CN104262737A - Preparation method of additive for daily necessities, and application thereof - Google Patents
Preparation method of additive for daily necessities, and application thereof Download PDFInfo
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- CN104262737A CN104262737A CN201410331904.2A CN201410331904A CN104262737A CN 104262737 A CN104262737 A CN 104262737A CN 201410331904 A CN201410331904 A CN 201410331904A CN 104262737 A CN104262737 A CN 104262737A
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- daily necessities
- additive
- preparation
- vitamin
- water
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L23/00—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
- C08L23/02—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers not modified by chemical after-treatment
- C08L23/04—Homopolymers or copolymers of ethene
- C08L23/06—Polyethene
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
Abstract
The invention provides a preparation method of an additive for daily necessities. According to the preparation method, an algae plant is used as a raw material; extraction efficiency of the algae active substances is obviously increased through acid-base extraction, enzymolysis, microwave treatment and addition of anti-corrosion agents; and bacteria fermentation is used to modify the active ingredients, so that the active ingredients have the functions of decomposing large molecular clusters and removing harmful substances. Due to the addition of the anti-corrosion agents, the additive for the daily necessities can be applied in the field of the daily necessities, and is used for improving air environment.
Description
Technical field
The present invention relates to a kind of preparation method and application thereof of daily necessities additive, in particular to the biological extraction process of seaweed plant functional activity material, the daily necessities additive application prepared using seaweed plant as raw material is when daily necessities, the macromolecular mass in the material contacted with these daily necessities can be disperseed, and play the effect of sterilizing and removal objectionable impurities.
Background technology
Marine alga belongs to lower plant, whole frond can both absorb inorganics from seawater and small organic molecule matter makes nutriment, also can secrete organic or inorganic material towards periphery simultaneously, the marine alga of growth in seawater complex environment, its metabolic process and meta-bolites are very different compared with land plant.Most of marine alga contains abundant carbohydrate (xylan, the poly-Saccharide and saccharide alcohols of dry dew etc.), nitrogenous compound (amino acid, peptide class, amine, cytochrome C, Benzazole compounds and carbohydrase class etc.), pigment (chlorophyll, class is trailing plants b element and phycobiliprotein recklessly), lipoid substance (triacylglycerol, hydro carbons, wax ester, lipid acid, phospholipid and glycolipid class etc.), phenolic compound, VITAMIN (precursor of vitamin A and D and vitamin-E, the water-soluble vitaminss such as liposoluble vitamin and vitamin B group such as K), marine alga medicine class (lectin etc.) and inorganic components etc.Therefore, marine alga has abundant nutritive value and pharmaceutical use.
Seaweed Extract has drawn from the large-scale economic algae in region, deep-sea, it contains abundant amino acid, mineral substance, polysaccharide, VITAMIN and physiologically active substance, to improving crop yield, oil recovery enhancement and premature ripening and all have obvious effect in fruit freshness preserving and opposing disease and pest etc.Large quantifier elimination shows that the extract in some marine algae can promote plant growth, increase yield, minimizing disease and pest, increase crop cold resistance, drought-resistant ability.And be used for decomposing macromolecular mass about making the daily necessities additive come with Seaweed Extract, sterilizing, remove the effect of objectionable impurities and have not been reported.
In fact, the character of Seaweed Extract and result of use very large by the impact of extracting mode.At present, the preparation technology of Seaweed Extract mainly contains alkali extraction method, neutral water solution, acid extraction method and Mechanical Crushing extraction method.In addition, sonioation method, enzymolysis process and hot-water soak method is also had.But, in the extracting method that these are traditional, the bioactive ingredients of marine alga is by the cellulosic obstruction of cell walls main component, often be difficult to be extracted efficiently, traditional extraction, enzymolysis process combine to improve extraction efficiency with microwave treatment by the present invention rightly, simultaneously by content and the character of activeconstituents in flora fermentation regulation extract, each component in extract is acted synergistically better, thus promote the decomposition of macromolecular mass, remove the function such as objectionable impurities, expand it and improving the application in healthy or air, soil, water surrounding.
Summary of the invention
The object of this invention is to provide a kind of preparation method and application thereof of daily necessities additive.
