CN107988816A - A kind of reactive dye quickly go up dyeing technique - Google Patents

A kind of reactive dye quickly go up dyeing technique Download PDF

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Publication number
CN107988816A
CN107988816A CN201711376690.0A CN201711376690A CN107988816A CN 107988816 A CN107988816 A CN 107988816A CN 201711376690 A CN201711376690 A CN 201711376690A CN 107988816 A CN107988816 A CN 107988816A
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dyeing
cylinder
water
computer
setting
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施鹤鸣
沈江锋
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ZHEJIANG HANGMIN STOCK CO Ltd
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ZHEJIANG HANGMIN STOCK CO Ltd
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Priority to CN201711376690.0A priority Critical patent/CN107988816A/en
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    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/38General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using reactive dyes
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06LDRY-CLEANING, WASHING OR BLEACHING FIBRES, FILAMENTS, THREADS, YARNS, FABRICS, FEATHERS OR MADE-UP FIBROUS GOODS; BLEACHING LEATHER OR FURS
    • D06L1/00Dry-cleaning or washing fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods
    • D06L1/12Dry-cleaning or washing fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods using aqueous solvents
    • D06L1/14De-sizing
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06LDRY-CLEANING, WASHING OR BLEACHING FIBRES, FILAMENTS, THREADS, YARNS, FABRICS, FEATHERS OR MADE-UP FIBROUS GOODS; BLEACHING LEATHER OR FURS
    • D06L4/00Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs
    • D06L4/10Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs using agents which develop oxygen
    • D06L4/12Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs using agents which develop oxygen combined with specific additives
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06LDRY-CLEANING, WASHING OR BLEACHING FIBRES, FILAMENTS, THREADS, YARNS, FABRICS, FEATHERS OR MADE-UP FIBROUS GOODS; BLEACHING LEATHER OR FURS
    • D06L4/00Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs
    • D06L4/10Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs using agents which develop oxygen
    • D06L4/13Bleaching fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods; Bleaching leather or furs using agents which develop oxygen using inorganic agents
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/16General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dispersed, e.g. acetate, dyestuffs
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P3/00Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
    • D06P3/82Textiles which contain different kinds of fibres
    • D06P3/8204Textiles which contain different kinds of fibres fibres of different chemical nature
    • D06P3/8223Textiles which contain different kinds of fibres fibres of different chemical nature mixtures of fibres containing hydroxyl and ester groups
    • D06P3/8228Textiles which contain different kinds of fibres fibres of different chemical nature mixtures of fibres containing hydroxyl and ester groups using one kind of dye
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P5/00Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
    • D06P5/02After-treatment

Abstract

The present invention is a kind of quickly upper dyeing technique, the quick upper dyeing technique of more particularly to a kind of reactive dye.Carry out according to the following steps:Choose sample cloth → technical flow design → alkali desizing design → fabric pre-setting → openpore singe → mercerising setting → oxygen bleaching setting → dyeing recipe and a dyeing setting → sample cylinder dyeing → drying (oiling) shape setting → final finishing calendering → final finishing finished product preshrunk → product inspection.Production capacity is increased substantially, shortens production time positive effect, reduces human intervention, the correctness of color is improved, can meet the requirement of different clients in various quality in index etc..

Description

A kind of reactive dye quickly go up dyeing technique
Technical field
The present invention is a kind of quickly upper dyeing technique, the quick upper dyeing technique of more particularly to a kind of reactive dye.
Background technology
In existing vital staining, the traditional processing technology of generally use, i.e., go up anhydrous sodium sulphate in batches, and upper dyestuff, is protected in batches Wen Houzai upper soda ash, then keep the temperature in batches, water outlet, soaps, and technological process length, human intervention factor is big, and stability, repeatability are poor.
The content of the invention
The present invention mainly solves the deficiencies in the prior art, there is provided a kind of production department coordinates, it is desirable to the production work Skill improves reactive dyeing productivity effect on the premise of various fastness are not influenced, and reduces one kind activity dye of energy consumption The quick upper dyeing technique of material.
