CN104213434A - Production method for outside pasting product pretreatment and cationic dye one-bath process dyeing - Google Patents
Production method for outside pasting product pretreatment and cationic dye one-bath process dyeing Download PDFInfo
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- CN104213434A CN104213434A CN201410399060.5A CN201410399060A CN104213434A CN 104213434 A CN104213434 A CN 104213434A CN 201410399060 A CN201410399060 A CN 201410399060A CN 104213434 A CN104213434 A CN 104213434A
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Abstract
The invention relates to a printing and dyeing method, and especially relates to a production method for outside pasting product pretreatment and cationic dye one-bath process dyeing. The method comprises the following steps: selecting a sample cloth, pre-setting a grey, singeing the grey, preparing a complex formulation assistant according to a formula, using the complex formulation assistant according to a ratio, designing a dyeing formula, carrying out jar dyeing on the cloth sample, carrying out hot setting, singeing the obtained color body, washing by water, drying, carrying out oiling setting, carrying out after-finishing calendering, carrying out after-finishing full decatizing, and examining the obtained finished product. The production method for for outside pasting product pretreatment and cationic dye one-bath process dyeing has obvious energy saving and emission reduction effects, and the handle elasticity, the color fullness and various quality indexes of fabrics obtained in the invention can meet requirements of different clients.
Description
Technical field
The present invention is a kind of dyeing method, particularly a kind of production method for the sticky product pre-treatment of sun, cation dyes one-bath dyeing.
Background technology
The sticky product of sun is generally all divided into two bath processings by fabric pretreatment and cationic dyeing in the time of dyeing and printing process, because the treatment fluid pH value difference in two kinds of processing and treating methods, meta-alkali is wanted in pre-treatment, and cationic dyeing requires meta-acid; If two kinds of processing modes are incorporated in in bathing and are processed, will have influence on processing or Color separately; Research and develop a kind of pre-treatment compound auxiliary that can allow the sticky product of sun process positive binding textiles under acid condition, for the production technology that changes the sticky pre-treatment dyeing processing of sun, the sticky production technology of sun is simplified, become particularly important.Be mainly to solve existing processing method long processing time, energy consumption is high, the problem that production cost is large.
Summary of the invention
The present invention solves the deficiencies in the prior art, replace the sticky product pre-treatment of traditional sun and cation dyes two and bathe production method, shorten the dyeing work flow of positive binding textiles, enhance productivity, reduce the energy resource consumption of water, electricity and gas, the production method for the sticky product pre-treatment of sun, cation dyes one-bath dyeing reducing production costs.
Above-mentioned technical problem of the present invention is mainly solved by following technical proposals:
For a production method for the sticky product pre-treatment of sun, cation dyes one-bath dyeing, carry out according to the following steps:
(1), choose sample cloth:
Choose a positive binding textiles sample cloth, openpore door width 166cm, grammes per square metre 285g/m, dyes Dark grey, washs strip and stays white;
The woven that the sticky product of sun is made up of 5% polyster fibre, 60% Cationic Dyeable Pet fiber and 35% viscose;
(2), grey cloth pre-setting:
Adopting Korea S to produce reason and 9 saves baking oven setting machines and carries out sample cloth pre-setting, setting process: in temperature is the environment of 175 DEG C, process, the speed of processing is 70m/min;
Grey cloth situation after pre-setting: door width 154cm, grammes per square metre 296g/m, shrinkage 3%;
(3), openpore is singed:
Adopt natural gas gassing frame positive and negative each method of burning once in Taizhou, Jiangsu to singe to sample cloth, singeing: 12 of gas discharges, speed of a motor vehicle 110m/min;
12 of gas discharges refer to the flow of 12 cubic meters per hour;
(4), compound auxiliary formula Design, preparation and consumption:
The design of compound auxiliary: OPE bleeding agent 5%, PAW refining agent 15%, C levelling agent 10%, water 70%, dyeing adds glacial acetic acid 2.5g/l while production;
The compound method of compound auxiliary: add 40% normal-temperature water in material bucket, add OPE bleeding agent 5%, PAW refining agent 15% and C levelling agent 10%, stirring and dissolving is after 15 minutes, then add 30% water, till continuing to be stirred to evenly;
The consumption of compound auxiliary: add compound auxiliary 2-4g/l when production;
Synthetic compound auxiliary must possess following performance:
1. must meet positive binding textiles pre-treatment and synchronize the condition of carrying out with cationic dyeing;
2. after processing, positive binding textiles capillary effect reaches traditional handicraft effect, little to the strength loss of fabric;
3. reproducibility is good, and process pH value stabilization is between 4-5, relatively little on the impact of cationic dyeing coloured light, and can improve the look flower being prone under traditional dyeing condition, the problem of dyestuff generation cohesion;
4. environmental protection, not containing banned substance, easily biological-degradable;
5. will have certain stability, long-term storage can keep relative stability.
