CN104213434B - The production method of product pre-treatment, cation dyes one-bath dyeing is glued for sun - Google Patents
The production method of product pre-treatment, cation dyes one-bath dyeing is glued for sun Download PDFInfo
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- CN104213434B CN104213434B CN201410399060.5A CN201410399060A CN104213434B CN 104213434 B CN104213434 B CN 104213434B CN 201410399060 A CN201410399060 A CN 201410399060A CN 104213434 B CN104213434 B CN 104213434B
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Abstract
The present invention is a kind of dyeing method, particularly a kind of production method of gluing product pre-treatment, cation dyes one-bath dyeing for sun.Carry out according to the following steps: choose singe → compound auxiliary formula Design, preparation and consumption → dyeing recipe design → sample cylinder dyeing → drying and shaping → look base of sample cloth → grey cloth pre-setting → openpore and singe → wash and dry → oil sizing → Final finishing calendering → Final finishing tank steaming → finished product inspection.Glue the production method of product pre-treatment, cation dyes one-bath dyeing for sun, effects of energy saving and emission reduction is obvious, and the pleasant softness, full color degree etc. of fabric after production and processing; The inherent index of various quality etc. can meet the requirement of different client.
Description
Technical field
The present invention is a kind of dyeing method, particularly a kind of production method of gluing product pre-treatment, cation dyes one-bath dyeing for sun.
Background technology
Fabric pretreatment and cationic dyeing are generally all divided into two bath processings when dyeing and printing process by the sticky product of sun, because the treatment fluid pH value in two kinds of processing and treating methods is different, meta-alkali is wanted in pre-treatment, and cationic dyeing requires meta-acid; If be incorporated in by two kinds of processing modes with process in bath, respective process or Color will be had influence on; Research and develop a kind of pre-treatment compound auxiliary that the sticky product of sun can be allowed under the condition of acidity to process positive binding textiles, for the production technology changing the sticky pre-treatment Colour Difference of sun, the production technology making sun sticky is simplified, and becomes particularly important.Mainly can solve existing processing method long processing time, energy consumption is high, the problem that production cost is large.
Summary of the invention
The present invention mainly solves the deficiencies in the prior art, replace traditional sun and glue product pre-treatment and cation dyes two bathe production method, shorten the Colour Difference flow process of positive binding textiles, enhance productivity, reduce the energy resource consumption of water, electricity and gas, reduce the production method of gluing product pre-treatment, cation dyes one-bath dyeing for sun of production cost.
Above-mentioned technical problem of the present invention is mainly solved by following technical proposals:
Glue a production method for product pre-treatment, cation dyes one-bath dyeing for sun, carry out according to the following steps:
(1) sample cloth, is chosen:
Choose a positive binding textiles sample cloth, openpore door width 166cm, grammes per square metre 285g/m, dye Dark grey, washs strip and stays white;
The woven that the sticky product of sun is made up of 5% polyster fibre, 60% Cationic Dyeable Pet fiber and 35% viscose;
(2), grey cloth pre-setting:
Korea S's product reason and 9 joint baking oven setting machines are adopted to carry out sample cloth pre-setting, setting process: be process in the environment of 175 DEG C in temperature, the speed of process is 70m/min;
Grey cloth situation after pre-setting: door width 154cm, grammes per square metre 296g/m, shrinkage 3%;
(3), openpore is singed:
The method adopting Taizhou, Jiangsu natural gas gassing frame positive and negative respectively to burn once is singed to sample cloth, singeing: gas discharge 12, speed of a motor vehicle 110m/min;
Gas discharge 12 refers to the flow of 12 cubic meters per hour;
(4), compound auxiliary formula Design, preparation and consumption:
The design of compound auxiliary: OPE bleeding agent 5%, PAW refining agent 15%, C levelling agent 10%, water 70%, adds glacial acetic acid 2.5g/l when dyeing is produced;
The compound method of compound auxiliary: add the normal-temperature water of 40% in material bucket, adds OPE bleeding agent 5%, PAW refining agent 15% and C levelling agent 10%, and stirring and dissolving after 15 minutes, then adds the water of 30%, till continuing to be stirred to evenly;
The consumption of compound auxiliary: add compound auxiliary 2-4g/l during production;
The compound auxiliary of synthesis must possess following performance:
1. the condition that positive binding textiles pre-treatment and cationic dyeing synchronously carry out must be met;
2. after process, positive binding textiles capillary effect reaches traditional handicraft effect, little to the strength loss of fabric;
3. reproducibility is good, and process pH value is stabilized between 4-5, relatively little on the impact of cationic dyeing coloured light, and the look easily occurred under can improving traditional dyeing condition flower, dyestuff produce the problem of cohesion;
4. environmental protection, not containing banned substance, easily biological-degradable;
5. will have certain stability, long-term storage can keep relative stability.