In a first aspect of the present invention, provide a kind of daily necessities additive dispersibling agglomerate molecule, by weight percentage, its main component is water 91.7%, acetic acid 4.2%, carbohydrate 2.4%, protein 0.1%.In addition, the lipid also containing trace, ash content, sodium, potassium, calcium, magnesium, phosphorus, iron, sub-lead, copper, titanium, zinc, zirconium, rhodium, palladium, Vitamin A, vitamin D, Vitamin B1 hcl, Vitamin B2, nicotinic acid, Vitamin B6, vitamin B12, folic acid, pantothenic acid, vitamin C.
Another aspect of the present invention, provide the above-mentioned preparation method dispersibling the daily necessities additive of agglomerate molecule, it comprises the following steps:
(1) extraction treatment:
Marine alga is cleaned chopping, and with the water of 10 ~ 30 times or 10 ~ 95% extraction using alcohols, temperature is 50 ~ 100 DEG C, extracts 3 times altogether, merges No. 3 extracting solutions;
(2) microwave treatment:
Microwave treatment is carried out to the extracting solution of step (1), radiated time 5-10min, microwave power 800-1200W;
(3) enzymolysis:
The microwave treatment extracting solution of step (1) is evaporated to the 1/3-1/4 of original volume, add the compound enzymic preparation comprising cellulase, beta-glucanase, papoid, took out after constant temperature 30 DEG C of water-bath 8-12 hours, quick-frozen Cheng Bing at putting-18 DEG C, thaw at room temperature is put in taking-up, and this quick-frozen thaw cycle in triplicate;
(4) flora fermentation:
In the enzymolysis solution of step (3), press the volume ratio access fermentative microflora of 1-5%, and at 25 ~ 30 DEG C sealed fermenting 3 ~ 6 days, obtain seaweed extracted liquor; The fermentative microflora that described fermentative microflora is aspergillus niger, head mold, Trichodermareesei, Bacillus licheniformis, subtilis, Micrococcus roseum, lactobacillus plantarum, pseudomonas, Alteromonad, plant yeast, yeast rich in selenium form;
(5) charcoal absorption is discolored:
Seaweed extracted liquor in step (4) adds activated carbon column and carries out decolorization adsorption process, filters removal activated carbon column and obtain daily necessities additive after the color substantially transparent of this seaweed extracted liquor.
Particularly, described marine alga raw material can be selected from bulk kelp, black wrack, sargassun, extra large capsule algae, bladder wrack, red algae any one, or select the mixing of two or more marine alga thing.Preferred sargassun, more preferably state, Wei sargassun or Sargassum henslowianum.
According to another aspect of the present invention, mechanical shock cutting mill, air blast ultramicro powder comminution, ball mill, Ball-stirring mill or vibration mill can be adopted in above-mentioned steps (1) to carry out micronizing.
According to another aspect of the present invention, the compound enzymic preparation adopted in above-mentioned steps (3) by ratio of weight and number be the cellulase of 1.2 ~ 3.6:2.1 ~ 5.2:1.6 ~ 4.5, beta-glucanase, papoid form.Preferred ratio of weight and number 1.2:2.1:1.6.
According to another aspect of the present invention, described in above-mentioned steps (4), fermentation condition is: temperature 28 DEG C, initial pH value 6.5, stirring velocity 100r/min, intermittent stirring 5min/2h, fermentation period 72 hours.
According to another aspect of the invention, in above-mentioned steps (4) fermentative microflora by ratio of weight and number be the aspergillus niger of 1.8:1.2:1.6:1.1:1.5:3.1:2.4:2.7:1.9:1.3:1, head mold, Trichodermareesei, Bacillus licheniformis, subtilis, Micrococcus roseum, lactobacillus plantarum, pseudomonas, Alteromonad, plant yeast, yeast rich in selenium form.
Described daily necessities comprise kitchenware and sanitary ware, bath accessory.
Described kitchenware and sanitary ware comprises ferment bucket, lunch box, chopsticks basket, energy cup, and described bath accessory comprises tooth glass, toothbrush.
Described daily necessities additive is added in food-grade polyethylene plastic pellet, by injection moulding, described food-grade polyethylene plastic pellet is injection molded into energy cup.
