CN104254536B - 用二取代碳二亚胺和二亚丙基三胺生产1,5,7‑三氮杂双环[4.4.0]癸‑5‑烯 - Google Patents

用二取代碳二亚胺和二亚丙基三胺生产1,5,7‑三氮杂双环[4.4.0]癸‑5‑烯 Download PDF

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Publication number
CN104254536B
CN104254536B CN201380021646.1A CN201380021646A CN104254536B CN 104254536 B CN104254536 B CN 104254536B CN 201380021646 A CN201380021646 A CN 201380021646A CN 104254536 B CN104254536 B CN 104254536B
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Prior art keywords
dipropylenetriamine
ene
triazabicyclo
dec
reaction
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CN201380021646.1A
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English (en)
Chinese (zh)
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CN104254536A (zh
Inventor
C·A·达克
R·F·卡拉宾
C·A·威尔逊
S·R·佐瓦奇
G·J·麦克拉姆
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PPG Industries Ohio Inc
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PPG Industries Ohio Inc
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Priority claimed from US13/455,651 external-priority patent/US9108968B2/en
Application filed by PPG Industries Ohio Inc filed Critical PPG Industries Ohio Inc
Priority to CN201610981485.6A priority Critical patent/CN106518881B/zh
Publication of CN104254536A publication Critical patent/CN104254536A/zh
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D487/00—Heterocyclic compounds containing nitrogen atoms as the only ring hetero atoms in the condensed system, not provided for by groups C07D451/00 - C07D477/00
    • C07D487/02—Heterocyclic compounds containing nitrogen atoms as the only ring hetero atoms in the condensed system, not provided for by groups C07D451/00 - C07D477/00 in which the condensed system contains two hetero rings
    • C07D487/04—Ortho-condensed systems
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D243/00—Heterocyclic compounds containing seven-membered rings having two nitrogen atoms as the only ring hetero atoms
    • C07D243/06—Heterocyclic compounds containing seven-membered rings having two nitrogen atoms as the only ring hetero atoms having the nitrogen atoms in positions 1 and 4
    • C07D243/10—Heterocyclic compounds containing seven-membered rings having two nitrogen atoms as the only ring hetero atoms having the nitrogen atoms in positions 1 and 4 condensed with carbocyclic rings or ring systems
    • C07D243/14—1,4-Benzodiazepines; Hydrogenated 1,4-benzodiazepines
    • C07D243/16—1,4-Benzodiazepines; Hydrogenated 1,4-benzodiazepines substituted in position 5 by aryl radicals
    • C07D243/18—1,4-Benzodiazepines; Hydrogenated 1,4-benzodiazepines substituted in position 5 by aryl radicals substituted in position 2 by nitrogen, oxygen or sulfur atoms
    • C07D243/20—Nitrogen atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D487/00—Heterocyclic compounds containing nitrogen atoms as the only ring hetero atoms in the condensed system, not provided for by groups C07D451/00 - C07D477/00
    • C07D487/02—Heterocyclic compounds containing nitrogen atoms as the only ring hetero atoms in the condensed system, not provided for by groups C07D451/00 - C07D477/00 in which the condensed system contains two hetero rings
    • C07D487/08—Bridged systems
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Electrochromic Elements, Electrophoresis, Or Variable Reflection Or Absorption Elements (AREA)
  • Paints Or Removers (AREA)
  • Nitrogen Condensed Heterocyclic Rings (AREA)
CN201380021646.1A 2012-04-25 2013-04-23 用二取代碳二亚胺和二亚丙基三胺生产1,5,7‑三氮杂双环[4.4.0]癸‑5‑烯 Active CN104254536B (zh)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610981485.6A CN106518881B (zh) 2012-04-25 2013-04-23 用二取代碳二亚胺和二亚丙基三胺生产1,5,7-三氮杂双环[4.4.0]癸-5-烯

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
US13/455,651 2012-04-25
US13/455,651 US9108968B2 (en) 2012-04-25 2012-04-25 Methods for producing 1,5,7-triazabicyclo[4.4.0]dec-5-ene by reaction of a disubstituted carbodiimide and dipropylene triamine
US13/780,469 2013-02-28
US13/780,469 US20130289273A1 (en) 2012-04-25 2013-02-28 Methods for producing 1,5,7-triazabicyclo[4.4.0]dec-5-ene by reaction of a disubstituted carbodiimide and dipropylene triamine
PCT/US2013/037713 WO2013163130A1 (en) 2012-04-25 2013-04-23 Methods for producing 1,5,7-triazabicyclo[4.4.0] dec-5-ene by reaction of a disubstituted carbodiimide and dipropylene triamine

Related Child Applications (1)

Application Number Title Priority Date Filing Date
CN201610981485.6A Division CN106518881B (zh) 2012-04-25 2013-04-23 用二取代碳二亚胺和二亚丙基三胺生产1,5,7-三氮杂双环[4.4.0]癸-5-烯

Publications (2)