(5), dyeing recipe design:
Heavily cation dyes formula is carried out: 250%X-BL is blue: 0.2g/kg, 250%X-GL are golden yellow: 5.2g/kg, 250%X-GRL are red: 3.2g/kg by cloth;
Dyeing assistant is filled a prescription: compound auxiliary 2.5g/l, glacial acetic acid 2.5g/l; Dyeing: be process 40min in the environment of 135 DEG C in temperature;
REACTIVE DYES is filled a prescription: ED-Q is black: 13g/kg, BF-3R are yellow: 0.8g/kg, BF-3B are red: 1.6g/kg;
Vital staining auxiliary formula: glauber salt: 40g/l, soda ash: 5kg, substitute alkali 2g/l;
Activity staining procedure: be process 70min in the environment of 60 DEG C in temperature;
To soap after vital staining formula: SW soaping agent: 2kg, glacial acetic acid: 2kg;
To soap technique: be process 10min in the environment of 75 DEG C in temperature;
Heavily carry out filling a prescription by cloth;
(6), a sample cylinder dyeing:
Adopt east, a Taiwan military essence sample overflow dyeing machine to dye, dying operation work presses dyeing recipe and sample cloth weight adjusts dye material to accounting place, and by the good cation dyes of regulationization and active dye dyestuff, material evenly exists without suspended particulate dyestuff;
Dyeing production procedure computer whole-process control dyeing production technology, dye bath ratio presses 1:9 dyeing:
Pre-treatment and cation dyes single bath process production overall process: conputer controlled discharge water position → point out into cloth → operative employee enter by hand cloth → operation after 2 minutes termination of pumping sensed water level → material cylinder reflux to add in material water → material cylinder compound auxiliary → open cycle stir material liquid → conputer controlled enter auxiliary agent → material cylinder reflux to add in material water → material cylinder glacial acetic acid → open cycle stir material liquid → conputer controlled enter auxiliary agent → material cylinder reflux to add in material water → material cylinder cation dyes → open cycle stir material liquid → conputer controlled enter dye solution → prompting detect pH value → conputer controlled heat up → be incubated 40min → cooling → 65 DEG C point out sample cutting check colors → conputer controlled washes;
Reactive dyeing: put water level to the material back in the water and chemical material cylinder cylinder stir in reactive dye solution - > open loop, the material liquid - computer control in dye - is expected to return the water to the material cylinder on stir in 1/6 sodium sulphate - > open loop in the material liquid - computer control into sodium sulphate solution - change is expected to return the water to the material cylinder on stir in 2/6 sodium sulphate - > open loop in the material liquid - computer control into sodium sulphate solution - the cylinder to add 3/6 sodium sulphate - > open loop mix the material liquid to computer control into sodium sulphate solution, prompt detection conductivity 30 min - > change to computer control temperature, heat preservation material cylinder back in the water and chemical material cylinder stir in soda ash - > open loop, the material liquid - computer control into the soda solution - the expected return the water to the material cylinder on stir in 2/5 the substitution alkali - > open loop in the material liquid - computer control into the substitution alkali solution - the material cylinder on stir in 3/5 the substitution alkali - > open loop in the material liquid - computer control into the substitution alkali solution - 40 min insulation - tip sample cutting for color - computer control water;
Soap: add in the position that discharges water → material cylinder backflow material water → material cylinder glacial acetic acid → open cycle stir in material liquid → conputer controlled charging → material cylinder backflow material water → material cylinder add SW soaping agent → open cycle stir material liquid → conputer controlled charging → conputer controlled heat up → be incubated 10min → cooling → 65 DEG C point out a sample cutting check colors → conputer controlled washes → points out out cloth;
(7), drying and shaping:
Adopt Korea S's product reason and 9 joint baking oven setting machines to carry out sample cloth drying and shaping, this operation is singed for follow-up semi-finished product look base and is provided smooth fabrics cloth cover, to obtain quality of singing preferably;
Drying and shaping technique: be in the environment of 185 DEG C in temperature, processing speed is 60m/min;
Grey cloth situation after drying and shaping: door width 154cm, grammes per square metre 286g/m;
(8), look base is singed:
The method adopting Taizhou, Jiangsu natural gas gassing frame positive and negative respectively to burn once is singed to semi-finished product look base sample cloth, the fine hair that during to remove dyed, fabric produces, and increases the fineness of fabrics cloth cover;
Singeing: gas discharge 7, speed of a motor vehicle 110m/min;
Gas discharge 7 refers to the flow of 7 cubic meters per hour;
(9), washing is dried:
Full-width rinsing machine is adopted to wash, the fine hair dust that during to remove because singing, fabric face is residual, for Final finishing processing provides reliable quality assurance;
Washing process: water temperature is normal temperature, speed of a motor vehicle 50m/min, drying cylinder steam pressure is 0.2MPa;
(10), oil sizing:
Adopt Korea S to produce reason and 9 joint baking oven setting machines to oil sizing to sample cloth, the feel that this operation acquisition fabric is good and fabric have good DIMENSIONAL STABILITY and set;
Production technology: be in the environment of 195 DEG C in temperature, processing speed is 30m/min, 130 softener 15g/l;
Grey cloth situation after sizing: door width 152cm, grammes per square metre 290g/m, shrinkage 6%;
(11), Final finishing calendering:
Adopt German KKT calender to carry out calendering, the setting of this operation obtains fabrics cloth cover good gloss;
Calen-dering process: temperature is 60 DEG C, pressure is 150 handkerchiefs, speed of a motor vehicle 50m/min;
After calendering, sample cloth door width is 150cm;
(12), Final finishing tank steams:
Adopt Italian TMT tank to steam machine to arrange sample cloth, to obtain the simulate wool effect of fabric, after fabric sends into tank steaming machine, can swelling be there is in fabric fiber under the state that high temperature is damp and hot, the temperature that tank steams in machine steaming pot is 100-102 DEG C, and tank steaming machine adopts wool flannelette blanket to be rolled in tightly in interlayer by fabric, pass through high-temperature steam again, steam pressure is 0.3-0.4MPa, the temperature of high-temperature steam is 160-170 DEG C, Steam soak mode is first permeated from inside to outside, ecto-entad infiltration again, fabric cannot be swelling at diametric(al) fiber, can only be swelling towards warp-wise, again fabric is taken out cold front heavy rain after warp-wise is swelling, make the stabilization of fiber, the time arranged in tank steaming machine is 20-30 minute, the swelling resilience making fabric of warp-wise, stiffness improves greatly, wool-like effect is desirable,
The comfort property that tank makes fabric reach not only plentiful but also well-pressed after steaming, possesses all good feel;
(13), finished product inspection:
The presentation quality of fabric and inherent quality index are tested.
Pre-treatment and cation dyes single bath process are produced and are summed up: because the compound auxiliary developed has particularity, can dye to modified polyester fibre under acidic high-temperature condition of high voltage, the slurry of can decompose, separating out in emulsification fabric and oligomer, fabric can be prevented and treated and produce look flower at dyeing course, dyestuff produces cohesion, avoids the effect that specking produces; In addition owing to being the dyeing of computer whole-process control, the major control index (as water consumption, pH value, temperature rate etc.) in dyeing course can effectively be ensured, makes the stability of whole dyeing course have raising.And to put sample process also more identical with laboratory; Thus solving the long processing time of traditional mode of production processing technology, energy consumption is high, the problem that production cost is large; Reach the object of abridged edition consumption reduction.
Therefore, production method of gluing product pre-treatment, cation dyes one-bath dyeing for sun provided by the invention, effects of energy saving and emission reduction is obvious, and the pleasant softness, full color degree etc. of fabric after production and processing; The inherent index of various quality etc. can meet the requirement of different client.
Detailed description of the invention
Below by embodiment, technical scheme of the present invention is described in further detail.
