CN104264262B - A kind of method extracting araboxylan and protein fibre from wheat bran - Google Patents
A kind of method extracting araboxylan and protein fibre from wheat bran Download PDFInfo
- Publication number
- CN104264262B CN104264262B CN201410439430.3A CN201410439430A CN104264262B CN 104264262 B CN104264262 B CN 104264262B CN 201410439430 A CN201410439430 A CN 201410439430A CN 104264262 B CN104264262 B CN 104264262B
- Authority
- CN
- China
- Prior art keywords
- wheat bran
- araboxylan
- protein fibre
- product
- suspension
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Landscapes
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The invention discloses a kind of method extracting araboxylan and protein fibre from wheat bran, belong to food processing field, extracting method mainly comprises the steps: that wheat bran is tentatively pulverized, after alcohol pre-treatment, centrifugal gained insoluble matter, after squeezing machine is tentatively extracted, again through ultramicro grinding, utilize complex enzyme and Action of Gravity Field, go out enzyme, supernatant is separated with precipitation, obtain the mixed liquor being rich in araboxylan, supernatant is through concentrated, organic solvent deposit, concentrate drying obtains the product being rich in araboxylan, sediment vacuumize obtains azelon product.Method provided by the invention can extract the high araboxylan of added value from grain processing accessory substance wheat bran, and the accessory substance in leaching process can be used as animal feed and uses, and adds value-added content of product, improves the economic benefit of grain processing enterprise.
Description
Technical field
The invention belongs to food processing technology field, be specifically related to a kind of method extracting araboxylan and protein fibre from wheat bran.
Background technology
Wheat is as the main raw material of human diet, the nutrition had mainly concentrates on the cortex of wheat, namely in wheat bran, therefore wheat bran is more and more subject to people's attention as the raw material of health food, China's wheat annual production is more than 100,000,000 tons, the wheat bran processed every year reaches more than 2,000 ten thousand tons, and wherein more than 85% all for brewageing and feedstuff industry, the rarely health food of wheat bran class.Containing abundant enzyme system, protein, carbohydrate, vitamin and mineral matter etc. in wheat bran, source is sufficient and cheap, if make full use of, will have significant economic benefit and social benefit.
Being rich in cellulose and hemicellulose in wheat bran skin, is the good source preparing compound sugar.Pentosan has the baking quality significantly acting on and have influence on bread to dough property, the pentosan in wheat is mainly present in wheat bran, the pentosan about containing about 20% in wheat bran.Therefore, be that pentosan prepared by raw material with wheat bran, and be developed as bread additives, there is good DEVELOPMENT PROSPECT.In addition, pentosan has the character such as high viscosity oxidative gelation, can also be applied to food service industry as thickener and humectant.
Araboxylan has good Bifidobacterium cultivation effect and low thermal performance and good surface-activity, and the araboxylan therefore prepared can be used as Growth Factors of Bifidus Bacteria and is applied in food.Reduce cholesterol, the production of inhibition cancer cell and activity, simultaneously, due to the low thermal performance that it has, belong to indigestibility sugar, can be used as the ideal sugar source of the patients such as diabetes, obesity, high fat of blood, the food of exploitation reduction postprandial blood sugar is a research whereabouts of araboxylan.
Summary of the invention
The object of this invention is to provide a kind of method that technique is simple, effect extracts araboxylan and protein fibre preferably from wheat bran.
For achieving the above object, the technical solution used in the present invention is, a kind of method extracting araboxylan and protein fibre from wheat bran, comprises the following steps:
(1) wheat bran is crushed to 30 ~ 50 orders, clean with alcohol flushing at 60 ~ 65 DEG C, centrifugally obtains solid, extracts, obtain pretreated wheat bran through squeezing machine;
(2) step (1) being processed the wheat bran obtained utilizes micronizer to be ground into 400 ~ 500 orders, adds water, water add 10 ~ 15 times that quality is wheat bran, stir into suspension;
(3) by suspension that step (2) is made, adjust ph is 4.0 ~ 7.0, suspension temperature maintains 30 ~ 60 DEG C, complex enzyme is added in suspension, the addition of complex enzyme is 1 ~ 10% of wheat bran quality, complex enzyme is made up of zytase and cellulase, mass ratio 1:2 ~ 5 of zytase and cellulase, stirs lower reaction and within 1 ~ 1.5 hour, obtains enzymolysis liquid;
(4) enzymolysis liquid obtained in step (3) is heated to 80 ~ 100 DEG C, keeps 30 ~ 60min, and then enzymolysis liquid is joined settling tank, carry out gravitational settling, sedimentation 8 ~ 10h at 30 ~ 60 DEG C, is precipitated and supernatant;
(5) get 3/5 ~ 4/5 of supernatant in step (4), concentrated, thickening temperature 40 ~ 50 DEG C, makes the concentration of the solids in concentrated rear concentrate control 20% ~ 30%;
(6) add ethanol in the concentrate of step (5) gained, obtain mixed solution, in mixed solution, the mass fraction of ethanol is more than 65%, temperature controls at 5 ~ 15 DEG C, then centrifugation is precipitated thing, by sediment vacuumize at 50 ~ 60 DEG C, obtains araboxylan product;
(7) precipitation in step (4) obtains protein fibre through centrifugal, vacuumize.