Daily necessities additive provided by the invention, metallic element wherein can form metal oxide or metal complex during the fermentation, the extract obtained after above-mentioned fermentation is made in the supercritical state the super micro nano particle of metal oxide, this super micro nano particle has high far infrared transmission ability, the far infrared rays of its radiation acts on neighbouring contact or non-contacting material, as large water clusters, water molecules is made to produce resonance absorption, thus make the hydrogen bond rupture between portion of water, this portion of water can be separated, and then water molecule cluster is diminished and is activated.And these daily necessities by injection moulding or other dry means make powder or other solids exist in daily necessities time, its super micro nano particle can the form in ultra-fine nanocrystallines exist, still there is activity, thus can the material contacted with daily necessities be purified, as rice, water.
Embodiment
Embodiment 1: containing the preparation of the daily necessities additive of state, Wei gulfweed extract
Get state, 100g Wei sargassun and clean chopping, prepare according to following step:
(1) extraction treatment:
With the water extraction of 30 times, temperature is 100 DEG C, extracts 3 times altogether, merges No. 3 extracting solutions;
(2) microwave treatment:
Microwave treatment is carried out to the extracting solution of step (1), radiated time 10min, microwave power 1200W;
(3) enzymolysis:
The microwave treatment extracting solution of step (1) is evaporated to 1/3 of original volume, add the compound enzymic preparation of the cellulase of ratio of weight and number 1.2:2.1:1.6, beta-glucanase, papoid composition, take out after 8 hours through constant temperature 30 DEG C of water-baths, quick-frozen Cheng Bing at putting-18 DEG C, thaw at room temperature is put in taking-up, and this quick-frozen thaw cycle in triplicate;
(4) flora fermentation:
By the volume ratio access fermentative microflora of 5% in the enzymolysis solution of step (3), and at 25 DEG C sealed fermenting 3 days, obtain extracting solution; The fermentative microflora that described fermentative microflora is aspergillus niger, head mold, Trichodermareesei, Bacillus licheniformis, subtilis, Micrococcus roseum, lactobacillus plantarum, pseudomonas, Alteromonad, plant yeast, yeast rich in selenium form;
(5) charcoal absorption is discolored:
Seaweed extracted liquor in step (4) adds activated carbon column and carries out decolorization adsorption process, filters removal activated carbon column and obtain daily necessities additive after the color substantially transparent of this seaweed extracted liquor.By desolventing technology, make this daily necessities additive there is no color, thus the color of daily necessities can not be affected when applying.
Embodiment 2: the preparation of going back the daily necessities additive of Sargassum henslowianum extracting solution
Get 100g Sargassum henslowianum and clean chopping, prepare according to following step:
(1) extraction treatment:
With 95% extraction using alcohol of 10 times, temperature is 50 DEG C, extracts 3 times altogether, merges No. 3 extracting solutions;
(2) microwave treatment:
Microwave treatment is carried out to the extracting solution of step (1), radiated time 5min, microwave power 800W;
(3) enzymolysis:
The microwave treatment extracting solution of step (1) is evaporated to 1/4 of original volume, add the compound enzymic preparation of the cellulase of ratio of weight and number 3.6:5.2:4.5, beta-glucanase, papoid composition, take out after 8 hours through constant temperature 30 DEG C of water-baths, quick-frozen Cheng Bing at putting-18 DEG C, thaw at room temperature is put in taking-up, and this quick-frozen thaw cycle in triplicate;
(4) flora fermentation:
By the volume ratio access fermentative microflora of 2% in the enzymolysis solution of step (3), and at 30 DEG C sealed fermenting 6 days, obtain extracting solution; The fermentative microflora that described fermentative microflora is aspergillus niger, head mold, Trichodermareesei, Bacillus licheniformis, subtilis, Micrococcus roseum, lactobacillus plantarum, pseudomonas, Alteromonad, plant yeast, yeast rich in selenium form;
(5) charcoal absorption is discolored:
Seaweed extracted liquor in step (4) adds activated carbon column and carries out decolorization adsorption process, filters removal activated carbon column and obtain daily necessities additive after the color substantially transparent of this seaweed extracted liquor.By desolventing technology, make this daily necessities additive there is no color, thus the color of daily necessities can not be affected when applying.