(5), dyeing recipe design:
Heavily carry out cation dyes formula by cloth: 250%X-BL orchid: 0.2g/kg, 250%X-GL is golden yellow: 5.2g/kg, 250%X-GRL is red: 3.2g/kg;
Dyeing assistant formula: compound auxiliary 2.5g/l, glacial acetic acid 2.5g/l; Dyeing: process 40min in temperature is the environment of 135 DEG C;
REACTIVE DYES formula: ED-Q is black: 13g/kg, BF-3R Huang: 0.8g/kg, BF-3B is red: 1.6g/kg;
Vital staining auxiliary formula: glauber salt: 40g/l, soda ash: 5kg, substitute alkali 2g/l;
Vital staining technique: process 70min in temperature is the environment of 60 DEG C;
The formula of soaping after vital staining: SW soaping agent: 2kg, glacial acetic acid: 2kg;
The technique of soaping: process 10min in temperature is the environment of 75 DEG C;
Heavily fill a prescription by cloth;
(6), a sample cylinder dyeing:
Adopt east, a Taiwan military essence sample overflow dyeing machine to dye, dying operation work is adjusted and is dyed material to accounting place by dyeing recipe and sample cloth weight, has changed in accordance with regulations cation dyes and activity dyestuff, and material evenly exists without suspended particulate dyestuff;
The omnidistance dyeing production technology of controlling of computer for dyeing production procedure, dye bath ratio is pressed 1:9 dyeing:
Pre-treatment and cation dyes single bath process production overall process: discharge water position → point out of computer control is entered by hand cloth → operation into cloth → operative employee and after 2 minutes, in termination of pumping sensed water level → material cylinder backflow material water → material cylinder, added compound auxiliary → open cycle to stir the control of material liquid → computer to enter to add in auxiliary agent → material cylinder backflow material water → material cylinder glacial acetic acid → open cycle to stir the control of material liquid → computer to enter to add in auxiliary agent → material cylinder backflow material water → material cylinder cation dyes → open cycle to stir the control of material liquid → computer to enter dye solution → prompting and detect pH value → computer control 40min → cooling → 65 DEG C of heating up → be incubated and point out the control of check colors → computer of sample cutting to wash;
Reactive dyeing: put water level to the material back in the water and chemical material cylinder cylinder stir in reactive dye solution - > open loop, the material liquid - computer control in dye - is expected to return the water to the material cylinder on stir in 1/6 sodium sulphate - > open loop in the material liquid - computer control into sodium sulphate solution - change is expected to return the water to the material cylinder on stir in 2/6 sodium sulphate - > open loop in the material liquid - computer control into sodium sulphate solution - the cylinder to add 3/6 sodium sulphate - > open loop mix the material liquid to computer control into sodium sulphate solution, prompt detection conductivity 30 min - > change to computer control temperature, heat preservation material cylinder back in the water and chemical material cylinder stir in soda ash - > open loop, the material liquid - computer control into the soda solution - the expected return the water to the material cylinder on stir in 2/5 the substitution alkali - > open loop in the material liquid - computer control into the substitution alkali solution - the material cylinder on stir in 3/5 the substitution alkali - > open loop in the material liquid - computer control into the substitution alkali solution - 40 min insulation - tip sample cutting for color - computer control water;
Soap: in the position → material that discharges water cylinder backflow material water → material cylinder, add glacial acetic acid → open cycle to stir to add in material liquid → computer control charging → material cylinder backflow material water → material cylinder SW soaping agent → open cycle to stir material liquid → computer control charging → computer control 10min → cooling → 65 DEG C of heating up → be incubated and point out the control of check colors → computer of sample cutting to wash → point out out cloth;
(7), drying and shaping:
Adopt Korea S's product reason and 9 joint baking oven setting machines to carry out sample cloth drying and shaping, this operation is singed smooth fabrics cloth cover is provided for follow-up semi-finished product look base, to obtain the quality of singing preferably;
Drying and shaping technique: in temperature is the environment of 185 DEG C, processing speed is 60m/min;
Grey cloth situation after drying and shaping: door width 154cm, grammes per square metre 286g/m;
(8), look base is singed:
Adopt natural gas gassing frame positive and negative each method of burning once in Taizhou, Jiangsu to singe to semi-finished product look base sample cloth, the fine hair that when dyed to remove, fabric produces, the fineness of increase fabrics cloth cover;
Singeing: 7 of gas discharges, speed of a motor vehicle 110m/min;
7 of gas discharges refer to the flow of 7 cubic meters per hour;
(9), washing is dried:
Adopt Full-width rinsing machine to wash, to remove the residual fine hair dust of fabric face when singing, process reliable quality assurance is provided for rear arrangement;
Washing process: water temperature is normal temperature, speed of a motor vehicle 50m/min, drying cylinder steam pressure is 0.2MPa;
(10), the sizing that oils:
Adopt Korea S to produce reason and 9 and save baking oven setting machines to the sizing that oils of sample cloth, this operation is obtained feel that fabric is good and fabric and is had good DIMENSIONAL STABILITY and set;
Production technology: in temperature is the environment of 195 DEG C, processing speed is 30m/min, 130 softener 15g/l;
Grey cloth situation after sizing: door width 152cm, grammes per square metre 290g/m, shrinkage 6%;
(11), rear arrangement calendering:
Adopt German KKT calender to carry out calendering, the setting of this operation is to obtain fabrics cloth cover good gloss;
Calendering technique: temperature is 60 DEG C, pressure is 150 handkerchiefs, speed of a motor vehicle 50m/min;
After calendering, sample cloth door width is 150cm;
(12), rear arrangement tank steams:
Adopt Italian TMT tank to steam machine sample cloth is arranged, to obtain the simulate wool effect of fabric, fabric is sent into after tank steaming machine, can there is swelling in fabric fiber under the damp and hot state of high temperature, the temperature that tank steams in machine steaming pot is 100-102 DEG C, and tank steaming machine adopts wool flannelette blanket that fabric is rolled in interlayer tightly, pass through again high-temperature steam, steam pressure is 0.3-0.4MPa, the temperature of high-temperature steam is 160-170 DEG C, steam penetration mode is infiltration from inside to outside first, ecto-entad infiltration again, fabric cannot be swelling at diametric(al) fiber, can only be swelling towards warp-wise, after warp-wise is swelling, again fabric is taken out to cold wind cooling, make the stabilization of fiber, the time arranging in tank steaming machine is 20-30 minute, the swelling resilience that makes fabric of warp-wise, stiffness improves greatly, wool-like effect ideal,
Tank makes fabric reach not only plentiful but also well-pressed comfort property after steaming, and possesses all good feels;
(13), finished product inspection:
Presentation quality to fabric and inherent quality index are tested.
Pre-treatment and cation dyes single bath process are produced and are summed up: because the compound auxiliary of development has particularity, can under acid high-temperature and high-pressure conditions, dye to modified polyester fibre, slurry and the oligomer that can decompose, separate out in emulsification fabric, can prevent and treat fabric and produce look flower at dyeing course, dyestuff produces cohesion, the effect of avoiding specking to produce; Owing to being that omnidistance control of computer dyeed, the major control index (as water consumption, pH value, temperature rate etc.) in dyeing course can effectively be ensured, makes the stability of whole dyeing course have raising in addition.And to put sample process also more identical with laboratory; Thereby the long processing time that has solved traditional mode of production processing technology, energy consumption is high, the problem that production cost is large; Reach the object of abridged edition consumption reduction.
Therefore, the production method for the sticky product pre-treatment of sun, cation dyes one-bath dyeing provided by the invention, effects of energy saving and emission reduction is obvious, and pleasant softness, the color and luster plumpness etc. of fabric after production and processing; The inherent index of various quality etc. can meet different clients' requirement.
Detailed description of the invention
Below by embodiment, technical scheme of the present invention is described in further detail.