Embodiment 1: a kind of production method of gluing product pre-treatment, cation dyes one-bath dyeing for sun, carry out according to the following steps:
(1) sample cloth, is chosen:
Choose a positive binding textiles sample cloth, openpore door width 166cm, grammes per square metre 285g/m, dye Dark grey, washs strip and stays white;
The woven that the sticky product of sun is made up of 5% polyster fibre, 60% Cationic Dyeable Pet fiber and 35% viscose;
(2), grey cloth pre-setting:
Korea S's product reason and 9 joint baking oven setting machines are adopted to carry out sample cloth pre-setting, setting process: be process in the environment of 175 DEG C in temperature, the speed of process is 70m/min;
Grey cloth situation after pre-setting: door width 154cm, grammes per square metre 296g/m, shrinkage 3%;
(3), openpore is singed:
The method adopting Taizhou, Jiangsu natural gas gassing frame positive and negative respectively to burn once is singed to sample cloth, singeing: gas discharge 12, speed of a motor vehicle 110m/min;
Gas discharge 12 refers to the flow of 12 cubic meters per hour;
(4), compound auxiliary formula Design, preparation and consumption:
The design of compound auxiliary: OPE bleeding agent 5%, PAW refining agent 15%, C levelling agent 10%, water 70%, adds glacial acetic acid 2.5g/l when dyeing is produced;
The compound method of compound auxiliary: add the normal-temperature water of 40% in material bucket, adds OPE bleeding agent 5%, PAW refining agent 15% and C levelling agent 10%, and stirring and dissolving after 15 minutes, then adds the water of 30%, till continuing to be stirred to evenly;
The consumption of compound auxiliary: add compound auxiliary 2g/l during production;
The compound auxiliary of synthesis must possess following performance:
1. the condition that positive binding textiles pre-treatment and cationic dyeing synchronously carry out must be met;
2. after process, positive binding textiles capillary effect reaches traditional handicraft effect, little to the strength loss of fabric;
3. reproducibility is good, and process pH value is stabilized between 4-5, relatively little on the impact of cationic dyeing coloured light, and the look easily occurred under can improving traditional dyeing condition flower, dyestuff produce the problem of cohesion;
4. environmental protection, not containing banned substance, easily biological-degradable;
5. will have certain stability, long-term storage can keep relative stability.
(5), dyeing recipe design:
Heavily cation dyes formula is carried out: 250%X-BL is blue: 0.2g/kg, 250%X-GL are golden yellow: 5.2g/kg, 250%X-GRL are red: 3.2g/kg by cloth;
Dyeing assistant is filled a prescription: compound auxiliary 2.5g/l, glacial acetic acid 2.5g/l; Dyeing: be process 40min in the environment of 135 DEG C in temperature;
REACTIVE DYES is filled a prescription: ED-Q is black: 13g/kg, BF-3R are yellow: 0.8g/kg, BF-3B are red: 1.6g/kg;
Vital staining auxiliary formula: glauber salt: 40g/l, soda ash: 5kg, substitute alkali 2g/l;
Activity staining procedure: be process 70min in the environment of 60 DEG C in temperature;
To soap after vital staining formula: SW soaping agent: 2kg, glacial acetic acid: 2kg;
To soap technique: be process 10min in the environment of 75 DEG C in temperature;
Heavily carry out filling a prescription by cloth;
(6), a sample cylinder dyeing:
Adopt east, a Taiwan military essence sample overflow dyeing machine to dye, dying operation work presses dyeing recipe and sample cloth weight adjusts dye material to accounting place, and by the good cation dyes of regulationization and active dye dyestuff, material evenly exists without suspended particulate dyestuff;
Dyeing production procedure computer whole-process control dyeing production technology, dye bath ratio presses 1:9 dyeing:
Pre-treatment and cation dyes single bath process production overall process: conputer controlled discharge water position → point out into cloth → operative employee enter by hand cloth → operation after 2 minutes termination of pumping sensed water level → material cylinder reflux to add in material water → material cylinder compound auxiliary → open cycle stir material liquid → conputer controlled enter auxiliary agent → material cylinder reflux to add in material water → material cylinder glacial acetic acid → open cycle stir material liquid → conputer controlled enter auxiliary agent → material cylinder reflux to add in material water → material cylinder cation dyes → open cycle stir material liquid → conputer controlled enter dye solution → prompting detect pH value → conputer controlled heat up → be incubated 40min → cooling → 65 DEG C point out sample cutting check colors → conputer controlled washes;
Reactive dyeing: put water level to the material back in the water and chemical material cylinder cylinder stir in reactive dye solution - > open loop, the material liquid - computer control in dye - is expected to return the water to the material cylinder on stir in 1/6 sodium sulphate - > open loop in the material liquid - computer control into sodium sulphate solution - change is expected to return the water to the material cylinder on stir in 2/6 sodium sulphate - > open loop in the material liquid - computer control into sodium sulphate solution - the cylinder to add 3/6 sodium sulphate - > open loop mix the material liquid to computer control into sodium sulphate solution, prompt detection conductivity 30 min - > change to computer control temperature, heat preservation material cylinder back in the water and chemical material cylinder stir in soda ash - > open loop, the material liquid - computer control into the soda solution - the expected return the water to the material cylinder on stir in 2/5 the substitution alkali - > open loop in the material liquid - computer control into the substitution alkali solution - the material cylinder on stir in 3/5 the substitution alkali - > open loop in the material liquid - computer control into the substitution alkali solution - 40 min insulation - tip sample cutting for color - computer control water;
