operation cap, medical protective garment or the medical isolation clothes processed using this medical textile material, it can keep the dry and comfortable comfortable of body, mitigate fatigue strength caused by work, improve procedure efficiency and quality.

Description

Medical textile material and preparation method and application
Technical field
The present invention relates to medical textile field of material technology, and in particular to a kind of medical textile material and its preparation side Method and application.
Background technology
The material used in medical textile currently on the market mainly has two categories below:PE laminations non-woven fabrics and PE overlay films without Woven fabric, its purpose and function are barrier bacterium and virus, to protect doctor and patient both sides' safety.The structure of PE lamination non-woven fabrics For upper and lower two layers, upper strata is non-woven fabrics, and lower floor is PE films.Its production technology is to pass through screw rod after PE pellet meltings are formed fluid Extrude and uniformly apply to scrape with glued membrane head and form PE protective films after cooling on non-woven fabrics.The structure of PE overlay film non-woven fabrics is upper and lower Two layers, upper strata is non-woven fabrics, and lower floor is PE films.Its production technology is using pressure sensitive adhesive or hot melt adhesive as adhesive, by PE films Pass through combination process pressing and forming with non-woven fabrics.The PE laminations non-woven fabrics and PE overlay films non-woven fabrics of prior art production are main to be lacked It is no moisture-inhibiting function to fall into, manufactured operating coat, operating cap, sheet, hole towel, and human body is coated or contacted during use, human body Sweat and moisture can not discharge, and cause extremely uncomfortable.It is a kind of non-porous film, liquid water and moisture that this defect, which is primarily due to PE films, Can not be by, thus can be permeated with waterproof resistant to blood, but therefore do not have moisture-inhibiting perspiration functions yet.Therefore, it is also desirable to develop new The medical textile material of type.
The content of the invention
For in the prior art the defects of, present invention aims at provide a kind of medical textile material and its preparation side Method, with by using the high moisture-inhibiting performance of thermoplastic elastomer films, the medical textile material with three-decker being prepared Expect ensureing waterproof, resistant to blood, anti-alcohol and obstructing outside the safeguard function of bacterial virus, moreover it is possible to rapid to absorb what human body was formed Sweat, makes medical staff put on the medical surgical gown processed using this medical textile material, Medical operation cap, medical protection When clothes or medical isolation clothes, the dry and comfortable comfortable of body can be kept, mitigates fatigue strength caused by work, improves procedure efficiency and matter Amount.
To achieve the above object, technical solution provided by the invention is:
In a first aspect, the present invention provides a kind of medical textile material, medical textile material includes three layers, from up to Under be followed successively by polypropylene (PP) nonwoven layer, thermoplastic elastomer films layer (TPE) and polypropylene (PP) nonwoven layer;Wherein, it is hot The thickness of thermoplastic elastic film layer is 0.008~0.01mm.It should be noted that thermoplastic elastomer films, i.e. TPE Waterproof Breathables Film is a kind of novel high polymer waterproof material, with polyurethanes (TPU) for main material, imports hydrophilic group, film surface Pore-free, therefore can have excellent infiltration energy.Because there is hydrophilic group, it is conducted through by the attached moisture absorption of absorption-desorption Journey, so that with excellent water vapour permeability.The power of its moisture-inhibiting function comes from:Concentration difference, temperature difference and pressure differential.TPE prevents After the compound PP non-woven fabrics in water moisture permeable membrane both sides, formed three-decker, the TPE waterproof humidity-permeant film thin to dynode play protection and Supporting role so that waterproof resistant to blood splash function can reach PE (polyethylene) the lamination non-woven fabrics property identical with overlay film non-woven fabrics Can index.The thickness of TPE film is 0.008~0.01mm, is that not only can guarantee that water resistance at present but also to take into account water vapour permeability optimal The section of change.
Second aspect, the present invention provides the preparation method of medical textile material, includes the following steps:S1:Will melting Adhesive blade coating or be injected in the surface of polypropylene non-woven fabric protrusion;S2:By thermoplastic elastomer films it is smooth be fitted in by The surface of the polypropylene non-woven fabric of S1 processing, then presses close by pressure roller, and standing makes adhesive moisture curing, obtain half into Product;S3:The adhesive of melting is scratched or is injected in the surface of polypropylene non-woven fabric protrusion;S4:It is fitted in semi-finished product are smooth By the surface of the S3 polypropylene non-woven fabrics handled, then pressed closely by pressure roller, standing makes adhesive moisture curing, obtains Medical textile finished material;Wherein, what is be bonded with the surface of polypropylene non-woven fabric is thermoplastic elastomer films side in semi-finished product Surface.It should be noted that must apply three layers of PP non-woven fabrics, TPE film, PP non-woven fabrics composite machine being combined with each other Scrape or spray-bonding craft.The advantages of both techniques is that spread is minimum, therefore the TPE film surface area blocked is minimum, water vapour permeability Lose minimumization.Wherein, it is uniformly to apply the hot melt adhesive fluid of molten condition using compounding machine gluing die head to scrape to apply and scrape technique The surface of non-woven fabrics protrusion, then be fitted in TPE film is smooth on non-woven fabrics, pressed by pressure roller close.Heated after when 24 is small Glue moisture curing, the semi-finished product after curing repeat above-mentioned technique, another layer of PP non-woven fabrics are fitted in TPE film.It is small by 24 When moisture curing after, new medical textile material i.e. be molded.Spray-bonding craft refers to hot melt adhesive by internal pressure from compounding machine The nozzle of gluing die head quickly sprays collodion silk, uniform and random be distributed in nonwoven surface, then one that TPE film is bonded therewith Kind of gluing complex method, it is identical that other processes with painting scrape method.Connection relation between the component and component of the equipment complex Refer to the attached drawing 2 (hot melt adhesive compounding machine flow sheet).