Embodiment 3: the measure of merit of activated water
Daily necessities additive obtained for above-described embodiment 1,2 is added in food-grade polyethylene plastic pellet respectively, by injection moulding, described food-grade polyethylene plastic pellet is injection molded into energy cup 1 and energy cup 2.
A group: get in undressed common 10mL tap water, filter after 10min, centrifugation, get supernatant liquor test water molecule
17o nucleus magnetic resonance halfwidth (NMRFWHM).
B group: get undressed common 10mL tap water and put into energy cup 1, filter after static 12 hours, centrifugation, gets supernatant liquor test water molecule
17o nucleus magnetic resonance halfwidth (NMRFWHM).
C group: get undressed common 10mL tap water and put into energy cup 2, filter after static 12 hours, centrifugation, gets supernatant liquor test water molecule
17o nucleus magnetic resonance halfwidth (NMRFWHM).
Testing tool is the NMR spectrometer with superconducting magnet of BruckerAVANCE III400MHz, measures according to JY/T007-1996 superconducting pulse fourier transform NMR spectral method.
Test result: it is as shown in the table for half peak height of 3 groups of samples:
| Sample | Half peak height/Hz |
| A group: tap water | 78 |
| B group: activated water | 54 |
| C group: activated water | 52 |
Table 1
Show thus, energy cup 1,2 all can reduce the 17ONMR halfwidth of water molecules, namely improves in water the ratio of the subset with 5 ~ 6 associated water molecules, and water molecules activity is improved.
Embodiment 4: the measure of merit of ferment
Daily necessities additive obtained for above-described embodiment 1,2 is added in food-grade polyethylene plastic pellet respectively, by injection moulding, described food-grade polyethylene plastic pellet is injection molded into ferment bucket 1 and ferment bucket 2.Prepare ferment 1 and ferment 2 with ferment bucket 1 and ferment bucket 2 respectively, according to GB19297-2003, GB2760-2011 national standard, detection method is tested to prepared ferment 1 and ferment 2.(experiment condition: temperature 20 DEG C ± 2 DEG C; Relative humidity 50% ± 10%), detected result sees the following form:
Sample detection account
To sum up, daily necessities additive provided by the invention, metallic element wherein can form metal oxide or metal complex during the fermentation, the extract obtained after above-mentioned fermentation is made in the supercritical state the super micro nano particle of metal oxide, this super micro nano particle has high far infrared transmission ability, the far infrared rays of its radiation acts on neighbouring contact or non-contacting material, as large water clusters, water molecules is made to produce resonance absorption, thus make the hydrogen bond rupture between portion of water, this portion of water can be separated, and then water molecule cluster is diminished and is activated.And these daily necessities by injection moulding or other dry means make powder or other solids exist in daily necessities time, its super micro nano particle can the form in ultra-fine nanocrystallines exist, still there is activity, thus can the material contacted with daily necessities be purified, as rice, water.
Should be understood that, above-mentioned embodiment of the present invention only for exemplary illustration or explain principle of the present invention, and is not construed as limiting the invention.Therefore, any amendment made when without departing from the spirit and scope of the present invention, equivalent replacement, improvement etc., all should be included within protection scope of the present invention.In addition, claims of the present invention be intended to contain fall into claims scope and border or this scope and border equivalents in whole change and modification.
Claims (8)
1. a preparation method for daily necessities additive, is characterized in that comprising the following steps:
(1) extraction treatment:
Marine alga is cleaned chopping, and with the water of 10 ~ 30 times or 10 ~ 95% extraction using alcohols, temperature is 50 ~ 100 DEG C, extracts 3 times altogether, merges No. 3 extracting solutions;
(2) microwave treatment:
Microwave treatment is carried out to the extracting solution of step (1), radiated time 5-10min, microwave power 800-1200W;
(3) enzymolysis:
The microwave treatment extracting solution of step (1) is evaporated to the 1/3-1/4 of original volume, add the compound enzymic preparation comprising cellulase, beta-glucanase, papoid, took out after constant temperature 30 DEG C of water-bath 8-12 hours, quick-frozen Cheng Bing at putting-18 DEG C, thaw at room temperature is put in taking-up, and this quick-frozen thaw cycle in triplicate;
(4) flora fermentation:
In the enzymolysis solution of step (3), press the volume ratio access fermentative microflora of 1-5%, and at 25 ~ 30 DEG C sealed fermenting 3 ~ 6 days, obtain seaweed extracted liquor; The fermentative microflora that described fermentative microflora is aspergillus niger, head mold, Trichodermareesei, Bacillus licheniformis, subtilis, Micrococcus roseum, lactobacillus plantarum, pseudomonas, Alteromonad, plant yeast, yeast rich in selenium form;
(5) charcoal absorption is discolored:
Seaweed extracted liquor in step (4) adds activated carbon column and carries out decolorization adsorption process, filters removal activated carbon column and obtain daily necessities additive after the color substantially transparent of this seaweed extracted liquor.