The protein fibre that described step (7) obtains is through pneumatic conveying drying, and temperature controls at 80 ~ 100 DEG C, can obtain moisture azelon product below 14%.
In described step (1), the volume fraction of ethanol used is not less than 60%.
The volume fraction of described step (6) ethanol used is more than 90%.
The beneficial effect that the present invention produces is, the synergy of complex enzyme and gravity is adopted to be hydrolyzed to wheat bran, in Action of Gravity Field process, the complex enzyme of not destroyed active minute quantity resolves into the relatively low araboxylan of molecule to cellulose and macromolecular pentosan further; The moisture of product of the araboxylan that the present invention extracts below 10%, purity more than 50%, in protein fibre product moisture 10 ~ 14%, the content of protein fibre is 30 ~ 40%; Improve grain processing value-added content of product, add economic benefit.
Accompanying drawing explanation
Fig. 1 is process chart of the present invention.
Detailed description of the invention
Below in conjunction with specific embodiment, the invention will be further described, but protection scope of the present invention is not limited thereto.
Embodiment 1
As shown in Figure 1, a kind of method extracting araboxylan and protein fibre from wheat bran, comprise the following steps: (1) wheat bran is crushed to 30 orders, rinse with ethanol (volume fraction is 60%) at 60 DEG C, ethanol consumption hourly is 15 times of wheat bran volume, rinses 2.5h, centrifugally obtains solid, extract through squeezing machine, obtain pretreated wheat bran;
(2) step (1) being processed the wheat bran obtained utilizes micronizer to be ground into 400 ~ 500 orders, adds water, water add 10 times that quality is wheat bran quality, stir into suspension;
(3) by suspension prepared by step (2), adjust ph is 4.0, suspension temperature controls at 30 DEG C, complex enzyme is added in suspension, the addition of complex enzyme is 1% of wheat bran quality, complex enzyme is made up of zytase and cellulase, the mass ratio 1:2 of zytase and cellulase, stirs lower reaction and within 1 hour, obtains enzymolysis liquid;
(4) enzymolysis liquid obtained in step (3) is heated to 80 DEG C, keeps 60min, and then enzymolysis liquid is joined settling tank, carry out gravitational settling, sedimentation 8h at 30 DEG C, is precipitated and supernatant;
(5) 3/5 of supernatant in step (4) is got, concentrated, thickening temperature 40 DEG C, the mass concentration of the solids after concentrated in concentrate is 20%;
(6) ethanol (volume fraction is 90%) is added in the concentrate to step (5) gained, obtain mixed solution, in mixed solution, the mass fraction of ethanol is 65%, temperature controls at 5 DEG C, then centrifugation is precipitated thing, by sediment in vacuumize at 50 DEG C, obtain araboxylan product;
(7) precipitation in step (4) through centrifugal, at 80 DEG C vacuumize obtain protein fibre product.
In the araboxylan product prepared in the present embodiment, the content of araboxylan is 50%, moisture 6%; Moisture 10% in protein fibre product, the content of protein fibre is 30%.