In the further embodiment of the present invention, medical textile material is to use polyurethane hot melt compounding machine (PUR Hot melt adhesive compounding machine) prepared;In step S2 and step S4, the time of standing is 20~28h, is preferably 24h.
In the further embodiment of the present invention, adhesive includes polyurethane hot melt (PUR hot melt adhesive).
It should be noted that the method that medical textile material is prepared using polyurethane hot melt compounding machine is specifically wrapped Include following steps:S1:Thermoplastic elastomer films (TPE) coiled strip is placed on the first station, film is drawn to the patch of the 4th station At combined pressure roller;Polypropylene (PP) non-woven fabrics coiled strip is placed on the 5th station, PP non-woven fabrics is drawn to blade coating or glue spraying die head Position;The PUR hot melt adhesive of melting is scratched or is injected in the surface of PP non-woven fabrics protrusion;S2:By the PP after blade coating or glue spraying without Woven fabric is drawn to fitting pressure roller, with thermoplastic elastomer films (TPE) film it is smooth be bonded and by pressure roller pressing closely, and draw Wound to second station;Standing makes PUR hot melt adhesive moisture curings, obtains semi-finished product;S3:Semi-finished product are placed on the first station, Semi-finished product are drawn to the fitting pressure roller of the 4th station;Polypropylene (PP) non-woven fabrics coiled strip is placed on the 5th station, by PP Non-woven fabrics is drawn to blade coating or glue spraying die head position;The PUR hot melt adhesive of melting is scratched or is injected in the table of PP non-woven fabrics protrusion Face;S4:PP non-woven fabrics after blade coating or glue spraying is drawn to fitting pressure roller, the table with thermoplastic elastomer films side in semi-finished product Face is smooth to be bonded and is pressed closely by pressure roller, and is drawn to second station and wound;Standing makes PUR hot melt adhesive moisture curings, obtains To medical textile finished material.
In the further embodiment of the present invention, adhesive further includes:Haloflex and polyacrylate material; Wherein, the mass ratio of polyurethane hot melt, haloflex and polyacrylate material is 1:(0.05~0.1):(0.1~ 0.2)。
In the further embodiment of the present invention, the preparation method of polyacrylate material includes the following steps:Will Water, hydroxy-ethyl acrylate and diallyldimethylammonium chloride are with (40~50):1:The mass ratio of (20~30) is uniformly mixed, so After be warming up to 68~70 DEG C, and adjust pH value to 5.4~5.6;Initiator is added, after 10~15min of insulation reaction, continues to heat up To 90~92 DEG C, and pH value is adjusted to 7.3~7.5, methyl acrylate and butyl methacrylate are then added dropwise respectively;Drip 2~2.5h is kept the temperature after finishing, obtains polyacrylate material.
In the further embodiment of the present invention, initiator is dibenzoyl peroxide, initiator, methyl acrylate, The mass ratio of butyl methacrylate and hydroxy-ethyl acrylate is (0.2~0.3):(20~30):(6~8):1.
In the further embodiment of the present invention, polypropylene non-woven fabric is the polypropylene non-woven fabric by pre-processing, in advance Processing specifically includes:Polypropylene non-woven fabric is soaked into 8~10h in soak, then drying at room temperature;Wherein, the system of soak Preparation Method includes the following steps:Heated after the leaf of bamboo, wormwood and ethanol water are mixed, the mixture after heating is filtered, point The first filtrate and filter residue are not collected;Filter residue and water are mixed, pH value is adjusted to 8.5~8.8, then carries out decoction extraction, extract After, filtering, collects the second filtrate;First filtrate and the second filtrate are uniformly mixed, decolorization is then carried out, is soaked Steep liquid.
In the further embodiment of the present invention, the mass ratio of the leaf of bamboo, wormwood and ethanol water is 1:(20~28), The volume fraction of ethanol is 60%~70% in ethanol water, and the temperature of heating is 75~85 DEG C, time of heating for 1~ 2h;The mass ratio of filter residue and water is 1:(10~15), the time for decocting extraction are 20~30min.
The third aspect, the present invention also protect medical textile material preparing medical surgical gown, Medical operation cap, medical anti- Protect the application in clothes, medical isolation clothes, johnny, medical hole towel and medical sheet.
Technical solution provided by the invention, has following beneficial effect:(1) medical textile material provided by the invention Structure include three layers, waterproof resistant to blood permeance property is high, can reach the index of correlation of prior art products, such as water resistance JIS L 1092-1998A standards can be passed through;Resistant to blood and bacterium blocking performance can be marked by ASTM 1670 and ASTM 1671 It is accurate;Its unique water vapour permeability can pass through JIS L1099 standards;(2) medical textile material provided by the invention, by abundant Using the performance of TPE film high moisture-inhibiting, so as at utmost keep the dry and comfortable comfort level of doctor and patient, solves conventional medical spinning When fabric is worn the problem of humid;(3) preparation method of medical textile material provided by the invention is simple, production cost It is low.
The additional aspect and advantage of the present invention will be set forth in part in the description, and will partly become from the following description Obtain substantially, or recognized by the practice of the present invention.
Brief description of the drawings
Fig. 1 is the structure diagram of medical textile material provided by the invention;
Fig. 2 is the flow diagram of the preparation method of medical textile material provided by the invention.
Reference numeral:
The first stations of 1-;2- second stations;3- 3rd stations;The 4th stations of 4-;The 5th stations of 5-;6- thermoplastic elastomer (TPE)s (TPE) film;At 7- windings;8- joint places;At 9- gluings;10- polypropylene (PP) non-woven fabrics.
Embodiment
Below in conjunction with the attached drawing in the embodiment of the present invention, the technical solution in the embodiment of the present invention is carried out clear, complete Site preparation describes.The following examples are only intended to illustrate the technical solution of the present invention more clearly, therefore is intended only as example, without It can be limited the scope of the invention with this.