Publication Number Publication Date
CN104254536A CN104254536A (zh) 2014-12-31
CN104254536B true CN104254536B (zh) 2017-03-15

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Application Number Title Priority Date Filing Date
CN201380021646.1A Active CN104254536B (zh) 2012-04-25 2013-04-23 用二取代碳二亚胺和二亚丙基三胺生产1,5,7‑三氮杂双环[4.4.0]癸‑5‑烯
CN201610981485.6A Active CN106518881B (zh) 2012-04-25 2013-04-23 用二取代碳二亚胺和二亚丙基三胺生产1,5,7-三氮杂双环[4.4.0]癸-5-烯

Family Applications After (1)

Application Number Title Priority Date Filing Date
CN201610981485.6A Active CN106518881B (zh) 2012-04-25 2013-04-23 用二取代碳二亚胺和二亚丙基三胺生产1,5,7-三氮杂双环[4.4.0]癸-5-烯

Country Status (13)

Country Link
US (1) US20130289273A1 (enExample)
EP (1) EP2841436B1 (enExample)
KR (1) KR101684044B1 (enExample)
CN (2) CN104254536B (enExample)
CA (1) CA2871328C (enExample)
ES (1) ES2644284T3 (enExample)
HK (1) HK1202871A1 (enExample)
HU (1) HUE037194T2 (enExample)
IN (1) IN2014DN08729A (enExample)
MX (1) MX351408B (enExample)
PL (1) PL2841436T3 (enExample)
RU (1) RU2600741C2 (enExample)
WO (1) WO2013163130A1 (enExample)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
TW201434882A (zh) * 2013-03-13 2014-09-16 Momentive Performance Mat Inc 可濕氣固化之有機聚矽氧烷組成物
US9688874B2 (en) 2013-10-25 2017-06-27 Ppg Industries Ohio, Inc. Method of making a bicyclic guanidine-cured acrylic coating
EP3131994B1 (de) * 2014-04-16 2021-06-09 Sika Technology AG Schnell härtende migrationsfreie zusammensetzung auf basis von silangruppen-haltigen organischen polymeren
FI129024B (en) 2017-11-08 2021-05-14 Helsingin Yliopisto Process for the preparation of bicyclic guanidine and its derivatives
CN112638913A (zh) * 2018-09-06 2021-04-09 瓦克化学股份公司 用于制备双环胍的方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101802109A (zh) * 2007-08-08 2010-08-11 Ppg工业俄亥俄公司 包含环状胍的可电沉积涂料组合物
WO2011079041A1 (en) * 2009-12-24 2011-06-30 Novomer, Inc. Methods for the synthesis of polycyclic guanidine compounds
US20110224328A1 (en) * 2010-03-10 2011-09-15 Mccollum Gregory J Method of making a cyclic guanidine from a guanidinium salt and a weak acid and coating compositions containing the same

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8563560B2 (en) 2011-02-25 2013-10-22 Ppg Industries Ohio, Inc. Preparation of bicyclic guanidine salts in an aqueous media

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101802109A (zh) * 2007-08-08 2010-08-11 Ppg工业俄亥俄公司 包含环状胍的可电沉积涂料组合物
WO2011079041A1 (en) * 2009-12-24 2011-06-30 Novomer, Inc. Methods for the synthesis of polycyclic guanidine compounds
US20110224328A1 (en) * 2010-03-10 2011-09-15 Mccollum Gregory J Method of making a cyclic guanidine from a guanidinium salt and a weak acid and coating compositions containing the same

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
"PROGRESS IN THE CHEMISTRY OF THE CARBODIIMIDES";B. V. Bocharov;《RUSSIAN CHEMICAL REVIEWS》;19650331;第34卷(第3期);第212-219页 *
"Ti-amide Catalyzed Synthesis of Cyclic Guanidines from Di-/Triamines and Carbodiimides";Hao Shen et al.;《ORGANIC LETTERS》;20110804;第13卷(第17期);第4562-4565页 *

Also Published As

Publication number Publication date
MX2014012932A (es) 2015-02-10
CA2871328C (en) 2017-10-03
EP2841436A1 (en) 2015-03-04
US20130289273A1 (en) 2013-10-31
CN106518881B (zh) 2018-11-09
ES2644284T3 (es) 2017-11-28
IN2014DN08729A (enExample) 2015-05-22
CA2871328A1 (en) 2013-10-31
WO2013163130A1 (en) 2013-10-31
KR20140139579A (ko) 2014-12-05
EP2841436B1 (en) 2017-08-23
MX351408B (es) 2017-10-12
PL2841436T3 (pl) 2018-01-31
HK1202871A1 (en) 2015-10-09
CN106518881A (zh) 2017-03-22
HUE037194T2 (hu) 2018-08-28
RU2600741C2 (ru) 2016-10-27
CN104254536A (zh) 2014-12-31
KR101684044B1 (ko) 2016-12-07
RU2014147324A (ru) 2016-06-10

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