CN104245609B - 用于制备合成石英玻璃粒料的方法 - Google Patents

用于制备合成石英玻璃粒料的方法 Download PDF

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Publication number
CN104245609B
CN104245609B CN201380022734.3A CN201380022734A CN104245609B CN 104245609 B CN104245609 B CN 104245609B CN 201380022734 A CN201380022734 A CN 201380022734A CN 104245609 B CN104245609 B CN 104245609B
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China
Prior art keywords
drum
pellets
mullite
quartz glass
sio2
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Chinese (zh)
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CN104245609A (zh
Inventor
W.莱曼
A.霍夫曼
T.凯泽
M.阿尔恩特
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Heraeus Quarzglas GmbH and Co KG
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Heraeus Quarzglas GmbH and Co KG
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    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03BMANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B20/00Processes specially adapted for the production of quartz or fused silica articles, not otherwise provided for
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/01Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
    • C04B35/16Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on silicates other than clay
    • C04B35/18Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on silicates other than clay rich in aluminium oxide
    • C04B35/185Mullite 3Al2O3-2SiO2
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03BMANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B19/00Other methods of shaping glass
    • C03B19/10Forming beads
    • C03B19/1095Thermal after-treatment of beads, e.g. tempering, crystallisation, annealing
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/626Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
    • C04B35/62605Treating the starting powders individually or as mixtures
    • C04B35/62645Thermal treatment of powders or mixtures thereof other than sintering
    • C04B35/62665Flame, plasma or melting treatment
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/64Burning or sintering processes
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C4/00Coating by spraying the coating material in the molten state, e.g. by flame, plasma or electric discharge
    • C23C4/04Coating by spraying the coating material in the molten state, e.g. by flame, plasma or electric discharge characterised by the coating material
    • C23C4/10Oxides, borides, carbides, nitrides or silicides; Mixtures thereof
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C4/00Coating by spraying the coating material in the molten state, e.g. by flame, plasma or electric discharge
    • C23C4/04Coating by spraying the coating material in the molten state, e.g. by flame, plasma or electric discharge characterised by the coating material
    • C23C4/10Oxides, borides, carbides, nitrides or silicides; Mixtures thereof
    • C23C4/11Oxides
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C4/00Coating by spraying the coating material in the molten state, e.g. by flame, plasma or electric discharge
    • C23C4/18After-treatment
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C4/00Coating by spraying the coating material in the molten state, e.g. by flame, plasma or electric discharge
    • C23C4/18After-treatment
    • C23C4/185Separation of the coating from the substrate
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27BFURNACES, KILNS, OVENS OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
    • F27B7/00Rotary-drum furnaces, i.e. horizontal or slightly inclined
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27BFURNACES, KILNS, OVENS OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
    • F27B7/00Rotary-drum furnaces, i.e. horizontal or slightly inclined
    • F27B7/02Rotary-drum furnaces, i.e. horizontal or slightly inclined of multiple-chamber or multiple-drum type
    • F27B7/04Rotary-drum furnaces, i.e. horizontal or slightly inclined of multiple-chamber or multiple-drum type with longitudinal divisions
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27BFURNACES, KILNS, OVENS OR RETORTS IN GENERAL; OPEN SINTERING OR LIKE APPARATUS
    • F27B7/00Rotary-drum furnaces, i.e. horizontal or slightly inclined
    • F27B7/20Details, accessories or equipment specially adapted for rotary-drum furnaces
    • F27B7/34Arrangements of heating devices
    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03BMANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B2201/00Type of glass produced
    • C03B2201/02Pure silica glass, e.g. pure fused quartz
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/50Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
    • C04B2235/54Particle size related information
    • C04B2235/5418Particle size related information expressed by the size of the particles or aggregates thereof
    • C04B2235/5427Particle size related information expressed by the size of the particles or aggregates thereof millimeter or submillimeter sized, i.e. larger than 0,1 mm
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/70Aspects relating to sintered or melt-casted ceramic products
    • C04B2235/74Physical characteristics
    • C04B2235/77Density
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/70Aspects relating to sintered or melt-casted ceramic products
    • C04B2235/94Products characterised by their shape