Experimental method in following embodiments, is conventional method unless otherwise specified.Examination used in following embodiments Material is tested, is to be commercially available from regular shops unless otherwise specified.Quantitative test in following embodiments, is respectively provided with three Secondary to repeat to test, data are the average value or mean+SD of three repeated experiments.
The present invention provides a kind of medical textile material, including three layers, is followed successively by polypropylene non-woven layer of cloth, heat from top to bottom Thermoplastic elastic film layer and polypropylene non-woven layer of cloth;Wherein, the thickness of thermoplastic elastomer films layer is 0.008~0.01mm.
Medical textile material is prepared using polyurethane hot melt compounding machine, is specifically comprised the following steps:
S1:Thermoplastic elastomer films (TPE) coiled strip is placed on the first station, the stroke as shown in attached drawing 2 draws film To the fitting pressure roller of the 4th station;Polypropylene (PP) non-woven fabrics coiled strip is placed on the 5th station, as the stroke shown in attached drawing 2 PP non-woven fabrics is drawn to blade coating or glue spraying die head position;The adhesive of melting is scratched or is injected in the table of PP non-woven fabrics protrusion Face;Wherein, adhesive is polyurethane hot melt.
S2:PP non-woven fabrics after blade coating or glue spraying is drawn to fitting pressure roller, is put down with thermoplastic elastomer films (TPE) film It is whole to be bonded and pressed closely by pressure roller, and draw to second station and wind;20~28h is stood, makes adhesive moisture curing, obtains To semi-finished product.
S3:Semi-finished product are placed on the first station, the stroke as shown in attached drawing 2 draws semi-finished product to the patch of the 4th station At combined pressure roller;Polypropylene (PP) non-woven fabrics coiled strip is placed on the 5th station, the stroke as shown in attached drawing 2 draws PP non-woven fabrics To blade coating or glue spraying die head position;The adhesive of melting is scratched or is injected in the surface of PP non-woven fabrics protrusion;Wherein, adhesive For polyurethane hot melt.
S4:PP non-woven fabrics after blade coating or glue spraying is drawn to fitting pressure roller, with thermoplastic elastomer films in semi-finished product The surfacing of side is bonded and passes through pressure roller pressing closely, and draws to second station and wind;20~28h is stood, makes to glue Mixture moisture curing, obtains medical textile finished material.
Preferably, the adhesive in step S1 and S3 further includes haloflex and polyacrylate material;Polyurethane The mass ratio of hot melt adhesive, haloflex and polyacrylate material is 1:(0.05~0.1):(0.1~0.2);Polypropylene The preparation method of esters of gallic acid material includes the following steps:By water, hydroxy-ethyl acrylate and diallyldimethylammonium chloride with (40 ~50):1:The mass ratio of (20~30) is uniformly mixed, and then heats to 68~70 DEG C, and adjusts pH value to 5.4~5.6;Add Initiator dibenzoyl peroxide, after 10~15min of insulation reaction, is continuously heating to 90~92 DEG C, and adjust pH value to 7.3~ 7.5, be then added dropwise methyl acrylate and butyl methacrylate respectively, initiator, methyl acrylate, butyl methacrylate and The mass ratio of hydroxy-ethyl acrylate is (0.2~0.3):(20~30):(6~8):1;2~2.5h is kept the temperature after being added dropwise, is obtained Polyacrylate material.
Preferably, polypropylene non-woven fabric is to be specifically included by the polypropylene non-woven fabric of pretreatment, pretreatment:By polypropylene Non-woven fabrics soaks 8~10h in soak, then drying at room temperature;Wherein, the preparation method of soak includes the following steps:Will The ethanol water that the leaf of bamboo, wormwood and volume fraction are 60%~70% is with 1:(0.2~0.3):The mass ratio of (20~28) mixes After conjunction, 75~85 DEG C of 1~2h of heating, the mixture after heating is filtered, collects the first filtrate and filter residue respectively;By filter residue and water With 1:The mass ratio mixing of (10~15), adjusts pH value to 8.5~8.8, then carries out decocting 20~30min of extraction, extracted Bi Hou, filtering, collects the second filtrate;First filtrate and the second filtrate are uniformly mixed, decolorization is then carried out, is soaked Liquid.
Medical textile material provided by the invention and preparation method thereof is made furtherly with reference to specific embodiment It is bright.
Embodiment one
The present embodiment provides a kind of medical textile material, including three layers, be followed successively by from top to bottom polypropylene non-woven layer of cloth, Thermoplastic elastomer films layer and polypropylene non-woven layer of cloth;Wherein, the thickness of thermoplastic elastomer films layer is 0.01mm.
Medical textile material is prepared using polyurethane hot melt compounding machine, is specifically comprised the following steps:
S1:Thermoplastic elastomer films (TPE) coiled strip is placed on the first station, the stroke as shown in attached drawing 2 draws film To the fitting pressure roller of the 4th station;Polypropylene (PP) non-woven fabrics coiled strip is placed on the 5th station, as the stroke shown in attached drawing 2 PP non-woven fabrics is drawn to blade coating die head position;The adhesive of melting is scratched or is injected in the surface of PP non-woven fabrics protrusion;Its In, adhesive is polyurethane hot melt.
S2:PP non-woven fabrics after blade coating is drawn to fitting pressure roller, and thermoplastic elastomer films (TPE) film is smooth is bonded And it is close by pressure roller pressing, and draw to second station and wind;24h is stood, makes adhesive moisture curing, obtains semi-finished product.
S3:Semi-finished product are placed on the first station, the stroke as shown in attached drawing 2 draws semi-finished product to the patch of the 4th station At combined pressure roller;Polypropylene (PP) non-woven fabrics coiled strip is placed on the 5th station, the stroke as shown in attached drawing 2 draws PP non-woven fabrics To blade coating die head position;The adhesive of melting is scratched or is injected in the surface of PP non-woven fabrics protrusion;Wherein, adhesive is poly- ammonia Ester hot melt adhesive.