Embodiment 1: a kind of production method for the sticky product pre-treatment of sun, cation dyes one-bath dyeing, carry out according to the following steps:
(1), choose sample cloth:
Choose a positive binding textiles sample cloth, openpore door width 166cm, grammes per square metre 285g/m, dyes Dark grey, washs strip and stays white;
The woven that the sticky product of sun is made up of 5% polyster fibre, 60% Cationic Dyeable Pet fiber and 35% viscose;
(2), grey cloth pre-setting:
Adopting Korea S to produce reason and 9 saves baking oven setting machines and carries out sample cloth pre-setting, setting process: in temperature is the environment of 175 DEG C, process, the speed of processing is 70m/min;
Grey cloth situation after pre-setting: door width 154cm, grammes per square metre 296g/m, shrinkage 3%;
(3), openpore is singed:
Adopt natural gas gassing frame positive and negative each method of burning once in Taizhou, Jiangsu to singe to sample cloth, singeing: 12 of gas discharges, speed of a motor vehicle 110m/min;
12 of gas discharges refer to the flow of 12 cubic meters per hour;
(4), compound auxiliary formula Design, preparation and consumption:
The design of compound auxiliary: OPE bleeding agent 5%, PAW refining agent 15%, C levelling agent 10%, water 70%, dyeing adds glacial acetic acid 2.5g/l while production;
The compound method of compound auxiliary: add 40% normal-temperature water in material bucket, add OPE bleeding agent 5%, PAW refining agent 15% and C levelling agent 10%, stirring and dissolving is after 15 minutes, then add 30% water, till continuing to be stirred to evenly;
The consumption of compound auxiliary: add compound auxiliary 2g/l when production;
Synthetic compound auxiliary must possess following performance:
1. must meet positive binding textiles pre-treatment and synchronize the condition of carrying out with cationic dyeing;
2. after processing, positive binding textiles capillary effect reaches traditional handicraft effect, little to the strength loss of fabric;
3. reproducibility is good, and process pH value stabilization is between 4-5, relatively little on the impact of cationic dyeing coloured light, and can improve the look flower being prone under traditional dyeing condition, the problem of dyestuff generation cohesion;
4. environmental protection, not containing banned substance, easily biological-degradable;
5. will have certain stability, long-term storage can keep relative stability.
(5), dyeing recipe design:
Heavily carry out cation dyes formula by cloth: 250%X-BL orchid: 0.2g/kg, 250%X-GL is golden yellow: 5.2g/kg, 250%X-GRL is red: 3.2g/kg;
Dyeing assistant formula: compound auxiliary 2.5g/l, glacial acetic acid 2.5g/l; Dyeing: process 40min in temperature is the environment of 135 DEG C;
REACTIVE DYES formula: ED-Q is black: 13g/kg, BF-3R Huang: 0.8g/kg, BF-3B is red: 1.6g/kg;
Vital staining auxiliary formula: glauber salt: 40g/l, soda ash: 5kg, substitute alkali 2g/l;
Vital staining technique: process 70min in temperature is the environment of 60 DEG C;
The formula of soaping after vital staining: SW soaping agent: 2kg, glacial acetic acid: 2kg;
The technique of soaping: process 10min in temperature is the environment of 75 DEG C;
Heavily fill a prescription by cloth;
(6), a sample cylinder dyeing:
Adopt east, a Taiwan military essence sample overflow dyeing machine to dye, dying operation work is adjusted and is dyed material to accounting place by dyeing recipe and sample cloth weight, has changed in accordance with regulations cation dyes and activity dyestuff, and material evenly exists without suspended particulate dyestuff;
The omnidistance dyeing production technology of controlling of computer for dyeing production procedure, dye bath ratio is pressed 1:9 dyeing:
Pre-treatment and cation dyes single bath process production overall process: discharge water position → point out of computer control is entered by hand cloth → operation into cloth → operative employee and after 2 minutes, in termination of pumping sensed water level → material cylinder backflow material water → material cylinder, added compound auxiliary → open cycle to stir the control of material liquid → computer to enter to add in auxiliary agent → material cylinder backflow material water → material cylinder glacial acetic acid → open cycle to stir the control of material liquid → computer to enter to add in auxiliary agent → material cylinder backflow material water → material cylinder cation dyes → open cycle to stir the control of material liquid → computer to enter dye solution → prompting and detect pH value → computer control 40min → cooling → 65 DEG C of heating up → be incubated and point out the control of check colors → computer of sample cutting to wash;
Reactive dyeing: put water level to the material back in the water and chemical material cylinder cylinder stir in reactive dye solution - > open loop, the material liquid - computer control in dye - is expected to return the water to the material cylinder on stir in 1/6 sodium sulphate - > open loop in the material liquid - computer control into sodium sulphate solution - change is expected to return the water to the material cylinder on stir in 2/6 sodium sulphate - > open loop in the material liquid - computer control into sodium sulphate solution - the cylinder to add 3/6 sodium sulphate - > open loop mix the material liquid to computer control into sodium sulphate solution, prompt detection conductivity 30 min - > change to computer control temperature, heat preservation material cylinder back in the water and chemical material cylinder stir in soda ash - > open loop, the material liquid - computer control into the soda solution - the expected return the water to the material cylinder on stir in 2/5 the substitution alkali - > open loop in the material liquid - computer control into the substitution alkali solution - the material cylinder on stir in 3/5 the substitution alkali - > open loop in the material liquid - computer control into the substitution alkali solution - 40 min insulation - tip sample cutting for color - computer control water;
Soap: in the position → material that discharges water cylinder backflow material water → material cylinder, add glacial acetic acid → open cycle to stir to add in material liquid → computer control charging → material cylinder backflow material water → material cylinder SW soaping agent → open cycle to stir material liquid → computer control charging → computer control 10min → cooling → 65 DEG C of heating up → be incubated and point out the control of check colors → computer of sample cutting to wash → point out out cloth;
(7), drying and shaping:
Adopt Korea S's product reason and 9 joint baking oven setting machines to carry out sample cloth drying and shaping, this operation is singed smooth fabrics cloth cover is provided for follow-up semi-finished product look base, to obtain the quality of singing preferably;
Drying and shaping technique: in temperature is the environment of 185 DEG C, processing speed is 60m/min;
Grey cloth situation after drying and shaping: door width 154cm, grammes per square metre 286g/m;
(8), look base is singed:
Adopt natural gas gassing frame positive and negative each method of burning once in Taizhou, Jiangsu to singe to semi-finished product look base sample cloth, the fine hair that when dyed to remove, fabric produces, the fineness of increase fabrics cloth cover;
Singeing: 7 of gas discharges, speed of a motor vehicle 110m/min;
7 of gas discharges refer to the flow of 7 cubic meters per hour;
(9), washing is dried:
Adopt Full-width rinsing machine to wash, to remove the residual fine hair dust of fabric face when singing, process reliable quality assurance is provided for rear arrangement;
Washing process: water temperature is normal temperature, speed of a motor vehicle 50m/min, drying cylinder steam pressure is 0.2MPa;
(10), the sizing that oils:
Adopt Korea S to produce reason and 9 and save baking oven setting machines to the sizing that oils of sample cloth, this operation is obtained feel that fabric is good and fabric and is had good DIMENSIONAL STABILITY and set;
Production technology: in temperature is the environment of 195 DEG C, processing speed is 30m/min, 130 softener 15g/l;
Grey cloth situation after sizing: door width 152cm, grammes per square metre 290g/m, shrinkage 6%;
(11), rear arrangement calendering:
Adopt German KKT calender to carry out calendering, the setting of this operation is to obtain fabrics cloth cover good gloss;
Calendering technique: temperature is 60 DEG C, pressure is 150 handkerchiefs, speed of a motor vehicle 50m/min;
After calendering, sample cloth door width is 150cm;
(12), rear arrangement tank steams:
Adopt Italian TMT tank to steam machine sample cloth is arranged, to obtain the simulate wool effect of fabric, fabric is sent into after tank steaming machine, can there is swelling in fabric fiber under the damp and hot state of high temperature, the temperature that tank steams in machine steaming pot is 100 DEG C, and tank steaming machine adopts wool flannelette blanket that fabric is rolled in interlayer tightly, pass through again high-temperature steam, steam pressure is 0.3MPa, the temperature of high-temperature steam is 160 DEG C, steam penetration mode is infiltration from inside to outside first, ecto-entad infiltration again, fabric cannot be swelling at diametric(al) fiber, can only be swelling towards warp-wise, after warp-wise is swelling, again fabric is taken out to cold wind cooling, make the stabilization of fiber, the time arranging in tank steaming machine is 20 minutes, the swelling resilience that makes fabric of warp-wise, stiffness improves greatly, wool-like effect ideal,
Tank makes fabric reach not only plentiful but also well-pressed comfort property after steaming, and possesses all good feels;
(13), finished product inspection:
Presentation quality to fabric and inherent quality index are tested.