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  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Mechanical Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Ceramic Engineering (AREA)
  • Plasma & Fusion (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Metallurgy (AREA)
  • Structural Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Thermal Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Glass Melting And Manufacturing (AREA)
  • Ceramic Products (AREA)
  • Silicon Compounds (AREA)
CN201380022734.3A 2012-04-30 2013-04-17 用于制备合成石英玻璃粒料的方法 Active CN104245609B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE201210008437 DE102012008437B3 (de) 2012-04-30 2012-04-30 Verfahren zur Herstellung synthetischer Quarzglaskörnung
DE102012008437.4 2012-04-30
PCT/EP2013/057957 WO2013164189A1 (de) 2012-04-30 2013-04-17 Verfahren zur herstellung synthetischer quarzglaskörnung

Publications (2)

Publication Number Publication Date
CN104245609A CN104245609A (zh) 2014-12-24
CN104245609B true CN104245609B (zh) 2016-08-24

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CN201380022734.3A Active CN104245609B (zh) 2012-04-30 2013-04-17 用于制备合成石英玻璃粒料的方法

Country Status (6)

Country Link
US (1) US9580348B2 (enExample)
EP (1) EP2844618B1 (enExample)
JP (1) JP6150882B2 (enExample)
CN (1) CN104245609B (enExample)
DE (1) DE102012008437B3 (enExample)
WO (1) WO2013164189A1 (enExample)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108779015B (zh) * 2015-12-18 2021-10-26 贺利氏石英玻璃有限两合公司 从二氧化硅粉末制备石英玻璃体
EP3390303B1 (de) 2015-12-18 2024-02-07 Heraeus Quarzglas GmbH & Co. KG Herstellung von quarzglaskörpern mit taupunktkontrolle im schmelzofen
CN108698883A (zh) 2015-12-18 2018-10-23 贺利氏石英玻璃有限两合公司 石英玻璃制备中的二氧化硅的喷雾造粒
CN108698894A (zh) 2015-12-18 2018-10-23 贺利氏石英玻璃有限两合公司 在多腔式烘箱中制备石英玻璃体
KR20180094087A (ko) 2015-12-18 2018-08-22 헤래우스 크바르츠글라스 게엠베하 & 컴파니 케이지 실리카 과립으로부터 실리카 유리 제품의 제조
TWI733723B (zh) 2015-12-18 2021-07-21 德商何瑞斯廓格拉斯公司 不透明石英玻璃體的製備
KR20180095619A (ko) 2015-12-18 2018-08-27 헤래우스 크바르츠글라스 게엠베하 & 컴파니 케이지 실리카 유리 제조 동안 규소 함량의 증가
WO2017103131A1 (de) 2015-12-18 2017-06-22 Heraeus Quarzglas Gmbh & Co. Kg Verringern des erdalkalimetallgehalts von siliziumdioxidgranulat durch behandlung von kohlenstoffdotiertem siliziumdioxidgranulat bei hoher temperatur
JP6940235B2 (ja) 2015-12-18 2021-09-22 ヘレウス クワルツグラス ゲーエムベーハー ウント コンパニー カーゲー 高融点金属の溶融坩堝内での石英ガラス体の調製
TWI764879B (zh) * 2015-12-18 2022-05-21 德商何瑞斯廓格拉斯公司 降低二氧化矽顆粒之碳含量及石英玻璃體之製備
US10427970B1 (en) * 2016-10-03 2019-10-01 Owens-Brockway Glass Container Inc. Glass coatings and methods to deposit same
EP3739283B1 (de) * 2019-05-17 2022-02-23 Heraeus Quarzglas GmbH & Co. KG Verfahren zur behandlung rieselfähiger anorganischer körnung sowie zur durchführung des verfahrens geeignetes drehrohr
CN113149622B (zh) * 2021-05-29 2022-08-09 山东鲁铭新型材料股份有限公司 一种微晶氧化铝高温回转窑用内衬的制备方法
CN120289169B (zh) * 2025-06-12 2025-08-19 湖南旗滨医药材料科技有限公司 一种高抗蚀性药用玻璃旋转管及其制备方法

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4225443A (en) * 1978-03-22 1980-09-30 The Taulman Company Sintered-glass-granule filter medium
DE3001371A1 (de) * 1980-01-16 1981-08-06 Langlet, Weber KG Oberflächenveredlung Nachf., 5270 Gummersbach Keramischer oder oxidkeramischer, bindemittelfreier hohlkoerper und verfahren zu seiner herstellung
JPS62292642A (ja) * 1986-06-11 1987-12-19 Hitachi Chem Co Ltd シリカガラスの製造法
CN1498196A (zh) * 2001-03-23 2004-05-19 �����ɷ� 石英玻璃的构造元件及其制造方法