S4:PP non-woven fabrics after blade coating is drawn to fitting pressure roller, the table with thermoplastic elastomer films side in semi-finished product Face is smooth to be bonded and is pressed closely by pressure roller, and is drawn to second station and wound;24h is stood, consolidates adhesive moisture absorption Change, obtain medical textile finished material.
Embodiment two
The present embodiment provides a kind of medical textile material, including three layers, be followed successively by from top to bottom polypropylene non-woven layer of cloth, Thermoplastic elastomer films layer and polypropylene non-woven layer of cloth;Wherein, the thickness of thermoplastic elastomer films layer is 0.01mm.
Medical textile material is prepared using polyurethane hot melt compounding machine, is specifically comprised the following steps:
S1:Thermoplastic elastomer films (TPE) coiled strip is placed on the first station, the stroke as shown in attached drawing 2 draws film To the fitting pressure roller of the 4th station;Polypropylene (PP) non-woven fabrics coiled strip is placed on the 5th station, as the stroke shown in attached drawing 2 PP non-woven fabrics is drawn to blade coating die head position;The adhesive of melting is scratched or is injected in the surface of PP non-woven fabrics protrusion;Its In, adhesive is polyurethane hot melt, haloflex and polyacrylate material with 1:0.05:0.1 mass ratio mixing The product uniformly obtained;The preparation method of polyacrylate material includes the following steps:By water, hydroxy-ethyl acrylate and diene Diallyidimethylammonium chloride is with 40:1:20 mass ratio is uniformly mixed, and then heats to 68 DEG C, and adjusts pH value to 5.4;Add Initiator dibenzoyl peroxide, after insulation reaction 10min, is continuously heating to 90 DEG C, and adjusts pH value to 7.3, then distinguishes Methyl acrylate and butyl methacrylate, initiator, methyl acrylate, butyl methacrylate and hydroxy-ethyl acrylate is added dropwise Mass ratio be 0.2:20:6:1;2h is kept the temperature after being added dropwise, obtains polyacrylate material.
S2:PP non-woven fabrics after blade coating is drawn to fitting pressure roller, and thermoplastic elastomer films (TPE) film is smooth is bonded And it is close by pressure roller pressing, and draw to second station and wind;24h is stood, makes adhesive moisture curing, obtains semi-finished product.
S3:Semi-finished product are placed on the first station, the stroke as shown in attached drawing 2 draws semi-finished product to the patch of the 4th station At combined pressure roller;Polypropylene (PP) non-woven fabrics coiled strip is placed on the 5th station, the stroke as shown in attached drawing 2 draws PP non-woven fabrics To blade coating die head position;The adhesive of melting is scratched or is injected in the surface of PP non-woven fabrics protrusion;Wherein, the same step of adhesive Adhesive in S1.
S4:PP non-woven fabrics after blade coating is drawn to fitting pressure roller, the table with thermoplastic elastomer films side in semi-finished product Face is smooth to be bonded and is pressed closely by pressure roller, and is drawn to second station and wound;24h is stood, consolidates adhesive moisture absorption Change, obtain medical textile finished material.
Embodiment three
The present embodiment provides a kind of medical textile material, including three layers, be followed successively by from top to bottom polypropylene non-woven layer of cloth, Thermoplastic elastomer films layer and polypropylene non-woven layer of cloth;Wherein, the thickness of thermoplastic elastomer films layer is 0.01mm.
Medical textile material is prepared using polyurethane hot melt compounding machine, is specifically comprised the following steps:
S1:Thermoplastic elastomer films (TPE) coiled strip is placed on the first station, the stroke as shown in attached drawing 2 draws film To the fitting pressure roller of the 4th station;Polypropylene (PP) non-woven fabrics coiled strip is placed on the 5th station, as the stroke shown in attached drawing 2 PP non-woven fabrics is drawn to blade coating die head position;The adhesive of melting is scratched or is injected in the surface of PP non-woven fabrics protrusion;Its In, adhesive is polyurethane hot melt, haloflex and polyacrylate material with 1:0.1:0.2 mass ratio mixing is equal Even obtained product;The preparation method of polyacrylate material includes the following steps:By water, hydroxy-ethyl acrylate and two allyls Base alkyl dimethyl ammonium chloride is with 50:1:30 mass ratio is uniformly mixed, and then heats to 70 DEG C, and adjusts pH value to 5.6;Addition is drawn Agent dibenzoyl peroxide is sent out, after insulation reaction 15min, is continuously heating to 92 DEG C, and adjusts pH value to 7.5, is then dripped respectively Add methyl acrylate and butyl methacrylate, initiator, methyl acrylate, butyl methacrylate and hydroxy-ethyl acrylate Mass ratio is 0.3:30:8:1;2.5h is kept the temperature after being added dropwise, obtains polyacrylate material.
S2:PP non-woven fabrics after blade coating is drawn to fitting pressure roller, and thermoplastic elastomer films (TPE) film is smooth is bonded And it is close by pressure roller pressing, and draw to second station and wind;24h is stood, makes adhesive moisture curing, obtains semi-finished product.
S3:Semi-finished product are placed on the first station, the stroke as shown in attached drawing 2 draws semi-finished product to the patch of the 4th station At combined pressure roller;Polypropylene (PP) non-woven fabrics coiled strip is placed on the 5th station, the stroke as shown in attached drawing 2 draws PP non-woven fabrics To blade coating die head position;The adhesive of melting is scratched or is injected in the surface of PP non-woven fabrics protrusion;Wherein, the same step of adhesive Adhesive in S1.