2. a preparation method for daily necessities additive as claimed in claim 1, it is characterized in that described marine alga be bulk kelp, black wrack, sargassun, extra large capsule algae, bladder wrack, red algae any one, or select the mixing of two or more marine alga thing.
3. a preparation method for daily necessities additive as claimed in claim 1, is characterized in that consisting of of compound enzymic preparation described in step (3): cellulase, beta-glucanase, papoid weight are 1.2 ~ 3.6:2.1 ~ 5.2:1.6 ~ 4.5.
4. the preparation method of a daily necessities additive as claimed in claim 1, it is characterized in that described in step (4), fermentation condition is: temperature 28 DEG C, initial pH value 6.5, stirring velocity 100r/min, intermittent stirring 5min/2h, fermentation period 72 hours.
5. a preparation method for daily necessities additive as claimed in claim 1, is characterized in that described seaweed extracted liquor, and its extracting solution comprises following main component:
And the lipid of trace, ash content, sodium, potassium, calcium, magnesium, phosphorus, iron, sub-lead, copper, titanium, zinc, zirconium, rhodium, palladium, Vitamin A, vitamin D, Vitamin B1 hcl, Vitamin B2, nicotinic acid, Vitamin B6, vitamin B12, folic acid, pantothenic acid, vitamin C.
6. a preparation method for daily necessities additive as claimed in claim 1, is characterized in that, described daily necessities comprise kitchenware and sanitary ware, bath accessory.
7. a preparation method for daily necessities additive as claimed in claim 6, is characterized in that, described kitchenware and sanitary ware comprises ferment bucket, lunch box, chopsticks basket, energy cup, and described bath accessory comprises tooth glass, toothbrush.
8. an application for daily necessities additive, is characterized in that, is added in food-grade polyethylene plastic pellet by the daily necessities additive prepared by method according to claim 1, by injection moulding, described food-grade polyethylene plastic pellet is injection molded into energy cup.
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| CN201410331904.2A CN104262737B (en) | 2014-07-14 | 2014-07-14 | A kind of preparation method and applications of article of everyday use additive |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107287271A (en) * | 2017-05-12 | 2017-10-24 | 正和清生命科技实业有限公司 | A kind of method that microbe fermentation method prepares fiber used for textiles |
| CN107573544A (en) * | 2017-07-31 | 2018-01-12 | 浦江县昂宝生物技术有限公司 | The preparation method of edible packing membrane based on sargassan |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101445819A (en) * | 2008-12-22 | 2009-06-03 | 重庆大学 | Method for preparing hydrolyzed oligosaccharides and short peptides from salt algae residues |
| US20110275118A1 (en) * | 2008-10-09 | 2011-11-10 | De Crecy Eudes | Method of producing fatty acids for biofuel, biodiesel, and other valuable chemicals |
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2014
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20110275118A1 (en) * | 2008-10-09 | 2011-11-10 | De Crecy Eudes | Method of producing fatty acids for biofuel, biodiesel, and other valuable chemicals |
| CN101445819A (en) * | 2008-12-22 | 2009-06-03 | 重庆大学 | Method for preparing hydrolyzed oligosaccharides and short peptides from salt algae residues |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107287271A (en) * | 2017-05-12 | 2017-10-24 | 正和清生命科技实业有限公司 | A kind of method that microbe fermentation method prepares fiber used for textiles |
| CN107573544A (en) * | 2017-07-31 | 2018-01-12 | 浦江县昂宝生物技术有限公司 | The preparation method of edible packing membrane based on sargassan |
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