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US3758318A (en) * 1971-03-29 1973-09-11 Kaiser Aluminium Chem Corp Production of mullite refractory
US4225332A (en) 1978-08-14 1980-09-30 Owens-Corning Fiberglas Corporation Energy efficient pollution abating glass manufacturing process with external recovery of heat from furnace flue gases
JPS61286264A (ja) * 1985-06-11 1986-12-16 株式会社ニッカト− 加熱炉用管状部材及びその製造方法
JPS639964A (ja) * 1986-06-30 1988-01-16 Nec Corp 半導体記憶素子製造法
GB8627735D0 (en) * 1986-11-20 1986-12-17 Tsl Group Plc Vitreous silica
DE3836934A1 (de) * 1988-10-29 1990-05-03 Heraeus Schott Quarzschmelze Verfahren zum reinigen von teilchenfoermigem siliziumdioxid
DE4039504A1 (de) * 1990-12-11 1992-06-17 Vaw Ver Aluminium Werke Ag Verfahren zur extraktion von metallen aus metallhaltigen rohstoffen
EP0737653B1 (en) * 1995-04-10 1998-01-14 Heraeus Quarzglas GmbH Process for continuously refining of quartz powder
JPH10148469A (ja) * 1996-11-20 1998-06-02 Mitsubishi Chem Corp 外熱式ロータリキルン及びこれを用いた粉粒状高純度材料の製造方法
JPH10287416A (ja) * 1997-04-08 1998-10-27 Mitsubishi Chem Corp 合成石英粉の製造方法
DE19729505A1 (de) * 1997-07-10 1999-01-14 Heraeus Quarzglas Verfahren zur Herstellung von Si0¶2¶-Granulat
DE19937861C2 (de) 1999-08-13 2003-03-20 Heraeus Quarzglas Verfahren für die Herstellung dichter Quarzglas-Körnung
EP1088789A3 (en) 1999-09-28 2002-03-27 Heraeus Quarzglas GmbH & Co. KG Porous silica granule, its method of production and its use in a method for producing quartz glass
JP4548625B2 (ja) * 1999-09-28 2010-09-22 信越石英株式会社 高純度合成石英ガラス粉の製造方法
JP3813413B2 (ja) * 2000-06-09 2006-08-23 トーカロ株式会社 外熱式ロータリーキルン
JP2005076959A (ja) * 2003-08-29 2005-03-24 Murata Mfg Co Ltd 連続式熱処理装置
DE102004038602B3 (de) * 2004-08-07 2005-12-29 Heraeus Quarzglas Gmbh & Co. Kg Elektrogeschmolzenes, synthetisches Quarzglas, insbesondere für den Einsatz in der Lampen- und in der Halbleiterfertigung und Verfahren zur Herstellung desselben
US20130219963A1 (en) * 2010-10-28 2013-08-29 Heraeus Quarzglas Gmbh & Co. Kg Method for producing synthetic quartz glass granules

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4225443A (en) * 1978-03-22 1980-09-30 The Taulman Company Sintered-glass-granule filter medium
DE3001371A1 (de) * 1980-01-16 1981-08-06 Langlet, Weber KG Oberflächenveredlung Nachf., 5270 Gummersbach Keramischer oder oxidkeramischer, bindemittelfreier hohlkoerper und verfahren zu seiner herstellung
JPS62292642A (ja) * 1986-06-11 1987-12-19 Hitachi Chem Co Ltd シリカガラスの製造法
CN1498196A (zh) * 2001-03-23 2004-05-19 �����ɷ� 石英玻璃的构造元件及其制造方法

Also Published As

Publication number Publication date
CN104245609A (zh) 2014-12-24
JP2015516941A (ja) 2015-06-18
DE102012008437B3 (de) 2013-03-28
WO2013164189A1 (de) 2013-11-07
US20150107301A1 (en) 2015-04-23
US9580348B2 (en) 2017-02-28
JP6150882B2 (ja) 2017-06-21
EP2844618A1 (de) 2015-03-11
EP2844618B1 (de) 2016-08-10

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