S4:PP non-woven fabrics after blade coating is drawn to fitting pressure roller, the table with thermoplastic elastomer films side in semi-finished product Face is smooth to be bonded and is pressed closely by pressure roller, and is drawn to second station and wound;24h is stood, consolidates adhesive moisture absorption Change, obtain medical textile finished material.
Example IV
The present embodiment provides a kind of medical textile material, including three layers, be followed successively by from top to bottom polypropylene non-woven layer of cloth, Thermoplastic elastomer films layer and polypropylene non-woven layer of cloth;Wherein, the thickness of thermoplastic elastomer films layer is 0.01mm.
Medical textile material is prepared using polyurethane hot melt compounding machine, is specifically comprised the following steps:
S1:Thermoplastic elastomer films (TPE) coiled strip is placed on the first station, the stroke as shown in attached drawing 2 draws film To the fitting pressure roller of the 4th station;Polypropylene (PP) non-woven fabrics coiled strip is placed on the 5th station, as the stroke shown in attached drawing 2 PP non-woven fabrics is drawn to blade coating die head position;The adhesive of melting is scratched or is injected in the surface of PP non-woven fabrics protrusion;
Wherein, adhesive is polyurethane hot melt, haloflex and polyacrylate material with 1:0.05:0.1 The product that mass ratio is uniformly mixed;The preparation method of polyacrylate material includes the following steps:By water, acrylic acid hydroxyl Ethyl ester and diallyldimethylammonium chloride are with 40:1:20 mass ratio is uniformly mixed, and then heats to 68 DEG C, and adjust pH value To 5.4;Add initiator dibenzoyl peroxide, after insulation reaction 10min, be continuously heating to 90 DEG C, and adjust pH value to 7.3, be then added dropwise methyl acrylate and butyl methacrylate respectively, initiator, methyl acrylate, butyl methacrylate and The mass ratio of hydroxy-ethyl acrylate is 0.2:20:6:1;2h is kept the temperature after being added dropwise, obtains polyacrylate material;
Polypropylene non-woven fabric is to be specifically included by the polypropylene non-woven fabric of pretreatment, pretreatment:By polypropylene non-woven fabric 8h is soaked in soak, then drying at room temperature;Wherein, the preparation method of soak includes the following steps:By the leaf of bamboo, wormwood and The ethanol water that volume fraction is 60% is with 1:0.2:After 20 mass ratio mixing, 75 DEG C of heating 1h, by the mixing after heating Thing filters, and collects the first filtrate and filter residue respectively;By filter residue and water with 1:10 mass ratio mixing, adjusting pH value to 8.5, then Carry out decocting extraction 20min, after extraction, filtering, collects the second filtrate;First filtrate and the second filtrate are uniformly mixed, Then decolorization is carried out, obtains soak.
S2:PP non-woven fabrics after blade coating is drawn to fitting pressure roller, and thermoplastic elastomer films (TPE) film is smooth is bonded And it is close by pressure roller pressing, and draw to second station and wind;24h is stood, makes adhesive moisture curing, obtains semi-finished product.
S3:Semi-finished product are placed on the first station, the stroke as shown in attached drawing 2 draws semi-finished product to the patch of the 4th station At combined pressure roller;Polypropylene (PP) non-woven fabrics coiled strip is placed on the 5th station, the stroke as shown in attached drawing 2 draws PP non-woven fabrics To blade coating die head position;The adhesive of melting is scratched or is injected in the surface of PP non-woven fabrics protrusion;Wherein, the same step of adhesive Adhesive in S1;The pretreatment of polypropylene non-woven fabric is the same as step S1.
S4:PP non-woven fabrics after blade coating is drawn to fitting pressure roller, the table with thermoplastic elastomer films side in semi-finished product Face is smooth to be bonded and is pressed closely by pressure roller, and is drawn to second station and wound;24h is stood, consolidates adhesive moisture absorption Change, obtain medical textile finished material.
Embodiment five
The present embodiment provides a kind of medical textile material, including three layers, be followed successively by from top to bottom polypropylene non-woven layer of cloth, Thermoplastic elastomer films layer and polypropylene non-woven layer of cloth;Wherein, the thickness of thermoplastic elastomer films layer is 0.01mm.
Medical textile material is prepared using polyurethane hot melt compounding machine, is specifically comprised the following steps:
S1:Thermoplastic elastomer films (TPE) coiled strip is placed on the first station, the stroke as shown in attached drawing 2 draws film To the fitting pressure roller of the 4th station;Polypropylene (PP) non-woven fabrics coiled strip is placed on the 5th station, as the stroke shown in attached drawing 2 PP non-woven fabrics is drawn to blade coating die head position;The adhesive of melting is scratched or is injected in the surface of PP non-woven fabrics protrusion;
Wherein, adhesive is polyurethane hot melt, haloflex and polyacrylate material with 1:0.1:0.2 matter Amount is than being uniformly mixed obtained product;The preparation method of polyacrylate material includes the following steps:By water, acrylic acid hydroxyl second Ester and diallyldimethylammonium chloride are with 50:1:30 mass ratio is uniformly mixed, and then heats to 70 DEG C, and adjust pH value to 5.6;Initiator dibenzoyl peroxide is added, after insulation reaction 15min, is continuously heating to 92 DEG C, and adjusts pH value to 7.5, Then methyl acrylate and butyl methacrylate, initiator, methyl acrylate, butyl methacrylate and propylene are added dropwise respectively The mass ratio of sour hydroxyl ethyl ester is 0.3:30:8:1;2.5h is kept the temperature after being added dropwise, obtains polyacrylate material;
Polypropylene non-woven fabric is to be specifically included by the polypropylene non-woven fabric of pretreatment, pretreatment:By polypropylene non-woven fabric 10h is soaked in soak, then drying at room temperature;Wherein, the preparation method of soak includes the following steps:By the leaf of bamboo, wormwood With volume fraction be 70% ethanol water with 1:0.3:After 28 mass ratio mixing, 85 DEG C of heating 2h will be mixed after heating Compound filters, and collects the first filtrate and filter residue respectively;By filter residue and water with 1:15 mass ratio mixing, adjusting pH value to 8.8, so After carry out decoct extraction 30min, after extraction, filtering, collect the second filtrate;First filtrate and the second filtrate are mixed equal It is even, decolorization is then carried out, obtains soak.