Embodiment 2: a kind of production method for the sticky product pre-treatment of sun, cation dyes one-bath dyeing, carry out according to the following steps:
(1), choose sample cloth:
Choose a positive binding textiles sample cloth, openpore door width 166cm, grammes per square metre 285g/m, dyes Dark grey, washs strip and stays white;
The woven that the sticky product of sun is made up of 5% polyster fibre, 60% Cationic Dyeable Pet fiber and 35% viscose;
(2), grey cloth pre-setting:
Adopting Korea S to produce reason and 9 saves baking oven setting machines and carries out sample cloth pre-setting, setting process: in temperature is the environment of 175 DEG C, process, the speed of processing is 70m/min;
Grey cloth situation after pre-setting: door width 154cm, grammes per square metre 296g/m, shrinkage 3%;
(3), openpore is singed:
Adopt natural gas gassing frame positive and negative each method of burning once in Taizhou, Jiangsu to singe to sample cloth, singeing: 12 of gas discharges, speed of a motor vehicle 110m/min;
12 of gas discharges refer to the flow of 12 cubic meters per hour;
(4), compound auxiliary formula Design, preparation and consumption:
The design of compound auxiliary: OPE bleeding agent 5%, PAW refining agent 15%, C levelling agent 10%, water 70%, dyeing adds glacial acetic acid 2.5g/l while production;
The compound method of compound auxiliary: add 40% normal-temperature water in material bucket, add OPE bleeding agent 5%, PAW refining agent 15% and C levelling agent 10%, stirring and dissolving is after 15 minutes, then add 30% water, till continuing to be stirred to evenly;
The consumption of compound auxiliary: add compound auxiliary 3g/l when production;
Synthetic compound auxiliary must possess following performance:
1. must meet positive binding textiles pre-treatment and synchronize the condition of carrying out with cationic dyeing;
2. after processing, positive binding textiles capillary effect reaches traditional handicraft effect, little to the strength loss of fabric;
3. reproducibility is good, and process pH value stabilization is between 4-5, relatively little on the impact of cationic dyeing coloured light, and can improve the look flower being prone under traditional dyeing condition, the problem of dyestuff generation cohesion;
4. environmental protection, not containing banned substance, easily biological-degradable;
5. will have certain stability, long-term storage can keep relative stability.
(5), dyeing recipe design:
Heavily carry out cation dyes formula by cloth: 250%X-BL orchid: 0.2g/kg, 250%X-GL is golden yellow: 5.2g/kg, 250%X-GRL is red: 3.2g/kg;
Dyeing assistant formula: compound auxiliary 2.5g/l, glacial acetic acid 2.5g/l; Dyeing: process 40min in temperature is the environment of 135 DEG C;
REACTIVE DYES formula: ED-Q is black: 13g/kg, BF-3R Huang: 0.8g/kg, BF-3B is red: 1.6g/kg;
Vital staining auxiliary formula: glauber salt: 40g/l, soda ash: 5kg, substitute alkali 2g/l;
Vital staining technique: process 70min in temperature is the environment of 60 DEG C;
The formula of soaping after vital staining: SW soaping agent: 2kg, glacial acetic acid: 2kg;
The technique of soaping: process 10min in temperature is the environment of 75 DEG C;
Heavily fill a prescription by cloth;
(6), a sample cylinder dyeing:
Adopt east, a Taiwan military essence sample overflow dyeing machine to dye, dying operation work is adjusted and is dyed material to accounting place by dyeing recipe and sample cloth weight, has changed in accordance with regulations cation dyes and activity dyestuff, and material evenly exists without suspended particulate dyestuff;
The omnidistance dyeing production technology of controlling of computer for dyeing production procedure, dye bath ratio is pressed 1:9 dyeing:
Pre-treatment and cation dyes single bath process production overall process: discharge water position → point out of computer control is entered by hand cloth → operation into cloth → operative employee and after 2 minutes, in termination of pumping sensed water level → material cylinder backflow material water → material cylinder, added compound auxiliary → open cycle to stir the control of material liquid → computer to enter to add in auxiliary agent → material cylinder backflow material water → material cylinder glacial acetic acid → open cycle to stir the control of material liquid → computer to enter to add in auxiliary agent → material cylinder backflow material water → material cylinder cation dyes → open cycle to stir the control of material liquid → computer to enter dye solution → prompting and detect pH value → computer control 40min → cooling → 65 DEG C of heating up → be incubated and point out the control of check colors → computer of sample cutting to wash;
Reactive dyeing: put water level to the material back in the water and chemical material cylinder cylinder stir in reactive dye solution - > open loop, the material liquid - computer control in dye - is expected to return the water to the material cylinder on stir in 1/6 sodium sulphate - > open loop in the material liquid - computer control into sodium sulphate solution - change is expected to return the water to the material cylinder on stir in 2/6 sodium sulphate - > open loop in the material liquid - computer control into sodium sulphate solution - the cylinder to add 3/6 sodium sulphate - > open loop mix the material liquid to computer control into sodium sulphate solution, prompt detection conductivity 30 min - > change to computer control temperature, heat preservation material cylinder back in the water and chemical material cylinder stir in soda ash - > open loop, the material liquid - computer control into the soda solution - the expected return the water to the material cylinder on stir in 2/5 the substitution alkali - > open loop in the material liquid - computer control into the substitution alkali solution - the material cylinder on stir in 3/5 the substitution alkali - > open loop in the material liquid - computer control into the substitution alkali solution - 40 min insulation - tip sample cutting for color - computer control water;