Embodiment 2
As shown in Figure 1, a kind of method extracting araboxylan and protein fibre from wheat bran, comprise the following steps: (1) wheat bran is crushed to 50 orders, rinse with ethanol (volume fraction is 70%) at 65 DEG C, ethanol consumption hourly is 20 times of wheat bran volume, rinses 2h, centrifugally obtains solid, extract through squeezing machine, obtain pretreated wheat bran;
(2) step (1) being processed the wheat bran obtained utilizes micronizer to be ground into 500 orders, adds water, water add 10 ~ 15 times that quality is wheat bran quality, stir into suspension;
(3) by suspension prepared by step (2), adjust ph is 7.0, suspension temperature maintains 60 DEG C, complex enzyme is added in suspension, the addition of complex enzyme is 10% of wheat bran quality, complex enzyme is made up of zytase and cellulase, the mass ratio 1:5 of zytase and cellulase, stirs lower reaction and within 1.5 hours, obtains enzymolysis liquid;
(4) enzymolysis liquid obtained in step (3) is heated to 100 DEG C, keeps 30min, and then enzymolysis liquid is joined settling tank, carry out gravitational settling, sedimentation 10h under temperature 60 C, is precipitated and supernatant;
(5) 4/5 of supernatant in step (4) is got, concentrated, thickening temperature 50 DEG C, the mass concentration of the solids after concentrated in concentrate is 30%;
(6) ethanol (volume fraction is 95%) is added in the concentrate to step (5) gained, obtain mixed solution, in mixed solution, the mass fraction of ethanol is 70%, temperature controls at 15 DEG C, centrifugation is precipitated thing, by sediment in vacuumize at 60 DEG C, obtain araboxylan product;
(7) precipitation in step (4) through centrifugal, at 80 DEG C vacuumize obtain protein fibre product.
In the araboxylan product prepared in the present embodiment, the content of araboxylan is 60%, moisture 10%; Moisture 14% in protein fibre product, the content of protein fibre is 40%.
Embodiment 3
A kind of method extracting araboxylan and protein fibre from wheat bran, comprise the following steps: (1) wheat bran is crushed to 40 orders, rinse with ethanol (volume fraction is 80%) at 62 DEG C, ethanol consumption hourly is 18 times of wheat bran volume, rinse 2.2h, centrifugally obtain solid, extract through squeezing machine, obtain pretreated wheat bran raw material;
(2) step (1) being processed the wheat bran obtained utilizes micronizer to be ground into 450 orders, adds water, water add 12 times that quality is wheat bran quality, stir into suspension;
(3) by suspension prepared by step (2), adjust ph is 5.5, suspension temperature maintains 45 DEG C, complex enzyme is added in suspension, the addition of complex enzyme is 5% of wheat bran quality, complex enzyme is made up of zytase and cellulase, the mass ratio 1:3.5 of zytase and cellulase, stirs lower reaction and within 1.2 hours, obtains enzymolysis liquid;
(4) enzymolysis liquid obtained in step (3) is heated to 90 DEG C, keeps 45min, and then enzymolysis liquid is joined settling tank, carry out gravitational settling, sedimentation 9h at 45 DEG C, is precipitated and supernatant;
(5) 70% of supernatant in step (4) is got, concentrated, thickening temperature 45 DEG C, the concentration of the solids after concentrated in concentrate is 25%;
(6) add absolute ethyl alcohol in the concentrate of step (5) gained, obtain mixed solution, in mixed solution, the mass fraction of ethanol is 75%, temperature controls at 10 DEG C, centrifugation is precipitated thing, by sediment vacuumize at 55 DEG C, obtains araboxylan product;
(7) precipitation in step (4) through centrifugal, at 80 DEG C vacuumize obtain protein fibre product.
In the araboxylan product prepared in the present embodiment, the content of araboxylan is 55%, moisture 8%; Moisture 12% in protein fibre product, the content of protein fibre is 35%.