Soap: add in the position that discharges water → material cylinder backflow material water → material cylinder glacial acetic acid → open cycle stir in material liquid → conputer controlled charging → material cylinder backflow material water → material cylinder add SW soaping agent → open cycle stir material liquid → conputer controlled charging → conputer controlled heat up → be incubated 10min → cooling → 65 DEG C point out a sample cutting check colors → conputer controlled washes → points out out cloth;
(7), drying and shaping:
Adopt Korea S's product reason and 9 joint baking oven setting machines to carry out sample cloth drying and shaping, this operation is singed for follow-up semi-finished product look base and is provided smooth fabrics cloth cover, to obtain quality of singing preferably;
Drying and shaping technique: be in the environment of 185 DEG C in temperature, processing speed is 60m/min;
Grey cloth situation after drying and shaping: door width 154cm, grammes per square metre 286g/m;
(8), look base is singed:
The method adopting Taizhou, Jiangsu natural gas gassing frame positive and negative respectively to burn once is singed to semi-finished product look base sample cloth, the fine hair that during to remove dyed, fabric produces, and increases the fineness of fabrics cloth cover;
Singeing: gas discharge 7, speed of a motor vehicle 110m/min;
Gas discharge 7 refers to the flow of 7 cubic meters per hour;
(9), washing is dried:
Full-width rinsing machine is adopted to wash, the fine hair dust that during to remove because singing, fabric face is residual, for Final finishing processing provides reliable quality assurance;
Washing process: water temperature is normal temperature, speed of a motor vehicle 50m/min, drying cylinder steam pressure is 0.2MPa;
(10), oil sizing:
Adopt Korea S to produce reason and 9 joint baking oven setting machines to oil sizing to sample cloth, the feel that this operation acquisition fabric is good and fabric have good DIMENSIONAL STABILITY and set;
Production technology: be in the environment of 195 DEG C in temperature, processing speed is 30m/min, 130 softener 15g/l;
Grey cloth situation after sizing: door width 152cm, grammes per square metre 290g/m, shrinkage 6%;
(11), Final finishing calendering:
Adopt German KKT calender to carry out calendering, the setting of this operation obtains fabrics cloth cover good gloss;
Calen-dering process: temperature is 60 DEG C, pressure is 150 handkerchiefs, speed of a motor vehicle 50m/min;
After calendering, sample cloth door width is 150cm;
(12), Final finishing tank steams:
Adopt Italian TMT tank to steam machine to arrange sample cloth, to obtain the simulate wool effect of fabric, after fabric sends into tank steaming machine, can swelling be there is in fabric fiber under the state that high temperature is damp and hot, the temperature that tank steams in machine steaming pot is 100 DEG C, and tank steaming machine adopts wool flannelette blanket to be rolled in tightly in interlayer by fabric, pass through high-temperature steam again, steam pressure is 0.3MPa, the temperature of high-temperature steam is 160 DEG C, Steam soak mode is first permeated from inside to outside, ecto-entad infiltration again, fabric cannot be swelling at diametric(al) fiber, can only be swelling towards warp-wise, again fabric is taken out cold front heavy rain after warp-wise is swelling, make the stabilization of fiber, the time arranged in tank steaming machine is 20 minutes, the swelling resilience making fabric of warp-wise, stiffness improves greatly, wool-like effect is desirable,
The comfort property that tank makes fabric reach not only plentiful but also well-pressed after steaming, possesses all good feel;
(13), finished product inspection:
The presentation quality of fabric and inherent quality index are tested.
Embodiment 2: a kind of production method of gluing product pre-treatment, cation dyes one-bath dyeing for sun, carry out according to the following steps:
(1) sample cloth, is chosen:
Choose a positive binding textiles sample cloth, openpore door width 166cm, grammes per square metre 285g/m, dye Dark grey, washs strip and stays white;
The woven that the sticky product of sun is made up of 5% polyster fibre, 60% Cationic Dyeable Pet fiber and 35% viscose;
(2), grey cloth pre-setting:
Korea S's product reason and 9 joint baking oven setting machines are adopted to carry out sample cloth pre-setting, setting process: be process in the environment of 175 DEG C in temperature, the speed of process is 70m/min;
Grey cloth situation after pre-setting: door width 154cm, grammes per square metre 296g/m, shrinkage 3%;
(3), openpore is singed:
The method adopting Taizhou, Jiangsu natural gas gassing frame positive and negative respectively to burn once is singed to sample cloth, singeing: gas discharge 12, speed of a motor vehicle 110m/min;
Gas discharge 12 refers to the flow of 12 cubic meters per hour;
(4), compound auxiliary formula Design, preparation and consumption:
The design of compound auxiliary: OPE bleeding agent 5%, PAW refining agent 15%, C levelling agent 10%, water 70%, adds glacial acetic acid 2.5g/l when dyeing is produced;
The compound method of compound auxiliary: add the normal-temperature water of 40% in material bucket, adds OPE bleeding agent 5%, PAW refining agent 15% and C levelling agent 10%, and stirring and dissolving after 15 minutes, then adds the water of 30%, till continuing to be stirred to evenly;
The consumption of compound auxiliary: add compound auxiliary 3g/l during production;
The compound auxiliary of synthesis must possess following performance:
1. the condition that positive binding textiles pre-treatment and cationic dyeing synchronously carry out must be met;
2. after process, positive binding textiles capillary effect reaches traditional handicraft effect, little to the strength loss of fabric;
3. reproducibility is good, and process pH value is stabilized between 4-5, relatively little on the impact of cationic dyeing coloured light, and the look easily occurred under can improving traditional dyeing condition flower, dyestuff produce the problem of cohesion;
4. environmental protection, not containing banned substance, easily biological-degradable;
5. will have certain stability, long-term storage can keep relative stability.