Soap: in the position → material that discharges water cylinder backflow material water → material cylinder, add glacial acetic acid → open cycle to stir to add in material liquid → computer control charging → material cylinder backflow material water → material cylinder SW soaping agent → open cycle to stir material liquid → computer control charging → computer control 10min → cooling → 65 DEG C of heating up → be incubated and point out the control of check colors → computer of sample cutting to wash → point out out cloth;
(7), drying and shaping:
Adopt Korea S's product reason and 9 joint baking oven setting machines to carry out sample cloth drying and shaping, this operation is singed smooth fabrics cloth cover is provided for follow-up semi-finished product look base, to obtain the quality of singing preferably;
Drying and shaping technique: in temperature is the environment of 185 DEG C, processing speed is 60m/min;
Grey cloth situation after drying and shaping: door width 154cm, grammes per square metre 286g/m;
(8), look base is singed:
Adopt natural gas gassing frame positive and negative each method of burning once in Taizhou, Jiangsu to singe to semi-finished product look base sample cloth, the fine hair that when dyed to remove, fabric produces, the fineness of increase fabrics cloth cover;
Singeing: 7 of gas discharges, speed of a motor vehicle 110m/min;
7 of gas discharges refer to the flow of 7 cubic meters per hour;
(9), washing is dried:
Adopt Full-width rinsing machine to wash, to remove the residual fine hair dust of fabric face when singing, process reliable quality assurance is provided for rear arrangement;
Washing process: water temperature is normal temperature, speed of a motor vehicle 50m/min, drying cylinder steam pressure is 0.2MPa;
(10), the sizing that oils:
Adopt Korea S to produce reason and 9 and save baking oven setting machines to the sizing that oils of sample cloth, this operation is obtained feel that fabric is good and fabric and is had good DIMENSIONAL STABILITY and set;
Production technology: in temperature is the environment of 195 DEG C, processing speed is 30m/min, 130 softener 15g/l;
Grey cloth situation after sizing: door width 152cm, grammes per square metre 290g/m, shrinkage 6%;
(11), rear arrangement calendering:
Adopt German KKT calender to carry out calendering, the setting of this operation is to obtain fabrics cloth cover good gloss;
Calendering technique: temperature is 60 DEG C, pressure is 150 handkerchiefs, speed of a motor vehicle 50m/min;
After calendering, sample cloth door width is 150cm;
(12), rear arrangement tank steams:
Adopt Italian TMT tank to steam machine sample cloth is arranged, to obtain the simulate wool effect of fabric, fabric is sent into after tank steaming machine, can there is swelling in fabric fiber under the damp and hot state of high temperature, the temperature that tank steams in machine steaming pot is 101 DEG C, and tank steaming machine adopts wool flannelette blanket that fabric is rolled in interlayer tightly, pass through again high-temperature steam, steam pressure is 0.35MPa, the temperature of high-temperature steam is 165 DEG C, steam penetration mode is infiltration from inside to outside first, ecto-entad infiltration again, fabric cannot be swelling at diametric(al) fiber, can only be swelling towards warp-wise, after warp-wise is swelling, again fabric is taken out to cold wind cooling, make the stabilization of fiber, the time arranging in tank steaming machine is 25 minutes, the swelling resilience that makes fabric of warp-wise, stiffness improves greatly, wool-like effect ideal,
Tank makes fabric reach not only plentiful but also well-pressed comfort property after steaming, and possesses all good feels;
(13), finished product inspection:
Presentation quality to fabric and inherent quality index are tested.
Embodiment 3: a kind of production method for the sticky product pre-treatment of sun, cation dyes one-bath dyeing, carry out according to the following steps:
(1), choose sample cloth:
Choose a positive binding textiles sample cloth, openpore door width 166cm, grammes per square metre 285g/m, dyes Dark grey, washs strip and stays white;
The woven that the sticky product of sun is made up of 5% polyster fibre, 60% Cationic Dyeable Pet fiber and 35% viscose;
(2), grey cloth pre-setting:
Adopting Korea S to produce reason and 9 saves baking oven setting machines and carries out sample cloth pre-setting, setting process: in temperature is the environment of 175 DEG C, process, the speed of processing is 70m/min;
Grey cloth situation after pre-setting: door width 154cm, grammes per square metre 296g/m, shrinkage 3%;
(3), openpore is singed:
Adopt natural gas gassing frame positive and negative each method of burning once in Taizhou, Jiangsu to singe to sample cloth, singeing: 12 of gas discharges, speed of a motor vehicle 110m/min;
12 of gas discharges refer to the flow of 12 cubic meters per hour;
(4), compound auxiliary formula Design, preparation and consumption:
The design of compound auxiliary: OPE bleeding agent 5%, PAW refining agent 15%, C levelling agent 10%, water 70%, dyeing adds glacial acetic acid 2.5g/l while production;
The compound method of compound auxiliary: add 40% normal-temperature water in material bucket, add OPE bleeding agent 5%, PAW refining agent 15% and C levelling agent 10%, stirring and dissolving is after 15 minutes, then add 30% water, till continuing to be stirred to evenly;
The consumption of compound auxiliary: add compound auxiliary 4g/l when production;
Synthetic compound auxiliary must possess following performance:
1. must meet positive binding textiles pre-treatment and synchronize the condition of carrying out with cationic dyeing;
2. after processing, positive binding textiles capillary effect reaches traditional handicraft effect, little to the strength loss of fabric;
3. reproducibility is good, and process pH value stabilization is between 4-5, relatively little on the impact of cationic dyeing coloured light, and can improve the look flower being prone under traditional dyeing condition, the problem of dyestuff generation cohesion;
4. environmental protection, not containing banned substance, easily biological-degradable;
5. will have certain stability, long-term storage can keep relative stability.