Embodiment 4
As shown in Figure 1, a kind of method extracting araboxylan and protein fibre from wheat bran, comprise the following steps: (1) wheat bran is crushed to 45 orders, rinse with ethanol (volume fraction is 90%) at 63 DEG C, ethanol consumption hourly is 17 times of wheat bran volume, rinses 2.2h, centrifugally obtains solid, extract through squeezing machine, obtain pretreated wheat bran;
(2) step (1) being processed the wheat bran obtained utilizes micronizer to be ground into 420 orders, adds water, water add 13 times that quality is wheat bran quality, stir into suspension;
(3) by suspension prepared by step (2), adjust ph is 5.0, suspension temperature remains on 40 DEG C, complex enzyme is added in suspension, the addition of complex enzyme is 3% of wheat bran quality, complex enzyme is made up of zytase and cellulase, the mass ratio 1:4 of zytase and cellulase, stirs lower reaction and within 1.3 hours, obtains enzymolysis liquid;
(4) enzymolysis liquid obtained in step (3) is heated to 90 DEG C, keeps 40min, and then enzymolysis liquid is joined settling tank, carry out gravitational settling, sedimentation 8h at temperature 40 DEG C, is precipitated and supernatant;
(5) 3/5 of supernatant in step (4) is got, concentrated, thickening temperature 42 DEG C, the concentration making the solids in concentrated rear concentrate is 20%;
(6) ethanol (volume fraction is 95%) is added in the concentrate to step (5) gained, obtain mixed solution, in mixed solution, the mass fraction of ethanol is 69%, temperature controls at 15 DEG C, centrifugation is precipitated thing, by sediment in vacuumize at 52 DEG C, obtain araboxylan product;
(7) precipitation in step (4) through centrifugal, at 90 DEG C vacuumize obtain protein fibre product.
In the araboxylan product prepared in the present embodiment, the content of araboxylan is 53%, moisture 7%; Moisture 11% in protein fibre product, the content of protein fibre is 33%.
Embodiment 5
As shown in Figure 1, a kind of method extracting araboxylan and protein fibre from wheat bran, comprises the following steps:
(1) wheat bran is crushed to 30 orders, and rinse with ethanol (volume fraction is 90%) at 65 DEG C, ethanol consumption hourly is 20 times of wheat bran volume, rinses 2.5h, centrifugally obtains solid, extract, obtain pretreated wheat bran through squeezing machine;
(2) step (1) being processed the wheat bran obtained utilizes micronizer to be ground into 400 orders, adds water, and the addition of water is 15 times of wheat bran quality, stirs into suspension;
(3) by suspension prepared by step (2), adjust ph is 6.0, suspension temperature maintains 50 DEG C, complex enzyme is added in suspension, the addition of complex enzyme is 8% of wheat bran quality, complex enzyme is made up of zytase and cellulase, the mass ratio 1:3 of zytase and cellulase, stirs lower reaction and within 1.5 hours, obtains enzymolysis liquid;
(4) enzymolysis liquid obtained in step (3) is heated to 85 DEG C, keeps 30min, and then enzymolysis liquid is added settling tank, carry out gravitational settling, sedimentation 8h under temperature 60 C, is precipitated and supernatant;
(5) 4/5 of supernatant in step (4) is got, concentrated, thickening temperature 50 DEG C, the concentration of the solids after concentrated in concentrate is 30%;
(6) ethanol (volume fraction is 93%) is added in the concentrate to step (5) gained, obtain mixed solution, in mixed solution, the mass fraction of ethanol is 71%, temperature controls at 12 DEG C, centrifugation is precipitated thing, by sediment in vacuumize at 50 DEG C, obtain araboxylan product;
(7) precipitation in step (4) through centrifugal, at 100 DEG C vacuumize obtain protein fibre product.
The moisture 7% of the product of araboxylan prepared by the present embodiment, the content of araboxylan are 53%, in protein fibre product moisture 13%, the content of protein fibre is 33%.
Claims (3)
1. one kind is extracted the method for araboxylan and protein fibre from wheat bran, it is characterized in that, comprise the following steps: (1) wheat bran is crushed to 30 ~ 50 orders, clean with alcohol flushing at 60 ~ 65 DEG C, centrifugally obtain solid, extract through squeezing machine, obtain pretreated wheat bran;
(2) step (1) being processed the wheat bran obtained utilizes micronizer to be ground into 400 ~ 500 orders, adds water, and the quality that water adds is 10 ~ 15 times of wheat bran quality, stirs into suspension;
(3) by suspension that step (2) is made, adjust ph is 4.0 ~ 7.0, suspension temperature maintains 30 ~ 60 DEG C, complex enzyme is added in suspension, the addition of complex enzyme is 1 ~ 10% of wheat bran quality, complex enzyme is made up of zytase and cellulase, mass ratio 1:2 ~ 5 of zytase and cellulase, stirs lower reaction and within 1 ~ 1.5 hour, obtains enzymolysis liquid;
(4) enzymolysis liquid obtained in step (3) is heated to 80 ~ 100 DEG C, keeps 30 ~ 60min, and then enzymolysis liquid is joined settling tank, carry out gravitational settling, sedimentation 8 ~ 10h at 30 ~ 60 DEG C, is precipitated and supernatant;
(5) get 3/5 ~ 4/5 of supernatant in step (4), concentrated, thickening temperature 40 ~ 50 DEG C, makes the mass concentration of the solids in concentrated rear concentrate control 20% ~ 30%;
(6) add ethanol in the concentrate of step (5) gained, obtain mixed solution, in mixed solution, the mass fraction of ethanol is more than 65%, temperature controls at 5 ~ 15 DEG C, then centrifugation is precipitated thing, by sediment vacuumize at 50 ~ 60 DEG C, obtains araboxylan product;
(7) precipitation in step (4) obtains protein fibre product through centrifugal, vacuumize.