(5), dyeing recipe design:
Heavily cation dyes formula is carried out: 250%X-BL is blue: 0.2g/kg, 250%X-GL are golden yellow: 5.2g/kg, 250%X-GRL are red: 3.2g/kg by cloth;
Dyeing assistant is filled a prescription: compound auxiliary 2.5g/l, glacial acetic acid 2.5g/l; Dyeing: be process 40min in the environment of 135 DEG C in temperature;
REACTIVE DYES is filled a prescription: ED-Q is black: 13g/kg, BF-3R are yellow: 0.8g/kg, BF-3B are red: 1.6g/kg;
Vital staining auxiliary formula: glauber salt: 40g/l, soda ash: 5kg, substitute alkali 2g/l;
Activity staining procedure: be process 70min in the environment of 60 DEG C in temperature;
To soap after vital staining formula: SW soaping agent: 2kg, glacial acetic acid: 2kg;
To soap technique: be process 10min in the environment of 75 DEG C in temperature;
Heavily carry out filling a prescription by cloth;
(6), a sample cylinder dyeing:
Adopt east, a Taiwan military essence sample overflow dyeing machine to dye, dying operation work presses dyeing recipe and sample cloth weight adjusts dye material to accounting place, and by the good cation dyes of regulationization and active dye dyestuff, material evenly exists without suspended particulate dyestuff;
Dyeing production procedure computer whole-process control dyeing production technology, dye bath ratio presses 1:9 dyeing:
Pre-treatment and cation dyes single bath process production overall process: conputer controlled discharge water position → point out into cloth → operative employee enter by hand cloth → operation after 2 minutes termination of pumping sensed water level → material cylinder reflux to add in material water → material cylinder compound auxiliary → open cycle stir material liquid → conputer controlled enter auxiliary agent → material cylinder reflux to add in material water → material cylinder glacial acetic acid → open cycle stir material liquid → conputer controlled enter auxiliary agent → material cylinder reflux to add in material water → material cylinder cation dyes → open cycle stir material liquid → conputer controlled enter dye solution → prompting detect pH value → conputer controlled heat up → be incubated 40min → cooling → 65 DEG C point out sample cutting check colors → conputer controlled washes;
Reactive dyeing: put water level to the material back in the water and chemical material cylinder cylinder stir in reactive dye solution - > open loop, the material liquid - computer control in dye - is expected to return the water to the material cylinder on stir in 1/6 sodium sulphate - > open loop in the material liquid - computer control into sodium sulphate solution - change is expected to return the water to the material cylinder on stir in 2/6 sodium sulphate - > open loop in the material liquid - computer control into sodium sulphate solution - the cylinder to add 3/6 sodium sulphate - > open loop mix the material liquid to computer control into sodium sulphate solution, prompt detection conductivity 30 min - > change to computer control temperature, heat preservation material cylinder back in the water and chemical material cylinder stir in soda ash - > open loop, the material liquid - computer control into the soda solution - the expected return the water to the material cylinder on stir in 2/5 the substitution alkali - > open loop in the material liquid - computer control into the substitution alkali solution - the material cylinder on stir in 3/5 the substitution alkali - > open loop in the material liquid - computer control into the substitution alkali solution - 40 min insulation - tip sample cutting for color - computer control water;
Soap: add in the position that discharges water → material cylinder backflow material water → material cylinder glacial acetic acid → open cycle stir in material liquid → conputer controlled charging → material cylinder backflow material water → material cylinder add SW soaping agent → open cycle stir material liquid → conputer controlled charging → conputer controlled heat up → be incubated 10min → cooling → 65 DEG C point out a sample cutting check colors → conputer controlled washes → points out out cloth;
(7), drying and shaping:
Adopt Korea S's product reason and 9 joint baking oven setting machines to carry out sample cloth drying and shaping, this operation is singed for follow-up semi-finished product look base and is provided smooth fabrics cloth cover, to obtain quality of singing preferably;
Drying and shaping technique: be in the environment of 185 DEG C in temperature, processing speed is 60m/min;
Grey cloth situation after drying and shaping: door width 154cm, grammes per square metre 286g/m;
(8), look base is singed:
The method adopting Taizhou, Jiangsu natural gas gassing frame positive and negative respectively to burn once is singed to semi-finished product look base sample cloth, the fine hair that during to remove dyed, fabric produces, and increases the fineness of fabrics cloth cover;
Singeing: gas discharge 7, speed of a motor vehicle 110m/min;
Gas discharge 7 refers to the flow of 7 cubic meters per hour;
(9), washing is dried:
Full-width rinsing machine is adopted to wash, the fine hair dust that during to remove because singing, fabric face is residual, for Final finishing processing provides reliable quality assurance;
Washing process: water temperature is normal temperature, speed of a motor vehicle 50m/min, drying cylinder steam pressure is 0.2MPa;
(10), oil sizing:
Adopt Korea S to produce reason and 9 joint baking oven setting machines to oil sizing to sample cloth, the feel that this operation acquisition fabric is good and fabric have good DIMENSIONAL STABILITY and set;
Production technology: be in the environment of 195 DEG C in temperature, processing speed is 30m/min, 130 softener 15g/l;
Grey cloth situation after sizing: door width 152cm, grammes per square metre 290g/m, shrinkage 6%;
(11), Final finishing calendering:
Adopt German KKT calender to carry out calendering, the setting of this operation obtains fabrics cloth cover good gloss;
Calen-dering process: temperature is 60 DEG C, pressure is 150 handkerchiefs, speed of a motor vehicle 50m/min;
After calendering, sample cloth door width is 150cm;
(12), Final finishing tank steams:
Adopt Italian TMT tank to steam machine to arrange sample cloth, to obtain the simulate wool effect of fabric, after fabric sends into tank steaming machine, can swelling be there is in fabric fiber under the state that high temperature is damp and hot, the temperature that tank steams in machine steaming pot is 101 DEG C, and tank steaming machine adopts wool flannelette blanket to be rolled in tightly in interlayer by fabric, pass through high-temperature steam again, steam pressure is 0.35MPa, the temperature of high-temperature steam is 165 DEG C, Steam soak mode is first permeated from inside to outside, ecto-entad infiltration again, fabric cannot be swelling at diametric(al) fiber, can only be swelling towards warp-wise, again fabric is taken out cold front heavy rain after warp-wise is swelling, make the stabilization of fiber, the time arranged in tank steaming machine is 25 minutes, the swelling resilience making fabric of warp-wise, stiffness improves greatly, wool-like effect is desirable,
The comfort property that tank makes fabric reach not only plentiful but also well-pressed after steaming, possesses all good feel;
(13), finished product inspection:
The presentation quality of fabric and inherent quality index are tested.