S2:PP non-woven fabrics after blade coating is drawn to fitting pressure roller, and thermoplastic elastomer films (TPE) film is smooth is bonded And it is close by pressure roller pressing, and draw to second station and wind;24h is stood, makes adhesive moisture curing, obtains semi-finished product.
S3:Semi-finished product are placed on the first station, the stroke as shown in attached drawing 2 draws semi-finished product to the patch of the 4th station At combined pressure roller;Polypropylene (PP) non-woven fabrics coiled strip is placed on the 5th station, the stroke as shown in attached drawing 2 draws PP non-woven fabrics To blade coating die head position;The adhesive of melting is scratched or is injected in the surface of PP non-woven fabrics protrusion;Wherein, the same step of adhesive Adhesive in S1;The pretreatment of polypropylene non-woven fabric is the same as step S1.
S4:PP non-woven fabrics after blade coating is drawn to fitting pressure roller, the table with thermoplastic elastomer films side in semi-finished product Face is smooth to be bonded and is pressed closely by pressure roller, and is drawn to second station and wound;24h is stood, consolidates adhesive moisture absorption Change, obtain medical textile finished material.
Comparative example one
This comparative example provides a kind of medical textile material, including three layers, be followed successively by from top to bottom polypropylene non-woven layer of cloth, Thermoplastic elastomer films layer and polypropylene non-woven layer of cloth;Wherein, the thickness of thermoplastic elastomer films layer is 0.01mm.
Medical textile material is prepared using polyurethane hot melt compounding machine, is specifically comprised the following steps:
S1:Thermoplastic elastomer films (TPE) coiled strip is placed on the first station, the stroke as shown in attached drawing 2 draws film To the fitting pressure roller of the 4th station;Polypropylene (PP) non-woven fabrics coiled strip is placed on the 5th station, as the stroke shown in attached drawing 2 PP non-woven fabrics is drawn to blade coating die head position;The adhesive of melting is scratched or is injected in the surface of PP non-woven fabrics protrusion;
Wherein, adhesive is polyurethane hot melt;
Polypropylene non-woven fabric is to be specifically included by the polypropylene non-woven fabric of pretreatment, pretreatment:By polypropylene non-woven fabric 10h is soaked in soak, then drying at room temperature;Wherein, the preparation method of soak includes the following steps:By the leaf of bamboo, wormwood With volume fraction be 70% ethanol water with 1:0.3:After 28 mass ratio mixing, 85 DEG C of heating 2h will be mixed after heating Compound filters, and collects the first filtrate and filter residue respectively;By filter residue and water with 1:15 mass ratio mixing, adjusting pH value to 8.8, so After carry out decoct extraction 30min, after extraction, filtering, collect the second filtrate;First filtrate and the second filtrate are mixed equal It is even, decolorization is then carried out, obtains soak.
S2:PP non-woven fabrics after blade coating is drawn to fitting pressure roller, and thermoplastic elastomer films (TPE) film is smooth is bonded And it is close by pressure roller pressing, and draw to second station and wind;24h is stood, makes adhesive moisture curing, obtains semi-finished product.
S3:Semi-finished product are placed on the first station, the stroke as shown in attached drawing 2 draws semi-finished product to the patch of the 4th station At combined pressure roller;Polypropylene (PP) non-woven fabrics coiled strip is placed on the 5th station, the stroke as shown in attached drawing 2 draws PP non-woven fabrics To blade coating die head position;The adhesive of melting is scratched or is injected in the surface of PP non-woven fabrics protrusion;Wherein, the same step of adhesive Adhesive in S1;The pretreatment of polypropylene non-woven fabric is the same as step S1.
S4:PP non-woven fabrics after blade coating is drawn to fitting pressure roller, the table with thermoplastic elastomer films side in semi-finished product Face is smooth to be bonded and is pressed closely by pressure roller, and is drawn to second station and wound;24h is stood, consolidates adhesive moisture absorption Change, obtain medical textile finished material.
Comparative example two
This comparative example provides a kind of medical textile material, including three layers, be followed successively by from top to bottom polypropylene non-woven layer of cloth, Thermoplastic elastomer films layer and polypropylene non-woven layer of cloth;Wherein, the thickness of thermoplastic elastomer films layer is 0.01mm.
Medical textile material is prepared using polyurethane hot melt compounding machine, is specifically comprised the following steps:
S1:Thermoplastic elastomer films (TPE) coiled strip is placed on the first station, the stroke as shown in attached drawing 2 draws film To the fitting pressure roller of the 4th station;Polypropylene (PP) non-woven fabrics coiled strip is placed on the 5th station, as the stroke shown in attached drawing 2 PP non-woven fabrics is drawn to blade coating die head position;The adhesive of melting is scratched or is injected in the surface of PP non-woven fabrics protrusion;
Wherein, adhesive is polyurethane hot melt, haloflex and polyacrylate material with 1:0.1:0.2 matter Amount is than being uniformly mixed obtained product;The preparation method of polyacrylate material includes the following steps:By water, acrylic acid hydroxyl second Ester and diallyldimethylammonium chloride are with 50:1:30 mass ratio is uniformly mixed, and then heats to 70 DEG C, and adjust pH value to 5.6;Initiator dibenzoyl peroxide is added, after insulation reaction 15min, is continuously heating to 92 DEG C, and adjusts pH value to 7.5, Then methyl acrylate and butyl methacrylate, initiator, methyl acrylate, butyl methacrylate and propylene are added dropwise respectively The mass ratio of sour hydroxyl ethyl ester is 0.3:30:8:1;2.5h is kept the temperature after being added dropwise, obtains polyacrylate material;
Polypropylene non-woven fabric is to be specifically included by the polypropylene non-woven fabric of pretreatment, pretreatment:By polypropylene non-woven fabric 10h is soaked in soak, then drying at room temperature;Wherein, the preparation method of soak includes the following steps:By the leaf of bamboo, wormwood With volume fraction be 70% ethanol water with 1:0.3:After 28 mass ratio mixing, 85 DEG C of heating 2h will be mixed after heating Compound filters, and collects the first filtrate and filter residue respectively;By filter residue and water with 1:15 mass ratio mixing, then carries out decoction extraction 30min, after extraction, filtering, collects the second filtrate;First filtrate and the second filtrate are uniformly mixed, then decolourized Processing, obtains soak.