2. from wheat bran, extract the method for araboxylan and protein fibre as claimed in claim 1, it is characterized in that, in described step (1), the volume fraction of ethanol used is not less than 60%.
3. from wheat bran, extract the method for araboxylan and protein fibre as claimed in claim 1, it is characterized in that, the volume fraction of described step (6) ethanol used is more than 90%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410439430.3A CN104264262B (en) | 2014-09-01 | 2014-09-01 | A kind of method extracting araboxylan and protein fibre from wheat bran |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410439430.3A CN104264262B (en) | 2014-09-01 | 2014-09-01 | A kind of method extracting araboxylan and protein fibre from wheat bran |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104264262A CN104264262A (en) | 2015-01-07 |
| CN104264262B true CN104264262B (en) | 2016-02-03 |
Family
ID=52155830
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410439430.3A Expired - Fee Related CN104264262B (en) | 2014-09-01 | 2014-09-01 | A kind of method extracting araboxylan and protein fibre from wheat bran |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104264262B (en) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104762681A (en) * | 2015-03-26 | 2015-07-08 | 中南林业科技大学 | Biological technology natural silk |
| CN106317260B (en) * | 2016-08-23 | 2020-01-07 | 上海交通大学 | Method for extracting and purifying arabinoxylan from highland barley grains |
| RU2680384C1 (en) * | 2017-12-12 | 2019-02-20 | Федеральное государственное бюджетное образовательное учреждение высшего образования "Кемеровский государственный сельскохозяйственный институт" | Method of obtaining dry extracts of medical plants for farm animals and poultry |
| CN108191996A (en) * | 2018-02-28 | 2018-06-22 | 吉林农业大学 | A kind of preparation method of araboxylan |
| CN114015104B (en) * | 2021-12-02 | 2022-06-07 | 南京农业大学 | Production technology of environment-friendly food packaging film with freezing acceleration function |
Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101543285A (en) * | 2009-04-30 | 2009-09-30 | 福建省农业科学院农业工程技术研究所 | Wheat-bran dietary fiber composite functional fungus powder product and preparation process thereof |
| CN101607998A (en) * | 2009-05-14 | 2009-12-23 | 河南工业大学 | Testa Tritici enzyme engineering method transforms the method for piperylene and food fibre |
| CN102805351A (en) * | 2012-08-21 | 2012-12-05 | 运城学院 | Continuous preparation method of black wheat dietary fiber |
| CN103045658A (en) * | 2012-12-24 | 2013-04-17 | 保龄宝生物股份有限公司 | Method of taking bran as raw materials to prepare high-purity low-poly araboxylan and ferulic acid |
| CN103073913A (en) * | 2013-01-22 | 2013-05-01 | 山东农业大学 | Method for comprehensively extracting various functional components in color wheat bran |
| CN103589761A (en) * | 2013-11-08 | 2014-02-19 | 无锡群硕谷唐生物科技有限公司 | Method for preparing xylooligosaccharide by wheat bran and product obtained by method |
| GB2506125A (en) * | 2012-09-20 | 2014-03-26 | Cargill Inc | Method for extraction and isolation of arabinoxylan products from debranned cereal |
| CN103740683A (en) * | 2013-12-27 | 2014-04-23 | 湖南鸿鹰生物科技有限公司 | Wheat ration enzyme containing neutral protease and preparation method thereof |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP3079115B2 (en) * | 1990-10-30 | 2000-08-21 | 日清製粉株式会社 | Preparation of water-soluble arabinoxylan |
| KR100954217B1 (en) * | 2007-12-14 | 2010-04-21 | (주)세전 | Method for production of the extract containing L-arabinose by using organic acid |
| KR101345729B1 (en) * | 2011-10-28 | 2013-12-30 | 가천대학교 산학협력단 | Method of extracting arabinoxylan from rice bran |
-
2014
- 2014-09-01 CN CN201410439430.3A patent/CN104264262B/en not_active Expired - Fee Related
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101543285A (en) * | 2009-04-30 | 2009-09-30 | 福建省农业科学院农业工程技术研究所 | Wheat-bran dietary fiber composite functional fungus powder product and preparation process thereof |