Embodiment 3: a kind of production method of gluing product pre-treatment, cation dyes one-bath dyeing for sun, carry out according to the following steps:
(1) sample cloth, is chosen:
Choose a positive binding textiles sample cloth, openpore door width 166cm, grammes per square metre 285g/m, dye Dark grey, washs strip and stays white;
The woven that the sticky product of sun is made up of 5% polyster fibre, 60% Cationic Dyeable Pet fiber and 35% viscose;
(2), grey cloth pre-setting:
Korea S's product reason and 9 joint baking oven setting machines are adopted to carry out sample cloth pre-setting, setting process: be process in the environment of 175 DEG C in temperature, the speed of process is 70m/min;
Grey cloth situation after pre-setting: door width 154cm, grammes per square metre 296g/m, shrinkage 3%;
(3), openpore is singed:
The method adopting Taizhou, Jiangsu natural gas gassing frame positive and negative respectively to burn once is singed to sample cloth, singeing: gas discharge 12, speed of a motor vehicle 110m/min;
Gas discharge 12 refers to the flow of 12 cubic meters per hour;
(4), compound auxiliary formula Design, preparation and consumption:
The design of compound auxiliary: OPE bleeding agent 5%, PAW refining agent 15%, C levelling agent 10%, water 70%, adds glacial acetic acid 2.5g/l when dyeing is produced;
The compound method of compound auxiliary: add the normal-temperature water of 40% in material bucket, adds OPE bleeding agent 5%, PAW refining agent 15% and C levelling agent 10%, and stirring and dissolving after 15 minutes, then adds the water of 30%, till continuing to be stirred to evenly;
The consumption of compound auxiliary: add compound auxiliary 4g/l during production;
The compound auxiliary of synthesis must possess following performance:
1. the condition that positive binding textiles pre-treatment and cationic dyeing synchronously carry out must be met;
2. after process, positive binding textiles capillary effect reaches traditional handicraft effect, little to the strength loss of fabric;
3. reproducibility is good, and process pH value is stabilized between 4-5, relatively little on the impact of cationic dyeing coloured light, and the look easily occurred under can improving traditional dyeing condition flower, dyestuff produce the problem of cohesion;
4. environmental protection, not containing banned substance, easily biological-degradable;
5. will have certain stability, long-term storage can keep relative stability.
(5), dyeing recipe design:
Heavily cation dyes formula is carried out: 250%X-BL is blue: 0.2g/kg, 250%X-GL are golden yellow: 5.2g/kg, 250%X-GRL are red: 3.2g/kg by cloth;
Dyeing assistant is filled a prescription: compound auxiliary 2.5g/l, glacial acetic acid 2.5g/l; Dyeing: be process 40min in the environment of 135 DEG C in temperature;
REACTIVE DYES is filled a prescription: ED-Q is black: 13g/kg, BF-3R are yellow: 0.8g/kg, BF-3B are red: 1.6g/kg;
Vital staining auxiliary formula: glauber salt: 40g/l, soda ash: 5kg, substitute alkali 2g/l;
Activity staining procedure: be process 70min in the environment of 60 DEG C in temperature;
To soap after vital staining formula: SW soaping agent: 2kg, glacial acetic acid: 2kg;
To soap technique: be process 10min in the environment of 75 DEG C in temperature;
Heavily carry out filling a prescription by cloth;
(6), a sample cylinder dyeing:
Adopt east, a Taiwan military essence sample overflow dyeing machine to dye, dying operation work presses dyeing recipe and sample cloth weight adjusts dye material to accounting place, and by the good cation dyes of regulationization and active dye dyestuff, material evenly exists without suspended particulate dyestuff;
Dyeing production procedure computer whole-process control dyeing production technology, dye bath ratio presses 1:9 dyeing:
Pre-treatment and cation dyes single bath process production overall process: conputer controlled discharge water position → point out into cloth → operative employee enter by hand cloth → operation after 2 minutes termination of pumping sensed water level → material cylinder reflux to add in material water → material cylinder compound auxiliary → open cycle stir material liquid → conputer controlled enter auxiliary agent → material cylinder reflux to add in material water → material cylinder glacial acetic acid → open cycle stir material liquid → conputer controlled enter auxiliary agent → material cylinder reflux to add in material water → material cylinder cation dyes → open cycle stir material liquid → conputer controlled enter dye solution → prompting detect pH value → conputer controlled heat up → be incubated 40min → cooling → 65 DEG C point out sample cutting check colors → conputer controlled washes;
Reactive dyeing: put water level to the material back in the water and chemical material cylinder cylinder stir in reactive dye solution - > open loop, the material liquid - computer control in dye - is expected to return the water to the material cylinder on stir in 1/6 sodium sulphate - > open loop in the material liquid - computer control into sodium sulphate solution - change is expected to return the water to the material cylinder on stir in 2/6 sodium sulphate - > open loop in the material liquid - computer control into sodium sulphate solution - the cylinder to add 3/6 sodium sulphate - > open loop mix the material liquid to computer control into sodium sulphate solution, prompt detection conductivity 30 min - > change to computer control temperature, heat preservation material cylinder back in the water and chemical material cylinder stir in soda ash - > open loop, the material liquid - computer control into the soda solution - the expected return the water to the material cylinder on stir in 2/5 the substitution alkali - > open loop in the material liquid - computer control into the substitution alkali solution - the material cylinder on stir in 3/5 the substitution alkali - > open loop in the material liquid - computer control into the substitution alkali solution - 40 min insulation - tip sample cutting for color - computer control water;
Soap: add in the position that discharges water → material cylinder backflow material water → material cylinder glacial acetic acid → open cycle stir in material liquid → conputer controlled charging → material cylinder backflow material water → material cylinder add SW soaping agent → open cycle stir material liquid → conputer controlled charging → conputer controlled heat up → be incubated 10min → cooling → 65 DEG C point out a sample cutting check colors → conputer controlled washes → points out out cloth;
(7), drying and shaping:
Adopt Korea S's product reason and 9 joint baking oven setting machines to carry out sample cloth drying and shaping, this operation is singed for follow-up semi-finished product look base and is provided smooth fabrics cloth cover, to obtain quality of singing preferably;
Drying and shaping technique: be in the environment of 185 DEG C in temperature, processing speed is 60m/min;
Grey cloth situation after drying and shaping: door width 154cm, grammes per square metre 286g/m;
(8), look base is singed:
The method adopting Taizhou, Jiangsu natural gas gassing frame positive and negative respectively to burn once is singed to semi-finished product look base sample cloth, the fine hair that during to remove dyed, fabric produces, and increases the fineness of fabrics cloth cover;
Singeing: gas discharge 7, speed of a motor vehicle 110m/min;
Gas discharge 7 refers to the flow of 7 cubic meters per hour;
(9), washing is dried:
Full-width rinsing machine is adopted to wash, the fine hair dust that during to remove because singing, fabric face is residual, for Final finishing processing provides reliable quality assurance;
Washing process: water temperature is normal temperature, speed of a motor vehicle 50m/min, drying cylinder steam pressure is 0.2MPa;
(10), oil sizing:
Adopt Korea S to produce reason and 9 joint baking oven setting machines to oil sizing to sample cloth, the feel that this operation acquisition fabric is good and fabric have good DIMENSIONAL STABILITY and set;
Production technology: be in the environment of 195 DEG C in temperature, processing speed is 30m/min, 130 softener 15g/l;
Grey cloth situation after sizing: door width 152cm, grammes per square metre 290g/m, shrinkage 6%;
(11), Final finishing calendering:
Adopt German KKT calender to carry out calendering, the setting of this operation obtains fabrics cloth cover good gloss;
Calen-dering process: temperature is 60 DEG C, pressure is 150 handkerchiefs, speed of a motor vehicle 50m/min;
After calendering, sample cloth door width is 150cm;
(12), Final finishing tank steams:
Adopt Italian TMT tank to steam machine to arrange sample cloth, to obtain the simulate wool effect of fabric, after fabric sends into tank steaming machine, can swelling be there is in fabric fiber under the state that high temperature is damp and hot, the temperature that tank steams in machine steaming pot is 102 DEG C, and tank steaming machine adopts wool flannelette blanket to be rolled in tightly in interlayer by fabric, pass through high-temperature steam again, steam pressure is 0.4MPa, the temperature of high-temperature steam is 170 DEG C, Steam soak mode is first permeated from inside to outside, ecto-entad infiltration again, fabric cannot be swelling at diametric(al) fiber, can only be swelling towards warp-wise, again fabric is taken out cold front heavy rain after warp-wise is swelling, make the stabilization of fiber, the time arranged in tank steaming machine is 30 minutes, the swelling resilience making fabric of warp-wise, stiffness improves greatly, wool-like effect is desirable,
The comfort property that tank makes fabric reach not only plentiful but also well-pressed after steaming, possesses all good feel;
(14), finished product inspection:
The presentation quality of fabric and inherent quality index are tested.