(5), dyeing recipe design:
Heavily carry out cation dyes formula by cloth: 250%X-BL orchid: 0.2g/kg, 250%X-GL is golden yellow: 5.2g/kg, 250%X-GRL is red: 3.2g/kg;
Dyeing assistant formula: compound auxiliary 2.5g/l, glacial acetic acid 2.5g/l; Dyeing: process 40min in temperature is the environment of 135 DEG C;
REACTIVE DYES formula: ED-Q is black: 13g/kg, BF-3R Huang: 0.8g/kg, BF-3B is red: 1.6g/kg;
Vital staining auxiliary formula: glauber salt: 40g/l, soda ash: 5kg, substitute alkali 2g/l;
Vital staining technique: process 70min in temperature is the environment of 60 DEG C;
The formula of soaping after vital staining: SW soaping agent: 2kg, glacial acetic acid: 2kg;
The technique of soaping: process 10min in temperature is the environment of 75 DEG C;
Heavily fill a prescription by cloth;
(6), a sample cylinder dyeing:
Adopt east, a Taiwan military essence sample overflow dyeing machine to dye, dying operation work is adjusted and is dyed material to accounting place by dyeing recipe and sample cloth weight, has changed in accordance with regulations cation dyes and activity dyestuff, and material evenly exists without suspended particulate dyestuff;
The omnidistance dyeing production technology of controlling of computer for dyeing production procedure, dye bath ratio is pressed 1:9 dyeing:
Pre-treatment and cation dyes single bath process production overall process: discharge water position → point out of computer control is entered by hand cloth → operation into cloth → operative employee and after 2 minutes, in termination of pumping sensed water level → material cylinder backflow material water → material cylinder, added compound auxiliary → open cycle to stir the control of material liquid → computer to enter to add in auxiliary agent → material cylinder backflow material water → material cylinder glacial acetic acid → open cycle to stir the control of material liquid → computer to enter to add in auxiliary agent → material cylinder backflow material water → material cylinder cation dyes → open cycle to stir the control of material liquid → computer to enter dye solution → prompting and detect pH value → computer control 40min → cooling → 65 DEG C of heating up → be incubated and point out the control of check colors → computer of sample cutting to wash;
Reactive dyeing: put water level to the material back in the water and chemical material cylinder cylinder stir in reactive dye solution - > open loop, the material liquid - computer control in dye - is expected to return the water to the material cylinder on stir in 1/6 sodium sulphate - > open loop in the material liquid - computer control into sodium sulphate solution - change is expected to return the water to the material cylinder on stir in 2/6 sodium sulphate - > open loop in the material liquid - computer control into sodium sulphate solution - the cylinder to add 3/6 sodium sulphate - > open loop mix the material liquid to computer control into sodium sulphate solution, prompt detection conductivity 30 min - > change to computer control temperature, heat preservation material cylinder back in the water and chemical material cylinder stir in soda ash - > open loop, the material liquid - computer control into the soda solution - the expected return the water to the material cylinder on stir in 2/5 the substitution alkali - > open loop in the material liquid - computer control into the substitution alkali solution - the material cylinder on stir in 3/5 the substitution alkali - > open loop in the material liquid - computer control into the substitution alkali solution - 40 min insulation - tip sample cutting for color - computer control water;
Soap: in the position → material that discharges water cylinder backflow material water → material cylinder, add glacial acetic acid → open cycle to stir to add in material liquid → computer control charging → material cylinder backflow material water → material cylinder SW soaping agent → open cycle to stir material liquid → computer control charging → computer control 10min → cooling → 65 DEG C of heating up → be incubated and point out the control of check colors → computer of sample cutting to wash → point out out cloth;
(7), drying and shaping:
Adopt Korea S's product reason and 9 joint baking oven setting machines to carry out sample cloth drying and shaping, this operation is singed smooth fabrics cloth cover is provided for follow-up semi-finished product look base, to obtain the quality of singing preferably;
Drying and shaping technique: in temperature is the environment of 185 DEG C, processing speed is 60m/min;
Grey cloth situation after drying and shaping: door width 154cm, grammes per square metre 286g/m;
(8), look base is singed:
Adopt natural gas gassing frame positive and negative each method of burning once in Taizhou, Jiangsu to singe to semi-finished product look base sample cloth, the fine hair that when dyed to remove, fabric produces, the fineness of increase fabrics cloth cover;
Singeing: 7 of gas discharges, speed of a motor vehicle 110m/min;
7 of gas discharges refer to the flow of 7 cubic meters per hour;
(9), washing is dried:
Adopt Full-width rinsing machine to wash, to remove the residual fine hair dust of fabric face when singing, process reliable quality assurance is provided for rear arrangement;
Washing process: water temperature is normal temperature, speed of a motor vehicle 50m/min, drying cylinder steam pressure is 0.2MPa;
(10), the sizing that oils:
Adopt Korea S to produce reason and 9 and save baking oven setting machines to the sizing that oils of sample cloth, this operation is obtained feel that fabric is good and fabric and is had good DIMENSIONAL STABILITY and set;
Production technology: in temperature is the environment of 195 DEG C, processing speed is 30m/min, 130 softener 15g/l;
Grey cloth situation after sizing: door width 152cm, grammes per square metre 290g/m, shrinkage 6%;
(11), rear arrangement calendering:
Adopt German KKT calender to carry out calendering, the setting of this operation is to obtain fabrics cloth cover good gloss;
Calendering technique: temperature is 60 DEG C, pressure is 150 handkerchiefs, speed of a motor vehicle 50m/min;
After calendering, sample cloth door width is 150cm;
(12), rear arrangement tank steams:
Adopt Italian TMT tank to steam machine sample cloth is arranged, to obtain the simulate wool effect of fabric, fabric is sent into after tank steaming machine, can there is swelling in fabric fiber under the damp and hot state of high temperature, the temperature that tank steams in machine steaming pot is 102 DEG C, and tank steaming machine adopts wool flannelette blanket that fabric is rolled in interlayer tightly, pass through again high-temperature steam, steam pressure is 0.4MPa, the temperature of high-temperature steam is 170 DEG C, steam penetration mode is infiltration from inside to outside first, ecto-entad infiltration again, fabric cannot be swelling at diametric(al) fiber, can only be swelling towards warp-wise, after warp-wise is swelling, again fabric is taken out to cold wind cooling, make the stabilization of fiber, the time arranging in tank steaming machine is 30 minutes, the swelling resilience that makes fabric of warp-wise, stiffness improves greatly, wool-like effect ideal,
Tank makes fabric reach not only plentiful but also well-pressed comfort property after steaming, and possesses all good feels;
(14), finished product inspection:
Presentation quality to fabric and inherent quality index are tested.