S2:PP non-woven fabrics after blade coating is drawn to fitting pressure roller, and thermoplastic elastomer films (TPE) film is smooth is bonded And it is close by pressure roller pressing, and draw to second station and wind;24h is stood, makes adhesive moisture curing, obtains semi-finished product.
S3:Semi-finished product are placed on the first station, the stroke as shown in attached drawing 2 draws semi-finished product to the patch of the 4th station At combined pressure roller;Polypropylene (PP) non-woven fabrics coiled strip is placed on the 5th station, the stroke as shown in attached drawing 2 draws PP non-woven fabrics To blade coating die head position;The adhesive of melting is scratched or is injected in the surface of PP non-woven fabrics protrusion;Wherein, the same step of adhesive Adhesive in S1;The pretreatment of polypropylene non-woven fabric is the same as step S1.
S4:PP non-woven fabrics after blade coating is drawn to fitting pressure roller, the table with thermoplastic elastomer films side in semi-finished product Face is smooth to be bonded and is pressed closely by pressure roller, and is drawn to second station and wound;24h is stood, consolidates adhesive moisture absorption Change, obtain medical textile finished material.
The medical textile material that the embodiment of the present invention one to embodiment five is prepared, is by function assessment experiment System evaluates its effect, and is used as control using the medical textile material that comparative example one and comparative example two provide.
1st, water resistance, resistant to blood and bacterium blocking performance test
The medical textile material that the embodiment of the present invention one to embodiment five, comparative example one and comparative example two are prepared Material, carried out respectively using standard JIS L 1092-1998A, ASTM 1670 and ASTM 1671 water resistance, resistant to blood performance and Bacterium blocking performance test, the result tested are as shown in table 1 below.Qualification in table 1 is " zero infiltration ".
1 water resistance of table, resistant to blood and bacterium blocking performance test
2nd, water vapour permeability is tested
The medical textile material that the embodiment of the present invention one to embodiment five, comparative example one and comparative example two are prepared Material, carries out water vapour permeability test, the result tested is as shown in table 2 below using standard JIS L1099.
2 water vapour permeability of table is tested
3rd, antibacterium performance measurement
(1) assay method:The embodiment one of phase homogenous quantities to embodiment five, comparative example one and comparative example two are prepared Medical textile material, be added separately to every milliliter contain 1 × 104In the culture medium of a Escherichia coli, with 100 beats/min Frequency oscillation 24h, then dilutes 100 times by the solution after every group of concussion, and concussion is uniform, take respectively 1mL pour into ten pieces it is identical A period of time is cultivated in agar plate, the E. coli clones number of every group of corresponding ten pieces of tablets is recorded and is averaged, will Average value × 100 are remaining Escherichia coli number, so as to calculate the growth inhibition ratio of Escherichia coli.By every group of experiment weight Again three times, it is averaged.
With same method measure staphylococcus aureus, Candida albicans, micrococcus luteus, drying rod bacillus and copper The growth inhibition ratio of green pseudomonad, in triplicate.
(2) measurement result:The medical textile material being calculated records the growth inhibition ratio of different bacterium, Concrete outcome is as shown in table 3 below.As in result as can be seen that medical textile material provided by the invention have it is very strong antibacterial Effect, when largely can reduce medical staff and wear operating coat, because perspiration and caused by the growths of a large amount of bacteriums breed.
Growth inhibition ratio result of the 3 medical textile material of table to bacterium
It should be noted that except the situation that above-described embodiment one is enumerated to embodiment five, other preparation methods are selected Parameter is also feasible.
Technical solution provided by the invention, has following beneficial effect:(1) medical textile material provided by the invention Structure include three layers, waterproof resistant to blood permeance property is high, can reach the index of correlation of prior art products, such as water resistance JIS L 1092-1998A standards can be passed through;Resistant to blood and bacterium blocking performance can be marked by ASTM 1670 and ASTM 1671 It is accurate;Its unique water vapour permeability can pass through JIS L1099 standards;(2) medical textile material provided by the invention, by abundant Using the performance of TPE film high moisture-inhibiting, so as at utmost keep the dry and comfortable comfort level of doctor and patient, solves conventional medical spinning When fabric is worn the problem of humid;(3) preparation method of medical textile material provided by the invention is simple, production cost It is low.
It should be noted that unless otherwise indicated, technical term or scientific terminology used in this application should be this hair The ordinary meaning that bright one of ordinary skill in the art are understood.Unless specifically stated otherwise, otherwise illustrate in these embodiments Component and opposite step, numerical expression and the numerical value of step are not limit the scope of the invention.It is illustrated and described herein In all examples, unless otherwise prescribed, any occurrence should be construed as merely exemplary, not as limitation, because This, other examples of exemplary embodiment can have different values.
In the description of the present invention, it is to be understood that term " first ", " second " are only used for description purpose, and cannot It is interpreted as indicating or implies relative importance or imply the quantity of the technical characteristic indicated by indicating.Thus, define " the One ", one or more this feature can be expressed or be implicitly included to the feature of " second ".In the description of the present invention, " multiple " are meant that two or more, unless otherwise specifically defined.