Fabric described in embodiment 1 to 3 possesses following technical parameter:
Gram weight: meet designing requirement (GB/T4668)
Water-fastness COLOR FASTNESS: GB/T3921.3-1997
Colour fastness to rubbing: GB/T3920-1997
Colour fastness to perspiration: GB/T3922-1995
Washing size changing rate: GB/T8629-2001GB/T8630-2001GB/T8628-2001
Pilling: GB/T4802.1-1997
Ultimate strength: GB/T3923.1-1997
Tearing brute force: GB/T3917.1-1997
Wrinkle recovery angle: GB/T3819-1997
Cloth cover pH value: GB/T7573-1987.
Claims (1)
1. glue a production method for product pre-treatment, cation dyes one-bath dyeing for sun, it is characterized in that carrying out according to the following steps:
(1) sample cloth, is chosen:
Choose a positive binding textiles sample cloth, openpore door width 166cm, grammes per square metre 285g/m, dye Dark grey, washs strip and stays white;
The woven that the sticky product of sun is made up of 5% polyster fibre, 60% Cationic Dyeable Pet fiber and 35% viscose;
(2), grey cloth pre-setting:
Korea S's product reason and 9 joint baking oven setting machines are adopted to carry out sample cloth pre-setting, setting process: be process in the environment of 175 DEG C in temperature, the speed of process is 70m/min;
Grey cloth situation after pre-setting: door width 154cm, grammes per square metre 296g/m, shrinkage 3%;
(3), openpore is singed:
The method adopting Taizhou, Jiangsu natural gas gassing frame positive and negative respectively to burn once is singed to sample cloth, singeing: gas discharge 12, speed of a motor vehicle 110m/min;
Gas discharge 12 refers to the flow of 12 cubic meters per hour;
(4), compound auxiliary formula Design, preparation and consumption:
The design of compound auxiliary: OPE bleeding agent 5%, PAW refining agent 15%, C levelling agent 10%, water 70%, adds glacial acetic acid 2.5g/l when dyeing is produced;
The compound method of compound auxiliary: add the normal-temperature water of 40% in material bucket, adds OPE bleeding agent 5%, PAW refining agent 15% and C levelling agent 10%, and stirring and dissolving after 15 minutes, then adds the water of 30%, till continuing to be stirred to evenly;
The consumption of compound auxiliary: add compound auxiliary 2-4g/l during production;
The compound auxiliary of synthesis must possess following performance:
1. the condition that positive binding textiles pre-treatment and cationic dyeing synchronously carry out must be met;
2. after process, positive binding textiles capillary effect reaches traditional handicraft effect, little to the strength loss of fabric;
3. reproducibility is good, and process pH value is stabilized between 4-5, relatively little on the impact of cationic dyeing coloured light, and the look easily occurred under can improving traditional dyeing condition flower, dyestuff produce the problem of cohesion;
4. environmental protection, not containing banned substance, easily biological-degradable;
5. will have certain stability, long-term storage can keep relative stability;
(5), dyeing recipe design:
Heavily cation dyes formula is carried out: 250%X-BL is blue: 0.2g/kg, 250%X-GL are golden yellow: 5.2g/kg, 250%X-GRL are red: 3.2g/kg by cloth;
Dyeing assistant is filled a prescription: compound auxiliary 2.5g/l, glacial acetic acid 2.5g/l; Dyeing: be process 40min in the environment of 135 DEG C in temperature;
REACTIVE DYES is filled a prescription: ED-Q is black: 13g/kg, BF-3R are yellow: 0.8g/kg, BF-3B are red: 1.6g/kg;
Vital staining auxiliary formula: glauber salt: 40g/l, soda ash: 5kg, substitute alkali 2g/l;
Activity staining procedure: be process 70min in the environment of 60 DEG C in temperature;
To soap after vital staining formula: SW soaping agent: 2kg, glacial acetic acid: 2kg;
To soap technique: be process 10min in the environment of 75 DEG C in temperature;
Heavily fill a prescription by cloth;
(6), a sample cylinder dyeing:
Adopt east, a Taiwan military essence sample overflow dyeing machine to dye, dying operation work presses dyeing recipe and sample cloth weight adjusts dye material to accounting place, and by the good cation dyes of regulationization and REACTIVE DYES, material evenly exists without suspended particulate dyestuff;
Dyeing production procedure computer whole-process control dyeing production technology, dye bath ratio presses 1:9 dyeing:
Pre-treatment and cation dyes single bath process production overall process: conputer controlled discharge water position → point out into cloth → operative employee enter by hand cloth → operation after 2 minutes termination of pumping sensed water level → material cylinder reflux to add in material water → material cylinder compound auxiliary → open cycle stir material liquid → conputer controlled enter auxiliary agent → material cylinder reflux to add in material water → material cylinder glacial acetic acid → open cycle stir material liquid → conputer controlled enter auxiliary agent → material cylinder reflux to add in material water → material cylinder cation dyes → open cycle stir material liquid → conputer controlled enter dye solution → prompting detect pH value → conputer controlled heat up → be incubated 40min → cooling → 65 DEG C point out sample cutting check colors → conputer controlled washes;