Fabric described in embodiment 1 to 3 possesses following technical parameter:
Gram weight: meet designing requirement (GB/T4668)
Water-fastness COLOR FASTNESS: GB/T 3921.3-1997
Colour fastness to rubbing: GB/T 3920-1997
Colour fastness to perspiration: GB/T 3922-1995
Washing size changing rate: GB/T 8629-2001 GB/T 8630-2001 GB/T 8628-2001
Pilling: GB/T 4802.1-1997
Ultimate strength: GB/T 3923.1-1997
Tearing brute force: GB/T 3917.1-1997
Wrinkle recovery angle: GB/T 3819-1997
Cloth cover pH value: GB/T 7573-1987.
Claims (1)
1. for a production method for the sticky product pre-treatment of sun, cation dyes one-bath dyeing, it is characterized in that carrying out according to the following steps:
(1), choose sample cloth:
Choose a positive binding textiles sample cloth, openpore door width 166cm, grammes per square metre 285g/m, dyes Dark grey, washs strip and stays white;
The woven that the sticky product of sun is made up of 5% polyster fibre, 60% Cationic Dyeable Pet fiber and 35% viscose;
(2), grey cloth pre-setting:
Adopting Korea S to produce reason and 9 saves baking oven setting machines and carries out sample cloth pre-setting, setting process: in temperature is the environment of 175 DEG C, process, the speed of processing is 70m/min;
Grey cloth situation after pre-setting: door width 154cm, grammes per square metre 296g/m, shrinkage 3%;
(3), openpore is singed:
Adopt natural gas gassing frame positive and negative each method of burning once in Taizhou, Jiangsu to singe to sample cloth, singeing: 12 of gas discharges, speed of a motor vehicle 110m/min;
12 of gas discharges refer to the flow of 12 cubic meters per hour;
(4), compound auxiliary formula Design, preparation and consumption:
The design of compound auxiliary: OPE bleeding agent 5%, PAW refining agent 15%, C levelling agent 10%, water 70%, dyeing adds glacial acetic acid 2.5g/l while production;
The compound method of compound auxiliary: add 40% normal-temperature water in material bucket, add OPE bleeding agent 5%, PAW refining agent 15% and C levelling agent 10%, stirring and dissolving is after 15 minutes, then add 30% water, till continuing to be stirred to evenly;
The consumption of compound auxiliary: add compound auxiliary 2-4g/l when production;
Synthetic compound auxiliary must possess following performance:
1. must meet positive binding textiles pre-treatment and synchronize the condition of carrying out with cationic dyeing;
2. after processing, positive binding textiles capillary effect reaches traditional handicraft effect, little to the strength loss of fabric;
3. reproducibility is good, and process pH value stabilization is between 4-5, relatively little on the impact of cationic dyeing coloured light, and can improve the look flower being prone under traditional dyeing condition, the problem of dyestuff generation cohesion;
4. environmental protection, not containing banned substance, easily biological-degradable;
5. will have certain stability, long-term storage can keep relative stability;
(5), dyeing recipe design:
Heavily carry out cation dyes formula by cloth: 250%X-BL orchid: 0.2g/kg, 250%X-GL is golden yellow: 5.2g/kg, 250%X-GRL is red: 3.2g/kg;
Dyeing assistant formula: compound auxiliary 2.5g/l, glacial acetic acid 2.5g/l; Dyeing: process 40min in temperature is the environment of 135 DEG C;
REACTIVE DYES formula: ED-Q is black: 13g/kg, BF-3R Huang: 0.8g/kg, BF-3B is red: 1.6g/kg;
Vital staining auxiliary formula: glauber salt: 40g/l, soda ash: 5kg, substitute alkali 2g/l;
Vital staining technique: process 70min in temperature is the environment of 60 DEG C;
The formula of soaping after vital staining: SW soaping agent: 2kg, glacial acetic acid: 2kg;
The technique of soaping: process 10min in temperature is the environment of 75 DEG C;
Heavily fill a prescription by cloth;
(6), a sample cylinder dyeing:
Adopt east, a Taiwan military essence sample overflow dyeing machine to dye, dying operation work is adjusted and is dyed material to accounting place by dyeing recipe and sample cloth weight, has changed in accordance with regulations cation dyes and activity dyestuff, and material evenly exists without suspended particulate dyestuff;
The omnidistance dyeing production technology of controlling of computer for dyeing production procedure, dye bath ratio is pressed 1:9 dyeing:
Pre-treatment and cation dyes single bath process production overall process: discharge water position → point out of computer control is entered by hand cloth → operation into cloth → operative employee and after 2 minutes, in termination of pumping sensed water level → material cylinder backflow material water → material cylinder, added compound auxiliary → open cycle to stir the control of material liquid → computer to enter to add in auxiliary agent → material cylinder backflow material water → material cylinder glacial acetic acid → open cycle to stir the control of material liquid → computer to enter to add in auxiliary agent → material cylinder backflow material water → material cylinder cation dyes → open cycle to stir the control of material liquid → computer to enter dye solution → prompting and detect pH value → computer control 40min → cooling → 65 DEG C of heating up → be incubated and point out the control of check colors → computer of sample cutting to wash;
Reactive dyeing: put water level to the material back in the water and chemical material cylinder cylinder stir in reactive dye solution - > open loop, the material liquid - computer control in dye - is expected to return the water to the material cylinder on stir in 1/6 sodium sulphate - > open loop in the material liquid - computer control into sodium sulphate solution - change is expected to return the water to the material cylinder on stir in 2/6 sodium sulphate - > open loop in the material liquid - computer control into sodium sulphate solution - the cylinder to add 3/6 sodium sulphate - > open loop mix the material liquid to computer control into sodium sulphate solution, prompt detection conductivity 30 min - > change to computer control temperature, heat preservation material cylinder back in the water and chemical material cylinder stir in soda ash - > open loop, the material liquid - computer control into the soda solution - the expected return the water to the material cylinder on stir in 2/5 the substitution alkali - > open loop in the material liquid - computer control into the substitution alkali solution - the material cylinder on stir in 3/5 the substitution alkali - > open loop in the material liquid - computer control into the substitution alkali solution - 40 min insulation - tip sample cutting for color - computer control water;