Finally it should be noted that:The above embodiments are only used to illustrate the technical solution of the present invention., rather than its limitations;To the greatest extent Pipe is described in detail the present invention with reference to foregoing embodiments, it will be understood by those of ordinary skill in the art that:Its according to Can so modify to the technical solution described in foregoing embodiments, either to which part or all technical characteristic into Row equivalent substitution;And these modifications or replacement, the essence of appropriate technical solution is departed from various embodiments of the present invention technology The scope of scheme, it should all cover among protection scope of the present invention.

Claims (10)

  1. A kind of 1. medical textile material, it is characterised in that:
    The medical textile material includes three layers, is followed successively by polypropylene non-woven layer of cloth, thermoplastic elastomer films layer from top to bottom With polypropylene non-woven layer of cloth;Wherein, the thickness of the thermoplastic elastomer films layer is 0.008~0.01mm.
  2. 2. the preparation method of the medical textile material described in claim 1, it is characterised in that include the following steps:
    S1:The adhesive of melting is scratched or is injected in the surface of polypropylene non-woven fabric protrusion;
    S2:By thermoplastic elastomer films it is smooth be fitted in by S1 handle polypropylene non-woven fabric surface, then by pressure roller Pressing is close, and standing makes adhesive moisture curing, obtains semi-finished product;
    S3:The adhesive of melting is scratched or is injected in the surface of polypropylene non-woven fabric protrusion;
    S4:By the smooth surface being fitted in by the S3 polypropylene non-woven fabrics handled of the semi-finished product, then pressed by pressure roller Closely, standing makes adhesive moisture curing, obtains medical textile finished material;Wherein, the surface with polypropylene non-woven fabric is pasted What is closed is the surface of thermoplastic elastomer films side in semi-finished product.
  3. 3. the preparation method of medical textile material according to claim 2, it is characterised in that:
    The medical textile material is prepared using polyurethane hot melt compounding machine;It is described in step S2 and step S4 The time of standing is 20~28h.
  4. 4. the preparation method of medical textile material according to claim 2, it is characterised in that:
    Described adhesive includes polyurethane hot melt.
  5. 5. the preparation method of medical textile material according to claim 4, it is characterised in that:
    Described adhesive further includes:Haloflex and polyacrylate material;Wherein, the polyurethane hot melt, described The mass ratio of haloflex and the polyacrylate material is 1:(0.05~0.1):(0.1~0.2).
  6. 6. the preparation method of medical textile material according to claim 5, it is characterised in that:
    The preparation method of the polyacrylate material includes the following steps:By water, hydroxy-ethyl acrylate and diallyl two Ammonio methacrylate is with (40~50):1:The mass ratio of (20~30) is uniformly mixed, and then heats to 68~70 DEG C, and adjust pH value To 5.4~5.6;Initiator is added, after 10~15min of insulation reaction, is continuously heating to 90~92 DEG C, and adjust pH value to 7.3 ~7.5, methyl acrylate and butyl methacrylate are then added dropwise respectively;2~2.5h is kept the temperature after being added dropwise, is obtained described poly- Esters of acrylic acid material.
  7. 7. the preparation method of medical textile material according to claim 6, it is characterised in that:
    The initiator is dibenzoyl peroxide, the initiator, the methyl acrylate, the butyl methacrylate and The mass ratio of the hydroxy-ethyl acrylate is (0.2~0.3):(20~30):(6~8):1.
  8. 8. the preparation method of medical textile material according to claim 2, it is characterised in that:
    The polypropylene non-woven fabric is to be specifically included by the polypropylene non-woven fabric of pretreatment, the pretreatment:By described poly- third Alkene non-woven fabrics soaks 8~10h in soak, then drying at room temperature;Wherein, the preparation method of the soak includes following step Suddenly:Heated after the leaf of bamboo, wormwood and ethanol water are mixed, the mixture after the heating is filtered, collect the first filter respectively Liquid and filter residue;The filter residue and water are mixed, pH value is adjusted to 8.5~8.8, then carries out decoction extraction, after extraction, mistake Filter, collects the second filtrate;First filtrate and second filtrate are uniformly mixed, then carry out decolorization, obtains institute State soak.
  9. 9. the preparation method of medical textile material according to claim 8, it is characterised in that:
    The mass ratio of the leaf of bamboo, the wormwood and the ethanol water is 1:(0.2~0.3):(20~28), the ethanol The volume fraction of ethanol is 60%~70% in aqueous solution, and the temperature of the heating is 75~85 DEG C, and the time of the heating is 1 ~2h;
    The mass ratio of the filter residue and the water is 1:(10~15), the time for decocting extraction is 20~30min.
  10. 10. the medical textile material described in claim 1 is preparing medical surgical gown, Medical operation cap, medical protective garment, doctor With the application in isolation clothes, johnny, medical hole towel and medical sheet.
CN201711167103.7A 2017-11-21 2017-11-21 Medical textile material and preparation method and application Pending CN107972334A (en)

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CN112810276A (en) * 2020-12-31 2021-05-18 新乐华宝医疗用品有限公司 TPE-non-woven fabric composite material and preparation method thereof
CN112899876A (en) * 2020-12-31 2021-06-04 浙江安吉锦韵无纺布有限公司 Medical non-woven fabric capable of preventing cross infection and preparation method thereof
CN114248517A (en) * 2022-01-04 2022-03-29 新乐华宝医疗器械有限公司 Composite material of moisture permeable and bacteriophage resistant and preparation method thereof
CN115847984A (en) * 2023-02-21 2023-03-28 天津市西青区天航临近空间材料科学研究院 Laminated polyurethane elastomer medical heat insulation material and preparation method and application thereof

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Application publication date: 20180501