Reactive dyeing: put water level to the material back in the water and chemical material cylinder cylinder stir in reactive dye solution - > open loop, the material liquid - computer control in dye - is expected to return the water to the material cylinder on stir in 1/6 sodium sulphate - > open loop in the material liquid - computer control into sodium sulphate solution - change is expected to return the water to the material cylinder on stir in 2/6 sodium sulphate - > open loop in the material liquid - computer control into sodium sulphate solution - the cylinder to add 3/6 sodium sulphate - > open loop mix the material liquid to computer control into sodium sulphate solution, prompt detection conductivity 30 min - > change to computer control temperature, heat preservation material cylinder back in the water and chemical material cylinder stir in soda ash - > open loop, the material liquid - computer control into the soda solution - the expected return the water to the material cylinder on stir in 2/5 the substitution alkali - > open loop in the material liquid - computer control into the substitution alkali solution - the material cylinder on stir in 3/5 the substitution alkali - > open loop in the material liquid - computer control into the substitution alkali solution - 40 min insulation - tip sample cutting for color - computer control water;
Soap: add in the position that discharges water → material cylinder backflow material water → material cylinder glacial acetic acid → open cycle stir in material liquid → conputer controlled charging → material cylinder backflow material water → material cylinder add SW soaping agent → open cycle stir material liquid → conputer controlled charging → conputer controlled heat up → be incubated 10min → cooling → 65 DEG C point out a sample cutting check colors → conputer controlled washes → points out out cloth;
(7), drying and shaping:
Adopt Korea S's product reason and 9 joint baking oven setting machines to carry out sample cloth drying and shaping, this operation is singed for follow-up semi-finished product look base and is provided smooth fabrics cloth cover, to obtain quality of singing preferably;
Drying and shaping technique: be in the environment of 185 DEG C in temperature, processing speed is 60m/min;
Grey cloth situation after drying and shaping: door width 154cm, grammes per square metre 286g/m;
(8), look base is singed:
The method adopting Taizhou, Jiangsu natural gas gassing frame positive and negative respectively to burn once is singed to semi-finished product look base sample cloth, the fine hair that during to remove dyed, fabric produces, and increases the fineness of fabrics cloth cover;
Singeing: gas discharge 7, speed of a motor vehicle 110m/min;
Gas discharge 7 refers to the flow of 7 cubic meters per hour;
(9), washing is dried:
Full-width rinsing machine is adopted to wash, the fine hair dust that during to remove because singing, fabric face is residual, for Final finishing processing provides reliable quality assurance;
Washing process: water temperature is normal temperature, speed of a motor vehicle 50m/min, drying cylinder steam pressure is 0.2MPa;
(10), oil sizing:
Adopt Korea S to produce reason and 9 joint baking oven setting machines to oil sizing to sample cloth, the feel that this operation acquisition fabric is good and fabric have good DIMENSIONAL STABILITY and set;
Production technology: be in the environment of 195 DEG C in temperature, processing speed is 30m/min, 130 softener 15g/l;
Grey cloth situation after sizing: door width 152cm, grammes per square metre 290g/m, shrinkage 6%;
(11), Final finishing calendering:
Adopt German KKT calender to carry out calendering, the setting of this operation obtains fabrics cloth cover good gloss;
Calen-dering process: temperature is 60 DEG C, pressure is 150 handkerchiefs, speed of a motor vehicle 50m/min;
After calendering, sample cloth door width is 150cm;
(12), Final finishing tank steams:
Adopt Italian TMT tank to steam machine to arrange sample cloth, to obtain the simulate wool effect of fabric, after fabric sends into tank steaming machine, can swelling be there is in fabric fiber under the state that high temperature is damp and hot, the temperature that tank steams in machine steaming pot is 100-102 DEG C, and tank steaming machine adopts wool flannelette blanket to be rolled in tightly in interlayer by fabric, pass through high-temperature steam again, steam pressure is 0.3-0.4MPa, the temperature of high-temperature steam is 160-170 DEG C, Steam soak mode is first permeated from inside to outside, ecto-entad infiltration again, fabric cannot be swelling at diametric(al) fiber, can only be swelling towards warp-wise, again fabric is taken out cold front heavy rain after warp-wise is swelling, make the stabilization of fiber, the time arranged in tank steaming machine is 20-30 minute, the swelling resilience making fabric of warp-wise, stiffness improves greatly, wool-like effect is desirable,
The comfort property that tank makes fabric reach not only plentiful but also well-pressed after steaming, possesses all good feel;
(13), finished product inspection:
The presentation quality of fabric and inherent quality index are tested.
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| CN105369446B (en) * | 2015-12-17 | 2017-10-13 | 浙江航民股份有限公司 | A kind of production technology for washing viscous imitative woollen style fabric |
| CN106958152A (en) * | 2017-03-20 | 2017-07-18 | 杭州澳美印染有限公司 | A kind of brocade/bafta defeathering and the bath process of reactive dyeing one |
| CN107574544A (en) * | 2017-09-29 | 2018-01-12 | 上海嘉麟杰纺织品股份有限公司 | A kind of wet-guide quick-drying wool knitting fabrics and preparation method thereof |
| CN108130763A (en) * | 2017-12-19 | 2018-06-08 | 浙江航民股份有限公司 | A kind of cotton-containing fabrics defeathering, dyeing are the same as bath production technology |
| CN109594266A (en) * | 2018-10-12 | 2019-04-09 | 徐州华奥纺织有限公司 | A kind of textile printing and dyeing process |
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| CN102493223B (en) * | 2011-12-05 | 2016-01-13 | 青岛大学 | A kind of composition of aqueous solution of reactive dye for pad dyeing and compound method |
| CN102493224B (en) * | 2011-12-05 | 2016-01-13 | 青岛大学 | A kind of auxiliary for pad stack dyeing of reactive dye |
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