The above-mentioned technical problem of the present invention is mainly what is be addressed by following technical proposals:
A kind of reactive dye quickly go up dyeing technique, are carried out according to the following steps:
(1), sample cloth is chosen:
The T/C fabric sample cloth that a coupe degree is 80 meters or so is chosen, openpore door width 160cm, grammes per square metre 120g/ ㎡, contaminate black Color;
The woven that T/C products are made of 65% polyester fiber and 35% cotton fiber;
(2), technical flow design:It is de- to turn over cloth → alkali desizing → pre-setting → openpore and singe → mercerising → oxygen bleaching → dyeing → Water → open-width → drying (oiling) sizing → calendering → finished product preshrunk → inspection yardstick;
(3), alkali desizing designs:Desizing is carried out to sample cloth using joint desizing machine;
Desizing auxiliary formula:
Alkali concn:30g/l
OD:2.5g/l
Hydrogen peroxide:2g/l
100 DEG C of temperature, soaking time:45 points;It is required that detection desizing is clean;
(4), fabric pre-setting:
Using South Korea production day it is new 9 section baking oven forming machine to sample cloth carry out pre-setting, 195 DEG C × 98m/min of setting process, Fabric situation after pre-setting:Door width 151cm, grammes per square metre 120g/ ㎡, shrinkage 3%;
(5), openpore is singed:
The method respectively burnt using Jiangsu Taizhou natural gas gassing frame positive and negative once singes sample cloth, singeing: Gas discharge 18, speed 120m/min.It is required that singe more than 4 grades;
(6), mercerising is set:Alkali concn:200g/l, speed:50m/min, door width:151cm, tension force:2kg;
(7), oxygen bleaching is set:Oxygen bleaching is carried out to fabric using joint oxygen bleaching machine:
Oxygenic bleaching aids formula:
Hydrogen peroxide:2g/l
Hydrogen peroxide stabilizer:0.2g/l
Make composite assistant by oneself:2g/l
100 DEG C of temperature, soaking time:40 points;
(8), dyeing recipe and dyeing are set:
Disperse dye prescription (o.w.f):
150% disperses black ECO:7%
100% disperse yellow brown 2RL:2%
100% dispersed ruby 5BL:0.16%
Glacial acetic acid 0.5g/l (adjusts dye bath pH value:5-5.5)
Dyeing:130℃×40min.
Reactive dye formula (o.w.f):
100% active black ED-Q:1.9%
100% active yellow BF-3R:0.96%
100% active red 3BSN:0.37%
Anhydrous sodium sulphate:44g/l,
Soda ash:1kg/ cylinders,
Substitute alkali:2.2g/l;
Activity staining procedure:60℃×70min;
Soap after vital staining formula:
Soaping agent SW:0.5g/l
Glacial acetic acid:0.2g/l
Soap technique:75℃×10min.
(9), a sample cylinder dyeing:
Using the eastern military essence sample overflow dyeing machine dyeing in Taiwan, dying operation work presses dyeing recipe and sample cloth weight to accounting Place adjusts dye material, and by the good disperse dyes of regulationization and activity dye dyestuff, material uniformly exists without suspended particulate dyestuff;
Dyeing production procedure, (with computer whole-process control dyeing production technology, dye bath ratio presses 1:9 dyeing):
Disperse dyeing overall process:Computer controls the position → prompting cloth feeding → operative employee's craft cloth feeding → operation 2 that discharges water to divide Glacial acetic acid → open cycle stirring material liquid → electricity is added after clock in termination of pumping sensed water level → material cylinder reflux material water → material cylinder Brain adds disperse dyes → open cycle stirring material liquid → electricity in controlling into glacial acetic acid → material cylinder reflux material water → material cylinder Brain is controlled into dye solution → prompting detection pH value → 130 DEG C → insulation of computer control heating 40min → cooling → 65 DEG C prompting Sample cutting is to color → computer control washing;
Reactive dyeing:Position → material cylinder reflux material water → the computer that discharges water control into anhydrous sodium sulphate solution (anhydrous sodium sulphate by Feed proportioning system is sent directly into material bucket) add in → prompting detection electrical conductivity → material cylinder reflux material water → material cylinder soda ash → Open cycle stirring material liquid → computer added in controlling into soda ash solution → material cylinder reflux material water → material cylinder substitute alkali → Open cycle stirring material liquid → computer adds activity dye in controlling into alternative aqueous slkali → material cylinder reflux material water → material cylinder Material solution → open cycle stirring material liquid → computer is controlled to be cut into dyestuff → computer control heating 60 DEG C → insulation 70min → prompting Sample is to color → computer control washing;
Soap:Discharge water add in position → material cylinder reflux material water → material cylinder glacial acetic acid → open cycle stirring material liquid → SW soaping agents → open cycle stirring material liquid → computer is added in computer control charging → material cylinder reflux material water → material cylinder Control charging → computer control heating 75 DEG C → insulation 10min → cooling → 65 DEG C prompting sample cutting to color → computer control washing → Prompt cloth outputting;
(10), (oiling) sizing setting is dried:Using South Korea's production day new 9 section baking oven forming machine
130 silicone oil of rivers and mountains:15g/l、
Temperature:195℃
Speed:80m/min
Door width:154cm
Grammes per square metre:118g/㎡
(11), final finishing calendering:
Calendering is carried out using German KKT calenders, the setting of this process mainly obtains fabrics cloth cover good gloss.Calendering Technique:100 DEG C, pressure 250kg, speed 50m/min of temperature;Sample cloth door width 150cm after calendering;
(12), final finishing finished product preshrunk:
Shrunk finish is carried out to galatea using Zheng's frame preshrinking machine, to obtain the good dimensional stability of galatea;Make Fabric reaches not only soft but also well-pressed comfort feel.Production technology:Rubber blanket pressure 15MPa, steam pressure 1.5kg, speed 45m/min, within shrinkage control 3%;
(13), product inspection:
Presentation quality and inherent quality index to fabric are tested.
To solve present situation, company technique exploitation section organizes related technical personnel, and research and design goes out the short stream of vital staining Journey technique, on the premise of quality is not influenced, reduces human intervention factor, improves the stability of dyeing, shorten technique, improve dye Cylinder production capacity, so as to achieve the purpose that abridged edition lowers consumption.
The present invention is used for the method for reactive dyeing production technology, increases substantially production capacity, shortens the production time Positive effect, reduces human intervention, improves the correctness of color, various quality are interior can to meet wanting for different clients in index etc. Ask.
Embodiment
Below by embodiment, the technical solutions of the present invention will be further described.
Embodiment 1:
(1), fabric is chosen:
Choose the T/C fabric sample cloth that a cylinder length is 2000 meters or so, openpore door width 160cm, grammes per square metre 120g/ ㎡, dye Grey;
The woven that T/C products are generally made of 65% polyester fiber and 35% cotton fiber;
(2) technical flow design:It is de- to turn over cloth → alkali desizing → pre-setting → openpore and singe → mercerising → oxygen bleaching → dyeing → Water → open-width → drying (oiling) sizing → calendering → finished product preshrunk → inspection yardstick;
(3), alkali desizing designs:Desizing is carried out to sample cloth using joint desizing machine;
Desizing auxiliary formula:
Alkali concn:30g/l
OD:2.5g/l
Hydrogen peroxide:2g/l
100 DEG C of temperature, soaking time:45 points;It is required that detection desizing is clean;
(4), fabric pre-setting:
Using South Korea production day it is new 9 section baking oven forming machine to fabric carry out pre-setting, 195 DEG C × 98m/min of setting process, Fabric situation after pre-setting:Door width 151cm, grammes per square metre 122g/ ㎡, shrinkage 3.5%;
(5), openpore is singed:
The method respectively burnt using Jiangsu Taizhou natural gas gassing frame positive and negative once singes sample cloth, singeing: Gas discharge 20, speed 110m/min.It is required that singe more than 4 grades;
(6), mercerising is set:Alkali concn:240g/l, speed:50m/min, door width:151cm, tension force:2kg;
(7), oxygen bleaching is set:Oxygen bleaching is carried out to fabric using joint oxygen bleaching machine:
Oxygenic bleaching aids formula:
Hydrogen peroxide:2.5g/l
Hydrogen peroxide stabilizer:0.25g/l
Make composite assistant by oneself:3g/l
100 DEG C of temperature, soaking time:50 points;
(8), dyeing recipe and dyeing are set:
Disperse dye prescription (o.w.f):
N ashes:1.3%
SE-RGFL is yellow:0.4%
3B is red:0.36%
Glacial acetic acid 0.5g/l
Dyeing:130℃×20min.
Reactive dye formula (o.w.f):
Refined lattice element BF-BN is dark blue:0.35%
Refined lattice element BF-3R is yellow:0.3%
Refined lattice element BF-3B is red:0.14%
Vital staining auxiliary formula:
Anhydrous sodium sulphate:25g/l
Soda ash:8kg/ cylinders
Substitute alkali:1.5g/l
Activity staining procedure:60℃×70min;
Soap after vital staining formula:
SW soaping agents:0.5g/l
Acetic acid:0.3g/l
Soap technique:75℃×10min.
(9), machine cylinder dyes:
Using the military smart overflow dyeing machine dyeing in 500kg east, dying operation work is by dyeing recipe and fabric weight at accounting Dye material is adjusted, by the good disperse dyes of regulationization and activity dye dyestuff, material uniformly exists without suspended particulate dyestuff;
Dyeing production procedure, (with computer whole-process control dyeing production technology, dye bath ratio presses 1:9 dyeing):
Disperse dyeing overall process:Computer controls the position → prompting cloth feeding → operative employee's craft cloth feeding → operation 2 that discharges water to divide Glacial acetic acid → open cycle stirring material liquid → electricity is added after clock in termination of pumping sensed water level → material cylinder reflux material water → material cylinder Brain adds disperse dyes → open cycle stirring material liquid → electricity in controlling into glacial acetic acid → material cylinder reflux material water → material cylinder Brain is controlled into dye solution → prompting detection pH value → 130 DEG C → insulation of computer control heating 20min → cooling → 65 DEG C prompting Sample cutting is to color → computer control washing;
Reactive dyeing:Position → material cylinder reflux material water → the computer that discharges water control into anhydrous sodium sulphate solution (anhydrous sodium sulphate by Feed proportioning system is sent directly into material bucket) add in → prompting detection electrical conductivity → material cylinder reflux material water → material cylinder soda ash → Open cycle stirring material liquid → computer added in controlling into soda ash solution → material cylinder reflux material water → material cylinder substitute alkali → Open cycle stirring material liquid → computer adds activity dye in controlling into alternative aqueous slkali → material cylinder reflux material water → material cylinder Material solution → open cycle stirring material liquid → computer is controlled to be cut into dyestuff → computer control heating 60 DEG C → insulation 70min → prompting Sample is to color → computer control washing;
Soap:Discharge water add in position → material cylinder reflux material water → material cylinder glacial acetic acid → open cycle stirring material liquid → SW soaping agents → open cycle stirring material liquid → computer is added in computer control charging → material cylinder reflux material water → material cylinder Control charging → computer control heating 75 DEG C → insulation 10min → cooling → 65 DEG C prompting sample cutting to color → computer control washing → Prompt cloth outputting;
(10), (oiling) sizing setting is dried:Using South Korea's production day new 9 section baking oven forming machine
130 silicone oil of rivers and mountains:15g/l
195 DEG C of temperature
Speed 70m/min
Door width 154cm
Grammes per square metre 118g/ ㎡;
(11), final finishing calendering:
Calendering is carried out using German KKT calenders, the setting of this process mainly obtains fabrics cloth cover good gloss.Calendering Technique:100 DEG C, pressure 250kg, speed 50m/min of temperature;Sample cloth door width 150cm after calendering;
(12), final finishing finished product preshrunk:
Shrunk finish is carried out to galatea using Zheng's frame preshrinking machine, to obtain the good dimensional stability of galatea;Make Fabric reaches not only soft but also well-pressed comfort feel.Production technology:Rubber blanket pressure 15MPa, steam pressure 1.5kg, speed 45m/min, within shrinkage control 3%;
(13) product inspection:
Presentation quality and inherent quality index to fabric are tested.
Embodiment 2:
(1), fabric is chosen:
Choose the T/R fabric sample cloth that a cylinder length is 1800 meters or so, openpore door width 160cm, grammes per square metre 135g/ ㎡, dye Navy;
The woven that T/R products are generally made of 65% polyester fiber and 35% viscose rayon;
(2) technical flow design:Turn over cloth → alkali desizing → pre-setting → openpore is singed → and dye → be dehydrated → open-width → baking Yardstick is examined in dry (oiling) sizing → calendering → tank steams →;
(3), alkali desizing designs:Desizing is carried out to sample cloth using joint desizing machine;
Desizing auxiliary formula:
Alkali concn:30g/l
OD:2.5g/l
100 DEG C of temperature, soaking time:40 points;It is required that detection desizing is clean;
(4), fabric pre-setting:
Using South Korea production day it is new 9 section baking oven forming machine to fabric carry out pre-setting, 190 DEG C × 98m/min of setting process, Fabric situation after pre-setting:Door width 151cm, grammes per square metre 132g/ ㎡, shrinkage 3%;
(5), openpore is singed:
The method respectively burnt using Jiangsu Taizhou natural gas gassing frame positive and negative once singes sample cloth, singeing: Gas discharge 16, speed 120m/min.It is required that singe more than 4 grades;
(6), dyeing recipe and dyeing are set:
Disperse dye prescription (o.w.f):
150%EX-SF is blue:2.8%
200%SE-3RLN oranges:0.66%
S-2GFL carbunclies:0.42%
Glacial acetic acid 0.7g/l
Dyeing:135℃×40min.
Reactive dye formula (o.w.f):
Refined lattice element BF-RRN is dark blue:2%
Refined lattice element BF-3R is yellow:0.8%
Refined lattice element BF-3B is red:0.9%
Vital staining auxiliary formula:
Anhydrous sodium sulphate:35g/l,
Soda ash:5kg/ cylinders;
Substitute alkali:1.5g/l
Activity staining procedure:65℃×70min;
Soap after vital staining formula:
SW soaping agents:2kg/ cylinders
Glacial acetic acid:2kg/ cylinders
Soap technique:75℃×10min
(7) machine cylinder dyes:
Using the military smart overflow dyeing machine dyeing in 500kg east, dying operation work is by dyeing recipe and fabric weight at accounting Dye material is adjusted, by the good disperse dyes of regulationization and activity dye dyestuff, material uniformly exists without suspended particulate dyestuff;
Dyeing production procedure, (with computer whole-process control dyeing production technology, dye bath ratio presses 1:9 dyeing):
Disperse dyeing overall process:Computer controls the position → prompting cloth feeding → operative employee's craft cloth feeding → operation 2 that discharges water to divide Glacial acetic acid → open cycle stirring material liquid → electricity is added after clock in termination of pumping sensed water level → material cylinder reflux material water → material cylinder Brain adds disperse dyes → open cycle stirring material liquid → electricity in controlling into glacial acetic acid → material cylinder reflux material water → material cylinder Brain is controlled into dye solution → prompting detection pH value → 130 DEG C → insulation of computer control heating 40min → cooling → 65 DEG C prompting Sample cutting is to color → computer control washing;
Reactive dyeing:Position → material cylinder reflux material water → the computer that discharges water control into anhydrous sodium sulphate solution (anhydrous sodium sulphate by Feed proportioning system is sent directly into material bucket) add in → prompting detection electrical conductivity → material cylinder reflux material water → material cylinder soda ash → Open cycle stirring material liquid → computer added in controlling into soda ash solution → material cylinder reflux material water → material cylinder substitute alkali → Open cycle stirring material liquid → computer adds activity dye in controlling into alternative aqueous slkali → material cylinder reflux material water → material cylinder Material solution → open cycle stirring material liquid → computer is controlled to be cut into dyestuff → computer control heating 60 DEG C → insulation 70min → prompting Sample is to color → computer control washing;
Soap:Discharge water add in position → material cylinder reflux material water → material cylinder glacial acetic acid → open cycle stirring material liquid → SW soaping agents → open cycle stirring material liquid → computer is added in computer control charging → material cylinder reflux material water → material cylinder Control charging → computer control heating 75 DEG C → insulation 10min → cooling → 65 DEG C prompting sample cutting to color → computer control washing → Prompt cloth outputting;
(8), (oiling) sizing setting is dried:Using South Korea's production day new 9 section baking oven forming machine
130 silicone oil of rivers and mountains:15g/l
150 silicone oil of rivers and mountains:5g/l
190 DEG C of temperature
Speed 40m/min
Door width 156cm
Grammes per square metre 130g/ ㎡
(9), final finishing calendering:
Calendering is carried out using German KKT calenders, the setting of this process mainly obtains fabrics cloth cover good gloss.Calendering Technique:150 DEG C, pressure 250kg, speed 50m/min of temperature;Sample cloth door width 153cm after calendering;
(10), final finishing tank steams:
Machine is steamed using Italy's production TMT tanks and carries out tank steaming:
Tank steams technique:It is 100-102 DEG C, steam pressure 0.3-0.4MPa that tank, which steams temperature, and Steam soak mode is first by interior Permeated to exosmosis, then ecto-entad, the time arranged in tank steaming machine is 30-35 minutes;(11) product inspection:
Presentation quality and inherent quality index to fabric are tested.
Embodiment 3:
(1), fabric is chosen:
Choose the cotton Bali voile fabric that a cylinder length is 2600 meters or so, openpore door width 160cm, grammes per square metre 80g/ ㎡, Contaminate black;
(2) technical flow design:Cloth → openpore is turned over to singe → alkali desizing → mercerising → oxygen bleaching → dyeing → dehydration → open-width → drying (oiling) sizing → inspection yardstick;
(3), openpore is singed:
The method respectively burnt using Jiangsu Taizhou natural gas gassing frame positive and negative once singes sample cloth, singeing: Gas discharge 12, speed 120m/min.It is required that singe more than 4 grades;
(3), alkali desizing designs:Desizing is carried out to fabric using joint desizing machine;
Desizing auxiliary formula:
Alkali concn:30g/l
OD:2.5g/l
Hydrogen peroxide:2g/l
100 DEG C of temperature, soaking time:45 points;It is required that detection desizing is clean;
(4), mercerising is set:Alkali concn:240g/l, speed:50m/min, door width:151cm, tension force, 2kg
(5), oxygen bleaching is set:Oxygen bleaching is carried out to fabric using joint oxygen bleaching machine;
Oxygenic bleaching aids formula:
Hydrogen peroxide:2.5g/l
Hydrogen peroxide stabilizer:0.25g/l
Make composite assistant by oneself:3g/l
(6) reactive dye formula (o.w.f):
ED-Q is black:4%
Refined lattice element BF-3R:0.5%
Refined lattice element BF-DR is red:0.2%
Vital staining auxiliary formula:
Anhydrous sodium sulphate:44g/l
Soda ash:8kg/ cylinders
Substitute alkali:2.5g/l
Activity staining procedure:60℃×80min;
Soap after vital staining formula:
SW soaping agents:2kg/ cylinders
Acetic acid:1kg/ cylinders
Soap technique:75℃×10min.
(7) machine cylinder dyes:
Using the military smart overflow dyeing machine dyeing in 500kg east, dying operation work is by dyeing recipe and fabric weight at accounting Dye material is adjusted, by the good reactive dye of regulationization, material uniformly exists without suspended particulate dyestuff;
Reactive dyeing:Position → material cylinder reflux material water → the computer that discharges water control into anhydrous sodium sulphate solution (anhydrous sodium sulphate by Feed proportioning system is sent directly into material bucket) add in → prompting detection electrical conductivity → material cylinder reflux material water → material cylinder soda ash → Open cycle stirring material liquid → computer added in controlling into soda ash solution → material cylinder reflux material water → material cylinder substitute alkali → Open cycle stirring material liquid → computer adds activity dye in controlling into alternative aqueous slkali → material cylinder reflux material water → material cylinder Material solution → open cycle stirring material liquid → computer is controlled to be cut into dyestuff → computer control heating 60 DEG C → insulation 80min → prompting Sample is to color → computer control washing;
Soap:Discharge water add in position → material cylinder reflux material water → material cylinder glacial acetic acid → open cycle stirring material liquid → SW soaping agents → open cycle stirring material liquid → computer is added in computer control charging → material cylinder reflux material water → material cylinder Control charging → computer control heating 75 DEG C → insulation 10min → cooling → 65 DEG C prompting sample cutting to color → computer control washing → Prompt cloth outputting;
(8), (oiling) sizing setting is dried:Using South Korea's production day new 9 section baking oven forming machine
130 silicone oil of rivers and mountains:5g/l
150 silicone oil of rivers and mountains:10g/l
190 DEG C of temperature
Speed 80m/min
Door width 150cm
Grammes per square metre 78g/ ㎡
(9) product inspection:
Presentation quality and inherent quality index to fabric are tested.
Fabric described in embodiment 1 to 3 possesses following technical parameter:
Gram weight:Meet design requirement (GB/T4668)
Washing color fastness:GB/T 3921.3-1997
Colour fastness to rubbing:GB/T 3920-1997
Colour fastness to perspiration:GB/T 3922-1995
Wash size changing rate:GB/T 8629-2001 GB/T 8630-2001 GB/T 8628-2001
Pilling:GB/T 4802.1-1997
Ultimate strength:GB/T 3923.1-1997
Tearing brute force:GB/T 3917.1-1997
Wrinkle recovery angle:GB/T 3819-1997
Cloth cover pH value:GB/T 7573-1987.

Claims (1)

1. a kind of reactive dye quickly go up dyeing technique, it is characterised in that carry out according to the following steps:
(1), sample cloth is chosen:
The T/C fabric sample cloth that a coupe degree is 80 meters or so is chosen, openpore door width 160cm, grammes per square metre 120g/ ㎡, contaminate black;
The woven that T/C products are made of 65% polyester fiber and 35% cotton fiber;
(2), technical flow design:Turn over cloth → alkali desizing → pre-setting → openpore singe → mercerising → oxygen bleaching → dyeing → dehydration → Open-width → drying (oiling) sizing → calendering → finished product preshrunk → inspection yardstick;
(3), alkali desizing designs:Desizing is carried out to sample cloth using joint desizing machine;
Desizing auxiliary formula:
Alkali concn:30g/l
OD:2.5g/l
Hydrogen peroxide:2g/l
100 DEG C of temperature, soaking time:45 points;It is required that detection desizing is clean;
(4), fabric pre-setting:
Pre-setting, 195 DEG C × 98m/min of setting process, pre-setting are carried out to sample cloth using South Korea's production day new 9 section baking oven forming machine Fabric situation afterwards:Door width 151cm, grammes per square metre 120g/ ㎡, shrinkage 3%;
(5), openpore is singed:
The method respectively burnt using Jiangsu Taizhou natural gas gassing frame positive and negative once singes sample cloth, singeing:Naturally Throughput 18, speed 120m/min.It is required that singe more than 4 grades;
(6), mercerising is set:Alkali concn:200g/l, speed:50m/min, door width:151cm, tension force:2kg;
(7), oxygen bleaching is set:Oxygen bleaching is carried out to fabric using joint oxygen bleaching machine:
Oxygenic bleaching aids formula:
Hydrogen peroxide:2g/l
Hydrogen peroxide stabilizer:0.2g/l
Make composite assistant by oneself:2g/l
100 DEG C of temperature, soaking time:40 points;
(8), dyeing recipe and dyeing are set:
Disperse dye prescription (o.w.f):
150% disperses black ECO:7%
100% disperse yellow brown 2RL:2%
100% dispersed ruby 5BL:0.16%
Glacial acetic acid 0.5g/l (adjusts dye bath pH value:5-5.5)
Dyeing:130℃×40min.
Reactive dye formula (o.w.f):
100% active black ED-Q:1.9%
100% active yellow BF-3R:0.96%
100% active red 3BSN:0.37%
Anhydrous sodium sulphate:44g/l,
Soda ash:1kg/ cylinders,
Substitute alkali:2.2g/l;
Activity staining procedure:60℃×70min;
Soap after vital staining formula:
Soaping agent SW:0.5g/l
Glacial acetic acid:0.2g/l
Soap technique:75℃×10min.
(9), a sample cylinder dyeing:
Using the military essence sample overflow dyeing machine dyeing in Taiwan east, dying operation work presses dyeing recipe and sample cloth the weight core at accounting Dye material is calculated, by the good disperse dyes of regulationization and activity dye dyestuff, material uniformly exists without suspended particulate dyestuff;
Dyeing production procedure, (with computer whole-process control dyeing production technology, dye bath ratio presses 1:9 dyeing):
Disperse dyeing overall process:Computer control discharges water after position → prompting cloth feeding → operative employee's craft cloth feeding → operation 2 minutes Glacial acetic acid → open cycle stirring material liquid → computer control is added in termination of pumping sensed water level → material cylinder reflux material water → material cylinder Disperse dyes → open cycle stirring material liquid → computer control is added in making into glacial acetic acid → material cylinder reflux material water → material cylinder Make into dye solution → prompting detection pH value → 130 DEG C → insulation of computer control heating 40min → cooling → 65 DEG C prompting sample cutting To color → computer control washing;
Reactive dyeing:Position → material cylinder reflux material water → the computer that discharges water controls that (anhydrous sodium sulphate is by dispensing into anhydrous sodium sulphate solution System is sent directly into material bucket) → prompt detection electrical conductivity → material cylinder reflux material water → adding soda ash in material cylinder → to open and follow Ring stirring material liquid → computer, which is controlled, to be opened and follows into soda ash solution → material cylinder reflux material water → substitute alkali is added in material cylinder → It is molten that ring stirring material liquid → computer adds reactive dye in controlling into alternative aqueous slkali → material cylinder reflux material water → material cylinder Liquid → open cycle stirring material liquid → computer is controlled into dyestuff → computer control heating 60 DEG C → insulation 70min → prompting sample cutting pair Color → computer control washing;
Soap:Discharge water and add glacial acetic acid → open cycle stirring material liquid → computer in position → material cylinder reflux material water → material cylinder Control and SW soaping agents → open cycle stirring material liquid → computer control is added in charging → material cylinder reflux material water → material cylinder Charging → 75 DEG C → insulation of computer control heating 10min → cooling → 65 DEG C prompting sample cutting controls washing → prompting to color → computer Cloth outputting;
(10), (oiling) sizing setting is dried:Using South Korea's production day new 9 section baking oven forming machine
130 silicone oil of rivers and mountains:15g/l、
Temperature:195℃
Speed:80m/min
Door width:154cm
Grammes per square metre:118g/㎡
(11), final finishing calendering:
Calendering is carried out using German KKT calenders, the setting of this process mainly obtains fabrics cloth cover good gloss.Calendering work Skill:100 DEG C, pressure 250kg, speed 50m/min of temperature;Sample cloth door width 150cm after calendering;
(12), final finishing finished product preshrunk:
Shrunk finish is carried out to galatea using Zheng's frame preshrinking machine, to obtain the good dimensional stability of galatea;Make fabric Reach not only soft but also well-pressed comfort feel.Production technology:Rubber blanket pressure 15MPa, steam pressure 1.5kg, speed 45m/ Min, within shrinkage control 3%;
(13), product inspection:
Presentation quality and inherent quality index to fabric are tested.
CN201711376690.0A 2017-12-19 2017-12-19 A kind of reactive dye quickly go up dyeing technique Pending CN107988816A (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108824034A (en) * 2018-06-22 2018-11-16 佛山市亨特纺织有限公司 A kind of dustless black processing method of polyester-cotton blend/cotton knitted fabric
CN109267270A (en) * 2018-08-22 2019-01-25 浙江乐高实业股份有限公司 A kind of sea island filament abbreviated system
CN109837771A (en) * 2019-03-05 2019-06-04 杭州澳美印染有限公司 A kind of technique of T/C fabric dispersion, vital staining production
CN109853266A (en) * 2019-03-05 2019-06-07 浙江航民股份有限公司 A kind of production technology of TR fabric stability dispersion dyeing pH value
CN109898348A (en) * 2019-03-05 2019-06-18 浙江航民股份有限公司 A kind of cotton, viscous blended fabric vital staining production technique

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS551365A (en) * 1978-06-21 1980-01-08 Kuraray Co Dyeing of suede like sheet with excellent fastness
CN106835741A (en) * 2017-03-20 2017-06-13 浙江航民股份有限公司 A kind of double branch dyeing production technologies of galatea

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS551365A (en) * 1978-06-21 1980-01-08 Kuraray Co Dyeing of suede like sheet with excellent fastness
CN106835741A (en) * 2017-03-20 2017-06-13 浙江航民股份有限公司 A kind of double branch dyeing production technologies of galatea

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108824034A (en) * 2018-06-22 2018-11-16 佛山市亨特纺织有限公司 A kind of dustless black processing method of polyester-cotton blend/cotton knitted fabric
CN109267270A (en) * 2018-08-22 2019-01-25 浙江乐高实业股份有限公司 A kind of sea island filament abbreviated system
CN109837771A (en) * 2019-03-05 2019-06-04 杭州澳美印染有限公司 A kind of technique of T/C fabric dispersion, vital staining production
CN109853266A (en) * 2019-03-05 2019-06-07 浙江航民股份有限公司 A kind of production technology of TR fabric stability dispersion dyeing pH value
CN109898348A (en) * 2019-03-05 2019-06-18 浙江航民股份有限公司 A kind of cotton, viscous blended fabric vital staining production technique

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Application publication date: 20180504