Soap: in the position → material that discharges water cylinder backflow material water → material cylinder, add glacial acetic acid → open cycle to stir to add in material liquid → computer control charging → material cylinder backflow material water → material cylinder SW soaping agent → open cycle to stir material liquid → computer control charging → computer control 10min → cooling → 65 DEG C of heating up → be incubated and point out the control of check colors → computer of sample cutting to wash → point out out cloth;
(7), drying and shaping:
Adopt Korea S's product reason and 9 joint baking oven setting machines to carry out sample cloth drying and shaping, this operation is singed smooth fabrics cloth cover is provided for follow-up semi-finished product look base, to obtain the quality of singing preferably;
Drying and shaping technique: in temperature is the environment of 185 DEG C, processing speed is 60m/min;
Grey cloth situation after drying and shaping: door width 154cm, grammes per square metre 286g/m;
(8), look base is singed:
Adopt natural gas gassing frame positive and negative each method of burning once in Taizhou, Jiangsu to singe to semi-finished product look base sample cloth, the fine hair that when dyed to remove, fabric produces, the fineness of increase fabrics cloth cover;
Singeing: 7 of gas discharges, speed of a motor vehicle 110m/min;
7 of gas discharges refer to the flow of 7 cubic meters per hour;
(9), washing is dried:
Adopt Full-width rinsing machine to wash, to remove the residual fine hair dust of fabric face when singing, process reliable quality assurance is provided for rear arrangement;
Washing process: water temperature is normal temperature, speed of a motor vehicle 50m/min, drying cylinder steam pressure is 0.2MPa;
(10), the sizing that oils:
Adopt Korea S to produce reason and 9 and save baking oven setting machines to the sizing that oils of sample cloth, this operation is obtained feel that fabric is good and fabric and is had good DIMENSIONAL STABILITY and set;
Production technology: in temperature is the environment of 195 DEG C, processing speed is 30m/min, 130 softener 15g/l;
Grey cloth situation after sizing: door width 152cm, grammes per square metre 290g/m, shrinkage 6%;
(11), rear arrangement calendering:
Adopt German KKT calender to carry out calendering, the setting of this operation is to obtain fabrics cloth cover good gloss;
Calendering technique: temperature is 60 DEG C, pressure is 150 handkerchiefs, speed of a motor vehicle 50m/min;
After calendering, sample cloth door width is 150cm;
(12), rear arrangement tank steams:
Adopt Italian TMT tank to steam machine sample cloth is arranged, to obtain the simulate wool effect of fabric, fabric is sent into after tank steaming machine, can there is swelling in fabric fiber under the damp and hot state of high temperature, the temperature that tank steams in machine steaming pot is 100-102 DEG C, and tank steaming machine adopts wool flannelette blanket that fabric is rolled in interlayer tightly, pass through again high-temperature steam, steam pressure is 0.3-0.4MPa, the temperature of high-temperature steam is 160-170 DEG C, steam penetration mode is infiltration from inside to outside first, ecto-entad infiltration again, fabric cannot be swelling at diametric(al) fiber, can only be swelling towards warp-wise, after warp-wise is swelling, again fabric is taken out to cold wind cooling, make the stabilization of fiber, the time arranging in tank steaming machine is 20-30 minute, the swelling resilience that makes fabric of warp-wise, stiffness improves greatly, wool-like effect ideal,
Tank makes fabric reach not only plentiful but also well-pressed comfort property after steaming, and possesses all good feels;
(13), finished product inspection:
Presentation quality to fabric and inherent quality index are tested.
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105239421A (en) * | 2015-10-19 | 2016-01-13 | 绍兴市华绅纺织品整理有限公司 | Method for producing heterochrome polyester viscose knitted fabric through low-salt and low-alkaline dyeing |
| CN105369446A (en) * | 2015-12-17 | 2016-03-02 | 浙江航民股份有限公司 | Production technology of polyester viscose imitation-wool style fabric |
| CN106958152A (en) * | 2017-03-20 | 2017-07-18 | 杭州澳美印染有限公司 | A kind of brocade/bafta defeathering and the bath process of reactive dyeing one |
| CN107574544A (en) * | 2017-09-29 | 2018-01-12 | 上海嘉麟杰纺织品股份有限公司 | A kind of wet-guide quick-drying wool knitting fabrics and preparation method thereof |
| CN108130763A (en) * | 2017-12-19 | 2018-06-08 | 浙江航民股份有限公司 | A kind of cotton-containing fabrics defeathering, dyeing are the same as bath production technology |
| CN109594266A (en) * | 2018-10-12 | 2019-04-09 | 徐州华奥纺织有限公司 | A kind of textile printing and dyeing process |
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| CN102493223A (en) * | 2011-12-05 | 2012-06-13 | 青岛大学 | Composition of aqueous solution of reactive dye for pad dyeing and preparation method thereof |
| CN102493224A (en) * | 2011-12-05 | 2012-06-13 | 青岛大学 | Auxiliary for pad stack dyeing of reactive dye |
| CN103422368A (en) * | 2012-05-22 | 2013-12-04 | 江南大学 | Dyeing method of cotton product reduced dye with low bath ratio |
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| JPH06184957A (en) * | 1992-12-17 | 1994-07-05 | Unitika Ltd | Production of animal hair textile product having multicolor effect |
| CN102493223A (en) * | 2011-12-05 | 2012-06-13 | 青岛大学 | Composition of aqueous solution of reactive dye for pad dyeing and preparation method thereof |
| CN102493224A (en) * | 2011-12-05 | 2012-06-13 | 青岛大学 | Auxiliary for pad stack dyeing of reactive dye |
| CN103422368A (en) * | 2012-05-22 | 2013-12-04 | 江南大学 | Dyeing method of cotton product reduced dye with low bath ratio |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105239421A (en) * | 2015-10-19 | 2016-01-13 | 绍兴市华绅纺织品整理有限公司 | Method for producing heterochrome polyester viscose knitted fabric through low-salt and low-alkaline dyeing |
| CN105369446A (en) * | 2015-12-17 | 2016-03-02 | 浙江航民股份有限公司 | Production technology of polyester viscose imitation-wool style fabric |
| CN106958152A (en) * | 2017-03-20 | 2017-07-18 | 杭州澳美印染有限公司 | A kind of brocade/bafta defeathering and the bath process of reactive dyeing one |
| CN107574544A (en) * | 2017-09-29 | 2018-01-12 | 上海嘉麟杰纺织品股份有限公司 | A kind of wet-guide quick-drying wool knitting fabrics and preparation method thereof |
| CN108130763A (en) * | 2017-12-19 | 2018-06-08 | 浙江航民股份有限公司 | A kind of cotton-containing fabrics defeathering, dyeing are the same as bath production technology |
| CN109594266A (en) * | 2018-10-12 | 2019-04-09 | 徐州华奥纺织有限公司 | A kind of textile printing and dyeing process |
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|---|---|
| CN104213434B (en) | 2016-03-09 |
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