| CN101607998A (en) * | 2009-05-14 | 2009-12-23 | 河南工业大学 | Testa Tritici enzyme engineering method transforms the method for piperylene and food fibre |
| CN102805351A (en) * | 2012-08-21 | 2012-12-05 | 运城学院 | Continuous preparation method of black wheat dietary fiber |
| GB2506125A (en) * | 2012-09-20 | 2014-03-26 | Cargill Inc | Method for extraction and isolation of arabinoxylan products from debranned cereal |
| CN103045658A (en) * | 2012-12-24 | 2013-04-17 | 保龄宝生物股份有限公司 | Method of taking bran as raw materials to prepare high-purity low-poly araboxylan and ferulic acid |
| CN103073913A (en) * | 2013-01-22 | 2013-05-01 | 山东农业大学 | Method for comprehensively extracting various functional components in color wheat bran |
| CN103589761A (en) * | 2013-11-08 | 2014-02-19 | 无锡群硕谷唐生物科技有限公司 | Method for preparing xylooligosaccharide by wheat bran and product obtained by method |
| CN103740683A (en) * | 2013-12-27 | 2014-04-23 | 湖南鸿鹰生物科技有限公司 | Wheat ration enzyme containing neutral protease and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN104264262A (en) | 2015-01-07 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104264262B (en) | A kind of method extracting araboxylan and protein fibre from wheat bran | |
| CN104140471B (en) | A kind of method preparing Rhizoma Dioscoreae high-purity polysaccharide from yam food processing fent | |
| CN101455403B (en) | Peanut peptide nutrient food and preparation method thereof | |
| CN103242423A (en) | Method for extracting silybum marianum protein | |
| CN102816633A (en) | Method for synchronously extracting corn germ oil and separation protein by using alcohol-assisted enzyme method | |
| CN102860450B (en) | Compound nutrition powder rich in kudzu root cellulose oligosaccharide and preparation method thereof | |
| CN108948227A (en) | A kind of method that high-voltage pulse extracts okra pectin | |
| CN106749750A (en) | A kind of preparation method of highland barley grain beta glucan | |
| CN102640935A (en) | Method for extracting dietary fiber in banana skin by adopting enzymic method | |
| CN102134285A (en) | Method for preparing polysaccharide of defective porphyra haitanensis | |
| CN104905205A (en) | Poultry bone condiment contributing to improving immunity | |
| CN105294868A (en) | Extraction method for mushroom polysaccharide and preparation method for double-mushroom soup-stock essence | |
| Chen et al. | Effect of in vitro digestion and fermentation of kiwifruit pomace polysaccharides on structural characteristics and human gut microbiota | |
| CN109170922B (en) | Preparation method of wheat bran soluble dietary fiber | |
| CN109369774A (en) | The extracting method of protein in a kind of acer truncatum seed dregs of rice | |
| CN117186264A (en) | Green and efficient highland barley beta-glucan extraction method | |
| CN1253475C (en) | Method for separating and preparing pentosan from wheat skin and use thereof | |
| CN104313086A (en) | Method for extracting soybean polysaccharose from soybean meal through biological enzyme method | |
| CN103518943A (en) | Method for extracting proteins from rape seed cakes by utilizing multi-frequency ultrasonic waves | |
| CN101455397A (en) | Animals and plants polysaccharide oligomerization method | |
| CN104522662A (en) | Red rice mycelium compound blood sugar-decreasing functional food and preparation method thereof | |
| CN111991836A (en) | Method for extracting nutrient from medicinal and edible plant | |
| CN105504098A (en) | Technology for extracting heparin sulfate from duodena | |
| CN104705662A (en) | Method for extracting composite flax dietary fiber | |
| CN102246966B (en) | Preparation method of pineapple dietary fiber |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160203 Termination date: 20160901 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |